CN106511256A - Transparent mask and preparation method thereof - Google Patents
Transparent mask and preparation method thereof Download PDFInfo
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- CN106511256A CN106511256A CN201611082648.3A CN201611082648A CN106511256A CN 106511256 A CN106511256 A CN 106511256A CN 201611082648 A CN201611082648 A CN 201611082648A CN 106511256 A CN106511256 A CN 106511256A
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/60—Sugars; Derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
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Abstract
The invention discloses a transparent mask. The transparent mask is prepared from components in parts by weight as follows: 1 part of an oily ingredient, 1 part of high alcohol, 0.35-0.4 parts of a PEG (polyethylene glycol) 6-20 mol nonionic surfactant, 0.35-0.4 parts of a PEG 30-80 mol nonionic surfactant and 99-110 parts of a transparent mask base material. The high alcohol, the PEG 6-20 mol nonionic surfactant and the PEG 30-80 mol nonionic surfactant are taken as solubilizers of the oily ingredient, the oily ingredient can be dispersed and solubilized until the oily ingredient is transparent and dissolved, so that the prepared transparent mask has the same stable transparency and appearance as a conventional mask, the oily ingredient can be solubilized until the grain size reaches 50 mu m or below, and the mask has good moisturizing and oil supplementing effects on skin, and the moisture retention and moisturizing effect on the skin is increased.
Description
Technical field
The present invention relates to cosmetic field, more particularly to a kind of transparent facial film and preparation method thereof.
Background technology
Facial film market has become that China's daily use chemicals industry is fastest-rising one of to segment market at present.Ground according to Nelson's retail
Study carefully data, up to 78.5 hundred million yuans (similarly hereinafter), continuous 3 years annual compound growth rates surpass Chinese facial film market sale scale in 2012
Cross 21.9%, mad growth will be continued in facial film market within 2014, it is contemplated that year in this year, the most conservative sales volume will be up to 30,000,000,000 yuan.
Facial film sale in 2013 occupies the 3rd in Cosmetic Market, accounts for the 16.3% of market sale total value.Data display, bends for 2012
13.9 hundred million yuan of Chen Shi facial films sales volume, is 11% in the sale accounting of Watson, and by 2013, its facial film sales volume was up to 17
Hundred million yuan, increase by 22% on a year-on-year basis.The facial film category gross sales amount of Taobao in 2013 is up to 2,200,000,000 yuan, wherein frivolous stealthy silk mask
Sales volume is 10.2 hundred million yuan, accounting 46.69%.The development speed of facial film it is closely bound up with its effect soon.Facial film can be simultaneously
Solve 5 big problem of skin：Moisturizing, whitening, oil-control, antiallergic sense and defying age.And everyday skincare is often just for portion therein
Divide problem, it is impossible to quickly improve skin condition comprehensively.Facial film is temporarily isolating the sky in the external world using the of short duration time for being covered in face
Gas and pollution, improve skin temperature and expansion pore, promote sweat gland secretion and metabolism, skin oxygen content is increased.Facial film
In moisture penetrate into skin horny layer so as to become soft, increase elasticity；Gumminess composition or powdered absorbent energy in facial film
Stick dirt in skin surface and pore, metabolic waste and excessive oils and fatss etc., and by its thorough removing.
Generally add oil components in facial film, but pellucidity can not be made.It is existing to add the saturating of high lubricant component
Bright facial film mainly has two kinds, and a class is translucent, and a class is milky.Translucent facial film has that outward appearance is not as clear as crystal enough to be lacked
Point, milky facial film are low viscous emulsion rather than facial film.If by the essence solubilising of oil components to transparent, general to adopt
The big nonionic surfactant of the HLB value such as PEG-60 castor oil hydrogenated, polysorbate -20 is by its solubilising to transparent, consumption
It is oil components i.e. the 2～5 of essence times.But this method still can not be by Vitamin E/tocopherol, tocopherol acetass, day
So oils and fatss, Jojoba oil, squalane, plant sterol/octyl dodecanol lauroyl glutamate ester, plant sterol isostearate,
The various oil components such as cholesterol oil solubilising is to transparent.
Therefore develop a kind of by said vitamin E/ tocopherols, tocopherol acetass, natural oil, Jojoba oil, spiny dogfish
Various oiliness such as alkane, plant sterol/octyl dodecanol lauroyl glutamate ester, plant sterol isostearate, cholesterol oil into
Point by higher alcohol, PEG 6-20mol tweens and PEG 30-80mol tweens solubilising to transparent, so as to
So that the transparent facial film for preparing is with the stable transparent outward appearance as traditional facial mask, and can be by above-mentioned oil components increase-volume
Less than 50 μm are reached to particle diameter so as to there is to skin good moisturizing, oil is supplemented, increase the saturating of skin water lock moistening effect
Bright facial film is significant.
The content of the invention
It is contemplated that be given one kind can by oil components disperse and solubilising extremely transparent can dissolve, with traditional facial mask
The same stable transparent outward appearance；And oil components solubilising can be reached less than 50 μm to particle diameter, there is guarantor well to skin
Wet, supplementary oil, increases the transparent facial film of skin water lock moistening effect.
Transparent facial film of the present invention, by weight, including following component：
Wherein, the oil components are selected from Vitamin E/tocopherol, tocopherol acetass, 3 fatty acids and glyceride group
Into triglyceride, Jojoba oil, squalane, plant sterol/octyl dodecanol lauroyl glutamate ester, the different Hard Fat of plant sterol
One or more in acid esters, cholesterol oil.
Wherein, the higher alcohol is selected from one or more in octyl dodecanol, isooctadecanol, hexyldecanol, oleyl alcohol.
Wherein, the PEG 6-20mol tweens are different hard selected from PEG-6 iso stearic acid of glycerine ester, PEG-8 glycerol
Fat acid ester, laureth -7, PEG-7 glyceryl cocoates, olive oil PEG-7 esters, PEG-6 certain herbaceous plants with big flowers acid esters, PEG-15 glycerol
Stearate, PEG-15 glyceryl oleates, PEG-20 glyceryl triisostearates, PEG-10 laurates, PEG-10 stearic acid
One or more in ester, PEG-6 oleates, PEG-10 oleates.
Wherein, the PEG 30-80mol tweens are selected from PEG-30 castor oil hydrogenated, PEG-40 hydrogenated castors
Oil, PEG-60 castor oil hydrogenated, PEG-80 castor oil hydrogenated, oleth -50, PEG-60 castor oil hydrogenated laurates,
PEG-35 castor oil hydrogenated, PEG-45 castor oil hydrogenated, PEG-50 castor oil hydrogenated, PEG-54 castor oil hydrogenated, PEG-55 hydrogen
Change Oleum Ricini, PEG-30 castor oil hydrogenated isostearates, Cremophor RH40 isostearate, PEG-50 hydrogenated castors
Oily isostearate, PEG-58 castor oil hydrogenated isostearates, three isostearate of PEG-30 castor oil hydrogenated, PEG-40 hydrogen
Change three isostearate of Oleum Ricini, three isostearate of PEG-50 castor oil hydrogenated, three isostearic acid of PEG-60 castor oil hydrogenated
One or more in ester.
Transparent facial film base material of the present invention, can include following component：
It is water 84-88 weight portions, 1,3 butylene glycol 3-5 weight portions, glycerol 1-3 weight portions, isoprene 1-3 weight portions, sweet
Dish alkali 0.5-1.5 weight portions, sodium lactate 0.1-0.3 weight portions, allantoin 0.00001g, Anjidew NL50 0.2-0.7 weight portions, Tremella
(TREMELLA FUCIFORMIS) extract 0.005-0.03 weight portions, PEG-60 castor oil hydrogenated 0.2-0.4 weight portions, perfume (or spice)
Smart 0.01-0.03 weight portions, Herba Portulacae 0.05-0.02 weight portions, sodium citrate 0.3-0.7 weight portions, citric acid 0.03-0.07
Weight portion, silver 0.2-0.4 weight portions, nicotiamide 0.05-0.15 weight portions, trehalose 0.05-0.15 weight portions, glucosan
0.0005-0.002 weight portions, 0.00003 weight portion of denatonium benzoate, PCA ZN0.00001 weight portions, Alteromonad fermentation
Product extract 0.03-0.1 weight portions, 0.00001 weight portion of Kaolin, Margarita extract 0.0005-0.002 weight portions, ink
Angle algae (FUCUS VESICULOSUS) extract 0.0005-0.002 weight portions, postfermented tea bit of a bridle son (RIBES NIGRUM) seed oil
0.0005-0.002 weight portions, sturgeon roe beans extract 0.0005-0.002 weight portions, acrylic acid (ester) analog copolymer sodium
0.00001 weight portion, 0.00001 weight portion of decoyl hydroximic acid, 0.00001 weight portion of Sensiva SC50, allantoin
0.00001 weight portion.
The applicant is had found through years of researches：As oil components are nonpolarity or the low oils and fatss of polarity, and it is transparent
The polarity highest of the water in facial film base material, the present invention is with oil components, higher alcohol, PEG 6-20mol tweens, PEG
The polarity of 30-80mol tweens is the starting point, by add higher alcohol (end is high with OH groups, polarity),
PEG6-20mol tweens (the low mol tweens of PEG, polarity between higher alcohol and PEG 30-80mol it is non-from
The centre of sub- activating agent) and PEG 30-80mol tweens (the high mol tweens of PEG, polarity are higher) conduct
The solubilizing agent of oil components so that the low oil components of nonpolarity or polarity make to have individual intermediate polarity connection between water and oil
Oil components solubilising so as to realize disperseing oil components and solubilising extremely transparent can dissolve, and can be reached 50 μm to particle diameter by person
Below.
Additionally, the invention also discloses a kind of preparation method of above-mentioned transparent facial film, comprises the steps：
1) water intaking, 1,3 butylene glycol, glycerol, isoprene, glycine betaine, Sensiva SC50, sodium lactate, allantoin, PCA
Sodium, adds water phase pot, after being heated to 70-75 DEG C, stirs, in suction vacuum emulsifying machine；
2) oil components, higher alcohol, PEG 6-20mol tweens, PEG 30-80mol tweens are taken,
Oil phase pot is added, 60-65 DEG C is heated to, is stirred, in suction vacuum emulsifying machine；
3) vacuum emulsifying machine is opened, after 800-1200rpm/ point of rotating speed stirring 20-40 minutes, stopping stirring, cooling
To 35-45 DEG C；Add Tremella (TREMELLA FUCIFORMIS) extract, PEG-60 castor oil hydrogenated, essence, Herba Portulacae, lemon
Lemon acid sodium, citric acid, silver, nicotiamide, trehalose, glucosan, denatonium benzoate, PCA ZN, Alteromonad tunning are carried
Take thing, Kaolin, Margarita extract, Fucus Vesiculosus (FUCUS VESICULOSUS) extract, postfermented tea bit of a bridle (RIBES NIGRUM)
Seed oil, sturgeon roe beans extract, acrylic acid (ester) analog copolymer sodium, decoyl hydroximic acid, continue to stir, are cooled to room temperature；
Fill, obtains final product transparent facial film.
Compared with prior art, the present invention has the advantages that：
The present invention is made by higher alcohol, PEG 6-20mol tweens and PEG 30-80mol tweens
For the solubilizing agent of oil components, extremely transparent can dissolve oil components dispersion simultaneously solubilized, so that what is prepared is saturating
Bright facial film with the stable transparent outward appearance as traditional facial mask, and can by oil components solubilising to particle diameter reach 50 μm with
Under so as to there is to skin good moisturizing, oil is supplemented, increase skin water lock moistening effect.
Specific embodiment
The present invention is further illustrated below by specific embodiment, following examples are the present invention preferably embodiment party
Formula, but embodiments of the present invention are not limited by following embodiments.
Embodiments of the invention and comparative example adopt raw material as shown in table 1, but are not limited only to these raw materials：
Table 1
The method of testing of each performance indications：
The method of testing of appearance transparence stability：Sample preparation：The transparent facial film is taken, 50mL deionized waters are added,
50mL1 is added, 3- butanediols, mix homogeneously obtain transparent facial film mixture, standby；Test method：Take transparent facial film mixing
Thing, is placed in 40 DEG C of storages 1 month, 25 DEG C of room temperature and deposits 1 month, the storage 1 month of 5 DEG C of low temperature, recover to room temperature to observe outward appearance
Transparency.
The method of testing of the particle diameter of oil components, is tested using American-European gram LS900 type laser particle size analyzers.
Outward appearance light transmittance method of testing, using Shanghai Techcomp Instrument Ltd.'s ultraviolet-uisible spectrophotometer
UV1000。
Embodiment 1-4 and comparative example 1-5：The preparation of transparent facial film
First by a part of transparent facial film base material (water 86.77997g, 1,3 butylene glycol 4g, glycerol 2g, isoprene
1.5g, glycine betaine 1g, Sensiva SC50 0.00001g, sodium lactate 0.2, allantoin 0.00001g, Anjidew NL50 0.5g) add water
Phase pot, after being heated to 70-75 DEG C, stirs, in suction vacuum emulsifying machine；Then according to the proportioning addition oil components of table 1,
Higher alcohol, PEG 6-20mol tweens, PEG 30-80mol tweens, add oil phase pot, are heated to 60-
65 DEG C, stir, in suction vacuum emulsifying machine；Vacuum emulsifying machine is then turned on, and 30 points is stirred with 1000rpm/ point of rotating speed
Zhong Hou, stops stirring, is cooled to 40 DEG C；(Tremella (TREMELLA FUCIFORMIS) is extracted to add remaining transparent facial film base material
Thing 0.015g, PEG-60 castor oil hydrogenated 0.3g, essence 0.015g, Herba Portulacae 0.1g, sodium citrate 0.5g, citric acid 0.05g,
Silver-colored 0.3g, nicotiamide 0.1g, trehalose 0.1g, glucosan 0.001g, denatonium benzoate 0.00003g, PCA ZN0.00001g,
Alteromonad tunning extract 0.05g, Kaolin 0.00001g, Margarita extract 0.001g, Fucus Vesiculosus (FUCUS
VESICULOSUS) extract 0.001g, postfermented tea bit of a bridle son (RIBES NIGRUM) seed oil 0.001g, sturgeon roe beans extract
0.001g, acrylic acid (ester) analog copolymer sodium 0.00001g, decoyl hydroximic acid 0.00001g), continue to stir, be cooled to room
Temperature；Fill, obtains final product transparent facial film；The performance indications such as tables such as the appearance transparence stability of the transparent facial film of gained, particle diameter, light transmittance
Shown in 1.
Each group distribution ratio (g) and each testing performance index result of 1 embodiment 1-4 of table and comparative example 1-5
Continued 1
Claims (7)
1. a kind of transparent facial film, it is characterised in that by weight, including following component：
1 part of oil components；
1 part of higher alcohol；
PEG 6-20mol tween 0.35-0.4 parts；
PEG 30-80mol tween 0.35-0.4 parts；
Transparent facial film base material 99-110 parts.
2. according to the transparent facial film described in claim 1, it is characterised in that the oil components are selected from Vitamin E/tocopherol, life
Educate phenol acetass, 3 fatty acids and glyceride composition triglyceride, Jojoba oil, squalane, plant sterol/octyl group 12
One or more in alcohol lauroyl glutamate ester, plant sterol isostearate, cholesterol oil.
3. according to the transparent facial film described in claim 1, it is characterised in that the higher alcohol selected from octyl dodecanol, isooctadecanol,
One or more in hexyldecanol, oleyl alcohol.
4. transparent facial film according to claim 1, it is characterised in that the PEG 6-20mol tweens are selected from
PEG-6 iso stearic acid of glycerine ester, PEG-8 iso stearic acid of glycerine ester, laureth -7, PEG-7 glyceryl cocoates, olive
Olive oil PEG-7 esters, PEG-6 certain herbaceous plants with big flowers acid esters, PEG-15 glyceryl stearate, PEG-15 glyceryl oleates, PEG-20 glycerol three
One kind or several in isostearate, PEG-10 laurates, PEG-10 stearates, PEG-6 oleates, PEG-10 oleates
Kind.
5. transparent facial film according to claim 1, it is characterised in that the PEG 30-80mol tweens are selected from
PEG-30 castor oil hydrogenated, Cremophor RH40, PEG-60 castor oil hydrogenated, PEG-80 castor oil hydrogenated, oleth-
50th, PEG-60 castor oil hydrogenated laurate, PEG-35 castor oil hydrogenated, PEG-45 castor oil hydrogenated, PEG-50 hydrogenated castors
Oil, PEG-54 castor oil hydrogenated, PEG-55 castor oil hydrogenated, PEG-30 castor oil hydrogenated isostearates, PEG-40 hydrogenations
Oleum Ricini isostearate, PEG-50 castor oil hydrogenated isostearates, PEG-58 castor oil hydrogenated isostearates, PEG-
30 castor oil hydrogenated, three isostearate, three isostearate of PEG-40 castor oil hydrogenated, PEG-50 castor oil hydrogenated three are different
One or more in stearate, three isostearate of PEG-60 castor oil hydrogenated.
6. transparent facial film according to claim 1, it is characterised in that the transparent facial film base material includes water 84-88 weight
Part, 1,3 butylene glycol 3-5 weight portions, glycerol 1-3 weight portions, isoprene 1-3 weight portions, glycine betaine 0.5-1.5 weight portions, breast
Sour sodium 0.1-0.3 weight portions, allantoin 0.00001g, PCA sodium 0.2-0.7 weight portions, Tremella（TREMELLA
FUCIFORMIS）Extract 0.005-0.03 weight portions, PEG-60 castor oil hydrogenated 0.2-0.4 weight portions, essence 0.01-
0.03 weight portion, Herba Portulacae 0.05-0.02 weight portions, sodium citrate 0.3-0.7 weight portions, citric acid 0.03-0.07 weight portions,
Silver-colored 0.2-0.4 weight portions, nicotiamide 0.05-0.15 weight portions, trehalose 0.05-0.15 weight portions, glucosan 0.0005-
0.002 weight portion, 0.00003 weight portion of denatonium benzoate, PCA ZN0.00001 weight portions, Alteromonad tunning are carried
Take thing 0.03-0.1 weight portions, 0.00001 weight portion of Kaolin, Margarita extract 0.0005-0.002 weight portions, Fucus Vesiculosus
（FUCUS VESICULOSUS）Extract 0.0005-0.002 weight portions, postfermented tea bit of a bridle（RIBES NIGRUM）Seed oil 0.0005-
0.002 weight portion, sturgeon roe beans extract 0.0005-0.002 weight portions, acrylic acid（Ester）0.00001 weight of analog copolymer sodium
Part, 0.00001 weight portion of decoyl hydroximic acid, 0.00001 weight portion of Sensiva SC50,0.00001 weight portion of allantoin.
7. a kind of preparation method of the transparent facial film as described in any one of claim 1-6, it is characterised in that including following step
Suddenly：
1）Water intaking, 1,3 butylene glycol, glycerol, isoprene, glycine betaine, Sensiva SC50, sodium lactate, allantoin, PCA sodium,
Water phase pot is added, after being heated to 70-75 DEG C, is stirred, in suction vacuum emulsifying machine；
2）Oil components, higher alcohol, PEG 6-20mol tweens, PEG 30-80mol tweens are taken, is added
Oil phase pot, is heated to 60-65 DEG C, stirs, in suction vacuum emulsifying machine；
3）Vacuum emulsifying machine is opened, after 800-1200 rpm/ point of rotating speed stirring 20-40 minutes, stopping stirring being cooled to
35-45℃；Add Tremella（TREMELLA FUCIFORMIS）Extract, PEG-60 castor oil hydrogenated, essence, Herba Portulacae, lemon
Lemon acid sodium, citric acid, silver, nicotiamide, trehalose, glucosan, denatonium benzoate, PCA ZN, Alteromonad tunning are carried
Take thing, Kaolin, Margarita extract, Fucus Vesiculosus（FUCUS VESICULOSUS）Extract, postfermented tea bit of a bridle（RIBES NIGRUM）
Seed oil, sturgeon roe beans extract, acrylic acid（Ester）Analog copolymer sodium, decoyl hydroximic acid, continue to stir, are cooled to room temperature；
Fill, obtains final product transparent facial film.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611082648.3A CN106511256A (en) | 2016-11-30 | 2016-11-30 | Transparent mask and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611082648.3A CN106511256A (en) | 2016-11-30 | 2016-11-30 | Transparent mask and preparation method thereof |
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Family
ID=58355301
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| Application Number | Title | Priority Date | Filing Date |
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| CN201611082648.3A Pending CN106511256A (en) | 2016-11-30 | 2016-11-30 | Transparent mask and preparation method thereof |
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| Country | Link |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108524347A (en) * | 2017-12-28 | 2018-09-14 | 花安堂生物科技集团有限公司 | A kind of moisture saver mask and preparation method thereof |
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