CN109021835A - A kind of high-hardness stainless steel grinding and polishing liquid - Google Patents
A kind of high-hardness stainless steel grinding and polishing liquid Download PDFInfo
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- CN109021835A CN109021835A CN201811019523.5A CN201811019523A CN109021835A CN 109021835 A CN109021835 A CN 109021835A CN 201811019523 A CN201811019523 A CN 201811019523A CN 109021835 A CN109021835 A CN 109021835A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
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Abstract
The present invention relates to stainless steel processing technique fields, and in particular to a kind of high-hardness stainless steel grinding and polishing liquid.The raw material components of grinding and polishing liquid include: magnesium stearate, polyethylene wax, complexing agent, grinding agent, corrosion inhibiter, wetting dispersing agent, silane coupling agent, hydrochloric acid solution and kerosene.Wherein, grinding agent uses the mixture of schmigel, cubic boron nitride, nano silica, cerium oxide, and grinding agent also passes through surface modification treatment, and the partial size of schmigel is 100-120 μm, and the partial size of cubic boron nitride is 50-80 μm；Complexing agent is the mixture of the molar ratio mixing of citric acid or ammonium lacate according to 3:1；Corrosion inhibiter benzotriazole or polyphosphate sodium；The concentration of hydrochloric acid solution is 6-8%；Wetting dispersing agent is polysorbas20 or sorbester p17.The polishing effect of the type grinding and polishing liquid is good, brightness is high；And because the stability of polishing fluid is high, good dispersion, so that the polishing effect consistency of workpiece is higher.
Description
Technical field
The present invention relates to stainless steel processing technique fields, and in particular to a kind of high-hardness stainless steel grinding and polishing liquid.
Background technique
Stainless steel is the abbreviation of stainless acid resistant steel, the weak corrosive medium such as resistance to air, steam, water or the steel grade with rustless property
Referred to as stainless steel；And the steel grade that medium resistant to chemical etching (chemical etchings such as acid, alkali, salt) corrode is known as acid resisting steel.Due to two
Difference of the person in chemical component and keep their corrosion resistance different, generally resistant to chemical media corrodes common stainless steel, and resistance to
Sour steel then generally has rustless property.Stainless steel does not refer to a type of steel not instead of singly, indicates that more than 100 kinds of industry are stainless
Steel, the stainless steel capital of every kind developed are with good performance in its specific application field.
The characteristics such as stainless steel has hardness high, and wearability is good, good corrosion resistance, and excellent appearance and service life are long, because
This is widely used in the industries such as building, auto industry, shipbuilding industry, marine device, mechanical equipment and chemical device.Building,
In the products application of the industries such as auto industry, shipbuilding industry, marine device, mechanical equipment and chemical device, it is often necessary to stainless
Steel board or tubing etc. carry out surface polishing treatment, so that mirror-polishing is realized on the surface of material, promote the aesthetics and reality of material
The property used.
According to the difference of stainless steel material type, stainless steel mirrorization processing mainly using mechanical polishing, chemical polishing and
Three kinds of techniques of electrochemical polish.Wherein, chemical polishing advantage is process equipment small investment, and Complex Parts can be thrown, and speed is fast, efficiency
Height, anti-corrosive properties are good.The disadvantage is that brightness is poor, there is gas overflowing, need ventilation equipment, heating is difficult, can cause environmental pollution.
The advantages of electrochemical polish is that bright luster keeps length, and process stabilizing, pollution is few, and single-piece work is at low cost, and anti-corrosive properties are good.Disadvantage
It is pollution height, process equipment one-time investment is big, and Complex Parts want tooling, auxiliary electrode, and mass production also needs cooling installation.
And the polishing effect mechanically polished is good, brightness is high, and suitable for the processing of small-sized simple Devices, equipment investment is relatively low；
The disadvantage is that the consistency of product polishing effect is poor, labor intensity is larger.
The product polishing effect of mechanical polishing depends primarily on the quality of polishing fluid, and conventional polishing fluid is using Buddha's warrior attendant
The dispersibility of the vegetable oil or dispersion oil of the grinding agents such as stone, boron nitride, this polishing fluid is poor, and stability is insufficient, throws
Phenomena such as property of light liquid is uneven, and flocculation, coalescence may occur in storage or filling process for polishing fluid, so as to cause adding
During work, the polishing effect of workpiece surface is had differences, and the consistency of product is insufficient, serious or even can be in workpiece surface shape
It is scratched at wiping；This greatly reduces buffer's task efficiency.
Summary of the invention
Aiming at the problems existing in the prior art, the present invention provides a kind of high-hardness stainless steel grinding and polishing liquid, should
The polishing effect of type grinding and polishing liquid is good, brightness is high；And because the stability of polishing fluid is high, good dispersion, so that workpiece
Polishing effect consistency it is higher.
In order to achieve the above object, the present invention is achieved through the following technical solutions:
A kind of high-hardness stainless steel grinding and polishing liquid, according to mass fraction, the raw material components of grinding and polishing liquid include: hard
16-19 parts of fatty acid magnesium, 9-13 parts of polyethylene wax, 1.5-1.9 parts of complexing agent, 4-8 parts of grinding agent, 2-3 parts of corrosion inhibiter, wetting and dispersing
1-2 parts of agent, 1.5-2.8 parts of silane coupling agent, 7-10 parts of hydrochloric acid solution, 100-130 parts of kerosene.
Preferably, according to mass fraction, the raw material components of grinding and polishing liquid include: 17-18 parts of magnesium stearate, polyethylene wax
10-12 parts, 1.6-1.8 parts of complexing agent, 5-7 parts of grinding agent, 2.4-2.7 parts of corrosion inhibiter, 1.3-1.8 parts of wetting dispersing agent, silane
1.9-2.5 parts of coupling agent, 8-9 parts of hydrochloric acid solution, 115-125 parts of kerosene.
It is further preferred that the raw material components of grinding and polishing liquid include: 17.5 parts of magnesium stearate according to mass fraction, gather
11 parts of ethylene waxes, 1.7 parts of complexing agent, 6 parts of grinding agent, 2.6 parts of corrosion inhibiter, 1.5 parts of wetting dispersing agent, 2.3 parts of silane coupling agent,
8.4 parts of hydrochloric acid solution, 120 parts of kerosene.
In the present invention, grinding agent is by surface treatment, preparation method are as follows: by schmigel, cubic boron nitride, nano-silica
SiClx, cerium oxide are uniformly mixed according to the mass ratio of 10:2:4:1, heat 40-60min with 300-450 DEG C of temperature, so
Temperature is reduced afterwards to room temperature, is then added mixture in the alcohol solvent of 3-5 times of volume, is added into alcohol solvent
The dodecyl sodium sulfate of the polypropylene glycol of 2.3wt%, the glycerol of 4wt% and 3.5wt% is added with 50-60 DEG C of temperature water bath
Heat, and with the revolving speed decentralized processing 13-16min of 350-420r/min, dispersion liquid filtering, by the solid content being obtained by filtration with 85-
95 DEG C of temperature drying, obtains required grinding agent.
Wherein, the partial size of schmigel is 100-120 μm, and the partial size of cubic boron nitride is 50-80 μm.
Preferably, complexing agent is the mixture of the molar ratio mixing of citric acid or ammonium lacate according to 3:1.
Preferably, corrosion inhibiter benzotriazole or polyphosphate sodium.
Preferably, the concentration of hydrochloric acid solution is 6-8%.
Preferably, wetting dispersing agent is polysorbas20 or sorbester p17.
Grinding and polishing liquid provided by the invention the preparation method comprises the following steps:
According to mass fraction, kerosene is added in Scattered Kettle, 50-53 DEG C in heating, then by magnesium stearate and poly- second
Alkene wax is added in Scattered Kettle, with the revolving speed decentralized processing 6-8min of 600-650r/min, by grinding agent, corrosion inhibiter and complexing agent
It is added in hydrochloric acid solution, stirs, be then added to dispersion liquid and wetting dispersing agent, silane coupling agent point together
It dissipates in kettle, continues decentralized processing 15-25min, obtained water-in-oil emulsion is required grinding and polishing liquid.
The present invention have it is following the utility model has the advantages that
Grinding and polishing liquid provided by the invention, the mirror-polishing processing of the martensitic stainless steel suitable for high rigidity, the type
Use kerosene as solvent in grinding and polishing liquid, using magnesium stearate and polyethylene wax as lubricant, and with the hydrochloric acid of low concentration
As detergent, to form the emulsion system of Water-In-Oil.Wherein, grinding agent uses schmigel, cubic boron nitride, nanometer
The hardness of silica, cerium oxide, the type abrasive is high, and thermostabilization is good, and high temperature resistance is prominent, and stability of material is strong, is grinding
It is not easy the problem of dusting occur or decomposing during mill.It is highly suitable for the grinding and polishing of high hardness martensitic stainless steel,
Polishing effect is good.In order to improve compatibility and dispersibility of the abrasive in emulsion system, abrasive is avoided to store or using
It settles or coalesces in the process, the present invention has carried out special surface treatment to abrasive, by heat treatment that abrasive is living first
Change, improves the gas porosity of abrasive, abrasive is then added to the second containing polypropylene glycol, glycerol and dodecyl sodium sulfate
Water-bath disperses in alcoholic solution, carries out to the surface of abrasive organically-modified.In order to further increase the dispersed and steady of abrasive
It is qualitative, complexing agent, wetting dispersing agent and silane coupling agent, San Zheke have also been used in component in grinding and polishing liquid of the invention
To play synergistic effect, so that the dispersion effect of abrasive is more stable, to promote the polishing effect of grinding and polishing liquid, promoted
The consistency of workpiece polishing effect.
Specific embodiment
Below with reference to embodiment, further description of the specific embodiments of the present invention, and following embodiment is only used for more
Technical solution of the present invention is clearly demonstrated, and not intended to limit the protection scope of the present invention.
Embodiment 1
A kind of high-hardness stainless steel grinding and polishing liquid, according to mass fraction, the raw material components of grinding and polishing liquid include: hard
It is 16 parts of fatty acid magnesium, 9 parts of polyethylene wax, 1.5 parts of complexing agent, 4 parts of grinding agent, 2 parts of corrosion inhibiter, 1 part of wetting dispersing agent, silane coupled
1.5 parts of agent, 7 parts of hydrochloric acid solution, 100 parts of kerosene.
In the present embodiment, grinding agent is by surface treatment, preparation method are as follows: by schmigel, cubic boron nitride, nanometer two
Silica, cerium oxide are uniformly mixed according to the mass ratio of 10:2:4:1, are heated 40min with 300 DEG C of temperature, are then reduced
Temperature then adds mixture in the alcohol solvent of 3 times of volumes to room temperature, the poly- of 2.3wt% is added into alcohol solvent
The dodecyl sodium sulfate of propylene glycol, the glycerol of 4wt% and 3.5wt% is heated with 50 DEG C of temperature water bath, and with 350r/min
Revolving speed decentralized processing 13min, the solid content being obtained by filtration dried with 85 DEG C of temperature, ground needed for obtaining by dispersion liquid filtering
Grinding agent.
Wherein, the partial size of schmigel is 100-120 μm, and the partial size of cubic boron nitride is 50-80 μm.
Complexing agent is the mixture of the molar ratio mixing of citric acid or ammonium lacate according to 3:1.
Corrosion inhibiter benzotriazole.
The concentration of hydrochloric acid solution is 6%.
Wetting dispersing agent is polysorbas20.
Grinding and polishing liquid provided in this embodiment the preparation method comprises the following steps:
According to mass fraction, kerosene is added in Scattered Kettle, 50 DEG C in heating, then by magnesium stearate and polyethylene wax
It is added in Scattered Kettle, with the revolving speed decentralized processing 6min of 600r/min, grinding agent, corrosion inhibiter and complexing agent is added to hydrochloric acid
It in solution, stirs, is then added to dispersion liquid and wetting dispersing agent, silane coupling agent in Scattered Kettle together, after
Continuous decentralized processing 15min, obtained water-in-oil emulsion is required grinding and polishing liquid.
Embodiment 2
A kind of high-hardness stainless steel grinding and polishing liquid, according to mass fraction, the raw material components of grinding and polishing liquid include: hard
19 parts of fatty acid magnesium, 13 parts of polyethylene wax, 1.9 parts of complexing agent, 8 parts of grinding agent, 3 parts of corrosion inhibiter, 2 parts of wetting dispersing agent, silane is even
2.8 parts of agent, 10 parts of hydrochloric acid solution, 130 parts of kerosene of connection.
In the present embodiment, grinding agent is by surface treatment, preparation method are as follows: by schmigel, cubic boron nitride, nanometer two
Silica, cerium oxide are uniformly mixed according to the mass ratio of 10:2:4:1, are heated 60min with 450 DEG C of temperature, are then reduced
Temperature then adds mixture in the alcohol solvent of 5 times of volumes to room temperature, the poly- of 2.3wt% is added into alcohol solvent
The dodecyl sodium sulfate of propylene glycol, the glycerol of 4wt% and 3.5wt% is heated with 60 DEG C of temperature water bath, and with 420r/min
Revolving speed decentralized processing 16min, the solid content being obtained by filtration dried with 95 DEG C of temperature, ground needed for obtaining by dispersion liquid filtering
Grinding agent.
Wherein, the partial size of schmigel is 100-120 μm, and the partial size of cubic boron nitride is 50-80 μm.
Complexing agent is the mixture of the molar ratio mixing of citric acid or ammonium lacate according to 3:1.
Corrosion inhibiter polyphosphate sodium.
The concentration of hydrochloric acid solution is 8%.
Wetting dispersing agent is sorbester p17.
Grinding and polishing liquid provided in this embodiment the preparation method comprises the following steps:
According to mass fraction, kerosene is added in Scattered Kettle, 53 DEG C in heating, then by magnesium stearate and polyethylene wax
It is added in Scattered Kettle, with the revolving speed decentralized processing 8min of 650r/min, grinding agent, corrosion inhibiter and complexing agent is added to hydrochloric acid
It in solution, stirs, is then added to dispersion liquid and wetting dispersing agent, silane coupling agent in Scattered Kettle together, after
Continuous decentralized processing 25min, obtained water-in-oil emulsion is required grinding and polishing liquid.
Embodiment 3
A kind of high-hardness stainless steel grinding and polishing liquid, according to mass fraction, the raw material components of grinding and polishing liquid include: hard
17.5 parts of fatty acid magnesium, 11 parts of polyethylene wax, 1.7 parts of complexing agent, 6 parts of grinding agent, 2.6 parts of corrosion inhibiter, 1.5 parts of wetting dispersing agent,
2.3 parts of silane coupling agent, 8.4 parts of hydrochloric acid solution, 120 parts of kerosene.
In the present embodiment, grinding agent is by surface treatment, preparation method are as follows: by schmigel, cubic boron nitride, nanometer two
Silica, cerium oxide are uniformly mixed according to the mass ratio of 10:2:4:1, are heated 50min with 400 DEG C of temperature, are then reduced
Temperature then adds mixture in the alcohol solvent of 4 times of volumes to room temperature, the poly- of 2.3wt% is added into alcohol solvent
The dodecyl sodium sulfate of propylene glycol, the glycerol of 4wt% and 3.5wt% is heated with 55 DEG C of temperature water bath, and with 380r/min
Revolving speed decentralized processing 15min, the solid content being obtained by filtration dried with 90 DEG C of temperature, ground needed for obtaining by dispersion liquid filtering
Grinding agent.
Wherein, the partial size of schmigel is 100-120 μm, and the partial size of cubic boron nitride is 50-80 μm.
Complexing agent is the mixture of the molar ratio mixing of citric acid or ammonium lacate according to 3:1.
Corrosion inhibiter benzotriazole.
The concentration of hydrochloric acid solution is 6-8%.
Wetting dispersing agent is polysorbas20.
Grinding and polishing liquid provided in this embodiment the preparation method comprises the following steps:
According to mass fraction, kerosene is added in Scattered Kettle, 52 DEG C in heating, then by magnesium stearate and polyethylene wax
It is added in Scattered Kettle, with the revolving speed decentralized processing 7min of 630r/min, grinding agent, corrosion inhibiter and complexing agent is added to hydrochloric acid
It in solution, stirs, is then added to dispersion liquid and wetting dispersing agent, silane coupling agent in Scattered Kettle together, after
Continuous decentralized processing 20min, obtained water-in-oil emulsion is required grinding and polishing liquid.
Performance test
1, it using the Cr13 type martensitic stainless steel material with a thickness of 10mm as workpiece sample, is mirror-finished, respectively
The grinding and polishing liquid in the present embodiment is selected, and conventional diadust polishing fluid is set as a control group, test each group produces
The polishing effect of product, evaluation index include the dispersibility of grinding with polishing agent, the finish after workpiece polishing, the throwing of 100 workpiece
The consistency of light effect, and there is surface abrasion workpiece accounting.
Table 1: the performance test results of the present embodiment and control group grinding and polishing liquid
Analyze the above experimental result discovery, the diadust polishing of grinding and polishing liquid and control group provided in this embodiment
Liquid phase ratio, all has good polishing effect, and the finish after workpiece polishing is higher.But the grinding and polishing liquid of the present embodiment
Dispersibility and stability are more preferable, there's almost no the settlement issues of grinding agent in storage process, therefore in workpiece polishing effect
Consistency, and workpiece surface is caused to wipe on the problems such as scratching, the performance of the present embodiment product is better than the product of control group.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, although referring to aforementioned reality
Applying example, invention is explained in detail, for those skilled in the art, still can be to aforementioned each implementation
Technical solution documented by example is modified or equivalent replacement of some of the technical features.It is all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of high-hardness stainless steel grinding and polishing liquid, it is characterised in that: according to mass fraction, the original of the grinding and polishing liquid
Material component includes: 16-19 parts of magnesium stearate, and 9-13 parts of polyethylene wax, 1.5-1.9 parts of complexing agent, 4-8 parts of grinding agent, corrosion inhibiter
2-3 parts, 1-2 parts of wetting dispersing agent, 1.5-2.8 parts of silane coupling agent, 7-10 parts of hydrochloric acid solution, 100-130 parts of kerosene.
2. a kind of high-hardness stainless steel grinding and polishing liquid according to claim 1, it is characterised in that: according to mass parts
Number, the raw material components of the grinding and polishing liquid include: 17-18 parts of magnesium stearate, and 10-12 parts of polyethylene wax, complexing agent 1.6-1.8
Part, 5-7 parts of grinding agent, 2.4-2.7 parts of corrosion inhibiter, 1.3-1.8 parts of wetting dispersing agent, 1.9-2.5 parts of silane coupling agent, hydrochloric acid is molten
8-9 parts of liquid, 115-125 parts of kerosene.
3. a kind of high-hardness stainless steel grinding and polishing liquid according to claim 2, it is characterised in that: according to mass parts
Number, the raw material components of the grinding and polishing liquid include: 17.5 parts of magnesium stearate, 11 parts of polyethylene wax, 1.7 parts of complexing agent, are ground
6 parts of agent, 2.6 parts of corrosion inhibiter, 1.5 parts of wetting dispersing agent, 2.3 parts of silane coupling agent, 8.4 parts of hydrochloric acid solution, 120 parts of kerosene.
4. a kind of high-hardness stainless steel grinding and polishing liquid according to claim 1, it is characterised in that: the grinding agent warp
Cross surface treatment, preparation method are as follows: by schmigel, cubic boron nitride, nano silica, cerium oxide according to 10:2:4:1's
Mass ratio is uniformly mixed, and heats 40-60min with 300-450 DEG C of temperature, is then reduced temperature to room temperature, will then be mixed
Object is closed to be added in the alcohol solvent of 3-5 times of volume, be added into alcohol solvent the polypropylene glycol of 2.3wt%, 4wt% glycerol and
The dodecyl sodium sulfate of 3.5wt% is heated with 50-60 DEG C of temperature water bath, and with the revolving speed decentralized processing of 350-420r/min
The solid content being obtained by filtration is dried with 85-95 DEG C of temperature, obtains required grinding agent by 13-16min, dispersion liquid filtering.
5. a kind of high-hardness stainless steel grinding and polishing liquid according to claim 4, it is characterised in that: the schmigel
Partial size is 100-120 μm, and the partial size of cubic boron nitride is 50-80 μm.
6. a kind of high-hardness stainless steel grinding and polishing liquid according to claim 1, it is characterised in that: the complexing agent is
The mixture that citric acid or ammonium lacate are mixed according to the molar ratio of 3:1.
7. a kind of high-hardness stainless steel grinding and polishing liquid according to claim 1, it is characterised in that: the corrosion inhibiter benzene
And triazole or polyphosphate sodium.
8. a kind of high-hardness stainless steel grinding and polishing liquid according to claim 1, it is characterised in that: the hydrochloric acid solution
Concentration be 6-8%.
9. a kind of high-hardness stainless steel grinding and polishing liquid according to claim 1, it is characterised in that: the wetting and dispersing
Agent is polysorbas20 or sorbester p17.
10. a kind of high-hardness stainless steel grinding and polishing liquid described in -9 any one according to claim 1, which is characterized in that
The grinding and polishing liquid the preparation method comprises the following steps:
According to mass fraction, kerosene is added in Scattered Kettle, 50-53 DEG C in heating, then by magnesium stearate and polyethylene wax
It is added in Scattered Kettle, with the revolving speed decentralized processing 6-8min of 600-650r/min, grinding agent, corrosion inhibiter and complexing agent is added
It into hydrochloric acid solution, stirs, dispersion liquid and wetting dispersing agent, silane coupling agent is then added to Scattered Kettle together
In, continue decentralized processing 15-25min, obtained water-in-oil emulsion is required grinding and polishing liquid.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811019523.5A CN109021835A (en) | 2018-09-03 | 2018-09-03 | A kind of high-hardness stainless steel grinding and polishing liquid |
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| CN201811019523.5A CN109021835A (en) | 2018-09-03 | 2018-09-03 | A kind of high-hardness stainless steel grinding and polishing liquid |
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| CN110722409A (en) * | 2019-11-19 | 2020-01-24 | 浦江县承煌光电技术有限公司 | High-precision ball processing method |
| CN110814928A (en) * | 2019-11-19 | 2020-02-21 | 浦江县承煌光电技术有限公司 | Method for processing high-surface-smoothness ball |
| CN115074087A (en) * | 2022-06-24 | 2022-09-20 | 广东优贝精细化工有限公司 | Glass grinding agent and preparation method thereof |
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Application publication date: 20181218 |