CN106435592B - A kind of stainless steel spring chemical polishing agent and preparation method thereof - Google Patents
A kind of stainless steel spring chemical polishing agent and preparation method thereof Download PDFInfo
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- CN106435592B CN106435592B CN201610683276.3A CN201610683276A CN106435592B CN 106435592 B CN106435592 B CN 106435592B CN 201610683276 A CN201610683276 A CN 201610683276A CN 106435592 B CN106435592 B CN 106435592B
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- stainless steel
- polishing agent
- chemical polishing
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- magnesium stearate
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
- C23F3/04—Heavy metals
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- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
The present invention relates to a kind of chemical polishing agents, and in particular to a kind of stainless steel spring chemical polishing agent and its preparation method；The polishing agent is by the aqueous solution that mass-volume concentration includes following substance：2 6g/L of paraffin, 2 5g/L of bromite, 5 12g/L of calcium carbonate, 4 11g/L of vegetable oil acid, 0.5 4g/L of magnesium stearate, 3 6g/L of polyethylene glycol 2000,2 5g/L of dioctyl sebacate, 1 6g/L of ethyl alcohol, 2 5g/L of dodecyl benzene sulfonic acid, 0.2 3g/L of surfactant；Polishing agent provided by the invention is environmentally friendly, efficient, easy to use.
Description
Technical field
The present invention relates to a kind of chemical polishing agents, and in particular to a kind of stainless steel spring chemical polishing agent and it
Preparation method.
Background technology
The microscopic structure of metal material directly influences the performance and used life of machine components, and Metallographic Analysis is control machine
The important means of tool part inherent quality.In new material, new process in the research and development of new product, is improving in metal product
In the scientific research of quality, it all be unable to do without Metallographic Techniques analysis.
During Metallographic Techniques are analyzed, polishing is an extremely important step, and polishing refers to utilizing machinery, chemistry
Or the effect of electrochemistry, so that workpiece surface roughness is reduced, the processing method to obtain bright, flat surface.The purpose of polishing
It is the polishing scratch removed on metallographic flour milling, obtains smooth viewing surface, the height of quality of finish directly determines that metallographic detects
The quality in face.It is by chemical reagent to sample that polishing, which mainly has mechanical polishing, chemical polishing and electrobrightening, chemical polishing,
A kind of method that the selective dissolution effect in surface irregularity region eliminates polishing scratch, corrodes leveling, it is easy to operate, it does not need
By mechanical equipment, live fitness is high, easy to carry, is very suitable for live metallographic and makes use.
Stainless steel hardness is relatively low, belongs to the metal of more difficult polishing, and conventional method is the side with mechanical polishing and electrobrightening
Formula, but scene does not often satisfy the requirements, and mechanical polishing and electrobrightening mode can not use, and therefore, scene is to parts of stainless steel
Metallographic make, polishing mode selects chemical polishing more convenient, the stainless steel polishing agent polishing that existing chemical polishing uses
Energy force difference, the poor dispersion of abrasive material, composition stability is poor, and dust phenomenon is more serious after polishing.
Invention content
In view of the deficiencies of the prior art, the present invention provides a kind of environmental protection, efficient stainless steel spring chemical polishing agent,
And its preparation method.
In order to achieve the above object, the present invention is achieved by the following technical programs：
A kind of stainless steel spring chemical polishing agent includes the aqueous solution of following substance by mass-volume concentration：
Paraffin 2-6g/L, bromite 2-5g/L, calcium carbonate 5-12g/L, vegetable oil acid 4-11g/L, magnesium stearate 0.5-
4g/L, polyethylene glycol 2000 3-6g/L, dioctyl sebacate 2-5g/L, ethyl alcohol 1-6g/L, dodecyl benzene sulfonic acid 2-5g/L, table
Face activating agent 0.2-3g/L.
Further, the stainless steel spring chemical polishing agent includes the water of following substance by mass-volume concentration
Solution：
Paraffin 3-5g/L, bromite 3-4g/L, calcium carbonate 6-10g/L, vegetable oil acid 5-10g/L, magnesium stearate 2-3g/
L, polyethylene glycol 2000 4-5g/L, dioctyl sebacate 3-4g/L, ethyl alcohol 2-5g/L, dodecyl benzene sulfonic acid 3-4g/L, surface
Activating agent 1-2g/L.
Further, the stainless steel spring chemical polishing agent includes the water of following substance by mass-volume concentration
Solution：
Paraffin 3g/L, bromite 3g/L, calcium carbonate 6g/L, vegetable oil acid 5g/L, magnesium stearate 2g/L, polyethylene glycol
20004g/L, dioctyl sebacate 3g/L, ethyl alcohol 2g/L, dodecyl benzene sulfonic acid 3g/L, surfactant 1g/L.
Further, the grain size of the magnesium stearate is 0.1-0.6um.
Further, the surfactant include sodium sulfate of polyethenoxy ether of fatty alcohol, neopelex and
Fatty alcohol polyoxyethylene ether.
A kind of preparation method of stainless steel spring chemical polishing agent, includes the following steps：By formula metering each component；With
A small amount of water-soluble dispersion bromite, calcium carbonate, magnesium stearate, dioctyl sebacate and dodecyl benzene sulfonic acid, are heated to solution
Boiling keeps the temperature 5-10min, stops heating；Excess water, paraffin, vegetable oil acid, polyethylene glycol 2000, ethyl alcohol and surface is added to live
Property agent, stirring 15-30min to get.
Beneficial effects of the present invention are：Polishing agent provided by the invention is environmentally friendly, efficient, easy to use：Material therefor safety
Environmental protection passes through paraffin, bromite, calcium carbonate, vegetable oil acid, magnesium stearate, polyethylene glycol 2000, dioctyl sebacate, second
The organic assembling of alcohol, dodecyl benzene sulfonic acid and surfactant so that product need not consume a large amount of electric energy and can obtain
The surface quality of finish close to electrochemical polish is obtained, unit product polishing cost is low, and raw material directly can voluntarily be matched on a small quantity
System, it is easy to use.
Specific implementation mode
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the implementation of the present invention
Example, technical scheme in the embodiment of the invention is clearly and completely described.Based on the embodiments of the present invention, this field
The every other embodiment that those of ordinary skill is obtained without creative efforts, belongs to protection of the present invention
Range.
Embodiment 1：
A kind of stainless steel spring chemical polishing agent includes the aqueous solution of following substance by mass-volume concentration：
Paraffin 3g/L, bromite 3g/L, calcium carbonate 6g/L, vegetable oil acid 5g/L, grain size are the stearic acid of 0.1-0.6um
Magnesium 2g/L, polyethylene glycol 2000 4g/L, dioctyl sebacate 3g/L, ethyl alcohol 2g/L, dodecyl benzene sulfonic acid 3g/L, poly alkyl alcohol
Ethylene oxide ether sodium sulfate 0.4g/L, neopelex 0.2g/L, fatty alcohol polyoxyethylene ether 0.4g/L.
Preparation method includes the following steps：By formula metering each component；With a small amount of water-soluble dispersion bromite, carbonic acid
Calcium, magnesium stearate, dioctyl sebacate and dodecyl benzene sulfonic acid are heated to solution boiling, keep the temperature 5-10min, stop heating；
Be added excess water, paraffin, vegetable oil acid, polyethylene glycol 2000, ethyl alcohol and surfactant, stirring 15-30min to get.
Embodiment 2：
A kind of stainless steel spring chemical polishing agent includes the aqueous solution of following substance by mass-volume concentration：
Paraffin 6g/L, bromite 2g/L, calcium carbonate 12g/L, vegetable oil acid 4g/L, grain size are the tristearin of 0.1-0.6um
Sour magnesium 4g/L, polyethylene glycol 2000 3g/L, dioctyl sebacate 5g/L, ethyl alcohol 1g/L, dodecyl benzene sulfonic acid 5g/L, fatty alcohol
Polyethenoxy ether sodium sulfate 0.05g/L, neopelex 0.1g/L, fatty alcohol polyoxyethylene ether 0.05g/L.
Preparation method is the same as embodiment 1.
Embodiment 3：
A kind of stainless steel spring chemical polishing agent includes the aqueous solution of following substance by mass-volume concentration：
Paraffin 5g/L, bromite 4g/L, calcium carbonate 10g/L, vegetable oil acid 10g/L, grain size are the tristearin of 0.1-0.6um
Sour magnesium 3g/L, polyethylene glycol 2000 5g/L, dioctyl sebacate 4g/L, ethyl alcohol 5g/L, dodecyl benzene sulfonic acid 4g/L, fatty alcohol
Polyethenoxy ether sodium sulfate 1g/L, neopelex 0.5g/L, fatty alcohol polyoxyethylene ether 0.5g/L.
Preparation method is the same as embodiment 1.
Embodiment 4：
A kind of stainless steel spring chemical polishing agent includes the aqueous solution of following substance by mass-volume concentration：
Paraffin 2g/L, bromite 5g/L, calcium carbonate 5g/L, vegetable oil acid 11g/L, grain size are the tristearin of 0.1-0.6um
Sour magnesium 0.5g/L, polyethylene glycol 2000 6g/L, dioctyl sebacate 2g/L, ethyl alcohol 6g/L, dodecyl benzene sulfonic acid 2g/L, fat
Alcohol polyethenoxy ether sodium sulfate 1g/L, neopelex 1g/L, fatty alcohol polyoxyethylene ether 1g/L.
Preparation method is the same as embodiment 1.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
Invention is explained in detail, it will be understood by those of ordinary skill in the art that：It still can be to aforementioned each implementation
Technical solution recorded in example is modified or equivalent replacement of some of the technical features；And these modification or
It replaces, the spirit and scope for various embodiments of the present invention technical solution that it does not separate the essence of the corresponding technical solution.
Claims (6)
1. a kind of stainless steel spring chemical polishing agent, which is characterized in that by mass-volume concentration include the water-soluble of following substance
Liquid：
Paraffin 2-6g/L, bromite 2-5g/L, calcium carbonate 5-12g/L, vegetable oil acid 4-11g/L, magnesium stearate 0.5-4g/L,
Polyethylene glycol 2000 3-6g/L, dioctyl sebacate 2-5g/L, ethyl alcohol 1-6g/L, dodecyl benzene sulfonic acid 2-5g/L, surface are lived
Property agent 0.2-3g/L.
2. stainless steel spring chemical polishing agent as described in claim 1, which is characterized in that by mass-volume concentration include with
The aqueous solution of lower substance：
Paraffin 3-5g/L, bromite 3-4g/L, calcium carbonate 6-10g/L, vegetable oil acid 5-10g/L, magnesium stearate 2-3g/L gather
Ethylene glycol 20004-5g/L, dioctyl sebacate 3-4g/L, ethyl alcohol 2-5g/L, dodecyl benzene sulfonic acid 3-4g/L, surface-active
Agent 1-2g/L.
3. stainless steel spring chemical polishing agent as described in claim 1, which is characterized in that by mass-volume concentration include with
The aqueous solution of lower substance：
Paraffin 3g/L, bromite 3g/L, calcium carbonate 6g/L, vegetable oil acid 5g/L, magnesium stearate 2g/L, polyethylene glycol
20004g/L, dioctyl sebacate 3g/L, ethyl alcohol 2g/L, dodecyl benzene sulfonic acid 3g/L, surfactant 1g/L.
4. stainless steel spring chemical polishing agent as described in claim 1, which is characterized in that the grain size of the magnesium stearate is
0.1-0.6um。
5. stainless steel spring chemical polishing agent as described in claim 1, which is characterized in that the surfactant includes fat
Fat alcohol polyethenoxy ether sodium sulfate, neopelex and fatty alcohol polyoxyethylene ether.
6. the preparation method of the stainless steel spring chemical polishing agent as described in any one of claim 1-5, which is characterized in that
Include the following steps：By formula metering each component；With a small amount of water-soluble dispersion bromite, calcium carbonate, magnesium stearate, decanedioic acid two
Monooctyl ester and dodecyl benzene sulfonic acid are heated to solution boiling, keep the temperature 5-10min, stop heating；Excess water, paraffin, plant is added
Oleic acid, polyethylene glycol 2000, ethyl alcohol and surfactant, stirring 15-30min to get.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610683276.3A CN106435592B (en) | 2016-08-17 | 2016-08-17 | A kind of stainless steel spring chemical polishing agent and preparation method thereof |
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| CN201610683276.3A CN106435592B (en) | 2016-08-17 | 2016-08-17 | A kind of stainless steel spring chemical polishing agent and preparation method thereof |
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| CN106435592A CN106435592A (en) | 2017-02-22 |
| CN106435592B true CN106435592B (en) | 2018-08-21 |
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| CN109021835A (en) * | 2018-09-03 | 2018-12-18 | 合肥久新不锈钢厨具有限公司 | A kind of high-hardness stainless steel grinding and polishing liquid |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386987A (en) * | 2007-09-12 | 2009-03-18 | 南通杰祥机械有限公司 | Chemical brightening solution for stainless steel |
| CN103451658A (en) * | 2013-08-23 | 2013-12-18 | 苏州长盛机电有限公司 | Environmentally-friendly metal polishing agent and preparation method thereof |
| CN103590044A (en) * | 2013-11-06 | 2014-02-19 | 天津圳鹏清洗技术开发有限公司 | Metal polishing agent and preparation method thereof |
| CN105200433A (en) * | 2015-09-09 | 2015-12-30 | 深圳市宏达威表面处理技术有限公司 | Stainless steel liquid polishing paste and preparation method thereof |
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2016
- 2016-08-17 CN CN201610683276.3A patent/CN106435592B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386987A (en) * | 2007-09-12 | 2009-03-18 | 南通杰祥机械有限公司 | Chemical brightening solution for stainless steel |
| CN103451658A (en) * | 2013-08-23 | 2013-12-18 | 苏州长盛机电有限公司 | Environmentally-friendly metal polishing agent and preparation method thereof |
| CN103590044A (en) * | 2013-11-06 | 2014-02-19 | 天津圳鹏清洗技术开发有限公司 | Metal polishing agent and preparation method thereof |
| CN105200433A (en) * | 2015-09-09 | 2015-12-30 | 深圳市宏达威表面处理技术有限公司 | Stainless steel liquid polishing paste and preparation method thereof |
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