CN206935363U - A kind of chemical laboratory reactor - Google Patents
A kind of chemical laboratory reactor Download PDFInfo
- Publication number
- CN206935363U CN206935363U CN201720690366.5U CN201720690366U CN206935363U CN 206935363 U CN206935363 U CN 206935363U CN 201720690366 U CN201720690366 U CN 201720690366U CN 206935363 U CN206935363 U CN 206935363U
- Authority
- CN
- China
- Prior art keywords
- kettle
- branch pipe
- lid
- support
- chemical laboratory
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000126 substance Substances 0.000 title claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 30
- 239000012528 membrane Substances 0.000 claims abstract description 7
- 238000007599 discharging Methods 0.000 claims description 11
- 230000000740 bleeding effect Effects 0.000 claims description 5
- 241000826860 Trapezium Species 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 abstract description 28
- 239000002994 raw material Substances 0.000 abstract description 13
- 239000007788 liquid Substances 0.000 abstract description 6
- 238000004140 cleaning Methods 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 3
- 230000036541 health Effects 0.000 abstract description 2
- 230000000149 penetrating effect Effects 0.000 abstract 1
- 238000000034 method Methods 0.000 description 8
- 230000008569 process Effects 0.000 description 5
- 239000002904 solvent Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 3
- 238000009835 boiling Methods 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000010008 shearing Methods 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 230000009471 action Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000008450 motivation Effects 0.000 description 1
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Chemical laboratory equipment technology is the utility model is related to, more particularly to a kind of chemical laboratory reactor, including kettle, lid and support frame；Connected by the groove of lifting support and lid, realize movement, the cleaning of lid, it is time saving and energy saving；The admission line of kettle includes annulus branch pipe and the vertical branch pipe of multi-quantity, and annulus branch pipe and vertical branch pipe are provided with air-vent and waterproof ventilated membrane, while making gas even into kettle, prevents liquid from penetrating into admission line, improves reaction efficiency；The outlet pipe connection exhaust gas processing device of lid, is discharged into air after the condensed processing of tail gas, avoids damaging to the health of staff；Agitating paddle includes central shaft, trapezoidal stirring support and blade, makes reaction raw materials mixing more abundant, stirs support and blade is provided with passage, increase sinuous flow, reduce the requirement to reactor power；The utility model is compact-sized rationally, improves reaction efficiency, safe operation environmental protection, is adapted to promote the use of in laboratory.
Description
Technical field
Chemical laboratory equipment technology is the utility model is related to, is reacted more particularly to a kind of chemical laboratory
Kettle.
Background technology
Reactor is the conventional reaction vessel of chemical laboratory, particularly for reaction raw materials dosage is larger, simple glass instrument
The chemical reaction that device can not be completed.Using laboratory traditional reactor when, it is necessary to operating personnel's manual teardown, installation, cleaning
With mobile response kettle, waste time and energy and potential safety hazard be present.Chinese patent CN 205182707U disclose a kind of laboratory and exempt to tear open
Formula reactor, only reactor body, avoid dismantling, installing the troublesome operation of reactor body, yet with being not provided with
Single kettle cover, need during cleaning to overturn reactor body, cause being not easy and being not easy to check whether clear inside reactor for cleaning
Wash clean, follow-up reaction is impacted.Chinese patent CN 205550290U disclose a kind of experiment reactor, are provided with
Liquid spraying device, the liquid material for being advantageous to newly to add equably are sprayed onto in reactor, and detachable kettle will conveniently be set
It is standby to clean up, but liquid outlet is located at reactor bottom, reaction still needs to artificial lift reactor tapping, and agitating paddle after terminating
It is connected with reactor bottom, although making partial reaction liquid produce sinuous flow by blade construction, more easily causes partial reaction thing
Deposited in reactor bottom, make reaction insufficient.
Utility model content
For in place of above-mentioned the deficiencies in the prior art, the utility model provides a kind of chemical laboratory reactor, is used for
Solve how to provide it is a kind of it is compact-sized rationally, improve reaction efficiency and the chemical laboratory reactor of safe operation environmental protection
Problem.
To realize object above, the utility model is achieved by the following technical programs：
A kind of chemical laboratory reactor, including kettle, lid and support frame, the lid are provided with motor, the electricity
The output end connection agitating paddle of motivation, the kettle are provided with charging aperture and discharging opening, it is characterised in that：The kettle is provided with left
Hand, left column is installed in the left handle, the left column is flexibly connected with lifting support, and the lifting support includes lasso
And bolt, the lid are provided with groove, the lasso is flexibly connected by bolt with groove；The kettle is provided with admission line,
The admission line is provided with aerometer gauge, and the admission line includes annulus branch pipe and vertical branch pipe, the annulus branch pipe
It is fixedly connected by buckle with inner wall of kettle, the vertical branch pipe is uniformly distributed around annulus branch pipe, the annulus branch pipe and vertical
The surface of branch pipe is provided with uniform air-vent, and the inwall of the annulus branch pipe and vertical branch pipe is provided with waterproof ventilated membrane；The lid
Body is provided with right handle, and the right handle is provided with right column, and the lid is provided with outlet pipe, and the outlet pipe is connected at tail gas
Device is managed, the exhaust gas processing device includes horizontal condenser and collecting tank, and the horizontal condenser and collecting tank pass through support
Right column is flexibly connected, the horizontal condenser is connected by pipeline with collecting tank, and the collecting tank is provided with air bleeding valve；It is described to stir
Mixing oar includes central shaft, stirring support and blade, and the stirring support is trapezium structure, the blade and stirring support up and down
Base center is threadedly coupled, and the stirring support and blade are provided with passage.
Further, the lid is connected with kettle by screw thread with flange, and sealing is provided between the lid and kettle
Circle.
Further, the discharging opening is arranged at the bottom of kettle.
Further, the angle of the charging aperture and kettle is 45 °.
Further, the blade is three leaf push type structures, and the length of side angle of the blade and stirring support is 45 °.
Further, the quantity of vertical branch pipe is 4.
Further, the kettle is provided with interior cooler pan.
The beneficial effects of the utility model are：
The utility model sets lifting support on kettle, is on the one hand moved easily and cleans lid, another aspect lid
Vertical state, protection motor are always maintained at, left column is fixedly connected with the left handle of kettle, left handle is played the work of pedestal
With, while additional space is not take up, it is compact-sized, and lid need to only be lifted, reduce the load-bearing of lifting support；
Outlet pipe is connected with exhaust gas processing device, effectively condenses, volatile gas caused by collection reaction, avoids having in tail gas
Evil composition is directly entered the health of indoor harm staff；Admission line is arranged to annulus branch pipe and multiple vertical branch
Pipe combines, and annulus branch pipe and vertical branch pipe are provided with the air-vent comprising waterproof ventilated membrane, makes mixed into the gas of kettle and reaction
Compound multi-surface contact, when the gas of entrance is as protection gas, the protection gas in kettle is set to be more evenly distributed, the gas conduct of entrance
During reaction raw materials, gas is fully contacted with other reaction raw materials, improve reaction efficiency, the presence of waterproof ventilated membrane, prevent
Reaction solution penetrates into admission line；When being reacted in reactor, due to Action of Gravity Field, reaction raw materials easily sink in reactor bottom
Product, sets trapezoidal stirring support, makes reactor bottom agitation more abundant, stirs connection blade in bottom center on support, makes to stir
Bigger shearing force can be born in whipping process by mixing support, stir support and blade is provided with passage, mitigate stirring
Weight, the requirement to reactor power is reduced, meanwhile, reaction solution and the reaction solution of stirring support periphery through passage are formed
Sinuous flow, make stirring more abundant, improve reaction efficiency.
To sum up, a kind of compact-sized change that is reasonable, improving reaction efficiency and safe operation environmental protection provided by the utility model
Learn laboratory reactor.
Brief description of the drawings
In order to illustrate more clearly of the technical scheme of the utility model embodiment, make required for being described below to embodiment
Accompanying drawing is briefly described, it should be apparent that, drawings in the following description are only some realities of the utility model protection
Example is applied, for those of ordinary skill in the art, on the premise of not paying creative work, can also be according to these accompanying drawings
Obtain other accompanying drawings.
Fig. 1 is structural representation of the present utility model；
Fig. 2 is the structural representation of lid and lifting support；
Fig. 3 is the top view of admission line；
Fig. 4 is the front view of admission line；
Fig. 5 is the structural representation of stirring support and blade；
In accompanying drawing, the part representated by each label is as follows：
1- kettlies, 2- lids, 3- support frames, 4- left handles, the right handles of 5-, 6- left columns, 7- right columns, 8- lifting branch
Frame, 9- agitating paddles, 10- motor, 11- exhaust gas processing devices, 12- admission lines, 13- outlet pipes, 14- aerometer gauge,
15- charging apertures, 16- discharging openings, 2a- grooves, 8a- lassos, 8b- bolts, 9a- central shafts, 9b- stirring supports, 9c- blades, 9d-
Passage, the horizontal condenser pipes of 11a-, 11b- collecting tanks, 12a- annulus branch pipes, the vertical branch pipes of 12b-, 12c- air-vents, 12d- prevent
Water ventilated membrane.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made
The all other embodiment obtained, belong to the scope of the utility model protection.
As Figure 1-5, a kind of chemical laboratory reactor, including kettle 1, lid 2 and support frame 3, lid 2 are provided with
Motor 10, the output end connection agitating paddle 9 of motor 10, kettle 1 are provided with charging aperture 15 and discharging opening 16, and kettle 1 is provided with a left side
Handle 4, left column 6 is installed in left handle 4, left column 6 connects lid 2 by lifting support 8, and lid 2 is provided with groove 2a, liter
Descending branch frame 8 includes lasso 8a and bolt 8b, and lasso 8a is flexibly connected with groove 2a by bolt；Kettle 1 is provided with admission line 12,
Admission line 12 is provided with aerometer gauge 14, and admission line 12 includes annulus branch pipe 12a and vertical branch pipe 12b, annulus branch pipe
12a is close to the inwall of kettle 1, is fixedly connected by buckle with the inwall of kettle 1, vertical branch pipe 12b uniformly divides around annulus branch pipe 12a
The inwall that cloth, annulus branch pipe 12a and vertical branch pipe 12b are equipped with air-vent 12c, annulus branch pipe 12a and vertical branch pipe 12b is provided with
Waterproof ventilated membrane 12d；Lid 2 is provided with right handle 5, and right handle 5 is provided with right column 7, and lid 2 is provided with outlet pipe 13, escape pipe
Road 13 connects exhaust gas processing device 11, and exhaust gas processing device 11 includes horizontal condenser pipe 11a and collecting tank 11b, horizontal condenser
11a is connected by pipeline with collecting tank 11b, and horizontal condenser 11a and collecting tank 11b are flexibly connected right column 7 by support, receive
Collection tank 11b is provided with air bleeding valve；Agitating paddle 9 includes central shaft 9a, stirring support 9b and blade 9c, and stirring support 9 is trapezium structure,
Blade 9c is threadedly coupled with stirring support 9b upper bottom center, and stirring support 9b and blade 9c is provided with passage 9d.
Wherein, the lid 2 is connected with kettle 1 by screw thread with flange, and sealing is provided between the lid 2 and kettle 1
Circle.
Wherein, discharging opening 16 is arranged at the bottom of kettle 1, coordinates the height of support frame 3, is directly discharged using container reception
The mixtures of the discharge of mouth 16, it is not necessary to artificial lift reactor.
Wherein, the angle of charging aperture 15 and kettle 1 is 45 °, and charging aperture 15 keeps inclined angle with kettle 1, conveniently adds
Add raw material.
Wherein, blade 9c is three leaf push type structures, and the blade 9c and stirring support 9b base angle are 45 °, is protected
While holding blade 9c and reaction solution has effective contact area, stirring support 9b is set to be born in whipping process bigger
Shearing force.
Wherein, vertical branch pipe 12b quantity is 4.
Wherein, kettle 1 is provided with interior cooler pan, kettle 1 can be cooled by interior cooler pan.
An embodiment of the present utility model is：
Raw material a and raw material b normal-temperature reaction 1h in solvent c generate product d and low-boiling by-products e, and reaction need to be in N2Protect
Shield is lower to be carried out.The lasso 8a of lifting support 8 is connected with the groove 2a of lid 2 by bolt 8b, raises the lifting on left column 6
Support 8, lid 2 is raised, add raw material a and solvent c, reduced lifting support 8, make kettle 1 and lid 2 by screw thread and flange
Connection；Turn on the power, agitating paddle 9 works, and raw material a is substantially dissolved in raw material c；Admission line 12 is connected into N2Tank, open
Collecting tank 11b air bleeding valve, N2Enter kettle 1 along annulus branch pipe 12a and vertical branch pipe 12b, contacted with raw material a solution, by sky
Gas is discharged along outlet pipe 13, exhaust gas processing device 11, passes through N2Pot valve gate control N2Enter the speed of kettle 1 from admission line 12
Degree；Charging aperture 15 is opened, the raw material b for being dissolved in solvent c is added into kettle 1 along charging aperture 15, closes charging aperture 15, stirring reaction
1h.The low-boiling by-products e of course of reaction generation and the solvent c of volatilization enter horizontal condenser 11a along outlet pipe 13, through sleeping
Formula condenser 11a enters collecting tank 11b, N after being condensed into liquid2Discharged along the air bleeding valve of collecting tank, after reaction terminates, close electricity
Source and N2Tank valve, the screw thread and flange of kettle 1 and lid 2 are unclamped, open discharging opening 16, by reactant mixture along discharging opening 16
It is put into reception container.Lid 2 is raised by lifting support 8, discharging opening 16 is closed, kettle 1 and lid 2 is cleaned, is cleaned
Waste liquid flowed out through discharging opening 16, the liquid in cleaning collecting tank 11b.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality
Body or operation make a distinction with another entity or operation, and not necessarily require or imply and deposited between these entities or operation
In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to
Nonexcludability includes, so that process, method, article or equipment including a series of elements not only will including those
Element, but also the other element including being not expressly set out, or it is this process, method, article or equipment also to include
Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that
Other identical element also be present in process, method, article or equipment including the key element.
The utility model preferred embodiment disclosed above is only intended to help and illustrates the utility model.Preferred embodiment is simultaneously
There is no the details that detailed descriptionthe is all, do not limit the embodiment that the utility model is only yet.Obviously, according to this specification
Content, can make many modifications and variations.This specification is chosen and specifically describes these embodiments, is to preferably explain
Principle and practical application of the present utility model, so that skilled artisan can be best understood by and utilize this practicality
It is new.The utility model is only limited by claims and its four corner and equivalent.
Claims (7)
1. a kind of chemical laboratory reactor, including kettle, lid and support frame, the lid is provided with motor, described electronic
The output end connection agitating paddle of machine, the kettle are provided with charging aperture and discharging opening, it is characterised in that：The kettle is provided with left
Hand, left column is installed in the left handle, the left column is flexibly connected with lifting support, and the lifting support includes lasso
And bolt, the lid are provided with groove, the lasso is flexibly connected by bolt with groove；The kettle is provided with admission line,
The admission line is provided with aerometer gauge, and the admission line includes annulus branch pipe and vertical branch pipe, the annulus branch pipe
It is fixedly connected by buckle with inner wall of kettle, the vertical branch pipe is uniformly distributed around annulus branch pipe, the annulus branch pipe and vertical
The surface of branch pipe is provided with uniform air-vent, and the inwall of the annulus branch pipe and vertical branch pipe is provided with waterproof ventilated membrane；The lid
Body is provided with right handle, and the right handle is provided with right column, and the lid is provided with outlet pipe, and the outlet pipe is connected at tail gas
Device is managed, the exhaust gas processing device includes horizontal condenser and collecting tank, and the horizontal condenser and collecting tank pass through support
Right column is flexibly connected, the horizontal condenser is connected by pipeline with collecting tank, and the collecting tank is provided with air bleeding valve；It is described to stir
Mixing oar includes central shaft, stirring support and blade, and the stirring support is trapezium structure, the blade and stirring support up and down
Base center is threadedly coupled, and the stirring support and blade are provided with passage.
2. chemical laboratory reactor according to claim 1, it is characterised in that：The lid and kettle by screw thread with
Flange is connected, and sealing ring is provided between the lid and kettle.
3. chemical laboratory reactor according to claim 1, it is characterised in that：The discharging opening is arranged at the bottom of kettle
Portion.
4. chemical laboratory reactor according to claim 1, it is characterised in that：The angle of the charging aperture and kettle is
45°。
5. chemical laboratory reactor according to claim 1, it is characterised in that：The blade is the pusher knot of three leaves
Structure, the base angle of the blade and stirring support is 45 °.
6. chemical laboratory reactor according to claim 1, it is characterised in that：The quantity of the vertical branch pipe is 4.
7. chemical laboratory reactor according to claim 1, it is characterised in that：The kettle is provided with interior cooler pan.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720690366.5U CN206935363U (en) | 2017-06-14 | 2017-06-14 | A kind of chemical laboratory reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720690366.5U CN206935363U (en) | 2017-06-14 | 2017-06-14 | A kind of chemical laboratory reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206935363U true CN206935363U (en) | 2018-01-30 |
Family
ID=61365142
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720690366.5U Active CN206935363U (en) | 2017-06-14 | 2017-06-14 | A kind of chemical laboratory reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206935363U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110404497A (en) * | 2019-07-31 | 2019-11-05 | 北京六合宁远科技有限公司 | Preparation method of polysubstituted bromofluorine substituted benzimidazole compound |
| CN114053961A (en) * | 2020-08-03 | 2022-02-18 | 中国石油化工股份有限公司 | Feeding distributor and reactor |
-
2017
- 2017-06-14 CN CN201720690366.5U patent/CN206935363U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110404497A (en) * | 2019-07-31 | 2019-11-05 | 北京六合宁远科技有限公司 | Preparation method of polysubstituted bromofluorine substituted benzimidazole compound |
| CN114053961A (en) * | 2020-08-03 | 2022-02-18 | 中国石油化工股份有限公司 | Feeding distributor and reactor |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN207254201U (en) | Liquid fast deployment equipment | |
| CN205461969U (en) | Chemical products are with high -efficient agitating unit of automatic pay -off | |
| CN206935363U (en) | A kind of chemical laboratory reactor | |
| CN108017257A (en) | Sludge for Treatment of Sludge is sufficiently mixed equipment with medicine | |
| CN205874151U (en) | Food and beverage waste water integration treatment device | |
| CN207130046U (en) | A kind of split type sewage-treatment plant | |
| CN206935355U (en) | A kind of industrial chemicals reactor | |
| CN206663582U (en) | A kind of spraying and cleaning apparatus of plastic flakes | |
| CN218653798U (en) | Spray type waste gas and tail gas recycling device | |
| CN208759774U (en) | A kind of building blender | |
| CN206519019U (en) | Filled type scrubbing tower is used in a kind of industrial organic exhaust gas processing | |
| CN102080044B (en) | Discharging mechanism of straw discharge cleaning on upper part of straw methane anaerobic tank | |
| CN206476793U (en) | Cooler crystallizer | |
| CN211098992U (en) | Reation kettle for chemical industry of clearance convenience | |
| CN206767822U (en) | A kind of sewage disposal device to stir | |
| CN206642641U (en) | Effectively improve the agitating device of cleaning efficiency | |
| CN207567071U (en) | A kind of organic matter separating and filtering device applied to sewage disposal | |
| CN204891678U (en) | Indoor sealed cement mixing plant | |
| CN208375586U (en) | A kind of construction agitator tank being convenient to clean carrying | |
| CN206315720U (en) | A kind of paint dispersion machine of easy cleaning | |
| CN219764978U (en) | Slag waste material preliminary treatment agitating unit | |
| CN110743454A (en) | Stirring and mixing device of gas-phase industrial deodorant | |
| CN211104744U (en) | A mixer for concrete mixing plant | |
| CN214261854U (en) | Reation kettle convenient to solid-liquid separation | |
| CN216400085U (en) | Utensil dustproof concrete reation kettle |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: Room 201, No. 5, Lane 3399, Kangxin Road, Pudong New Area, Shanghai, 201318 Patentee after: Shanghai Lingkai Technology Co.,Ltd. Country or region after: China Address before: Room 970, room 66, carnation Road, Nanhui new town, Pudong New Area, Shanghai Patentee before: SHANGHAI LINKCHEM TECHNOLOGY Co.,Ltd. Country or region before: China |