CN106497204A - A kind of SiO2Aeroge heat preservation putty and preparation method thereof - Google Patents
A kind of SiO2Aeroge heat preservation putty and preparation method thereof Download PDFInfo
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- CN106497204A CN106497204A CN201611091250.6A CN201611091250A CN106497204A CN 106497204 A CN106497204 A CN 106497204A CN 201611091250 A CN201611091250 A CN 201611091250A CN 106497204 A CN106497204 A CN 106497204A
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- parts
- aeroge
- heat preservation
- sio
- putty
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
Abstract
The invention discloses a kind of SiO2Aeroge heat preservation putty and preparation method thereof, which is by 1000～1100 parts of unsaturated polyester resin, 28～32 parts of titanium dioxide, 20～25 parts of organoclay, 1000～1200 parts of product powder spreading, 680～720 parts of mountain city powder, SiO290～100 parts of aeroge, 75～84 parts of triple superphosphate, 0.016 part of cobalt iso-octoate, 0.0003 part of methylamine are mixed into main putty successively, and are 100 by weight by main putty and firming agent:1～2 uniform mixing obtains final product SiO2Aeroge heat preservation putty.SiO is added in the heat preservation putty of the present invention2Aeroge, so as to improve its heat insulating ability, resistance to acids and bases and fire line, while utilize SiO2The thickening power of aeroge, reduces the addition of other components, reduces production cost.
Description
Technical field
The present invention relates to heat preservation putty technology of preparing, more particularly, to a kind of SiO2Aeroge heat preservation putty and its preparation side
Method.
Background technology
With continuous attention of the China to energy saving and environmental protection, energy-saving and emission-reduction are trends of the times, automobile making, work
The heat preservation technology of the industries such as industry equipment is also increasingly being strengthened.
Car paint is a kind of use requirement coating variety high and with high content of technology, in order to adapt to environmental requirement, drop
The VOC emission of low painting dressing automobiles, all in active development and utilizes environment-friendly type coating both at home and abroad, but the automobile of the production of prior art
Due to the restriction in equipment and process aspect, the heat-proof quality that produces car paint is poor, quality is low for coating.Therefore, existing market
Upper it is badly in need of a kind of heat preservation putty with excellent thermal insulation heat insulation effect.
Content of the invention
It is an object of the invention to overcoming above-mentioned technical deficiency, a kind of SiO is proposed2Aeroge heat preservation putty and its preparation side
Method, solve car paint in prior art heat-proof quality is poor, low-quality technical problem.
For reaching above-mentioned technical purpose, technical scheme provides a kind of SiO2Aeroge heat preservation putty, including weight
Amount is than being 100:1～2 main putty and firming agent, the main putty include following weight portion component：Unsaturated polyester resin
1000～1100 parts, 28～32 parts of titanium dioxide, 20～25 parts of organoclay, 1000～1200 parts of product powder spreading, mountain city powder 680～720
Part, SiO290～100 parts of aeroge, 75～84 parts of triple superphosphate, 0.016 part of cobalt iso-octoate, 0.0003 part of methylamine.
Preferably, the firming agent includes following weight portion component：35～45 parts of cyclohexanone peroxide, benzoyl peroxide first phthalein
35～45 parts, 2～3 parts of acetone, 13～15 parts of white carbon.
Preferably, the main putty includes following weight portion component：1000 parts of unsaturated polyester resin, 30 parts of titanium dioxide,
23 parts of organoclay, 1100 parts of product powder spreading, 700 parts of mountain city powder, SiO294 parts of aeroge, 80 parts of triple superphosphate, 0.016 part of cobalt iso-octoate,
0.0003 part of methylamine.
Preferably, the main putty includes following weight portion component：1100 parts of unsaturated polyester resin, 30 parts of titanium dioxide,
23 parts of organoclay, 1100 parts of product powder spreading, 700 parts of mountain city powder, SiO294 parts of aeroge, 80 parts of triple superphosphate, 0.016 part of cobalt iso-octoate,
0.0003 part of methylamine.
Preferably, the firming agent includes following weight portion component：40 parts of cyclohexanone peroxide, benzoyl peroxide first phthalein 40
Part, 2.5 parts of acetone, 14 parts of white carbon.
Preferably, the SiO2The specific surface area of aeroge is 800～10000m2/g.
Meanwhile, the present invention also provides a kind of preparation method of SiO2 aeroges heat preservation putty, comprises the steps：
(1) get the raw materials ready by following weight portion component：1000～1100 parts of unsaturated polyester resin, 28～32 parts of titanium dioxide, have
20～25 parts of machine soil, 1000～1200 parts of product powder spreading, 680～720 parts of mountain city powder, SiO290～100 parts of aeroge, triple superphosphate 75～
84 parts, 0.016 part of cobalt iso-octoate, 0.0003 part of methylamine, 35～45 parts of cyclohexanone peroxide, 35～45 parts of benzoyl peroxide first phthalein,
2～3 parts of acetone, 13～15 parts of white carbon；
(2) unsaturated polyester resin is added into reactor, then sequentially add titanium dioxide, organoclay, product powder spreading, mountain city
Powder, SiO2Aeroge, triple superphosphate, are stirring evenly and then adding into cobalt iso-octoate, are again stirring for uniform rear addition methylamine, stir and obtain final product
Main putty；
(3) uniformly cream will be ground after cyclohexanone peroxide, benzoyl peroxide first phthalein, acetone, white carbon mixing and stirring
Body obtains final product firming agent；
(4) it is 100 in mass ratio by main putty and firming agent:1～2 mix homogeneously, obtains final product SiO2 aeroge heat preservation putties.
Preferably, the mixing speed of step (2) is 300～500rad/min.
Preferably, the mixing speed of step (3) be 600～800rad/min, mixing time be 15～25 minutes.
Compared with prior art, SiO is added in heat preservation putty of the invention2Aeroge, so that improve its heat insulating ability, resistance to
Acidity of Aikalinity and fire line, while utilize SiO2The thickening power of aeroge, reduces the addition of other components, reduces production
Cost.
Specific embodiment
In order that the objects, technical solutions and advantages of the present invention become more apparent, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that specific embodiment described herein is not used to only in order to explain the present invention
Limit the present invention.
Embodiment 1
Embodiments of the invention 1 provide a kind of SiO2Aeroge heat preservation putty, its preparation method are as follows：
(1) main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1000g, titanium dioxide 30g, organoclay 23g, product are raised
Powder 1100g, mountain city powder 700g, SiO2Aeroge 94g, triple superphosphate 80g, cobalt iso-octoate 0.016g, methylamine 0.0003g, wherein, this reality
Apply a SiO2The preferred specific surface area of aeroge is 800～10000m2The SiO of/g2Aeroge；
Firming agent is got the raw materials ready by following weight：Cyclohexanone peroxide 40g, benzoyl peroxide first phthalein 40g, acetone 2.5g, white carbon
14g；
(2) unsaturated polyester resin is added into reactor, then sequentially add titanium dioxide, organoclay, product powder spreading, mountain city
Powder, SiO2Aeroge, triple superphosphate, are stirring evenly and then adding into cobalt iso-octoate, are again stirring for uniform rear addition methylamine, stir and obtain final product
Main putty；Wherein, reactor is preferably arranged to 300～500rad/min
(3) cyclohexanone peroxide, benzoyl peroxide first phthalein, acetone, white carbon are mixed and are incorporated in stirring for 600～800rad/min
Mix, uniformly mastic is ground after stirring and obtains final product firming agent；
(4) it is 100 in mass ratio by main putty and firming agent:1～2 mix homogeneously, obtains final product SiO2 aeroge heat preservation putties.
Embodiment 2
Embodiments of the invention 2 provide a kind of SiO2Aeroge heat preservation putty, its preparation method and 1 basic phase of embodiment
With its difference is, the present embodiment main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1100g, titanium dioxide 30g,
Organoclay 23g, product powder spreading 1100g, mountain city powder 700g, SiO2Aeroge 94g, triple superphosphate 80g, cobalt iso-octoate 0.016g, methylamine
0.0003g.
Embodiment 3
Embodiments of the invention 3 provide a kind of SiO2Aeroge heat preservation putty, its preparation method and 1 basic phase of embodiment
With its difference is, the present embodiment main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1150g, titanium dioxide 28g,
Organoclay 22g, product powder spreading 1050g, mountain city powder 690g, SiO2Aeroge 99g, triple superphosphate 75g, cobalt iso-octoate 0.016g, methylamine
0.0003g；Firming agent is got the raw materials ready by following weight：Cyclohexanone peroxide 35g, benzoyl peroxide first phthalein 37g, acetone 2g, white carbon
13g.
Embodiment 4
Embodiments of the invention 4 provide a kind of SiO2Aeroge heat preservation putty, its preparation method and 1 basic phase of embodiment
With its difference is, the present embodiment main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1000g, titanium dioxide 32g,
Organoclay 25g, product powder spreading 1200g, mountain city powder 700g, SiO2Aeroge 90g, triple superphosphate 80g, cobalt iso-octoate 0.016g, methylamine
0.0003g；Firming agent includes that following weight is got the raw materials ready：Cyclohexanone peroxide 38g, benzoyl peroxide first phthalein 35g, acetone 2g, white carbon
13g.
Embodiment 5
Embodiments of the invention 5 provide a kind of SiO2Aeroge heat preservation putty, its preparation method and 1 basic phase of embodiment
With its difference is, the present embodiment main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1020g, titanium dioxide 32g,
Organoclay 25g, product powder spreading 1000g, mountain city powder 710g, SiO2Aeroge 100g, triple superphosphate 83g, cobalt iso-octoate 0.016g, methylamine
0.0003g；Firming agent includes that following weight is got the raw materials ready：Cyclohexanone peroxide 40g, benzoyl peroxide first phthalein 43g, acetone 3g, white carbon
15g.
Embodiment 6
Embodiments of the invention 6 provide a kind of SiO2Aeroge heat preservation putty, its preparation method and 1 basic phase of embodiment
With its difference is, the present embodiment main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1080g, titanium dioxide 28g,
Organoclay 20g, product powder spreading 1100g, mountain city powder 680g, SiO2Aeroge 90g, triple superphosphate 75g, cobalt iso-octoate 0.016g, methylamine
0.0003g；Firming agent includes that following weight is got the raw materials ready：Cyclohexanone peroxide 45g, benzoyl peroxide first phthalein 36g, acetone 2g, white carbon
15g.
Embodiment 7
Embodiments of the invention 7 provide a kind of SiO2Aeroge heat preservation putty, its preparation method and 1 basic phase of embodiment
With its difference is, the present embodiment main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1029g, titanium dioxide 29g,
Organoclay 22g, product powder spreading 1000g, mountain city powder 720g, SiO2Aeroge 100g, triple superphosphate 81g, cobalt iso-octoate 0.016g, methylamine
0.0003g；Firming agent includes that following weight is got the raw materials ready：Cyclohexanone peroxide 44g, benzoyl peroxide first phthalein 44g, acetone 2g, white carbon
14g.
Embodiment 8
Embodiments of the invention 8 provide a kind of SiO2Aeroge heat preservation putty, its preparation method and 1 basic phase of embodiment
With its difference is, the present embodiment main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1100g, titanium dioxide 28g,
Organoclay 24g, product powder spreading 1050g, mountain city powder 712g, SiO2Aeroge 99g, triple superphosphate 78g, cobalt iso-octoate 0.016g, methylamine
0.0003g；Firming agent includes that following weight is got the raw materials ready：Cyclohexanone peroxide 41g, benzoyl peroxide first phthalein 37g, acetone 2.5g, Linesless charcoal
Black 14.5g.
Embodiment 9
Embodiments of the invention 9 provide a kind of SiO2Aeroge heat preservation putty, its preparation method and 1 basic phase of embodiment
With its difference is, the present embodiment main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1099g, titanium dioxide 31g,
Organoclay 23g, product powder spreading 1150g, mountain city powder 705g, SiO2Aeroge 93g, triple superphosphate 76g, cobalt iso-octoate 0.016g, methylamine
0.0003g；Firming agent includes that following weight is got the raw materials ready：Cyclohexanone peroxide 39g, benzoyl peroxide first phthalein 45g, acetone 3g, white carbon
13g.
Embodiment 10
Embodiments of the invention 10 provide a kind of SiO2Aeroge heat preservation putty, its preparation method are basic with embodiment 1
Identical, its difference is, the present embodiment main putty is got the raw materials ready by following weight：Unsaturated polyester resin 1011g, titanium dioxide
28g, organoclay 20g, product powder spreading 1111g, mountain city powder 680g, SiO2Aeroge 90g, triple superphosphate 77g, cobalt iso-octoate 0.016g, first
Amine 0.0003g；Firming agent includes that following weight is got the raw materials ready：Cyclohexanone peroxide 35g, benzoyl peroxide first phthalein 45g, acetone 3g, Linesless charcoal
Black 15g.
By the sample obtained by embodiment 1 to embodiment 10 and the comparison for carrying out multinomial performance with like product：
Heat conductivility is tested：Sample and like product obtained by embodiment 1 to embodiment 10 is respectively coated on one
On the external wall of testing cassete, test box body is provided with temperature sensor, test box body is placed at a temperature of 100 DEG C, is passed by temperature
The temperature change of sensor detection test tray interior.
Resistance to acids and bases is tested：Sample and like product obtained by embodiment 1 to embodiment 10 is respectively coated on one
On test board, by the test board 25 DEG C acid, place 30 days in aqueous slkali, observe the situation that coating weathers.
Fire line is tested：Sample and like product obtained by embodiment 1 to embodiment 10 is respectively coated on a survey
200 DEG C 1 hour of baking on test plate (panel), is carried out to test board, observes the situation that coating is cracked.
Viscosity is tested：Respectively to 2 kilograms of embodiments 1 to the sample and like product obtained by embodiment 10 in plus
Enter the water of 5L, be tuned into slip, respectively the material of embodiment 1 to 10 sample of embodiment and like product will be divided using consistometer
Do not tested, read slip diffusance size.
1. present invention of table and like product comparison sheet
As can be seen from Table 1, the present embodiment 1～10 prepare SiO2 aeroge heat preservation putties have good drying property,
Grinability, resistance to baking, resistance to impact and heat preservation and insulation, its can avoid automobile from being exposed to the sun and winter gas due to the summer sun
Temperature is too low and problem that vehicle interior temperature that cause is too high and too low, and the usage frequency and vehicle for reducing in-car air-conditioning is run hollow
The load of tune, saves oil consumption.And, SiO2 aeroges heat preservation putty tool prepared by the present embodiment 1～10 can be additionally used in industry
The insulation in the fields such as equipment, pipeline and shaped piece, improves the heat-insulating property of industrial equipment, pipeline and shaped piece etc. so that reach
The equipment coating being incubated to identical needed for purpose is thinner, and adhesive force is higher.
Compared with prior art, SiO is added in heat preservation putty of the invention2Aeroge, so that improve its heat insulating ability, resistance to
Acidity of Aikalinity and fire line, while utilize SiO2The thickening power of aeroge, reduces the addition of other components, reduces production
Cost, the preparation process is simple, easy to use of the present invention, starts from and is widely popularized.
The specific embodiment of present invention described above, does not constitute limiting the scope of the present invention.Any basis
Various other corresponding change and deformation that the technology design of the present invention is made, should be included in the guarantor of the claims in the present invention
In the range of shield.
Claims (9)
1. a kind of SiO2Aeroge heat preservation putty, it is characterised in that including weight ratio be 100:1～2 main putty and firming agent,
The main putty includes following weight portion component：1000～1100 parts of unsaturated polyester resin, 28～32 parts of titanium dioxide, organoclay
20～25 parts, 1000～1200 parts of product powder spreading, 680～720 parts of mountain city powder, SiO290～100 parts of aeroge, triple superphosphate 75～84
Part, 0.016 part of cobalt iso-octoate, 0.0003 part of methylamine.
2. SiO2 aeroges heat preservation putty according to claim 1, it is characterised in that the firming agent includes following weight
Part component：35～45 parts of cyclohexanone peroxide, 35～45 parts of benzoyl peroxide first phthalein, 2～3 parts of acetone, 13～15 parts of white carbon.
3. SiO2 aeroges heat preservation putty according to claim 1 and 2, it is characterised in that the main putty includes as follows
Weight portion component：1000 parts of unsaturated polyester resin, 30 parts of titanium dioxide, 23 parts of organoclay, 1100 parts of product powder spreading, mountain city powder 700
Part, SiO294 parts of aeroge, 80 parts of triple superphosphate, 0.016 part of cobalt iso-octoate, 0.0003 part of methylamine.
4. SiO2 aeroges heat preservation putty according to claim 1 and 2, it is characterised in that the main putty includes as follows
Weight portion component：1100 parts of unsaturated polyester resin, 30 parts of titanium dioxide, 23 parts of organoclay, 1100 parts of product powder spreading, mountain city powder 700
Part, SiO294 parts of aeroge, 80 parts of triple superphosphate, 0.016 part of cobalt iso-octoate, 0.0003 part of methylamine.
5. SiO2 aeroges heat preservation putty according to claim 2, it is characterised in that the firming agent includes following weight
Part component：40 parts of cyclohexanone peroxide, 40 parts of benzoyl peroxide first phthalein, 2.5 parts of acetone, 14 parts of white carbon.
6. SiO2 aeroges heat preservation putty according to claim 1, it is characterised in that the SiO2The specific surface of aeroge
Product is 800～10000m2/g.
7. a kind of preparation method of SiO2 aeroges heat preservation putty, it is characterised in that comprise the steps：
(1) get the raw materials ready by following weight portion component：1000～1100 parts of unsaturated polyester resin, 28～32 parts of titanium dioxide, organoclay
20～25 parts, 1000～1200 parts of product powder spreading, 680～720 parts of mountain city powder, SiO290～100 parts of aeroge, triple superphosphate 75～84
Part, 0.016 part of cobalt iso-octoate, 0.0003 part of methylamine, 35～45 parts of cyclohexanone peroxide, 35～45 parts of benzoyl peroxide first phthalein, third
2～3 parts of ketone, 13～15 parts of white carbon；
(2) into reactor add unsaturated polyester resin, then sequentially add titanium dioxide, organoclay, product powder spreading, mountain city powder,
SiO2Aeroge, triple superphosphate, are stirring evenly and then adding into cobalt iso-octoate, are again stirring for uniform rear addition methylamine, and stir i.e. winner
Body ash；
(3) will grind after cyclohexanone peroxide, benzoyl peroxide first phthalein, acetone, white carbon mixing and stirring uniformly that mastic is i.e.
Obtain firming agent；
(4) it is 100 in mass ratio by main putty and firming agent:1～2 mix homogeneously, obtains final product SiO2 aeroge heat preservation putties.
8. the preparation method of SiO2 aeroges heat preservation putty according to claim 7, it is characterised in that step (2)
Mixing speed be 300～500rad/min.
9. the preparation method of SiO2 aeroges heat preservation putty according to claim 7, it is characterised in that step (3)
Mixing speed be 600～800rad/min, mixing time be 15～25 minutes.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611091250.6A CN106497204A (en) | 2016-12-01 | 2016-12-01 | A kind of SiO2Aeroge heat preservation putty and preparation method thereof |
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| CN201611091250.6A CN106497204A (en) | 2016-12-01 | 2016-12-01 | A kind of SiO2Aeroge heat preservation putty and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106978003A (en) * | 2017-05-23 | 2017-07-25 | 龚伟 | A kind of automobile heat insulation insulation nanometer putty paste and preparation method thereof |
| CN108997903A (en) * | 2018-06-07 | 2018-12-14 | 上海沐皿新材料科技有限公司 | Aeroge insulation fire-proof and water-proof multifunctional combination application material and preparation method thereof |
| CN110387183A (en) * | 2019-08-22 | 2019-10-29 | 李金娣 | A kind of aeroge multifunctional material and preparation method thereof |
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| CN102504638A (en) * | 2011-11-28 | 2012-06-20 | 天长市通天化工有限责任公司 | Normal-temperature fast-drying polymer putty |
| CN102898110A (en) * | 2012-09-17 | 2013-01-30 | 江苏塞尚低碳科技有限公司 | Thick-layer putty for heat insulation of wall |
| CN105802318A (en) * | 2016-04-22 | 2016-07-27 | 北京虹霞正升涂料有限责任公司 | Paste energy storage nano heat insulating exterior wall putty and preparation method thereof |
| CN106009868A (en) * | 2015-03-24 | 2016-10-12 | 关西涂料株式会社 | Putty composition and repair coating method with same |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102504638A (en) * | 2011-11-28 | 2012-06-20 | 天长市通天化工有限责任公司 | Normal-temperature fast-drying polymer putty |
| CN102898110A (en) * | 2012-09-17 | 2013-01-30 | 江苏塞尚低碳科技有限公司 | Thick-layer putty for heat insulation of wall |
| CN106009868A (en) * | 2015-03-24 | 2016-10-12 | 关西涂料株式会社 | Putty composition and repair coating method with same |
| CN105802318A (en) * | 2016-04-22 | 2016-07-27 | 北京虹霞正升涂料有限责任公司 | Paste energy storage nano heat insulating exterior wall putty and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106978003A (en) * | 2017-05-23 | 2017-07-25 | 龚伟 | A kind of automobile heat insulation insulation nanometer putty paste and preparation method thereof |
| CN108997903A (en) * | 2018-06-07 | 2018-12-14 | 上海沐皿新材料科技有限公司 | Aeroge insulation fire-proof and water-proof multifunctional combination application material and preparation method thereof |
| CN110387183A (en) * | 2019-08-22 | 2019-10-29 | 李金娣 | A kind of aeroge multifunctional material and preparation method thereof |
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