CN106490007A - A kind of method of preventing and treating Citrus Huanglongbing pathogen - Google Patents

A kind of method of preventing and treating Citrus Huanglongbing pathogen Download PDF

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CN106490007A
CN106490007A CN201610869664.0A CN201610869664A CN106490007A CN 106490007 A CN106490007 A CN 106490007A CN 201610869664 A CN201610869664 A CN 201610869664A CN 106490007 A CN106490007 A CN 106490007A
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parts
salt
potassium
preventing
huanglongbing pathogen
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杨龙俊
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Zijin Mountain Jiaxin Fruit And Vegetable Co Ltd
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Zijin Mountain Jiaxin Fruit And Vegetable Co Ltd
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G13/00—Protecting plants
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/10—Aromatic or araliphatic carboxylic acids, or thio analogues thereof; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
    • A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
    • A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
    • A01N43/38—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06—Aluminium; Calcium; Magnesium; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/08—Alkali metal chlorides; Alkaline earth metal chlorides
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/12—Iodine, e.g. iodophors; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16—Heavy metals; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/26—Phosphorus; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia

Abstract

The invention discloses a kind of method of preventing and treating Citrus Huanglongbing pathogen, including winter clear garden, sprays the medicine for normally killing diaphorina citri, by the annual preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition 13 times of spraying before Citrus summer shoot is sprouted.The method of the present invention prevents and treats Citrus Huanglongbing pathogen, can improve yield and sugar content, and Citrus are in good taste, and appearance color and luster is mellow and full, and quality is high, higher than the using effect of conventional control Citrus Huanglongbing pathogen pharmaceutical composition.

Description

A kind of method of preventing and treating Citrus Huanglongbing pathogen
【Technical field】
The invention belongs to Citrus diseases prevention technical field, and in particular to a kind of method of preventing and treating Citrus Huanglongbing pathogen.
【Background technology】
Platymiscium under Citrus (Citrus reticulata Blanco) category Rutaceae.Property happiness warm and moist weather, resist cold Property is slightly strong compared with Fructus Citri grandiss, Citrus aurantium Linn., Fructus Citri sinensiss.Rutaceae Aurantioideae is distributed in 16 ° -37 ° of north latitude.It is tropical, subtropical evergreen fruit trees (are removed Beyond trifoliate orange), there are 3 category as Economical cultivation：Poncirus, Citrus and Fortunella.China and the Citrus chachiensis Hort. of other countries of world cultivation Fructus Citri tangerinae is mainly Citrus.
Citrus Huanglongbing pathogen is systemic disease, is commonly called as " cancer " of Citrus, still pasts medical help, can only chop at a tree after infection.Through Diaphorina citri is propagated, and is destroyed by the Citrus that Candidatus liberibacter (Candidatus Liberibacteria asiaticus) causes Sexually transmitted disease (STD) does harm to.In recent years, numerous Chinese scholars are studied to yellow twig, and achieve some gratifying results, but due to HUANGLONG Sick pathogen cannot artificial culture, the screening of the pathological research of yellow twig, disease-resistant medicament and disease-resistant variety is not still dashed forward Broken property progress, therefore currently without preventing and treating the effective agent of yellow twig.
The main media for propagating yellow twig is diaphorina citri.Diaphorina citri belongs to Homoptera, and Psyllidae, it are to propagate Citrus The main insect vector of yellow twig, is the main cause for causing Citrus Huanglongbing pathogen to propagate, spread.It is tender that diaphorina citri takes food band poison Poison can be passed just after leaf 2h, single adult passes sick rate and is up to 70%-80%, diaphorina citri have efficiently pass disease, lifelong band poison, with The features such as wind closely spreads and quickly passes poison.It was verified that just there is Citrus Huanglongbing pathogen where having diaphorina citri, Citrus are controlled Wood louse, it is the important measures for controlling Citrus Huanglongbing pathogen at present to cut off disease spread.So, diaphorina citri is prevented and kill off using chemical agent It is the topmost method of prevention and control Citrus Huanglongbing pathogen.However, present biological pesticide, effective drug duration is short, substantially no more than 6d, frequently Laxative both increased the burden of orchard worker, also increase labor cost, also cause diaphorina citri to generate a large amount of pesticide anti- The property of medicine, insecticidal effect decline substantially.Find the task of top priority that additive method prevention and control diaphorina citri is current Citrus Huanglongbing pathogen prevention and control.
Additionally, other existing preventing and treating Citrus Huanglongbing pathogens medicines using rear exist improve orange yield and sugar content rate low, The problems such as mouthfeel and general appearance color and luster.
【Content of the invention】
The present invention provides a kind of method of preventing and treating Citrus Huanglongbing pathogen, and to solve present biological pesticide, effective drug duration is short, effect Really poor, and the medicine of existing preventing and treating Citrus Huanglongbing pathogen using rear exist improve orange yield and sugar content rate is low, mouthfeel and outer The problems such as table color and luster is general.The method of the present invention prevents and treats Citrus Huanglongbing pathogen, can improve yield and sugar content, and Citrus are in good taste, Appearance color and luster is mellow and full, and quality is high, higher than the using effect of conventional control Citrus Huanglongbing pathogen pharmaceutical composition.
For solving above technical problem, the present invention is employed the following technical solutions：
A kind of method of preventing and treating Citrus Huanglongbing pathogen, including winter clear garden, sprays the medicine for normally killing diaphorina citri, passes through Annual preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition 1-3 time of spraying before Citrus summer shoot is sprouted；The preventing and treating Citrus Huanglongbing pathogen medicine Compositions in units of weight portion, including following raw material：Folium Artemisiae Argyi 120-150 parts, paulownia sawdust 100-120 part, Herba Sophorae alopecuroidiss 90- 110 parts, Cortex Magnoliae Officinalis 80-100 part, Melia azedarach L. 60-90 parts, Celastrus angulatus 55-86 parts, ailanthus altissima (mill.) swingle 52-78 parts, Caulis et Folium Lactucae sativae 45-68 parts, potassium salt 2-3 Part, microcosmic salt 1-3 parts, nitrogen salt 1-2 parts, calcium salt 0.6-0.9 parts, magnesium salt 0.6-0.9 parts, iodine salt 0.2-0.4 parts, boron salt 0.2-0.4 Part, molybdenum salt 0.2-0.4 parts, zinc salt 0.2-0.4 parts, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 parts, iron salt 0.2-0.4 parts, dimension life Plain 0.2-0.4 parts, aminoacid 0.2-0.3 parts, indolebutyric acid 0.06-0.09 parts, gibberellins 0.06-0.09 parts, 6- benzyl gland fats Purine 0.06-0.08 parts, naphthalene acetic acid 0.04-0.06 parts, agar 0.1-0.3 parts, kinetins 0.04-0.06 parts, polyvinylpyrrolidine Ketone 0.8-2.4 parts, sodium methylene bis-naphthalene sulfonate 0.6-1.8 parts, Dupont EEA2112AC compatilizer 1-1.5 parts, Pomacea canaliculata powder 0.6-1.5 parts, alkyl sulfate potassium 0.4-1.4 parts, acrylate 0.5-0.8 parts, glycidoxy-propyltrimethoxy silane 0.6-1.6 parts, xanthan gum 0.5-1.5 parts, ethanol 2000-6000 parts；
The potassium salt is composed of the following components：Potassium chloride 0.6-0.8 parts, potassium sulfate 0.5-0.6 parts, potassium nitrate 0.4-0.6 Part, potassium carbonate 0.3-0.5 parts, potassium bicarbonate 0.2-0.5 parts；
The microcosmic salt is composed of the following components：Calcium phosphate 0.3-0.8 parts, magnesium phosphate 0.3-0.8 parts, iron phosphate 0.2-0.7 Part, zinc phosphate 0.2-0.7 parts；
The nitrogen salt is composed of the following components：Ammonium hydrogen carbonate 0.4-0.8 parts, ammonium carbonate 0.3-0.6 parts, ammonium chloride 0.3- 0.6 part；
The calcium salt is composed of the following components：Calcium glycine 0.3-0.4 parts, calcium chloride 0.2-0.3 parts, sulphuric acid Asia calcium 0.1- 0.2 part；
The magnesium salt is composed of the following components：Magnesium glycinate 0.3-0.4 parts, magnesium chloride 0.2-0.3 parts, sulphuric acid Asia magnesium 0.1- 0.2 part；
The iodine salt is composed of the following components：Sodium iodide 0.1-0.2 parts, potassium iodate 0.1-0.2 parts；
The vitamin is composed of the following components：Raw element A0.08-0.14 parts, vitamin B10.08-0.12 parts, vitamin B20.02-0.08 parts, vitamin C 0.02-0.06 parts；
The aminoacid is composed of the following components：Glycine 0.08-0.1 parts, isoleucine 0.06-0.08 parts, proline 0.04-0.07 parts, phenylalanine 0.02-0.05 parts；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The xanthan gum is stabilizer；
The preparation method of described preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition, comprises the following steps：
S1：By Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae co-grinding, mixed Thing I, mixture I is added in ethanol, is 1 in solid-liquid ratio:14-16, ultrasonic power is 200-300W, and concentration of alcohol is 65%-80%, Extracting temperature are to extract medicinal liquid 18-24min at 66-72 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 3000-5000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Pomacea canaliculata powder, alkylsurfuric acid Ester potassium, acrylate, glycidoxy-propyltrimethoxy silane, xanthan gum, are 42-50 DEG C in temperature, and rotating speed is 100-300r/ Stirring and dissolving 20-30min under min, is obtained mixed liquor；
S4：Mixed liquor obtained in step S3 is concentrated into water content≤22% in the case where temperature is for 60-80 DEG C, mixture is obtained Ⅱ；
S5：Mixture obtained in step S4 II is dried to water content≤6% in the case where temperature is for 84-88 DEG C, is then crushed, 120-260 mesh sieve is crossed, gained powder adopts pulse vacuum pressure steam sterilizer in temperature for 134-136 DEG C, and pressure is Sterilize under 210-230KPa 3-4min, and preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition is obtained.
Further, the boron salt is sodium tetraborate.
Further, the molybdenum salt is potassium molybdate.
Further, the zinc salt is zinc chloride.
Further, the manganese salt is manganese chloride.
Further, the mantoquita is copper chloride.
Further, the iron salt is iron chloride.
The invention has the advantages that：
(1) preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition composition of the invention is nontoxic, and noresidue will not bring environmental pollution；
(2) method of the present invention preventing and treating Citrus Huanglongbing pathogen, can improve yield and sugar content, and Citrus are in good taste, appearance color Pool is mellow and full, and quality is high, higher than conventional control Citrus Huanglongbing pathogen pharmaceutical composition using effect and a kind of Patent Application Publication " Citrus Prevention and controls (the publication number of yellow twig：CN104521629A the butralin using effect in) "；
(3) preventing and treating Citrus Huanglongbing pathogen process for producing medicine composition of the invention is simple, and low cost is easy to use, drug effect For up to 1-2 month, application effect was good, is conducive to popularization and application.
【Specific embodiment】
For ease of more fully understanding the present invention, it is illustrated by following examples, these embodiments belong to the present invention's Protection domain, but do not limit the scope of the invention.
In an embodiment, the method for the preventing and treating Citrus Huanglongbing pathogen, including winter clear garden, sprays Medicine, by annual preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition 1-3 time of spraying before Citrus summer shoot is sprouted；The preventing and treating Citrus chachiensis Hort. Orange imperial medicine compositionss in units of weight portion, including following raw material：Folium Artemisiae Argyi 120-150 parts, paulownia sawdust 100-120 Part, Herba Sophorae alopecuroidiss 90-110 parts, Cortex Magnoliae Officinalis 80-100 part, Melia azedarach L. 60-90 parts, Celastrus angulatus 55-86 parts, ailanthus altissima (mill.) swingle 52-78 parts, Caulis et Folium Lactucae sativae 45- 68 parts, potassium salt 2-3 parts, microcosmic salt 1-3 parts, nitrogen salt 1-2 parts, calcium salt 0.6-0.9 parts, magnesium salt 0.6-0.9 parts, iodine salt 0.2-0.4 parts, Boron salt 0.2-0.4 part, molybdenum salt 0.2-0.4 parts, zinc salt 0.2-0.4 parts, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 parts, iron salt 0.2-0.4 parts, vitamin 0.2-0.4 parts, aminoacid 0.2-0.3 parts, indolebutyric acid 0.06-0.09 parts, gibberellins 0.06-0.09 Part, 6- benzyl gland fat purine 0.06-0.08 parts, naphthalene acetic acid 0.04-0.06 parts, agar 0.1-0.3 parts, kinetins 0.04-0.06 parts, Polyvinylpyrrolidone 0.8-2.4 parts, sodium methylene bis-naphthalene sulfonate 0.6-1.8 parts, Dupont EEA2112AC compatilizer 1- 1.5 parts, Pomacea canaliculata powder 0.6-1.5 parts, alkyl sulfate potassium 0.4-1.4 parts, acrylate 0.5-0.8 parts, epoxypropoxy Trimethoxy silane 0.6-1.6 parts, xanthan gum 0.5-1.5 parts, ethanol 2000-6000 parts；
The potassium salt is composed of the following components：Potassium chloride 0.6-0.8 parts, potassium sulfate 0.5-0.6 parts, potassium nitrate 0.4-0.6 Part, potassium carbonate 0.3-0.5 parts, potassium bicarbonate 0.2-0.5 parts；
The microcosmic salt is composed of the following components：Calcium phosphate 0.3-0.8 parts, magnesium phosphate 0.3-0.8 parts, iron phosphate 0.2-0.7 Part, zinc phosphate 0.2-0.7 parts；
The nitrogen salt is composed of the following components：Ammonium hydrogen carbonate 0.4-0.8 parts, ammonium carbonate 0.3-0.6 parts, ammonium chloride 0.3- 0.6 part；
The calcium salt is composed of the following components：Calcium glycine 0.3-0.4 parts, calcium chloride 0.2-0.3 parts, sulphuric acid Asia calcium 0.1- 0.2 part；
The magnesium salt is composed of the following components：Magnesium glycinate 0.3-0.4 parts, magnesium chloride 0.2-0.3 parts, sulphuric acid Asia magnesium 0.1- 0.2 part；
The iodine salt is composed of the following components：Sodium iodide 0.1-0.2 parts, potassium iodate 0.1-0.2 parts；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.08-0.14 parts, vitamin B10.08-0.12 parts, vitamin B20.02-0.08 parts, vitamin C 0.02-0.06 parts；
The aminoacid is composed of the following components：Glycine 0.08-0.1 parts, isoleucine 0.06-0.08 parts, proline 0.04-0.07 parts, phenylalanine 0.02-0.05 parts；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The xanthan gum is stabilizer；
The preparation method of described preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition, comprises the following steps：
S1：By Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae co-grinding, mixed Thing I, mixture I is added in ethanol, is 1 in solid-liquid ratio:14-16, ultrasonic power is 200-300W, and concentration of alcohol is 65%-80%, Extracting temperature are to extract medicinal liquid 18-24min at 66-72 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 3000-5000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Pomacea canaliculata powder, alkylsurfuric acid Ester potassium, acrylate, glycidoxy-propyltrimethoxy silane, xanthan gum, are 42-50 DEG C in temperature, and rotating speed is 100-300r/ Stirring and dissolving 20-30min under min, is obtained mixed liquor；
S4：Mixed liquor obtained in step S3 is concentrated into water content≤22% in the case where temperature is for 60-80 DEG C, mixture is obtained Ⅱ；
S5：Mixture obtained in step S4 II is dried to water content≤6% in the case where temperature is for 84-88 DEG C, is then crushed, 120-260 mesh sieve is crossed, gained powder adopts pulse vacuum pressure steam sterilizer in temperature for 134-136 DEG C, and pressure is Sterilize under 210-230KPa 3-4min, and preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition is obtained.
It is illustrated below by more specifically embodiment.
Embodiment 1
A kind of method of preventing and treating Citrus Huanglongbing pathogen, including winter clear garden, sprays the medicine for normally killing diaphorina citri, passes through The annual preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition 2 times of spraying before Citrus summer shoot is sprouted；The preventing and treating Citrus Huanglongbing pathogen medicine Compositionss in units of weight portion, including following raw material：135 parts of Folium Artemisiae Argyi, 110 parts of paulownia sawdust, 100 parts of Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis 90 Part, 75 parts of Melia azedarach L., 70 parts of Celastrus angulatus, 70 parts of ailanthus altissima (mill.) swingle, 55 parts of Caulis et Folium Lactucae sativae, 2.5 parts of potassium salt, 2 parts of microcosmic salt, 1.5 parts of nitrogen salt, calcium salt 0.8 Part, 0.8 part of magnesium salt, 0.3 part of iodine salt, 0.3 part of boron salt, 0.3 part of molybdenum salt, 0.3 part of zinc salt, 0.3 part of manganese salt, 0.3 part of mantoquita, iron salt 0.3 part, 0.3 part of vitamin, 0.2 part of aminoacid, 0.08 part of indolebutyric acid, 0.08 part of gibberellins, 0.07 part of 6- benzyl gland fats purine, 0.05 part of naphthalene acetic acid, 0.2 part of agar, 0.05 part of kinetins, 1.6 parts of polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate 1.2 Part, 1.2 parts of Dupont EEA2112AC compatilizers, 1 part of Pomacea canaliculata powder, 1 part of alkyl sulfate potassium, 0.7 part of acrylate, ring 1.2 parts of the third oxygen propyl trimethoxy silicane of oxygen, 1 part of xanthan gum, 4000 parts of ethanol；
The potassium salt is composed of the following components：0.7 part of potassium chloride, 0.5 part of potassium sulfate, 0.4 part of potassium nitrate, potassium carbonate 0.5 Part, 0.4 part of potassium bicarbonate；
The microcosmic salt is composed of the following components：0.6 part of calcium phosphate, 0.6 part of magnesium phosphate, 0.5 part of iron phosphate, zinc phosphate 0.3 Part；
The nitrogen salt is composed of the following components：0.6 part of ammonium hydrogen carbonate, 0.5 part of ammonium carbonate, 0.4 part of ammonium chloride；
The calcium salt is composed of the following components：0.3 part of calcium glycine, 0.3 part of calcium chloride, 0.2 part of the calcium in sulphuric acid Asia；
The magnesium salt is composed of the following components：0.3 part of magnesium glycinate, 0.3 part of magnesium chloride, 0.2 part of the magnesium in sulphuric acid Asia；
The iodine salt is composed of the following components：0.2 part of sodium iodide, 0.1 part of potassium iodate；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.1 parts, vitamin B10.1 part, vitamin B20.05 part, dimension life Plain C0.05 parts；
The aminoacid is composed of the following components：0.08 part of glycine, 0.06 part of isoleucine, 0.04 part of proline, benzene 0.02 part of alanine；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The xanthan gum is stabilizer；
The preparation method of described preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition, comprises the following steps：
S1：By Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae co-grinding, mixed Thing I, mixture I is added in ethanol, is 1 in solid-liquid ratio:15, ultrasonic power is 250W, and concentration of alcohol is 75%, extracts Temperature is to extract medicinal liquid 20min at 68 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 4000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Pomacea canaliculata powder, alkylsurfuric acid Ester potassium, acrylate, glycidoxy-propyltrimethoxy silane, xanthan gum, are 46 DEG C in temperature, and rotating speed is to stir under 200r/min Dissolving 25min is mixed, mixed liquor is obtained；
S4：It is 22% that mixed liquor obtained in step S3 is concentrated into water content in the case where temperature is for 70 DEG C, and mixture II is obtained；
S5：It is 6% that mixture obtained in step S4 II is dried to water content in the case where temperature is for 86 DEG C, then crushes, mistake 200 mesh sieve, gained powder adopt pulse vacuum pressure steam sterilizer in temperature for 135 DEG C, and pressure is to sterilize under 220KPa 3.5min, is obtained preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition.
Embodiment 2
A kind of method of preventing and treating Citrus Huanglongbing pathogen, including winter clear garden, sprays the medicine for normally killing diaphorina citri, passes through The annual preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition 3 times of spraying before Citrus summer shoot is sprouted；The preventing and treating Citrus Huanglongbing pathogen medicine Compositionss in units of weight portion, including following raw material：120 parts of Folium Artemisiae Argyi, 100 parts of paulownia sawdust, 90 parts of Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis 80 Part, 60 parts of Melia azedarach L., 55 parts of Celastrus angulatus, 52 parts of ailanthus altissima (mill.) swingle, 45 parts of Caulis et Folium Lactucae sativae, 2 parts of potassium salt, 1 part of microcosmic salt, 1 part of nitrogen salt, 0.6 part of calcium salt, magnesium 0.6 part of salt, 0.2 part of iodine salt, 0.2 part of boron salt, 0.2 part of molybdenum salt, 0.2 part of zinc salt, 0.2 part of manganese salt, 0.2 part of mantoquita, iron salt 0.2 Part, 0.2 part of vitamin, 0.2 part of aminoacid, 0.06 part of indolebutyric acid, 0.06 part of gibberellins, 0.06 part of 6- benzyl gland fats purine, naphthalene 0.04 part of acetic acid, 0.1 part of agar, 0.04 part of kinetins, 0.8 part of polyvinylpyrrolidone, 0.6 part of sodium methylene bis-naphthalene sulfonate, 1 part of Dupont EEA2112AC compatilizers, 0.6 part of Pomacea canaliculata powder, 0.4 part of alkyl sulfate potassium, 0.5 part of acrylate, epoxy Third 0.6 part of oxygen propyl trimethoxy silicane, 0.5 part of xanthan gum, 2000 parts of ethanol；
The potassium salt is composed of the following components：0.6 part of potassium chloride, 0.5 part of potassium sulfate, 0.4 part of potassium nitrate, potassium carbonate 0.3 Part, 0.2 part of potassium bicarbonate；
The microcosmic salt is composed of the following components：0.3 part of calcium phosphate, 0.3 part of magnesium phosphate, 0.2 part of iron phosphate, zinc phosphate 0.2 Part；
The nitrogen salt is composed of the following components：0.4 part of ammonium hydrogen carbonate, 0.3 part of ammonium carbonate, 0.3 part of ammonium chloride；
The calcium salt is composed of the following components：0.3 part of calcium glycine, 0.2 part of calcium chloride, 0.1 part of the calcium in sulphuric acid Asia；
The magnesium salt is composed of the following components：0.3 part of magnesium glycinate, 0.2 part of magnesium chloride, 0.1 part of the magnesium in sulphuric acid Asia；
The iodine salt is composed of the following components：0.1 part of sodium iodide, 0.1 part of potassium iodate；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.08 parts, vitamin B10.08 part, vitamin B20.02 part, dimension Raw element C0.02 parts；
The aminoacid is composed of the following components：0.08 part of glycine, 0.06 part of isoleucine, 0.04 part of proline, benzene 0.02 part of alanine；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The xanthan gum is stabilizer；
The preparation method of described preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition, comprises the following steps：
S1：By Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae co-grinding, mixed Thing I, mixture I is added in ethanol, is 1 in solid-liquid ratio:14, ultrasonic power is 200W, and concentration of alcohol is 65%, extracts Temperature is to extract medicinal liquid 24min at 66 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 3000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Pomacea canaliculata powder, alkylsurfuric acid Ester potassium, acrylate, glycidoxy-propyltrimethoxy silane, xanthan gum, are 42 DEG C in temperature, and rotating speed is to stir under 100r/min Dissolving 30min is mixed, mixed liquor is obtained；
S4：It is 20% that mixed liquor obtained in step S3 is concentrated into water content in the case where temperature is for 60 DEG C, and mixture II is obtained；
S5：It is 5% that mixture obtained in step S4 II is dried to water content in the case where temperature is for 84 DEG C, then crushes, mistake 120 mesh sieve, gained powder adopt pulse vacuum pressure steam sterilizer in temperature for 134 DEG C, and pressure is to sterilize under 210KPa 4min, is obtained preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition.
Embodiment 3
A kind of method of preventing and treating Citrus Huanglongbing pathogen, including winter clear garden, sprays the medicine for normally killing diaphorina citri, passes through The annual preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition 1 time of spraying before Citrus summer shoot is sprouted；The preventing and treating Citrus Huanglongbing pathogen medicine Compositionss in units of weight portion, including following raw material：150 parts of Folium Artemisiae Argyi, 120 parts of paulownia sawdust, 110 parts of Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis 100 Part, 90 parts of Melia azedarach L., 86 parts of Celastrus angulatus, 78 parts of ailanthus altissima (mill.) swingle, 68 parts of Caulis et Folium Lactucae sativae, 3 parts of potassium salt, 3 parts of microcosmic salt, 2 parts of nitrogen salt, 0.9 part of calcium salt, magnesium 0.9 part of salt, 0.4 part of iodine salt, 0.4 part of boron salt, 0.4 part of molybdenum salt, 0.4 part of zinc salt, 0.4 part of manganese salt, 0.4 part of mantoquita, iron salt 0.4 Part, 0.4 part of vitamin, 0.3 part of aminoacid, 0.09 part of indolebutyric acid, 0.09 part of gibberellins, 0.08 part of 6- benzyl gland fats purine, naphthalene 0.06 part of acetic acid, 0.3 part of agar, 0.06 part of kinetins, 2.4 parts of polyvinylpyrrolidone, 1.8 parts of sodium methylene bis-naphthalene sulfonate, 1.5 parts of Dupont EEA2112AC compatilizers, 1.5 parts of Pomacea canaliculata powder, 1.4 parts of alkyl sulfate potassium, 0.8 part of acrylate, ring 1.6 parts of the third oxygen propyl trimethoxy silicane of oxygen, 1.5 parts of xanthan gum, 6000 parts of ethanol；
The potassium salt is composed of the following components：0.8 part of potassium chloride, 0.6 part of potassium sulfate, 0.6 part of potassium nitrate, potassium carbonate 0.5 Part, 0.5 part of potassium bicarbonate；
The microcosmic salt is composed of the following components：0.8 part of calcium phosphate, 0.8 part of magnesium phosphate, 0.7 part of iron phosphate, zinc phosphate 0.7 Part；
The nitrogen salt is composed of the following components：0.8 part of ammonium hydrogen carbonate, 0.6 part of ammonium carbonate, 0.6 part of ammonium chloride；
The calcium salt is composed of the following components：0.4 part of calcium glycine, 0.3 part of calcium chloride, 0.2 part of the calcium in sulphuric acid Asia；
The magnesium salt is composed of the following components：0.4 part of magnesium glycinate, 0.3 part of magnesium chloride, 0.2 part of the magnesium in sulphuric acid Asia；
The iodine salt is composed of the following components：0.2 part of sodium iodide, 0.2 part of potassium iodate；
The boron salt is sodium tetraborate；
The molybdenum salt is potassium molybdate；
The zinc salt is zinc chloride；
The manganese salt is manganese chloride；
The mantoquita is copper chloride；
The iron salt is iron chloride；
The vitamin is composed of the following components：Raw element A0.14 parts, vitamin B10.12 part, vitamin B20.08 part, dimension Raw element C0.06 parts；
The aminoacid is composed of the following components：0.1 part of glycine, 0.08 part of isoleucine, 0.07 part of proline, phenylpropyl alcohol 0.05 part of propylhomoserin；
The polyvinylpyrrolidone is cosolvent；
The sodium methylene bis-naphthalene sulfonate is dispersant；
The Lumbricuss are powder conditioner；
The alkyl sulfate potassium is penetrating agent；
The acrylate is regulator；
The glycidoxy-propyltrimethoxy silane is viscosifier；
The xanthan gum is stabilizer；
The preparation method of described preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition, comprises the following steps：
S1：By Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae co-grinding, mixed Thing I, mixture I is added in ethanol, is 1 in solid-liquid ratio:16, ultrasonic power is 300W, and concentration of alcohol is 80%, extracts Temperature is to extract medicinal liquid 18min at 72 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 5000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc Salt, manganese salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, excitement Element, polyvinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Pomacea canaliculata powder, alkylsurfuric acid Ester potassium, acrylate, glycidoxy-propyltrimethoxy silane, xanthan gum, are 50 DEG C in temperature, and rotating speed is to stir under 300r/min Dissolving 20min is mixed, mixed liquor is obtained；
S4：It is 16% that mixed liquor obtained in step S3 is concentrated into water content in the case where temperature is for 80 DEG C, and mixture II is obtained；
S5：It is 4% that mixture obtained in step S4 II is dried to water content in the case where temperature is for 84-88 DEG C, then crushes, 260 mesh sieve are crossed, gained powder adopts pulse vacuum pressure steam sterilizer in temperature for 136 DEG C, pressure is to go out under 230KPa Bacterium 3min, is obtained preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition.
(1) test group：Method preventing and treating Citrus Huanglongbing pathogen using embodiment 1-3；(2) matched group 1：Using embodiment 1-3 Spray pattern preventing and treating Citrus Huanglongbing pathogen (using conventional preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition：Imidacloprid, consumption and test That organized is consistent)；(3) matched group 2：Spray pattern preventing and treating Citrus Huanglongbing pathogen using embodiment 1-3 is (using Patent Application Publication A kind of " prevention and controls (the publication number of Citrus Huanglongbing pathogen：CN104521629A the butralin in) "：Consumption and the one of test group Cause), as a result see the table below.
Project Yield (kg/ mus) Increase sugared rate (%)
Embodiment 1 3681.35 11.35
Embodiment 2 3612.54 10.78
Embodiment 3 3692.16 11.47
Matched group 1 3147.37-3325.69 1.13-1.68
Matched group 2 3418.37-3489.12 5.68-6.34
From upper table, the method preventing and treating Citrus Huanglongbing pathogen of embodiment of the present invention 1-3, yield and sugar content can be improved, and Citrus are in good taste, and appearance color and luster is mellow and full, and quality is high, higher than conventional control Citrus Huanglongbing pathogen pharmaceutical composition using effect and patent A kind of application documents " prevention and controls (the publication number of Citrus Huanglongbing pathogen：CN104521629A the butralin using effect in) ".
Above content it cannot be assumed that the present invention is embodied as being confined to these explanations, for the technical field of the invention Those of ordinary skill for, under the premise of without departing from present inventive concept, some simple deduction or replace can also be made, all answered When being considered as belonging to the scope of patent protection that determined by the claims that is submitted to of the present invention.

Claims (7)

1. a kind of method of preventing and treating Citrus Huanglongbing pathogen, including winter clear garden, sprays the medicine for normally killing diaphorina citri, its feature It is：By annual preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition 1-3 time of spraying before Citrus summer shoot is sprouted；The preventing and treating Citrus Yellow twig pharmaceutical composition in units of weight portion, including following raw material：Folium Artemisiae Argyi 120-150 parts, paulownia sawdust 100-120 part, Herba Sophorae alopecuroidiss 90-110 parts, Cortex Magnoliae Officinalis 80-100 part, Melia azedarach L. 60-90 parts, Celastrus angulatus 55-86 parts, ailanthus altissima (mill.) swingle 52-78 parts, Caulis et Folium Lactucae sativae 45-68 Part, potassium salt 2-3 parts, microcosmic salt 1-3 parts, nitrogen salt 1-2 parts, calcium salt 0.6-0.9 parts, magnesium salt 0.6-0.9 parts, iodine salt 0.2-0.4 parts, boron Salt 0.2-0.4 parts, molybdenum salt 0.2-0.4 parts, zinc salt 0.2-0.4 parts, manganese salt 0.2-0.4 part, mantoquita 0.2-0.4 parts, iron salt 0.2- 0.4 part, vitamin 0.2-0.4 parts, aminoacid 0.2-0.3 parts, indolebutyric acid 0.06-0.09 parts, gibberellins 0.06-0.09 parts, 6- benzyl gland fat purine 0.06-0.08 parts, naphthalene acetic acid 0.04-0.06 parts, agar 0.1-0.3 parts, kinetins 0.04-0.06 parts, poly- Vinylpyrrolidone 0.8-2.4 parts, sodium methylene bis-naphthalene sulfonate 0.6-1.8 parts, Dupont EEA2112AC compatilizer 1-1.5 Part, Pomacea canaliculata powder 0.6-1.5 parts, alkyl sulfate potassium 0.4-1.4 parts, acrylate 0.5-0.8 parts, epoxypropoxy front three TMOS 0.6-1.6 parts, xanthan gum 0.5-1.5 parts, ethanol 2000-6000 parts；
The potassium salt is composed of the following components：Potassium chloride 0.6-0.8 parts, potassium sulfate 0.5-0.6 parts, potassium nitrate 0.4-0.6 parts, carbon Sour potassium 0.3-0.5 parts, potassium bicarbonate 0.2-0.5 parts；
The microcosmic salt is composed of the following components：Calcium phosphate 0.3-0.8 parts, magnesium phosphate 0.3-0.8 parts, iron phosphate 0.2-0.7 parts, phosphorus Sour zinc 0.2-0.7 parts；
The nitrogen salt is composed of the following components：Ammonium hydrogen carbonate 0.4-0.8 parts, ammonium carbonate 0.3-0.6 parts, ammonium chloride 0.3-0.6 parts；
The calcium salt is composed of the following components：Calcium glycine 0.3-0.4 parts, calcium chloride 0.2-0.3 parts, sulphuric acid Asia calcium 0.1-0.2 Part；
The magnesium salt is composed of the following components：Magnesium glycinate 0.3-0.4 parts, magnesium chloride 0.2-0.3 parts, sulphuric acid Asia magnesium 0.1-0.2 Part；
The iodine salt is composed of the following components：Sodium iodide 0.1-0.2 parts, potassium iodate 0.1-0.2 parts；
The vitamin is composed of the following components：Raw element A0.08-0.14 parts, vitamin B10.08-0.12 parts, vitamin B2 0.02-0.08 parts, vitamin C 0.02-0.06 parts；
The aminoacid is composed of the following components：Glycine 0.08-0.1 parts, isoleucine 0.06-0.08 parts, proline 0.04- 0.07 part, phenylalanine 0.02-0.05 parts；
The preparation method of described preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition, comprises the following steps：
S1：By Folium Artemisiae Argyi, paulownia sawdust, Herba Sophorae alopecuroidiss, Cortex Magnoliae Officinalis, Melia azedarach L., Celastrus angulatus, ailanthus altissima (mill.) swingle, Caulis et Folium Lactucae sativae co-grinding, mixture I is obtained, Mixture I is added in ethanol, is 1 in solid-liquid ratio:14-16, ultrasonic power are 200-300W, and concentration of alcohol is 65%- 80%, Extracting temperature is to extract medicinal liquid 18-24min at 66-72 DEG C, and medicinal liquid is obtained；
S2：Medicinal liquid obtained in step S1 is crossed 3000-5000 mesh sieve, filtrate is obtained；
S3：Filtrate obtained in step S2 is added potassium salt, microcosmic salt, nitrogen salt, calcium salt, magnesium salt, iodine salt, boron salt, molybdenum salt, zinc salt, manganese Salt, mantoquita, iron salt, vitamin, aminoacid, indolebutyric acid, gibberellins, 6- benzyl gland fat purines, naphthalene acetic acid, agar, kinetins, poly- Vinylpyrrolidone, sodium methylene bis-naphthalene sulfonate, Dupont EEA2112AC compatilizers, Pomacea canaliculata powder, alkyl sulfate potassium, Acrylate, glycidoxy-propyltrimethoxy silane, xanthan gum, are 42-50 DEG C in temperature, and rotating speed is under 100-300r/min Stirring and dissolving 20-30min, is obtained mixed liquor；
S4：Mixed liquor obtained in step S3 is concentrated into water content≤22% in the case where temperature is for 60-80 DEG C, mixture II is obtained；
S5：Mixture obtained in step S4 II is dried to water content≤6% in the case where temperature is for 84-88 DEG C, is then crushed, mistake 120-260 mesh sieve, gained powder adopt pulse vacuum pressure steam sterilizer in temperature for 134-136 DEG C, and pressure is 210- Sterilize under 230KPa 3-4min, and preventing and treating Citrus Huanglongbing pathogen pharmaceutical composition is obtained.
2. according to claim 1 preventing and treating Citrus Huanglongbing pathogen method, it is characterised in that the boron salt be sodium tetraborate.
3. according to claim 1 preventing and treating Citrus Huanglongbing pathogen method, it is characterised in that the molybdenum salt be potassium molybdate.
4. according to claim 1 preventing and treating Citrus Huanglongbing pathogen method, it is characterised in that the zinc salt be zinc chloride.
5. according to claim 1 preventing and treating Citrus Huanglongbing pathogen method, it is characterised in that the manganese salt be manganese chloride.
6. according to claim 1 preventing and treating Citrus Huanglongbing pathogen method, it is characterised in that the mantoquita be copper chloride.
7. according to claim 1 preventing and treating Citrus Huanglongbing pathogen method, it is characterised in that the iron salt be iron chloride.
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CN107969443A (en) * 2017-12-16 2018-05-01 李竑靓 A kind of preparation method for preventing Citrus Huanglongbing pathogen medicament
CN108064891A (en) * 2017-12-01 2018-05-25 钟山县德福农产品有限公司 The pesticide control of Citrus Huanglongbing pathogen
CN108184513A (en) * 2018-03-22 2018-06-22 曾彦粤 A kind of Citrus Huanglongbing pathogen control method
CN110583704A (en) * 2019-09-10 2019-12-20 贵州香柚香生态农业有限公司 Biological agent for preventing and treating red-heart honey pomelo yellow dragon disease
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Application publication date: 20170315