CN106619379B - A kind of composition of the product containing plant fermentation and its preparation method and application - Google Patents
A kind of composition of the product containing plant fermentation and its preparation method and application Download PDFInfo
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- CN106619379B CN106619379B CN201611224221.2A CN201611224221A CN106619379B CN 106619379 B CN106619379 B CN 106619379B CN 201611224221 A CN201611224221 A CN 201611224221A CN 106619379 B CN106619379 B CN 106619379B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses composition of a kind of product containing plant fermentation and its preparation method and application, skin deep layer can be effectively penetrated by aiming to provide one kind, improve the water content of skin, and strengthen sebum barrier function, so as to skin discomfort caused by resist drying, make skin become smooth, soft, glossiness composition；Said composition mainly includes the component of following parts by weight：10 30 parts of plant fermentation product；10 25 parts of flat peach Cactus Pedicel extract；5 15 parts of PCA potassium；The plant fermentation product is made up of the raw material of following parts by weight：25 50 parts of rhizoma imperatae；20 40 parts of Bai Guo Quercetin parasitisms leaf；Belong to cosmetic field.
Description
Technical field
The present invention relates to a kind of composition, is the composition for being related to a kind of product containing plant fermentation specifically, the present invention
The preparation method and application of this composition are further related to, belong to cosmetic field.
Background technology
The active component of plant, such as vitamin, amino acid, mineral matter, polysaccharide, flavones, polyphenol etc. generally have well
Moisturizing, whitening, Shu Min and anti-aging and other effects.But the plant extracts prepared by traditional handicraft, it is molten due to extracting
The limitation of agent, technique and preparation method etc., composition is difficult to reach expected sometimes the effect of acquisition.
In recent years, fermentation technique has good application prospect in the exploitation of cosmetics plant Effect raw material.Utilize fermentation
Technology extracts more horn of plenty and the active nutritional material of more small molecule from the plant resources of green natural, strengthens plant material work(
Effect, toxic side effect is reduced, not only the validity to cosmetics plant Effect raw material, security have great help, and more hold
Easily it is absorbed by the skin, greatly promotes skin effect.
The content of the invention
In view of the above-mentioned problems, the first object of the present invention is to provide a kind of composition of product containing plant fermentation.
The second object of the present invention is to provide the preparation method of the composition of this product containing plant fermentation.
The third object of the present invention is to provide composition the answering as skin-care product additive of this product containing plant fermentation
With.
Therefore, first technical scheme provided by the invention is such：
A kind of composition of product containing plant fermentation, it includes the component of following parts by weight：Plant fermentation product 10-30
Part；Flat peach Cactus Pedicel extract 10-25 parts；PCA potassium 5-15 parts；The plant fermentation product by following parts by weight raw material system
Into：Rhizoma imperatae 25-50 parts；Bai Guo Quercetin parasitism leaf 20-40 parts.
Further, the composition of above-mentioned a kind of product containing plant fermentation, the plant fermentation product raw material also include
Eyebright 10-20 parts.
Further, the composition of above-mentioned a kind of product containing plant fermentation, the plant fermentation product raw material also include
Persimmon leaf 8-15 parts.
Second technical scheme of the present invention is to provide the preparation method of the composition of the above-mentioned product containing plant fermentation, the party
Method comprises the following steps：
1) rhizoma imperatae 25-50 parts, Bai Guo Quercetin parasitism leaf 20-40 parts are weighed, dries, is crushed to 20-50 mesh, mixes, obtains
Mixed-powder；
2) water of mixed-powder 30-40 times of volume of weight is added, adds the Mel Jujubae with mixed-powder weight 1-2%,
Mix, obtain mixed liquor；
3) mixed liquor cumulative volume 10-30% compound bacteria-fermented liquid is added, is fermented 2 months under conditions of 20-30 DEG C, is protected
PH value is held between 3-7, in 100-120 DEG C of autoclaving 10min, 5000r/min centrifugation, supernatant is taken, is concentrated in vacuo, obtains
Plant fermentation product；
4) the PCA potassium for being formulated dosage, flat peach Cactus Pedicel extract and step 3) plant fermentation product are measured with 2-5 times
After deionized water is mixed evenly, produce.
Further, the composition of above-mentioned a kind of product containing plant fermentation, eyebright 10- is also included when step 1) weighs
20 parts.
Further, the composition of above-mentioned a kind of product containing plant fermentation, persimmon leaf 8-15 is also included when step 1) weighs
Part.
Further, the composition of above-mentioned a kind of product containing plant fermentation, the compound bacteria-fermented liquid is by Bacillus acidi lactici
With saccharomycete 2-5 in proportion:1 composition, concentration 105-108CFU/ml。
Further, the composition of above-mentioned a kind of product containing plant fermentation, described compound bacteria-fermented liquid is by rhamnose
Lactobacillus and Bifidobacterium are 2 in proportion:3 compositions, concentration 105-108CFU/ml。
Last scheme of the present invention is composition the answering as skin-care product additive of the above-mentioned product containing plant fermentation
With.
Compared with prior art, technical scheme provided by the invention has the advantages that：
1st, in plant fermentation product provided by the invention, posted by Bacillus acidi lactici and saccharomycetes to make fermentation rhizoma imperatae, Bai Guo Quercetin
Leave, eyebright and persimmon leaf, acted on by the biological metabolism of compound bacteria, the toxic component metabolism in plant is fallen, increases plant
The security of extract；Large molecule active the material such as polysaccharide, protein etc. for making to be rich in Four Plants simultaneously are by lactic acid bar
Bacterium and saccharomycete are degraded into small molecule, add the permeability of plant extracts, and small molecule active thing is also possible to make by biology
New bioactive molecule is metabolized into assembled, strengthens the activity of active matter.The tunning of above various plants passes through holding
The double action of moisture of skin and enhancing sebum barrier, the water content of skin is improved, to resist drying, it is uncomfortable to alleviate skin.
2nd, flat peach cactus, it is a kind of very drought-resistant plant, colloid liquid, vitamin B, various plants is rich in its stem
The nutrients such as amino acid, carbohydrate, polyphenol, active mineral matter, therefore flat peach Cactus Pedicel extract is after skin deep layer is penetrated into,
Moist maintenance effect can be continually played, excites the water circulation of skin cell, dry line caused by improvement water shortage is coarse, additionally
There is inhibiting bacteria and diminishing inflammation.
3rd, the PCA potassium in the present composition, the wherein potassium ion of high content can enter cell help by absorbing moisture
Osmotic equilibrium is adjusted, increases ICW, PCA is the Main Ingredients and Appearance of NMF, energy growth-promoting epidermis lipid, strengthens skin
Fat barrier function, therefore PCA potassium provides high moisture-keeping efficacy by both the above approach.
In summary, the present invention by using compound bacteria by rhizoma imperatae, Bai Guo Quercetin parasitisms leaf, eyebright, four kinds of persimmon leaf into
Divide after preparing plant fermentation product, then coordinate with PCA potassium and flat peach Cactus Pedicel extract, skin depth can be effectively penetrated
Layer, improves the water content of skin, and strengthens sebum barrier function, so as to skin discomfort caused by resist drying, become skin
It is smooth, fine and smooth, soft, glossy.
Embodiment
With reference to embodiment, the claim of the present invention is described in further detail, but not formed pair
Any restrictions of the present invention, the modification of anyone limited number of time made in the claims in the present invention protection domain etc, still exist
Within the claims of the present invention.
It should be noted that the raw material employed in technical scheme provided by the invention, unless otherwise specified, by normal
Rule means are prepared or bought by commercial channel.Wherein, PCA potassium is purchased in Guangzhou Ming Hui Fine Chemical Co., Ltd；It is celestial
Peach Cactus Pedicel extract is purchased in celestial graceful (world) Co., Ltd.
Embodiment 1
A kind of composition of product containing plant fermentation provided by the invention, it is made up of the component of following weight number：Plant sends out
Ferment product 10g, flat peach Cactus Pedicel extract 10g, PCA potassium 15g；
The plant fermentation product is made up of the raw material of following weight number：Rhizoma imperatae 25g, Bai Guo Quercetin parasitism leaves 40g.
Embodiment 2
A kind of composition of product containing plant fermentation provided by the invention, it is made up of the component of following weight number：Plant sends out
Ferment product 30g, flat peach Cactus Pedicel extract 25g, PCA potassium 5g；
The plant fermentation product is made up of the raw material of following weight number：Rhizoma imperatae 50g, Bai Guo Quercetin parasitism leaves 20g.
Embodiment 3
A kind of composition of product containing plant fermentation provided by the invention, it is made up of the component of following weight number：Plant sends out
Ferment product 15g, flat peach Cactus Pedicel extract 20g, PCA potassium 10g；
The plant fermentation product is made up of the raw material of following weight number：Rhizoma imperatae 30g, Bai Guo Quercetin parasitism leaf 20g, millet
Careless 10g.
Embodiment 4
A kind of composition of product containing plant fermentation provided by the invention, it is made up of the component of following weight number：Plant sends out
Ferment product 20g, flat peach Cactus Pedicel extract 15g, PCA potassium 7g；
The plant fermentation product is made up of the raw material of following weight number：Rhizoma imperatae 40g, Bai Guo Quercetin parasitism leaf 30g, persimmon leaf
8g。
Embodiment 5
A kind of composition of product containing plant fermentation provided by the invention, it is made up of the component of following weight number：Plant sends out
Ferment product 18g, flat peach Cactus Pedicel extract 13g, PCA potassium 10g；
The plant fermentation product is made up of the raw material of following weight number：Rhizoma imperatae 35g, Bai Guo Quercetin parasitism leaf 35g, millet
Careless 20g, persimmon leaf 15g.
Embodiment 6
A kind of composition of product containing plant fermentation provided by the invention, it is made up of the component of following weight number：Plant sends out
Ferment product 25g, flat peach Cactus Pedicel extract 18g, PCA potassium 9g；
The plant fermentation product is made up of the raw material of following weight number：Rhizoma imperatae 40g, Bai Guo Quercetin parasitism leaf 30g, millet
Careless 15g, persimmon leaf 12g.
The preparation method of the composition of a kind of product containing plant fermentation of any one group of offer in embodiment 1 to 6, under
Step is stated to be made successively：
1) each raw material is weighed by any one group of weight number in embodiment 1 to 6, dries, be crushed to 20-50 mesh (preferably 30
Mesh), mix, obtain mixed-powder；
2) water of mixed-powder 30-40 times of (preferably 40 times) volume of weight is added, is added and mixed-powder weight 1-2%
The Mel Jujubae of (preferably 1.5%), mix, obtain mixed liquor；
3) mixed liquor cumulative volume 10-30% (preferably 20%) compound bacteria-fermented liquid is added, at 20-30 DEG C (preferably 25 DEG C)
Under conditions of ferment 2 months, keep pH value between 3-7 (preferable ph 5), gone out in 100-120 DEG C of (preferably 115 DEG C) high pressure
Bacterium 10min, 5000r/min centrifugation, takes supernatant, is concentrated in vacuo, obtains plant fermentation product；
4) the PCA potassium for being formulated dosage, flat peach Cactus Pedicel extract and step 3) plant fermentation product are measured with 2-5 times
After deionized water is mixed evenly, produce.
Wherein, the compound bacteria-fermented liquid in step 3) is by Bacillus acidi lactici and saccharomycete 2-5 in proportion:1 (preferably 3:1) group
Into concentration 105-108CFU/ml。
Preferably, the compound bacteria-fermented liquid in step 3) can also be 2 in proportion by Lactobacillus rhamnosus and Bifidobacterium:
3 compositions, concentration 105-108CFU/ml。
A kind of composition of product containing plant fermentation prepared by the present invention, various formulations can be directly appended in low temperature
In skin care item, such as aqua, elite, gel, emulsion, cream, addition 0.1-12%, preferably 1-8%.
In order to prove the effect of the present invention, the applicant is also provided with following comparative example, the embodiment provided with the application
Carry out Contrast on effect：
Comparative example 1
Without PCA potassium, remaining is same as Example 2.
Comparative example 2
Bai Guo Quercetin parasitism leaves are free of in plant fermentation product raw material, remaining is same as Example 5.
Comparative example 3
Containing only PCA potassium 5g.
Comparative example 4
Containing only Bai Guo Quercetin parasitism leaf 35g in plant fermentation product raw material, remaining is same as Example 5.
Comparative example 5
The a certain commercially available moisturizing cream of purchase.
In order to better illustrate advantages of the present invention, a kind of group of product containing plant fermentation provided by the invention is given below
The effect of compound, tests.
First, efficacy test
(1) performance of keeping humidity is tested
1st, test population：The subject of 120 dry skin water shortages, age 20-60 year, sex is random, is divided into 12 groups, often
10 people of group.
2nd, test sample：
1-6 of the present invention and comparative example 1-4 is prepared into composition, is added directly in cosmetics routine cream matrix, stirs
Mix uniformly, addition is the 3wt% of cream gross mass.
3rd, method of testing：
1) subject must not use any cosmetics in one week before testing, before test sample, be passed through by technical staff
Moisture of skin analyzer measures the moisture and trans epidermal water loss situation (TEWL value changes of every group of subject's cheek skin
Situation), it is designated as blank value.
2) every group of subject is in test sample corresponding to inboard arm dermal application, after continuous use 14 days and 28 days,
The moisture and trans epidermal water loss of every group of subject's cheek skin are measured using moisture of skin analyzer by technical staff
Situation, record numerical value.
3) according to the numerical computations moisture content of skin and the situation of change of trans epidermal water loss measured, with evaluation test sample
Performance of keeping humidity and strengthen sebum barrier function, the results are shown in Table 1.
Table 1
As a result show, after the cream prepared using 1-6 of embodiment of the present invention compositions 28 days, moisture content of skin has increasing
Add, and increment rate is above the commercially available moisturizing cream of comparative example 5 and the cream matrix of comparative example 6, illustrates that the embodiment of the present invention carries
The composition of confession can dramatically increase the moisturizing degree of skin.In addition, the guarantor of cream prepared by embodiment 5 and the composition of embodiment 6
Wet effect is better than cream prepared by embodiment 1-4 compositions, illustrates rhizoma imperatae, white fruit Quercetin parasitisms leaf, eyebright, persimmon leaf, PCA potassium
Cooperateed with flat peach Cactus Pedicel extract, the moistening effect reached is more preferable.
TEWL is the situation for showing moisture loss by determining the water vapor pressure gradient of skin surface, so as to reflect skin
Water permeability barrier.When barrier function damage, the increase of TEWL values, on the contrary, TEWL values reduce, represent that barrier function is repaiied
It is multiple.After the cream 28 days prepared using 1-6 of embodiment of the present invention compositions, TEWL values reduce, and slip is above
The commercially available moisturizing cream of comparative example 5 and the cream matrix of comparative example 6, illustrate that composition provided in an embodiment of the present invention can strengthen flesh
The lipid barrier function of skin, significantly reduce the water loss situation of skin.In addition, prepared by embodiment 5 and the composition of embodiment 6
The TEWL values slip of cream is higher than cream prepared by embodiment 1-4 compositions, illustrates rhizoma imperatae, white fruit Quercetin parasitisms leaf, millet
Grass, persimmon leaf, PCA potassium and the collaboration of flat peach Cactus Pedicel extract, preferably repair the barrier function of skin.
After the cream prepared using comparative example 1,3 and 2,4 compositions, moisture content of skin increment rate and TEWL value slips
The cream that respectively lower than prepared by embodiment 1 and the composition of embodiment 5, illustrate that PCA potassium, Bai Guo Quercetin parasitisms leaves and other compositions are assisted
Together, the moistening effect of the present composition is played an important role.
(2) sensory evaluation：
After the cream prepared using the present embodiment 1-6,100% subject represents the increase of skin water content, hence it is evident that improves
Caused by dry skin easily allergy, microgroove, scurf situations such as, 82-90% subject represents to significantly improve the light of skin
Damp degree, it is soft and smooth that 94-97% subject represents that skin becomes water profit.
In summary, the present invention by four kinds of rhizoma imperatae, Bai Guo Quercetin parasitisms leaf, eyebright, persimmon leaf compositions by preparing plant
After tunning, then coordinate with PCA potassium and flat peach Cactus Pedicel extract, skin deep layer can be effectively penetrated, improve skin
Water content, and strengthen sebum barrier function, so as to uncomfortable to skin caused by resist drying, skin is become smooth, fine and smooth, soft
It is soft, glossy.
Claims (9)
1. the composition of a kind of product containing plant fermentation, it is characterised in that it mainly includes the component of following parts by weight：Plant sends out
Ferment product 10-30 parts；Flat peach Cactus Pedicel extract 10-25 parts；PCA potassium 5-15 parts；The plant fermentation product by weighing as follows
The raw material of amount part is made：Rhizoma imperatae 25-50 parts；Bai Guo Quercetin parasitism leaf 20-40 parts.
A kind of 2. composition of product containing plant fermentation according to claim 1, it is characterised in that the plant fermentation production
Raw material also includes eyebright 10-20 parts.
A kind of 3. composition of product containing plant fermentation according to claim 1, it is characterised in that the plant fermentation production
Raw material also includes persimmon leaf 8-15 parts.
4. the preparation method of the composition of a kind of product containing plant fermentation described in claim 1, it is characterised in that including following
Step：
1) rhizoma imperatae 25-50 parts, Bai Guo Quercetin parasitism leaf 20-40 parts are weighed, dries, is crushed to 20-50 mesh, mixes, is mixed
Powder；
2) water of mixed-powder 30-40 times of volume of weight is added, mixed-powder weight 1-2% Mel Jujubae is added, mixes, obtain
To mixed liquor；
3) mixed liquor cumulative volume 10-30% compound bacteria-fermented liquid is added, is fermented 2 months under conditions of 20-30 DEG C, keeps pH
Value, in 100-120 DEG C of autoclaving 10min, 5000r/min centrifugation, takes supernatant, is concentrated in vacuo, obtains plant between 3-7
Tunning；
4) by be formulated the PCA potassium of dosage, flat peach Cactus Pedicel extract and step 3) plant fermentation product with 2-5 times measure go from
After sub- water is mixed evenly, produce.
A kind of 5. preparation method of the composition of product containing plant fermentation according to claim 4, it is characterised in that step
1) also include weighing eyebright 10-20 parts.
A kind of 6. preparation method of the composition of product containing plant fermentation according to claim 4, it is characterised in that step
1 also includes weighing persimmon leaf 8-15 parts.
7. the preparation method of the composition of a kind of product containing plant fermentation according to claim 4, it is characterised in that described
Compound bacteria-fermented liquid is by Bacillus acidi lactici and saccharomycete 2-5 in proportion:1 composition, concentration 105‐108CFU/mL。
8. the preparation method of the composition of a kind of product containing plant fermentation according to claim 4, it is characterised in that described
Compound bacteria-fermented liquid by Lactobacillus rhamnosus and Bifidobacterium be 2 in proportion:3 compositions, concentration 105‐108CFU/mL。
A kind of 9. application of the composition of product containing plant fermentation described in claim 1 as skin-care product additive.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109106637A (en) * | 2018-08-28 | 2019-01-01 | 珠海欧维斯科技有限公司 | A kind of anti-oxidant and fermented plant extract to delay senescence and its preparation method and application |
| CN109381389A (en) * | 2018-11-16 | 2019-02-26 | 北京思尔根生物科技有限公司 | A kind of persimmon leaf fermentation extracting solution and preparation method and application |
| CN109288754A (en) * | 2018-11-16 | 2019-02-01 | 北京思尔根生物科技有限公司 | A kind of Essence and preparation method containing persimmon leaf extractive from fermentative |
| CN112120983A (en) * | 2020-09-30 | 2020-12-25 | 海南希睿达生物技术有限公司 | Skin barrier liquid dressing for sunburn repair and preparation method thereof |
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