CN106669572A - Reaction kettle - Google Patents
Reaction kettle Download PDFInfo
- Publication number
- CN106669572A CN106669572A CN201611194056.0A CN201611194056A CN106669572A CN 106669572 A CN106669572 A CN 106669572A CN 201611194056 A CN201611194056 A CN 201611194056A CN 106669572 A CN106669572 A CN 106669572A
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- Prior art keywords
- reactor
- liquid
- reaction kettle
- inlet
- reactor body
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00245—Avoiding undesirable reactions or side-effects
- B01J2219/00252—Formation of deposits other than coke
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention belongs to the technical field of common chemical methods and special equipment for liquid and liquid reaction, and particularly discloses a reaction kettle. The reaction kettle comprises a reaction kettle body, wherein the side wall of the reaction kettle body is provided with a heating cavity; one side of the heating cavity is provided with a water filling port; a liquid absorbing pipe is wound at the exterior of the reaction kettle body, one end of the liquid absorbing liquid is provided with a funnel-shaped liquid inlet, a first check valve is arranged at the liquid inlet, the other end of the liquid absorbing pipe is provided with a liquid outlet, the liquid inlet and the liquid outlet are respectively positioned in the reaction kettle body, and the vertical distance between the liquid outlet and the bottom part of the reaction kettle body is 1 to 3cm; the upper part of the reaction kettle body is connected with a kettle cover by threads, a through hole is formed in the kettle cover, a stirring shaft is arranged in the through hole in a matching way, a driving device is arranged at the top part of the stirring shaft, a stirring wheel is eccentrically arranged at the bottom part of the stirring shaft, and is arranged corresponding to the liquid inlet, and the liquid inlet is extruded when the stirring wheel is rotated to the position of the maximum radius. Compared with the prior art, the reaction kettle has the advantage that the material in the reaction kettle is sufficiently stirred, and uniformly heated.
Description
Technical field
The invention belongs to make the general chemical method of liquid and liquid reactions；And its special equipment technical field.
Background technology
Now on the market most of reactors for preparing printing and dyeing assistant are not provided with agitating device so that the thing of reaction
Material stirring is insufficient and uneven, and this just directly results in response speed slowly, and reacts incomplete, wastes resource, improves life
Cost is produced, and some reaction mediums after reacting in tank under residual easily corrode, and have impact on consersion unit, it is impossible to improve economic effect
Benefit.
In order to solve the above problems, Chinese utility model patent CN203123964U discloses a kind of for preparing printing and dyeing
The reaction unit of auxiliary agent, it is provided with the shaft being inserted in can body on cover, and shaft bottom is provided with anchor blade,
The stirring to material is realized, accelerates response speed.
Above-mentioned reaction unit realizes the stirring to material and mixing only by the mode for adding shaft, but is installing
During shaft, in order to avoid shaft in whipping process scratch reactor bottom, the bottom of general shaft will not be with reactor
Bottom contacts, therefore in the whipping process of shaft, shaft cannot stir reactor substrate material, it is impossible to in reactor
Material is sufficiently stirred.
During chemical reaction in simultaneous reactions kettle, it is sometimes desirable to the certain heating environment of needs, tradition is only
Can by realizing the heating to material to tank body heating, firing rate is slow and tank in temperature of charge it is uneven, be unfavorable for anti-
That what is answered is smoothed out.
The content of the invention
It is an object of the invention to provide a kind of reactor, it is possible to achieve the material in reactor is carried out being sufficiently stirred for and
Uniform heating.
In order to achieve the above object, base case of the invention provides a kind of reactor, including reactor body, reactor
Heating chamber is provided with the side wall of body, heating chamber side is provided with the water filling port for adding hot-water flooding, and reactor is originally wound with vitro
Pipette, pipette one end is provided with funnel shaped inlet, and the first check valve is provided with inlet, and the other end of pipette is provided with
Liquid outlet, inlet and liquid outlet are respectively positioned on reactor body interior, and the vertical distance of liquid outlet and reactor body bottom portion
For 1~3cm；Reactor body upper part can be threaded connection with kettle cover, and through hole is provided with kettle cover, and shaft is combined with through hole, stir
Mix axle top and be provided with driving means, shaft bottom eccentric setting has stirring wheel, and stirring wheel is relative with inlet, and stir rotation
Inlet is extruded when moving to radius maximum.
The principle of this base case is：When preparing using this reactor, kettle cover is rotated first, kettle cover rotation is removed,
Then material is poured into reactor body interior, it would be desirable to which the material of hybrid reaction all added and again will after reactor body
Kettle cover is covered on reactor body, and rotation is tightened.
Start driving means to start working, while to hot water is injected from water filling port to heating chamber, it is intrinsic to reactor
Material is heated, and makes the intrinsic material of reactor reach the temperature of reaction, and driving means drive shaft to start to rotate, stir
Mixing drive stirring wheel to rotate while axle is rotated, and the liquid material in reactor is impacted when stirring wheel is rotated, and liquid is raised
Rise, the liquid that stirring wheel is kicked up sends into inlet.
Now the first check valve is opened, and liquid enters pipette, as stirring wheel is rotated, wind can be produced during rotation and pours into suction
Liquid pipe, by the liquid in pipette liquid outlet is pressed to, while stirring wheel can be squeezed into when stirring wheel turns to radius maximum
Liquid mouth, accelerates the liquid rate of outflow of liquid outlet.
Because the vertical distance of liquid outlet and reactor body bottom portion is 1~3cm, then the liquid that liquid outlet flows out will be direct
Contact with the liquid material of the bottom, flow out alluvium material using liquid and form stirring action, make the more abundant of material mixing.
The beneficial effect of this base case is：1st, while eccentric setting stirring wheel and pipette, will react in this programme
The liquid suction pipette of kettle body, and the liquid mobilization using liquid outlet causes agitation to substrate material, it is to avoid thing
Material bottom becomes retention layer, and liquid is stirred under the collective effect of shaft and liquid outlet, stirs more uniform；Simultaneously
Inlet is extruded using stirring wheel, accelerating liquid flow velocity enhances the agitaion to bottom liquid.
2nd, heating in water bath is carried out to material using heating chamber in this programme, reactor body is uniformly heated, while inhaling
Liquid pipe is wrapped on reactor body, it is ensured that the liquid in pipette also can be heated, while by the liquid in the pipette after heating
Body discharges into reactor body, can accelerate the firing rate of material, improves reaction efficiency.
Scheme two：Scheme is preferred based on this, and the liquid outlet end of the pipette is provided with cleaning pipe, and cleaning pipe is provided with
Second check valve, is provided with some scuppers on cleaning pipe, cleaning pipe is fitted with reactor inner body wall.
After the intrinsic material reaction of reactor is complete, the hot water of heating intracavity is poured out from water filling port, and will be fallen
Hot water out pours again reactor body into, and stirring wheel is rotated, and the water in reactor is clamp-oned into pipette, and now first is unidirectional
Valve and the second check valve are opened, and water enters cleaning pipe from pipette, and inwall of the water directly from scupper along reactor is flowed down, clearly
The inwall of clean reactor body.
Directly using the hot water after use, it is to avoid the wilful waste of water resource, while whole cleaning process is not required to very important person
Handss enter reactor body, it is to avoid chemical substance injures human body.
Scheme three：This is preferred for scheme two, and the cleaning pipe is positioned at the middle and upper part of reactor body.
The intrinsic material of reactor is typically in the bottom of reactor body, then what is be contaminated is typically also reactor
The bottom of body, therefore the water cleaned in pipe contributes to cleaning under overhead stream, improves the effectiveness of cleaning.
Scheme four：This is preferred for scheme three, and the reactor body is externally provided with vibrator.
In cleaning, Vibration on Start-up device can improve cleaning capacity.
Scheme five：Scheme is preferred based on this, and between the reactor body and kettle cover sealing gasket is provided with.
Improve the sealing of reactor, it is to avoid the harmful gass produced during material reaction are flown away in atmosphere, to people
Body causes damage.
Scheme six：Scheme is preferred based on this, and the through hole is opened in kettle cover near the side of inlet.
Ensure that stirring wheel can effectively extrude inlet in rotation process, strengthen flowing velocity of the liquid in pipette,
Improve stirring action of the liquid outlet to substrate material.
Description of the drawings
Fig. 1 is a kind of structural representation of reactor of the embodiment of the present invention.
Specific embodiment
Below by specific embodiment, the present invention is further detailed explanation：
Reference in Figure of description includes：Reactor body 10, kettle cover 11, heating chamber 12, water filling port 13, pipette
20th, liquid outlet 21, inlet 22, cleaning pipe 23, shaft 30, motor 40, stirring wheel 50, vibrator 60.
Embodiment
Substantially as shown in Figure 1：A kind of reactor, including reactor body 10, are provided with the wall of reactor body 10 and add
Hot water is full of in hot chamber 12, heating chamber 12, the right-hand member of heating chamber 12 is integrally formed with water filling port 13；Reactor external spiral is wound with suction
Liquid pipe 20, the right-hand member of pipette 20 is provided with the first check valve integrally formed with inlet 22 at inlet 22, inlet 22 is in a left side
Wide right narrow infundibulate, the left end of pipette 20 is integrally formed with vertical liquid outlet 21 and the cleaning pipe 23 of annular, liquid outlet 21
With reactor bottom distance and 1cm, clean pipe 23 and be arranged on the inwall of reactor, and it is unidirectional to be provided with second on cleaning pipe 23
Valve.
The top of reactor body 10 is threaded with kettle cover 11, and sealing is provided between kettle cover 11 and reactor body 10
Pad, the right part of kettle cover 11 offers through hole, and shaft 30 is combined with through hole, and the top of shaft 30 is provided with motor 40, shaft
30 bottoms are eccentrically mounted stirring wheel 50, and inlet 22 is correspondingly arranged with stirring wheel 50, and stirring wheel 50 extrudes inlet when stirring
22, the bottom of reactor body 10 is provided with vibrator 60.
When preparing using this reactor, kettle cover 11 is rotated first, the rotation of kettle cover 11 is removed, then to reactor body 10
Inside pours material into, it would be desirable to which the material of hybrid reaction is all added again to cover kettle cover 11 after reactor body 10 and reacted
On kettle body 10, and rotation is tightened.
When material in reactor starts reaction, start motor 40 and work, while to from water filling port 13 to the note of heating chamber 12
Enter hot water, heating in water bath is carried out to the material in reactor body 10, motor 40 drives shaft 30 to start to rotate, shaft 30
Drive stirring wheel 50 to start to rotate while rotation, the liquid material in reactor is impacted when stirring wheel 50 is rotated, and by liquid
Body is kicked up.
Because inlet 22 is correspondingly arranged with stirring wheel 50, then the liquid that stirring wheel 50 is kicked up will enter pipette 20,
Now the first check valve is opened, the second closed check valve, and due to the eccentric setting of stirring wheel 50, when stirring wheel 50, to turn to radius big
Side when contacting with inlet 22, stirring wheel 50 will extrude inlet 22, so as to by the liquid of pipette 20 to liquid outlet 21
Extruding, and finally flows out from liquid outlet 21, due to the bottom of liquid outlet 21 and reactor body 10 it is close, when liquid is from going out liquid
When mouth 21 flows out, directly contact with the liquid material of the bottom, as liquid constantly flows out from liquid outlet 21, to the bottom
Liquid carry out flow-disturbing, cause stirring so that material mixing it is more abundant.
After the material reaction in reactor body 10 is complete, kettle cover 11 is removed again, by the thing in reactor body 10
Material is derived and collected, while the hot water in heating chamber 12 is poured out from water filling port 13, and the hot water poured out is poured into again instead
Kettle body 10 is answered, kettle cover 11 is then covered, same to start motor 40, motor 40 drives stirring wheel 50 to rotate, by reactor
Water clamp-ons pipette 20, and now the first check valve and the second check valve are opened, and water enters cleaning pipe 23, cleaning from pipette 20
Some scuppers are provided with pipe 23, inwall of the water directly from scupper along reactor body 10 is flowed down, while Vibration on Start-up device 60,
Reactor body 10 is set to start vibration, so as to reach the purpose of cleaning reactor body 10, cleaning pulls down kettle cover 11 after finishing, will
Water is poured out and completes cleaning, is cleaned without staff, it is to avoid chemical substance injures human body.
Above-described is only embodiments of the invention, and the general knowledge here such as known concrete structure and characteristic is not made in scheme
Excessive description.It should be pointed out that for a person skilled in the art, on the premise of without departing from present configuration, can be with
Some deformations and improvement are made, these should also be considered as protection scope of the present invention, these are implemented all without the impact present invention
Effect and practical applicability.This application claims protection domain should be defined by the content of its claim, in description
Specific embodiment etc. records the content that can be used for explaining claim.
Claims (6)
1. a kind of reactor, including reactor body, it is characterised in that be provided with heating chamber in the side wall of reactor body, heating
Chamber side is provided with the water filling port for adding hot-water flooding, and reactor is originally wound with vitro pipette, and pipette one end is provided with infundibulate
Inlet, the first check valve is provided with inlet, the other end of pipette is provided with liquid outlet, and inlet and liquid outlet are respectively positioned on
Reactor body interior, and liquid outlet and the vertical distance of reactor body bottom portion are 1~3cm；Reactor body upper part can spiral shell
Stricture of vagina is connected with kettle cover, and through hole is provided with kettle cover, and shaft is combined with through hole, and shaft top is provided with driving means, shaft
Bottom eccentric setting has stirring wheel, and stirring wheel is relative with inlet, and stirring wheel extrudes inlet when turning to radius maximum.
2. a kind of reactor according to claim 1, it is characterised in that：The liquid outlet end of the pipette is provided with cleaning
Pipe, cleaning pipe is provided with the second check valve, and some scuppers are provided with cleaning pipe, and cleaning pipe is fitted with reactor inner body wall.
3. a kind of reactor according to claim 2, it is characterised in that：The cleaning pipe is located in reactor body
Portion.
4. a kind of reactor according to claim 3, it is characterised in that：The reactor body is externally provided with vibrator.
5. a kind of reactor according to claim 1, it is characterised in that：It is provided with close between the reactor body and kettle cover
Packing.
6. a kind of reactor according to claim 1, it is characterised in that：The through hole is opened in kettle cover near inlet
Side.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611194056.0A CN106669572B (en) | 2016-12-21 | 2016-12-21 | A kind of reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611194056.0A CN106669572B (en) | 2016-12-21 | 2016-12-21 | A kind of reaction kettle |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106669572A true CN106669572A (en) | 2017-05-17 |
| CN106669572B CN106669572B (en) | 2018-09-21 |
Family
ID=58871315
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611194056.0A Active CN106669572B (en) | 2016-12-21 | 2016-12-21 | A kind of reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106669572B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108355373A (en) * | 2018-02-09 | 2018-08-03 | 山东中医药大学 | A kind of automatic microwave extraction equipment |
| CN108579120A (en) * | 2018-02-09 | 2018-09-28 | 山东中医药大学 | A kind of auto-ultrasonic extraction equipment |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3847805A (en) * | 1972-12-07 | 1974-11-12 | Illinois Water Treatment Co | Ion exchange vessel |
| CN1482942A (en) * | 2000-09-22 | 2004-03-17 | - | Method and device for processing a set of liquid |
| CN103521159A (en) * | 2013-10-31 | 2014-01-22 | 罗江晨明生物制品有限公司 | Reaction kettle |
| CN104492338A (en) * | 2014-12-25 | 2015-04-08 | 常州商瑞服饰有限公司 | Interruption type spraying device |
| WO2015176092A2 (en) * | 2014-05-20 | 2015-11-26 | Geolyth Mineral Technologie Gmbh | Sequential continuous mixer apparatus |
| CN205253055U (en) * | 2015-12-24 | 2016-05-25 | 重庆凌峰橡塑制品有限公司 | Resin production reation kettle |
-
2016
- 2016-12-21 CN CN201611194056.0A patent/CN106669572B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3847805A (en) * | 1972-12-07 | 1974-11-12 | Illinois Water Treatment Co | Ion exchange vessel |
| CN1482942A (en) * | 2000-09-22 | 2004-03-17 | - | Method and device for processing a set of liquid |
| CN103521159A (en) * | 2013-10-31 | 2014-01-22 | 罗江晨明生物制品有限公司 | Reaction kettle |
| WO2015176092A2 (en) * | 2014-05-20 | 2015-11-26 | Geolyth Mineral Technologie Gmbh | Sequential continuous mixer apparatus |
| CN104492338A (en) * | 2014-12-25 | 2015-04-08 | 常州商瑞服饰有限公司 | Interruption type spraying device |
| CN205253055U (en) * | 2015-12-24 | 2016-05-25 | 重庆凌峰橡塑制品有限公司 | Resin production reation kettle |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108355373A (en) * | 2018-02-09 | 2018-08-03 | 山东中医药大学 | A kind of automatic microwave extraction equipment |
| CN108579120A (en) * | 2018-02-09 | 2018-09-28 | 山东中医药大学 | A kind of auto-ultrasonic extraction equipment |
| CN108579120B (en) * | 2018-02-09 | 2021-05-14 | 山东中医药大学 | Automatic ultrasonic extraction equipment |
| CN108355373B (en) * | 2018-02-09 | 2021-05-14 | 山东中医药大学 | Automatic microwave extraction equipment |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106669572B (en) | 2018-09-21 |
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| TR01 | Transfer of patent right |
Effective date of registration: 20190819 Address after: 102600 Unit 403, Unit 1, 15th Floor, Changfengyuan, Huangcun Town, Daxing District, Beijing Patentee after: Dong Jinhuan Address before: 400052 Building 8-1, District C, Jiulongpo District, Jiulongpo District, Jiulongpo District, Chongqing Patentee before: Chongqing Demengte Technical Development Co., Ltd. |
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| TR01 | Transfer of patent right |
Effective date of registration: 20191216 Address after: 276600 West Six Road, East Huaihai Second Road, Junan Economic Development Zone, Linyi City, Shandong Province Patentee after: Shandong Peak-tech New Material Co., Ltd. Address before: 102600 Unit 403, Unit 1, 15th Floor, Changfengyuan, Huangcun Town, Daxing District, Beijing Patentee before: Dong Jinhuan |