CN106420461A - Application of herbal extract composition in liquid shampoo with function of scalp nursing - Google Patents
Application of herbal extract composition in liquid shampoo with function of scalp nursing Download PDFInfo
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- CN106420461A CN106420461A CN201610890935.0A CN201610890935A CN106420461A CN 106420461 A CN106420461 A CN 106420461A CN 201610890935 A CN201610890935 A CN 201610890935A CN 106420461 A CN106420461 A CN 106420461A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/34—Free of silicones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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- Engineering & Computer Science (AREA)
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- Mycology (AREA)
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- Cosmetics (AREA)
Abstract
The invention discloses an application of a herbal extract composition in liquid shampoo with function of scalp nursing. The invention discloses liquid shampoo free of silicone oil. The liquid shampoo is prepared from, by weight, 0.05-1 part of herbal extract composition, 0.5-2 parts of positive ion conditioner, 10-50 parts of surface active agent, 0.1-1 part of humectant, 0.1-0.5 part of anti-dangdruff agent and 50-90 parts of deionized water. The liquid shampoo solves the problems that long-term use of liquid shampoo containing silicone oil and other hazardous substances causes blocking of hair follicles, prevents the scalp from breathing, affects health of the scalp and hair, and causes alopecia, hair loss, and hair breaking.
Description
Technical field
The present invention relates to cosmetic technical field, particularly to a kind of plant quintessence compositionss, there is scalp care effect
Shampoo in application.
Background technology
In recent years, research finds that existing washing uses silicone oil, mineral oilses, petroleum-type, nipalgin for a long time in shield compositionss
The raw materials such as esters, stain, will result in blocking hair follicle, hinder scalp breathing, thus affecting the health of scalp and hair, causing to take off
Send out, alopecia, disconnected send out；More importantly the person is caused with a lot of diseases.Therefore, consumer is to " silicate-containing oil shampoo is by hair
Wash more poor and more poor " complaint emerge in an endless stream.And the healthy hair of health comes from washing shield product and washing shield mode of health, in Japan 59%
The idea of people's recipient plant quintessence no silicone oil hair nursing, in America and Europe, this numeral has reached 63%.Plant essence no silicone oil is washed
Shield is as a kind of scalp care mode of health, it has also become wash now the main research direction of shield compositionss.
Chinese patent 201410683319.9 discloses one kind no silicon shampoo, mainly by alkylpolyoxyethylene sulfur
Sour sodium, cocamido propyl betaine, cocoanut oil diethan olamide, glycol stearate, cellulose quaternary ammonium salt, Fructus Citri Limoniae
Acid, sodium chloride, shredding, essence, disodium EDTA composition, but it is only without silicone oil, does not adopt
Silicone oil substitute, after hair washing, hair dries up, and does not have smooth feeling.
Content of the invention
The technical problem to be solved is to provide a kind of preparation method of plant essence compositionss.
It is a further object to provide the plant essence compositionss of above-mentioned preparation method gained have scalp shield
Application in the shampoo of reason effect.
The technical problem to be solved is achieved by the following technical programs：
A kind of preparation method of plant quintessence compositionss, comprises the steps of：
(1) first mixture will be formed after Flos Osmanthi Fragrantis, Caulis Seu Folium Lespedezae Bicoloris, Herba Leibnitziae, Radix Rhodiolae, Folium Agaves variegatae, Flos Rosae Rugosae combination drying；
(2) described mixture is placed in extractor, adds in the Extraction solvent containing Herba Rosmarini Officinalis extract, in 5000-
Extract under the rotating speed of 10000r/min, to be extracted after the completion of, extracting solution is filtered, discards filtering residue, collect supernatant；
(3) gained supernatant is carried out being evaporated under reduced pressure and concentrate, obtain concentrated solution；
(4) MCI resin column purification on described concentrated solution, through ion, 40-50% (volume fraction) ethanol remove impurity, 70-
85% (volume fraction) ethanol elution, collects eluent；
(5) described eluent adds activated carbon decolorizing, filters, and concentrates, and is dried, obtains refined plant quintessence compositionss.
Further, described Extraction solvent is the ethanol solution of 40-60% for concentration of volume percent；Described Herba Rosmarini Officinalis carries
Take the weight of thing and ethanol than for 1：(80-90).
Further, the weight of described Extraction solvent is 2-3 times of described mixture.
Further, the concentration of alcohol of ethanol remove impurity described in step (4) is 45-50%, and ethanol volume is 2-10 cylinder
Long-pending, the concentration of alcohol of described ethanol elution is 75-80%, and ethanol volume is 2-10 column volume.
Yet further, the activated carbon decolorizing described in step (5), activated carbon addition is mixture medical material weight
0.01-0.1 times.
Application in the shampoo with scalp care effect for the plant quintessence compositionss of described preparation method gained.
A kind of shampoo of no silicone oil, comprises the component of following parts by weight：
Plant quintessence compositionss 0.05-1 part of described preparation method gained；
0.5～2 part of cation opsonizing agent；
10～50 parts of surfactant；
0.1～1 part of wetting agent；
0.1～0.5 part of anti-dandruff agent；
50～90 parts of deionized water.
Further, described cation opsonizing agent is Polyquaternium-10 or cation guar gum.
Further, described surfactant is polyoxyethylenated alcohol sodium sulfate, sodium cocoyl glycinate, lauroyl
Vlmethyl sodium propionate, sodium lauroyl sarcosine cocamido propyl betaine, fatty monoethanol amide, glycerol coconut palm
At least one in oleate, LAA, sodium isostearoyl lactylate.
Further, described wetting agent be glycine betaine, PCA- sodium, ethoxy urea, at least one in polyhydric alcohol.
Yet further, described anti-dandruff agent is Zinc Pyrithione.
Its necessary preparation composition can also be added, for example in the present invention no silicone oil shampoo：Chelating agen, thickening agent, anti-
Rotten agent and essence.
The present invention has the advantages that：
Especially by fan, repeatedly extract is dissolved in ethanol the present invention, extracts together as extractant.Repeatedly extract has very fan
Strong antioxidant activity, additionally it is possible to reduce the loss of vegetable composition active component in extraction process, improves vegetable composition
Stability, increases extraction efficiency, in the product, product is oxidized fewer for particular application.
After the plant quintessence compositionss of preparation method gained of the present invention are used for shampoo, scalp can be effectively facilitated and moisten guarantor
Wet, repair damaged scalp and hair, supplement the nutrition run off, repair damaged scalp and hair, keep scalp and hair healthy shape
The effect of state.
The shampoo of the present invention no silicone oil solves life-time service silicate-containing oil and other harmful substances, and result in blockage hair follicle,
Hinder scalp breathing, thus affecting the health of scalp and hair, causing alopecia, alopecia, the disconnected problem sent out.
Specific embodiment
In order to the present invention is better described, with reference in the embodiment of the present invention, technical scheme is carried out clearly
Chu, it is fully described by.
Embodiment 1
A kind of preparation method of plant quintessence compositionss, comprises the steps of：
(1) first mixture will be formed after Flos Osmanthi Fragrantis, Caulis Seu Folium Lespedezae Bicoloris, Herba Leibnitziae, Radix Rhodiolae, Folium Agaves variegatae, Flos Rosae Rugosae combination drying；
(2) described mixture is placed in extractor, adds 3 times of 60% ethanol having dissolved Herba Rosmarini Officinalis extract in advance molten
In liquid, dissolving ratio is 1:80, under the rotating speed of 5000-10000r/min extract, to be extracted after the completion of, extracting solution is filtered,
Discard filtering residue, collect supernatant；
(3) gained supernatant is carried out being evaporated under reduced pressure and concentrate, obtain concentrated solution；
(4) MCI resin column purification on described concentrated solution, through 2 column volume purified water ion, 2 column volume 45% (volume
Fraction) ethanol remove impurity, collect 2 column volume 75% (volume fraction) ethanol active component eluents.
(5) described eluent adds activated carbon decolorizing, filters, and concentrates, and is dried, obtains refined plant quintessence compositionss；Described
Activated carbon addition is 0.01 times of mixture medical material weight.
The plant quintessence compositionss of the present embodiment gained can be used for having in the middle of the shampoo of scalp care effect.
Embodiment 2
A kind of preparation method of plant quintessence compositionss, comprises the steps of：
(1) first mixture will be formed after Flos Osmanthi Fragrantis, Caulis Seu Folium Lespedezae Bicoloris, Herba Leibnitziae, Radix Rhodiolae, Folium Agaves variegatae, Flos Rosae Rugosae combination drying；
(2) described mixture is placed in extractor, adds 2 times of 40% ethanol having dissolved Herba Rosmarini Officinalis extract in advance molten
In liquid, dissolving ratio is 1:90, under the rotating speed of 5000-10000r/min extract, to be extracted after the completion of, extracting solution is filtered,
Discard filtering residue, collect supernatant；
(3) gained supernatant is carried out being evaporated under reduced pressure and concentrate, obtain concentrated solution；
(4) MCI resin column purification on described concentrated solution, through 10 column volume purified water ion, 10 column volume 50% (body
Fraction) ethanol remove impurity, collect 10 column volume 80% (volume fraction) ethanol active component eluents.
(5) described eluent adds activated carbon decolorizing, filters, and concentrates, and is dried, obtains refined plant quintessence compositionss；Described
Activated carbon addition is 0.1 times of mixture medical material weight.
The plant quintessence compositionss of the present embodiment gained can be used for having in the middle of the shampoo of scalp care effect.
Embodiment 3
A kind of preparation method of plant quintessence compositionss, comprises the steps of：
(1) first mixture will be formed after Flos Osmanthi Fragrantis, Caulis Seu Folium Lespedezae Bicoloris, Herba Leibnitziae, Radix Rhodiolae, Folium Agaves variegatae, Flos Rosae Rugosae combination drying；
(2) described mixture is placed in extractor, adds 1 times of 50% ethanol having dissolved Herba Rosmarini Officinalis extract in advance molten
In liquid, dissolving ratio is 1:85, under the rotating speed of 5000-10000r/min extract, to be extracted after the completion of, extracting solution is filtered,
Discard filtering residue, collect supernatant；
(3) gained supernatant is carried out being evaporated under reduced pressure and concentrate, obtain concentrated solution；
(4) MCI resin column purification on described concentrated solution, through 5 column volume purified water ion, 5 column volume 45% (volume
Fraction) ethanol remove impurity, collect 5 column volume 80% (volume fraction) ethanol active component eluents.
(5) described eluent adds activated carbon decolorizing, filters, and concentrates, and is dried, obtains refined plant quintessence compositionss；Described
Activated carbon addition is 0.05 times of mixture medical material weight.
The plant quintessence compositionss of the present embodiment gained can be used for having in the middle of the shampoo of scalp care effect.
Comparative example 1
A kind of preparation method of plant quintessence compositionss, comprises the steps of：
(1) first mixture will be formed after Flos Osmanthi Fragrantis, Caulis Seu Folium Lespedezae Bicoloris, Herba Leibnitziae, Radix Rhodiolae, Folium Agaves variegatae, Flos Rosae Rugosae combination drying；
(2) described mixture is placed in extractor, adds in 1 times of 50% ethanol solution, dissolving ratio is 1:85,
Extract under the rotating speed of 5000-10000r/min, to be extracted after the completion of, extracting solution is filtered, discards filtering residue, collect supernatant；
(3) gained supernatant is carried out being evaporated under reduced pressure and concentrate, obtain concentrated solution；
(4) MCI resin column purification on described concentrated solution, through 5 column volume purified water ion, 5 column volume 45% (volume
Fraction) ethanol remove impurity, collect 5 column volume 80% (volume fraction) ethanol active component eluents.
(5) described eluent adds activated carbon decolorizing, filters, and concentrates, and is dried, obtains refined plant quintessence compositionss；Described
Activated carbon addition is 0.05 times of mixture medical material weight.
Embodiment 4
Plant 0.05 part of the compositionss of essence of embodiment 1 gained；2 parts of Polyquaternium-10；Fatty alcohol-polyoxyethylene ether sulphuric acid
3 parts of sodium；5 parts of sodium cocoyl glycinate；2 parts of lauroyl methylaminopropionic sodium；0.1 part of glycine betaine；Zinc Pyrithione 0.2
Part；0.1 part of EDETATE SODIUM；0.3 part of sodium benzoate；90 parts of deionized water.
Embodiment 5
Plant 1 part of the compositionss of essence of embodiment 1 gained；2 parts of cation guar gum；Sodium lauroyl sarcosine coconut oleoyl amine
5 parts of CAB；10 parts of fatty monoethanol amide；5 parts of glyceryl cocoate；LAA 10
Part；10 parts of lauroyl methylaminopropionic sodium；10 parts of sodium isostearoyl lactylate；0.5 part of ethoxy urea；Zinc Pyrithione 0.5；
0.1 part of KF88；50 parts of deionized water.
Embodiment 6
Plant 0.5 part of the compositionss of essence of embodiment 1 gained；1.5 parts of cation guar gum；Fatty alcohol-polyoxyethylene ether sulfur
10 parts of sour sodium；5 parts of sodium cocoyl glycinate；5 parts of sodium lauroyl sarcosine cocamido propyl betaine；Fatty acid distribution of coconut oil list second
10 parts of alkylolamides；0.5 part of PCA- sodium；Zinc Pyrithione 0.3；0.3 part of sodium benzoate；70 parts of deionized water.
Comparative example 2
Plant 0.5 part of the compositionss of essence of comparative example 1 gained；1.5 parts of cation guar gum；Fatty alcohol-polyoxyethylene ether sulfur
10 parts of sour sodium；5 parts of sodium cocoyl glycinate；5 parts of sodium lauroyl sarcosine cocamido propyl betaine；Fatty acid distribution of coconut oil list second
10 parts of alkylolamides；0.5 part of PCA- sodium；Zinc Pyrithione 0.3；0.3 part of sodium benzoate；70 parts of deionized water.
The efficacy assessments that above example 6 and comparative example 2 are carried out.
Test number is：50 volunteers.
Described hair washing test be：Mainly include following step：
(1) first shampoo is fallen 3-5 gram on the palm of the hand, then drip some water above, gently crumple, allow shampoo to start to send out
After bubble, uniform application is on hair；
(2) it is massaging 2-3 minute by sawtooth or in the way of drawing circle with finger pulp part both hands when washing hair, so permissible
Reach massaging scalp, the purpose of blood circulation promoting.
(3) after hair is thoroughly cleaned, with substantial amounts of warm water by hair wash clean.
Table 1 shampoo using effect is evaluated
Understand from upper table, the present embodiment 6 is compared with comparative example 2, has more preferable using effect.
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto,
Any those familiar with the art in the technical scope of present disclosure, the change or replacement that can readily occur in,
All should be included within the scope of the present invention.Therefore, protection scope of the present invention should be with the protection of claims
Scope is defined.
Claims (10)
1. a kind of preparation method of plant quintessence compositionss is it is characterised in that comprise the steps of：
(1) first mixture will be formed after Flos Osmanthi Fragrantis, Caulis Seu Folium Lespedezae Bicoloris, Herba Leibnitziae, Radix Rhodiolae, Folium Agaves variegatae, Flos Rosae Rugosae combination drying；
(2) described mixture is placed in extractor, adds in the Extraction solvent containing Herba Rosmarini Officinalis extract, in 5000-
Extract under the rotating speed of 10000r/min, to be extracted after the completion of, extracting solution is filtered, discards filtering residue, collect supernatant；
(3) gained supernatant is carried out being evaporated under reduced pressure and concentrate, obtain concentrated solution；
(4) MCI resin column purification on described concentrated solution, through ion, 40-50% (volume fraction) ethanol remove impurity, 70-85%
(volume fraction) ethanol elution, collects eluent；
(5) described eluent adds activated carbon decolorizing, filters, and concentrates, and is dried, obtains refined plant quintessence compositionss.
2. according to claim 1 a kind of preparation method of plant quintessence compositionss it is characterised in that described Extraction solvent is
Concentration of volume percent is the ethanol solution of 40-60%；The weight of described Herba Rosmarini Officinalis extract and ethanol is than for 1：(80-90).
3. according to claim 1 a kind of preparation method of plant quintessence compositionss it is characterised in that described Extraction solvent
Weight is 2-3 times of described mixture.
4. according to claim 1 a kind of preparation method of plant quintessence compositionss it is characterised in that described in step (4)
The concentration of alcohol of ethanol remove impurity is 45-50%, and ethanol volume is 2-10 column volume, and the concentration of alcohol of described ethanol elution is 75-
80%, ethanol volume is 2-10 column volume.
5. according to claim 1 a kind of preparation method of plant quintessence compositionss it is characterised in that described in step (5)
Activated carbon decolorizing, activated carbon addition is 0.01-0.1 times of mixture medical material weight.
6. the plant quintessence compositionss of the preparation method gained described in claim 1 are in the shampoo with scalp care effect
Application.
7. a kind of shampoo of no silicone oil is it is characterised in that comprise the component of following parts by weight：Preparation described in claim 1
Plant quintessence compositionss 0.05-1 part of method gained；
0.5～2 part of cation opsonizing agent；
10～50 parts of surfactant；
0.1～1 part of wetting agent；
0.1～0.5 part of anti-dandruff agent；
50～90 parts of deionized water.
8. according to claim 7 one kind no silicone oil shampoo it is characterised in that described cation opsonizing agent be polyquaternary amine
Salt -10 or cation guar gum.
9. according to claim 7 one kind no silicone oil shampoo it is characterised in that described surfactant be fatty alcohol polyoxy
Ethylene ether sodium sulfate, sodium cocoyl glycinate, lauroyl methylaminopropionic sodium, sodium lauroyl sarcosine cocamidopropyl propyl amide
In glycine betaine, fatty monoethanol amide, glyceryl cocoate, LAA, sodium isostearoyl lactylate
At least one.
10. according to claim 7 one kind no silicone oil shampoo it is characterised in that described wetting agent be glycine betaine, PCA-
At least one in sodium, ethoxy urea, polyhydric alcohol；Described anti-dandruff agent is Zinc Pyrithione.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610890935.0A CN106420461A (en) | 2016-10-12 | 2016-10-12 | Application of herbal extract composition in liquid shampoo with function of scalp nursing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610890935.0A CN106420461A (en) | 2016-10-12 | 2016-10-12 | Application of herbal extract composition in liquid shampoo with function of scalp nursing |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107468563A (en) * | 2017-08-09 | 2017-12-15 | 曾万祥 | A kind of anti-dandruff silk quality lubrication is without silicone oil shampoo |
| WO2018162834A1 (en) * | 2017-03-07 | 2018-09-13 | Laboratoires De Biologie Vegetale Yves Rocher | Use of extracts of agave for a hair application |
| CN108653027A (en) * | 2018-07-03 | 2018-10-16 | 广州仲思生物科技有限公司 | A kind of amino acid transparent hair shampoo and preparation method without dioxane and silica |
| CN112773751A (en) * | 2021-01-12 | 2021-05-11 | 吴维碧 | Infant shampoo and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105727234A (en) * | 2016-03-29 | 2016-07-06 | 四川力久知识产权服务有限公司 | Traditional Chinese medicine composition for treating alopecia as well as preparation method and application of traditional Chinese medicine composition |
-
2016
- 2016-10-12 CN CN201610890935.0A patent/CN106420461A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105727234A (en) * | 2016-03-29 | 2016-07-06 | 四川力久知识产权服务有限公司 | Traditional Chinese medicine composition for treating alopecia as well as preparation method and application of traditional Chinese medicine composition |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2018162834A1 (en) * | 2017-03-07 | 2018-09-13 | Laboratoires De Biologie Vegetale Yves Rocher | Use of extracts of agave for a hair application |
| FR3063637A1 (en) * | 2017-03-07 | 2018-09-14 | Laboratoires De Biologie Vegetale Yves Rocher | USE OF AGAVE EXTRACTS FOR A CAPILLARY APPLICATION |
| CN107468563A (en) * | 2017-08-09 | 2017-12-15 | 曾万祥 | A kind of anti-dandruff silk quality lubrication is without silicone oil shampoo |
| CN108653027A (en) * | 2018-07-03 | 2018-10-16 | 广州仲思生物科技有限公司 | A kind of amino acid transparent hair shampoo and preparation method without dioxane and silica |
| CN112773751A (en) * | 2021-01-12 | 2021-05-11 | 吴维碧 | Infant shampoo and preparation method thereof |
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