CN106498748A - A kind of use for synthetic leather cloudy surface velvet inorganic agent and preparation method thereof - Google Patents

A kind of use for synthetic leather cloudy surface velvet inorganic agent and preparation method thereof Download PDF

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Publication number
CN106498748A
CN106498748A CN201610969255.8A CN201610969255A CN106498748A CN 106498748 A CN106498748 A CN 106498748A CN 201610969255 A CN201610969255 A CN 201610969255A CN 106498748 A CN106498748 A CN 106498748A
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China
Prior art keywords
mass parts
inorganic agent
synthetic leather
cloudy surface
silica
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CN201610969255.8A
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Chinese (zh)
Inventor
陈勇刚
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Jiangsu Baoze Polymer Materials Co Ltd
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Jiangsu Baoze Polymer Materials Co Ltd
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Priority to CN201610969255.8A priority Critical patent/CN106498748A/en
Publication of CN106498748A publication Critical patent/CN106498748A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/144—Alcohols; Metal alcoholates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/165—Ethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402—Amides imides, sulfamic acids

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatment And Processing Of Natural Fur Or Leather (AREA)

Abstract

The present invention relates to a kind of use for synthetic leather cloudy surface velvet inorganic agent and preparation method thereof.The use for synthetic leather cloudy surface velvet inorganic agent includes following components：Modified polyurethane, silica flatting silica, isopropanol, butyl ether, toluene, butanone and oleamide.The each component of use for synthetic leather cloudy surface velvet inorganic agent of the present invention is mutually coordinated, collective effect, and after processing leather surface, feel is fine and smooth, and bottom of trench velvet is strong, the leather gloss nature that is made with this kind of inorganic agent, and color clarification, resultant effect are good.

Description

A kind of use for synthetic leather cloudy surface velvet inorganic agent and preparation method thereof
Technical field
The present invention relates to a kind of use for synthetic leather cloudy surface velvet inorganic agent, is more particularly to applied to the conjunction of synthetic leather FEOL Finished leather cloudy surface velvet inorganic agent, while the invention also discloses the preparation method of the use for synthetic leather cloudy surface velvet inorganic agent.
Background technology
At present, after existing use for synthetic leather cloudy surface velvet inorganic agent processes leather surface, feel, bottom of trench velvet, not ten sub-argument Think.The synthetic leather of such cloudy surface velvet inorganic agent is applied, its gloss and color and luster are poor, and resultant effect is not fully up to expectations.Therefore, Need a kind of improved cloudy surface velvet inorganic agent.
Content of the invention
It is an object of the invention to provide a kind of use for synthetic leather cloudy surface velvet inorganic agent.
The use for synthetic leather cloudy surface velvet inorganic agent of the present invention is achieved through the following technical solutions：
Use for synthetic leather cloudy surface velvet inorganic agent disclosed in this invention, comprising following components：Modified polyurethane, silica Flatting silica, isopropanol, butyl ether, toluene, butanone and oleamide.
On the basis of the gross weight of resin, the proportioning of each component of the use for synthetic leather cloudy surface velvet inorganic agent that the present invention is provided Can be：35～38 mass parts of modified polyurethane, 3～5 mass parts of silica flatting silica, 9～12 mass parts of isopropanol, butyl ether 13～15 mass parts, 9～12 mass parts of toluene, 18～20 mass parts of butanone, 0～1 mass parts of oleamide.
In one embodiment of the invention, the proportioning of each component of use for synthetic leather cloudy surface velvet inorganic agent is as follows：Modified 35 mass parts of polyurethane, 5 mass parts of silica flatting silica, 12 mass parts of isopropanol, 15 mass parts of butyl ether, 12 mass of toluene Part, 20 mass parts of butanone, 1 mass parts of oleamide.
In another embodiment of the invention, the proportioning of each component of use for synthetic leather cloudy surface velvet inorganic agent is as follows：Modified 38 mass parts of polyurethane, 3 mass parts of silica flatting silica, 12 mass parts of isopropanol, 14 mass parts of butyl ether, 12 mass of toluene Part, 20 mass parts of butanone, 1 mass parts of oleamide.
In another embodiment of the invention, the proportioning of each component of use for synthetic leather cloudy surface velvet inorganic agent is as follows：Modified 37 mass parts of polyurethane, 5 mass parts of silica flatting silica, 12 mass parts of isopropanol, 15 mass parts of butyl ether, 12 mass of toluene Part, 18 mass parts of butanone, 1 mass parts of oleamide.
The present invention also provides a kind of preparation method of use for synthetic leather cloudy surface velvet inorganic agent, comprises the steps of：
1) by a part of modified polyurethane in formula, silica flatting silica, isopropanol, butyl ether, toluene, butanone and oil Sour acid amides stirs to grind and filters；
2) in step 1) another part modified polyurethane, uniform stirring is added in the mixture that obtains.
The proportioning of each component in the preparation method of the use for synthetic leather cloudy surface velvet inorganic agent of the present invention can be as follows：Modified 35～38 mass parts of polyurethane, 3～5 mass parts of silica flatting silica, 9～12 mass parts of isopropanol, 13～15 mass of butyl ether Part, 9～12 mass parts of toluene, 18～20 mass parts of butanone, 0～1 mass parts of oleamide.
Preferably, the proportioning of each component is as follows：35 mass parts of modified polyurethane, 5 mass parts of silica flatting silica, isopropyl 12 mass parts of alcohol, 15 mass parts of butyl ether, 12 mass parts of toluene, 20 mass parts of butanone, 1 mass parts of oleamide.
It is highly preferred that the proportioning of each component is as follows：38 mass parts of modified polyurethane, 3 mass parts of silica flatting silica are different 12 mass parts of propyl alcohol, 14 mass parts of butyl ether, 12 mass parts of toluene, 20 mass parts of butanone, 1 mass parts of oleamide.
It is highly preferred that the proportioning of each component is as follows：37 mass parts of modified polyurethane, 5 mass parts of silica flatting silica are different 12 mass parts of propyl alcohol, 15 mass parts of butyl ether, 12 mass parts of toluene, 18 mass parts of butanone, 1 mass parts of oleamide.
Due to adopting above technical scheme, the present invention to have the advantage that compared with prior art：
1. each component of use for synthetic leather cloudy surface velvet inorganic agent of the present invention is mutually coordinated, collective effect, processes leather Behind face, feel is fine and smooth, and bottom of trench velvet is strong, the leather gloss nature that is made with this kind of inorganic agent, and color clarification, resultant effect are good；
2. use for synthetic leather cloudy surface velvet inorganic agent of the present invention is applied on existing synthetic leather production line, technique letter Single, it is a kind of new material of back segment process, need not change production equipment increases cost；
3. the preparation method of use for synthetic leather cloudy surface velvet inorganic agent of the present invention is simple, without the need for using complicated machinery Process, saved production cost, be suitable to industrialized production.
Specific embodiment
Below by embodiment, technical solution of the present invention is described in detail, but protection scope of the present invention not office It is limited to the embodiment.
Embodiment 1
Use for synthetic leather cloudy surface velvet inorganic agent include 35 mass parts modified polyurethanes, 5 mass parts silica flatting silicas, 12 Mass parts isopropanol, 15 mass parts butyl ether, 12 mass parts toluene, 20 mass parts butanone, 1 mass parts oleamide.
The preparation method of above-mentioned use for synthetic leather cloudy surface velvet inorganic agent is：By 20 mass parts modified polyurethanes in formula, 5 Mass parts silica flatting silica, 12 mass parts isopropanols, 15 mass parts butyl ether, 12 mass parts toluene, 20 mass parts butanone, 1 Mass parts oleamide stirs to grind and filters；Then 15 mass parts modified polyurethanes are added in the mixture of gained, Described use for synthetic leather cloudy surface velvet inorganic agent is obtained final product after even stirring.The performance of obtained use for synthetic leather cloudy surface velvet inorganic agent Index is shown in Table 1.
The methods such as stirring, grinding, filtration employed in above-mentioned preparation process are customary way in the art.
Embodiment 2
Use for synthetic leather cloudy surface velvet inorganic agent include 38 mass parts modified polyurethanes, 3 mass parts silica flatting silicas, 12 Mass parts isopropanol, 14 mass parts butyl ether, 12 mass parts toluene, 20 mass parts butanone, 1 mass parts oleamide.
The preparation method of above-mentioned use for synthetic leather cloudy surface velvet inorganic agent is：By 20 mass parts modified polyurethanes in formula, 3 Mass parts silica flatting silica, 12 mass parts isopropanols, 14 mass parts butyl ether, 12 mass parts toluene, 20 mass parts butanone, 1 Mass parts oleamide stirs to grind and filters；Then 18 mass parts modified polyurethanes are added in the mixture of gained, Described use for synthetic leather cloudy surface velvet inorganic agent is obtained final product after even stirring.The performance of obtained use for synthetic leather cloudy surface velvet inorganic agent Index is shown in Table 1.
The methods such as stirring, grinding, filtration employed in above-mentioned preparation process are customary way in the art.
Embodiment 3
Use for synthetic leather cloudy surface velvet inorganic agent include 37 mass parts modified polyurethanes, 5 mass parts silica flatting silicas, 12 Mass parts isopropanol, 15 mass parts butyl ether, 12 mass parts, toluene, 18 mass parts butanone, 1 mass parts oleamide are constituted.
The preparation method of above-mentioned use for synthetic leather cloudy surface velvet inorganic agent is：By 20 mass parts modified polyurethanes in formula, 5 Mass parts silica flatting silica, 12 mass parts isopropanols, 15 mass parts butyl ether, 12 mass parts, toluene, 18 mass parts butanone, 1 Mass parts oleamide stirs to grind and filters；Then 17 mass parts modified polyurethanes are added in the mixture of gained, Described use for synthetic leather cloudy surface velvet inorganic agent is obtained final product after even stirring.The performance of obtained use for synthetic leather cloudy surface velvet inorganic agent Index is shown in Table 1.
The methods such as stirring, grinding, filtration employed in above-mentioned preparation process are customary way in the art.
Table 1
Presently preferred embodiments of the present invention is the foregoing is only, is not used for the practical range for limiting the present invention；If do not taken off From the spirit and scope of the present invention, the present invention is modified or equivalent, all should be covered in the claims in the present invention In the middle of protection domain.

Claims (10)

1. a kind of use for synthetic leather cloudy surface velvet inorganic agent, it is characterised in that comprising following components：Modified polyurethane, silica Flatting silica, isopropanol, butyl ether, toluene, butanone and oleamide.
2. use for synthetic leather cloudy surface velvet inorganic agent according to claim 1, it is characterised in that each component with such as Under：35～38 mass parts of modified polyurethane, 3～5 mass parts of silica flatting silica, 9～12 mass parts of isopropanol, butyl ether 13～ 15 mass parts, 9～12 mass parts of toluene, 18～20 mass parts of butanone, 0～1 mass parts of oleamide.
3. use for synthetic leather cloudy surface velvet inorganic agent according to claim 2, it is characterised in that each component with such as Under：35 mass parts of modified polyurethane, 5 mass parts of silica flatting silica, 12 mass parts of isopropanol, 15 mass parts of butyl ether, toluene 12 mass parts, 20 mass parts of butanone, 1 mass parts of oleamide.
4. use for synthetic leather cloudy surface velvet inorganic agent according to claim 2, it is characterised in that each component with such as Under：38 mass parts of modified polyurethane, 3 mass parts of silica flatting silica, 12 mass parts of isopropanol, 14 mass parts of butyl ether, toluene 12 mass parts, 20 mass parts of butanone, 1 mass parts of oleamide.
5. use for synthetic leather cloudy surface velvet inorganic agent according to claim 2, it is characterised in that each component with such as Under：37 mass parts of modified polyurethane, 5 mass parts of silica flatting silica, 12 mass parts of isopropanol, 15 mass parts of butyl ether, toluene 12 mass parts, 18 mass parts of butanone, 1 mass parts of oleamide.
6. the preparation method of the use for synthetic leather cloudy surface velvet inorganic agent described in claim 1, it is characterised in that comprising following step Suddenly：
1) by a part of modified polyurethane in formula, silica flatting silica, isopropanol, butyl ether, toluene, butanone and oleic acid acyl Amine stirs to grind and filters；
2) in step 1) another part modified polyurethane, uniform stirring is added in the mixture that obtains.
7. the preparation method of use for synthetic leather cloudy surface velvet inorganic agent according to claim 6, it is characterised in that each component Proportioning is as follows：35～38 mass parts of modified polyurethane, 3～5 mass parts of silica flatting silica, 9～12 mass parts of isopropanol, fourth 13～15 mass parts of ether, 9～12 mass parts of toluene, 18～20 mass parts of butanone, 0～1 mass parts of oleamide.
8. the preparation method of use for synthetic leather cloudy surface velvet inorganic agent according to claim 7, it is characterised in that each component Proportioning is as follows：35 mass parts of modified polyurethane, 5 mass parts of silica flatting silica, 12 mass parts of isopropanol, 15 mass of butyl ether Part, 12 mass parts of toluene, 20 mass parts of butanone, 1 mass parts of oleamide.
9. the preparation method of use for synthetic leather cloudy surface velvet inorganic agent according to claim 7, it is characterised in that each component Proportioning is as follows：38 mass parts of modified polyurethane, 3 mass parts of silica flatting silica, 12 mass parts of isopropanol, 14 mass of butyl ether Part, 12 mass parts of toluene, 20 mass parts of butanone, 1 mass parts of oleamide.
10. the preparation method of use for synthetic leather cloudy surface velvet inorganic agent according to claim 7, it is characterised in that each component Proportioning as follows：37 mass parts of modified polyurethane, 5 mass parts of silica flatting silica, 12 mass parts of isopropanol, 15 mass of butyl ether Part, 12 mass parts of toluene, 18 mass parts of butanone, 1 mass parts of oleamide.
CN201610969255.8A 2016-10-28 2016-10-28 A kind of use for synthetic leather cloudy surface velvet inorganic agent and preparation method thereof Pending CN106498748A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107326679A (en) * 2017-08-18 2017-11-07 江苏宝泽高分子材料股份有限公司 A kind of use for synthetic leather injection cloudy surface powder velvet inorganic agent and preparation method thereof
CN107326682A (en) * 2017-08-18 2017-11-07 江苏宝泽高分子材料股份有限公司 A kind of use for synthetic leather color inhibition cloudy surface velvet inorganic agent and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN102182064A (en) * 2010-12-01 2011-09-14 江苏宝泽高分子材料股份有限公司 Super black flock oil wax sense polishing treatment agent for synthetic leather and preparation method thereof
CN103103777A (en) * 2011-11-14 2013-05-15 江苏宝泽高分子材料股份有限公司 Matte injection-molding waxy-feel treatment agent for synthetic leather and preparation method thereof
CN103290691A (en) * 2013-05-21 2013-09-11 江苏宝泽高分子材料股份有限公司 Matte scratch-resistant powder smooth printing treatment agent for synthetic leather and preparation method thereof
CN103966854A (en) * 2014-05-08 2014-08-06 合肥市科天化工有限公司 Metallic fog-brightening water based treatment agent and preparation method thereof
CN104131466A (en) * 2014-07-22 2014-11-05 嘉兴禾大科技化学有限公司 Velvet feeling polyurethane leather surface conditioning agent and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102182064A (en) * 2010-12-01 2011-09-14 江苏宝泽高分子材料股份有限公司 Super black flock oil wax sense polishing treatment agent for synthetic leather and preparation method thereof
CN103103777A (en) * 2011-11-14 2013-05-15 江苏宝泽高分子材料股份有限公司 Matte injection-molding waxy-feel treatment agent for synthetic leather and preparation method thereof
CN103290691A (en) * 2013-05-21 2013-09-11 江苏宝泽高分子材料股份有限公司 Matte scratch-resistant powder smooth printing treatment agent for synthetic leather and preparation method thereof
CN103966854A (en) * 2014-05-08 2014-08-06 合肥市科天化工有限公司 Metallic fog-brightening water based treatment agent and preparation method thereof
CN104131466A (en) * 2014-07-22 2014-11-05 嘉兴禾大科技化学有限公司 Velvet feeling polyurethane leather surface conditioning agent and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107326679A (en) * 2017-08-18 2017-11-07 江苏宝泽高分子材料股份有限公司 A kind of use for synthetic leather injection cloudy surface powder velvet inorganic agent and preparation method thereof
CN107326682A (en) * 2017-08-18 2017-11-07 江苏宝泽高分子材料股份有限公司 A kind of use for synthetic leather color inhibition cloudy surface velvet inorganic agent and preparation method thereof

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