CN106377458A - Shampoo composition containing tea seed cake extracts and preparation method thereof - Google Patents
Shampoo composition containing tea seed cake extracts and preparation method thereof Download PDFInfo
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- CN106377458A CN106377458A CN201610896888.0A CN201610896888A CN106377458A CN 106377458 A CN106377458 A CN 106377458A CN 201610896888 A CN201610896888 A CN 201610896888A CN 106377458 A CN106377458 A CN 106377458A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention discloses a shampoo composition containing tea seed cake extracts. The shampoo composition is prepared from the following ingredients: tea seed cake water extracts, Kathon, pure water, cationic guar gum, citric acid, EDTA (ethylene diamine tetraacetic acid)-2Na, cocamidopropyl betaine, fatty alcohol polyoxyethylene ether sulfate, ammonium lauryl sulfate, alkyl glucoside, PEG(polyethylene glycol)-7 cocinic acid glyceride, essence and refined salt. The invention also discloses a preparation method of the shampoo composition containing tea seed cake extracts. After being used, the shampoo composition has the advantages that the raw material cost is low; the bubble forming and bubble stabilizing effects of the product are good; the efficacies of removing dandruff, relieving itching and nourishing hair are achieved.
Description
Technical field
The present invention relates to a kind of daily hair washing product, more particularly, to a kind of shampoo Compositions containing tea seed cake extract；
The invention still further relates to a kind of preparation method of the shampoo Compositions containing tea seed cake extract.
Background technology
Oil tea is the distinctive woody oil tree species of southern china, and the oil tea history of existing more than 2300 year is cultivated by China.Its fruit
The oil coming of squeezing out in fact is referred to as Oleum Camelliae, and Oleum Camelliae is because containing having high nutritive value higher than 60% unsaturated fatty acid, matching in excellence or beauty
Olive oil, Semen Camelliae after being extracted oil by milling process remaining garbage be tea seed cake, before tea seed cake mainly as fuel with fertile
Material, burns as bavin or fertilising uses, actually tea seed cake can also kill the frog incubate, Tinea Ranae, Hirudo and spiral shell freshwater mussel, multiple wild fisheses shrimp
And pathogen, it is that one kind is preferably cleaned up the pond medicine.By tea seed cake pulverize soaked after, splash in early rice rice seedling bed, drum can be killed
Mud worm, to early rice seed rudiment, helps pin favourable.There is no detergent and soap epoch, people with tea seed cake soaked come clothes of doing washing,
Actually tea seed cake also has when shampoo is not yet popularized, and people do hair washing skin protection with tea seed cake bubble hot water and are used, and have anti-dandruff stopping
The effect itched.Above-mentioned use is also being followed so far.
The Oleum Camelliae that existing hair washing product is squeezed out using camellia oleosa seed as its active component, such as Chinese patent CN 102488634
B discloses a kind of Wild camellia oil shampoo, to refine the active component as product for the Wild camellia oil, has parasite killing, resists
Bacterium, anticreep and anti-dandruff effect.But hair washing product is applied to remaining tea seed cake after oil expression, the art is also in blank
State.
Content of the invention
The technical problem to be solved is, provides a kind of shampoo Compositions containing tea seed cake extract, former
Material low cost, product foaming foam stabilizing effect is good, has functions that removing scurf and relieving itching, nourishes hair.
The technical problem to be solved also resides in, and provides a kind of shampoo Compositions containing tea seed cake extract
Preparation method.
In order to solve above-mentioned technical problem, the invention provides a kind of shampoo Compositions containing tea seed cake extract, by A
Component, B component and component C are made；
Component A includes following raw material by weight percentage：
Tea seed cake water extract 0.5-2%；
Kazon 0.05-0.1%；
Pure water 2-8%；
B component includes following raw material by weight percentage：
Pure water 60-70%；
Cation guar gum 0.1-1%；
Citric acid 0.005-0.02%；
EDTA-2Na 0.05-0.2%；
Cocamido propyl betaine 2-8%；
Fatty alcohol polyoxyethylene ether sulfate 10-20%；
Ammonium lauryl sulfate 1-5%；
Alkyl androstanediol 0.1-1%；
PEG-7 glyceryl cocoate 0.5-2%；
Component C includes following raw material by weight percentage：
Essence 0.1-0.5%；
Refined salt 1-3%.
As the improvement of described shampoo Compositions, described tea seed cake water extract is obtained by following extracting method：
（1）Pulverize：Weigh quantitative tea seed cake, break into pieces, be subsequently adding Universalpulverizer and pulverized, obtain the tea of 20 ~ 50 mesh
Seedcake powder；
（2）Extract：Add water, heated and boiled 50 ~ 90min in tea seed cake powder, filter, obtain filtrate；
（3）Refined：Under 75 DEG C of temperature conditionss to filtrate in be separately added into weight be filtrate volume 0.4 ~ 0.8 ‰ ZTC- plant carry
Clarifier B group and the ZTC- that weight is filtrate volume 0.2 ~ 0.4 ‰ plant and put forward clarifier A group, stir, stand to room temperature, take
Supernatant, filters, obtains refined liquid；
（4）Concentrate：Using fine vacuum heat pump dual-effect concentrator, refined liquid is carried out being concentrated into the concentrated solution of solid contents >=30%
Body；
（5）It is dried：Concentrated liquid spray dryer is dried, obtains dry powdered tea seed cake extract.
As the improvement of described shampoo Compositions, the pure water of described component A is 45 DEG C of pure water.
As the improvement of described shampoo Compositions, it is made up of component A, B component and component C；
Component A includes following raw material by weight percentage：
Tea seed cake water extract 0.5-1%；
Kazon 0.08%；
Pure water 4-6%；
B component includes following raw material by weight percentage：
Pure water 65-68%；
Cation guar gum 0.3-0.6%；
Citric acid 0.01-0.015%；
EDTA-2Na 0.1-0.2%；
Cocamido propyl betaine 3-6%；
Fatty alcohol polyoxyethylene ether sulfate 15-18%；
Ammonium lauryl sulfate 2-5%；
Alkyl androstanediol 0.3-0.8%；
PEG-7 glyceryl cocoate 0.5-1.5%；
Component C includes following raw material by weight percentage：
Essence 0.2-0.4%；
Refined salt 1-2%.
The present invention also provides a kind of preparation method of the shampoo Compositions containing tea seed cake extract, comprises the following steps：
Step 1：By weight percentage the tea seed cake water extract of component A, Kazon are added to dissolving in pure water, stir,
Filtrate after filtration is expected stand-by as A；
Step 2：By weight percentage the pure water of B component, cation guar gum are added in pot, quick dispersed with stirring is uniform,
Add citric acid, after being warming up to 65 ~ 75 DEG C, be incubated 15 minutes；
Step 3：Add EDTA-2Na to stir, sequentially add cocamido propyl betaine, fatty alcohol-polyoxyethylene ether
Sulfate, ammonium lauryl sulfate, temperature is maintained at 65 ~ 75 DEG C and stirs to being completely dissolved, and is incubated 10 minutes；
Step 4：It is cooled to less than 65 DEG C, adds alkyl androstanediol, PEG-7 glyceryl cocoate, stir, obtain B material；
Step 5：It is cooled to less than 55 DEG C, A is expected to add in B material, stirs, obtain compound；
Step 6：Successively the essence of component C, refined salt are added in compound by weight percentage, stir；
Step 7：Sampling test control, Visual appearance state, survey pH value, viscosity, qualified rear shutdown discharging, obtain described shampoo
Compositionss.
As the preferred version of described preparation method, the filter cloth aperture filtering selection in described step 1 is 350-450 mesh.
Implement the embodiment of the present invention, have the advantages that：
The present invention removed by special water extraction method using tea seed cake water extract there is tannic acid, tannin of coagulated protein etc.
Be unfavorable for make hair washing product impurity, described tea seed cake water extract contain substantial amounts of tea saponin, tea polyphenols, Camellia Oleifera polysaccharide,
The various active composition such as polypeptide and flavone.When tea seed cake water extract is used for shampoo Compositions of the present invention, can play
Removing scurf and relieving itching, the effect of submissive hair, and with other agents coordinate in composite formula under not only increase foaming effect, make bubble
Foam is more, may also function as foam stabilizing effect, so that foam is held time longer.
The technology that tea seed cake extract is used for hair washing product has been filled up the blank in this field by the present invention, and tea seed cake
Low raw-material cost, the content of nutritional labeling is high and species is many, and effect of hair-washing hair-care significantly improves.
Specific embodiment
For making the object, technical solutions and advantages of the present invention clearer, the present invention will be made further detailed below
Description.
Semen Camelliae after being extracted oil by milling process remaining garbage be tea seed cake, tea seed cake contain a large amount of tea saponins, polysaccharide,
The various active composition such as polyphenol, polypeptide and flavone, can make hair washing skin protection and be used, have the effect of removing scurf and relieving itching.However, washing on the market
Sending out product adopts Oleum Camelliae as active component, and not only raw material sources are expensive, and can lack various active composition in tea seed cake.
The present invention exactly lacks, for prior art, the technical scheme being used for shampoo Compositions from tea seed cake extract, adopts
With special water extraction method, at utmost retain the active component in tea seed cake, not only act as good barbotage, also have
Effect of removing scurf and relieving itching.
Specifically, a kind of shampoo Compositions containing tea seed cake extract, are made up of component A, B component and component C；
Component A includes following raw material by weight percentage：
Tea seed cake water extract 0.5-2%；
Kazon 0.05-0.1%；
Pure water 2-8%；
B component includes following raw material by weight percentage：
Pure water 60-70%；
Cation guar gum 0.1-1%；
Citric acid 0.005-0.02%；
EDTA-2Na 0.05-0.2%；
Cocamido propyl betaine 2-8%；
Fatty alcohol polyoxyethylene ether sulfate 10-20%；
Ammonium lauryl sulfate 1-5%；
Alkyl androstanediol 0.1-1%；
PEG-7 glyceryl cocoate 0.5-2%；
Component C includes following raw material by weight percentage：
Essence 0.1-0.5%；
Refined salt 1-3%.
Preferably, the pure water of described component A is 45 DEG C of pure water.
Wherein, tea seed cake water extract is through pulverizing, and with flooding, adds ZTC- plant and carries clarifier, filter, concentrate,
Last mist projection granulating obtains, and removes and has the impurity that tannic acid, tannin of coagulated protein etc. are unfavorable for making hair washing product, described
Tea seed cake water extract contains the various active composition such as substantial amounts of tea saponin, tea polyphenols, Camellia Oleifera polysaccharide, polypeptide and flavone.
Tea saponin is a kind of natural nonionic surfactant, has foaming, decontamination, sterilization, antipruritic, moistening, soft
The function such as suitable, the nutrient substance such as flavone, polysaccharide, polypeptide has the function of nourishing hair, plays the effect of submissive hair；Tea polyphenols
It is water-soluble substanceses, washed hair with it and can remove greasy, the convergence pore of head, there is sterilization, resisting age of skin, reduce day
Ultraviolet radiation in light is to the effects such as the damage of skin.
Moreover, the cocamido propyl betaine in these active component and formula, fatty alcohol-polyoxyethylene ether sulfur
Synergism is played in hydrochlorate, ammonium lauryl sulfate and alkyl androstanediol cooperation, not only increases foaming effect, makes foam more,
May also function as foam stabilizing effect, so that foam is held time longer.
In addition, adopting kinds of surface activating agent in formula（Including cocamido propyl betaine, fatty alcohol-polyoxyethylene ether
Sulfate, ammonium lauryl sulfate and alkyl androstanediol）Compounding method, reduces the zest that single surfactant brings
Greatly, the problems such as too strong hair leading to of defat is dry and astringent.
The concrete extracting method of described tea seed cake water extract presented below：
（1）Pulverize：Weigh quantitative tea seed cake, break into pieces, be subsequently adding Universalpulverizer and pulverized, obtain the tea of 20 ~ 50 mesh
Seedcake powder；
（2）Extract：Add water, heated and boiled 50 ~ 90min in tea seed cake powder, filter, obtain filtrate；
（3）Refined：Under 75 DEG C of temperature conditionss to filtrate in be separately added into weight be filtrate volume 0.4 ~ 0.8 ‰ ZTC- plant carry
Clarifier B group and the ZTC- that weight is filtrate volume 0.2 ~ 0.4 ‰ plant and put forward clarifier A group, stir, stand to room temperature, take
Supernatant, filters, obtains refined liquid；
（4）Concentrate：Using fine vacuum heat pump dual-effect concentrator, refined liquid is carried out being concentrated into the concentrated solution of solid contents >=30%
Body；
（5）It is dried：Concentrated liquid spray dryer is dried, obtains dry powdered tea seed cake extract.
It should be noted that step（3）Add ZTC- plant and put forward clarifier A group and B group in filtrate, remove tannic acid, tan
While the impurity such as matter, pigment, farthest retain the various active compositions such as tea saponin, polysaccharide, polyphenol, polypeptide and flavone.
In addition, the tea seed cake extracting solution of water extraction contains substantial amounts of polysaccharide, saponin, these compositions are also easy to produce bubble when concentrating
, often bumping, runs material phenomenon, increase operation easier in foam, also reduces production efficiency simultaneously.Fine vacuum heat pump of the present invention
Dual-effect concentrator adopts heat pump economic benefits and social benefits technology and spraying mass transfer formula condenser, and it is high to have vacuum, good stability, energy-conserving and environment-protective
Feature, can be effectively prevented from when concentrating producing a large amount of foams it is ensured that concentration is smoothed out.
The preferred version of the shampoo Compositions containing tea seed cake extract of the present invention is, by component A, B component and C group
Divide and make；
Component A includes following raw material by weight percentage：
Tea seed cake water extract 0.5-1%；
Kazon 0.08%；
Pure water 4-6%；
B component includes following raw material by weight percentage：
Pure water 65-68%；
Cation guar gum 0.3-0.6%；
Citric acid 0.01-0.015%；
EDTA-2Na 0.1-0.2%；
Cocamido propyl betaine 3-6%；
Fatty alcohol polyoxyethylene ether sulfate 15-18%；
Ammonium lauryl sulfate 2-5%；
Alkyl androstanediol 0.3-0.8%；
PEG-7 glyceryl cocoate 0.5-1.5%；
Component C includes following raw material by weight percentage：
Essence 0.2-0.4%；
Refined salt 1-2%.
Correspondingly, the present invention also provides a kind of preparation method of the shampoo Compositions containing tea seed cake extract, including with
Lower step：
Step 1：By weight percentage the tea seed cake water extract of component A, Kazon are added to dissolving in pure water, stir,
Filtrate after filtration is expected stand-by as A；
Step 2：By weight percentage the pure water of B component, cation guar gum are added in pot, quick dispersed with stirring is uniform,
Add citric acid, after being warming up to 65 ~ 75 DEG C, be incubated 15 minutes；
Step 3：Add EDTA-2Na to stir, sequentially add cocamido propyl betaine, fatty alcohol-polyoxyethylene ether
Sulfate, ammonium lauryl sulfate, temperature is maintained at 65 ~ 75 DEG C and stirs to being completely dissolved, and is incubated 10 minutes；
Step 4：It is cooled to less than 65 DEG C, adds alkyl androstanediol, PEG-7 glyceryl cocoate, stir, obtain B material；
Step 5：It is cooled to less than 55 DEG C, A is expected to add in B material, stirs, obtain compound；
Step 6：Successively the essence of component C, refined salt are added in compound by weight percentage, stir；
Step 7：Sampling test control, Visual appearance state, survey pH value, viscosity, qualified rear shutdown discharging, obtain described shampoo
Compositionss.
Because the stirring of the nutritional labelings such as the Camellia Oleifera polysaccharide in the tea seed cake water extract in component A, polypeptide and flavone easily rises
Bubble, the present inventor will be separately manufactured to component A and B component according to this feature, can avoid under two kinds of component mixing situation through repeatedly stirring
Mix middle generation excessively to bubble, affect product quality.
It should be noted that the filter cloth aperture filtering selection in described step 1 is 350-450 mesh.Preferably, described step
The filter cloth aperture filtering selection in 1 is 400 mesh.
With reference to embodiment, the present invention is described in further detail, but embodiments of the present invention are not limited to
The scope that embodiment represents.
Embodiment 1
Formula：
The described shampoo Compositions containing tea seed cake extract are made up of component A, B component and component C；
Component A includes following raw material by weight percentage：
Tea seed cake water extract 1%；
Kazon 0.08%；
Pure water（45℃） 5%；
B component includes following raw material by weight percentage：
Pure water 66.0852%；
Cation guar gum 0.5%；
Citric acid 0.0148%；
EDTA-2Na 0.12%；
Cocamido propyl betaine 4%；
Fatty alcohol polyoxyethylene ether sulfate 17%；
Ammonium lauryl sulfate 3%；
Alkyl androstanediol 0.5%；
PEG-7 glyceryl cocoate 1%；
Component C includes following raw material by weight percentage：
Essence 0.3%；
Refined salt 1.4%.
Preparation method：
Step 1：By weight percentage the tea seed cake water extract of component A, Kazon are added to dissolving in pure water, stir,
Filtrate after filtration is expected stand-by as A；
Step 2：By weight percentage the pure water of B component, cation guar gum are added in pot, quick dispersed with stirring is uniform,
Add citric acid, after being warming up to 65 ~ 75 DEG C, be incubated 15 minutes；
Step 3：Add EDTA-2Na to stir, sequentially add cocamido propyl betaine, fatty alcohol-polyoxyethylene ether
Sulfate, ammonium lauryl sulfate, temperature is maintained at 65 ~ 75 DEG C and stirs to being completely dissolved, and is incubated 10 minutes；
Step 4：It is cooled to less than 65 DEG C, adds alkyl androstanediol, PEG-7 glyceryl cocoate, stir, obtain B material；
Step 5：It is cooled to less than 55 DEG C, A is expected to add in B material, stirs, obtain compound；
Step 6：Successively the essence of component C, refined salt are added in compound by weight percentage, stir；
Step 7：Sampling test control, Visual appearance state, survey pH value, viscosity, qualified rear shutdown discharging, obtain described shampoo
Compositionss.
Embodiment 2
Formula：
The described shampoo Compositions containing tea seed cake extract are made up of component A, B component and component C；
Component A includes following raw material by weight percentage：
Tea seed cake water extract 1.5%；
Kazon 0.06%；
Pure water（45℃） 7%；
B component includes following raw material by weight percentage：
Pure water 63.24%；
Cation guar gum 0.8%；
Citric acid 0.01%；
EDTA-2Na 0.08%；
Cocamido propyl betaine 6%；
Fatty alcohol polyoxyethylene ether sulfate 12%；
Ammonium lauryl sulfate 5%；
Alkyl androstanediol 1%；
PEG-7 glyceryl cocoate 1.2%；
Component C includes following raw material by weight percentage：
Essence 0.2%；
Refined salt 2%.
Preparation method：
Step 1：By weight percentage the tea seed cake water extract of component A, Kazon are added to dissolving in pure water, stir,
Filtrate after filtration is expected stand-by as A；
Step 2：By weight percentage the pure water of B component, cation guar gum are added in pot, quick dispersed with stirring is uniform,
Add citric acid, after being warming up to 65 ~ 75 DEG C, be incubated 15 minutes；
Step 3：Add EDTA-2Na to stir, sequentially add cocamido propyl betaine, fatty alcohol-polyoxyethylene ether
Sulfate, ammonium lauryl sulfate, temperature is maintained at 65 ~ 75 DEG C and stirs to being completely dissolved, and is incubated 10 minutes；
Step 4：It is cooled to less than 65 DEG C, adds alkyl androstanediol, PEG-7 glyceryl cocoate, stir, obtain B material；
Step 5：It is cooled to less than 55 DEG C, A is expected to add in B material, stirs, obtain compound；
Step 6：Successively the essence of component C, refined salt are added in compound by weight percentage, stir；
Step 7：Sampling test control, Visual appearance state, survey pH value, viscosity, qualified rear shutdown discharging, obtain described shampoo
Compositionss.
Embodiment 3
Formula：
The described shampoo Compositions containing tea seed cake extract are made up of component A, B component and component C；
Component A includes following raw material by weight percentage：
Tea seed cake water extract 0.8%；
Kazon 0.07%；
Pure water（45℃） 6%；
B component includes following raw material by weight percentage：
Pure water 66.318%；
Cation guar gum 0.4%；
Citric acid 0.012%；
EDTA-2Na 0.1%；
Cocamido propyl betaine 5%；
Fatty alcohol polyoxyethylene ether sulfate 15%；
Ammonium lauryl sulfate 4%；
Alkyl androstanediol 0.8%；
PEG-7 glyceryl cocoate 1.8%；
Component C includes following raw material by weight percentage：
Essence 0.5%；
Refined salt 1.2%.
Preparation method：
Step 1：By weight percentage the tea seed cake water extract of component A, Kazon are added to dissolving in pure water, stir,
Filtrate after filtration is expected stand-by as A；
Step 2：By weight percentage the pure water of B component, cation guar gum are added in pot, quick dispersed with stirring is uniform,
Add citric acid, after being warming up to 65 ~ 75 DEG C, be incubated 15 minutes；
Step 3：Add EDTA-2Na to stir, sequentially add cocamido propyl betaine, fatty alcohol-polyoxyethylene ether
Sulfate, ammonium lauryl sulfate, temperature is maintained at 65 ~ 75 DEG C and stirs to being completely dissolved, and is incubated 10 minutes；
Step 4：It is cooled to less than 65 DEG C, adds alkyl androstanediol, PEG-7 glyceryl cocoate, stir, obtain B material；
Step 5：It is cooled to less than 55 DEG C, A is expected to add in B material, stirs, obtain compound；
Step 6：Successively the essence of component C, refined salt are added in compound by weight percentage, stir；
Step 7：Sampling test control, Visual appearance state, survey pH value, viscosity, qualified rear shutdown discharging, obtain described shampoo
Compositionss.
Last should be noted that above example is only in order to illustrate technical scheme rather than to present invention guarantor
The restriction of shield scope, although being explained in detail to the present invention with reference to preferred embodiment, those of ordinary skill in the art should
Understand, technical scheme can be modified or equivalent, without deviating from the essence of technical solution of the present invention
And scope.
Claims (6)
1. a kind of shampoo Compositions containing tea seed cake extract are it is characterised in that be made up of component A, B component and component C；
Component A includes following raw material by weight percentage：
Tea seed cake water extract 0.5-2%；
Kazon 0.05-0.1%；
Pure water 2-8%；
B component includes following raw material by weight percentage：
Pure water 60-70%；
Cation guar gum 0.1-1%；
Citric acid 0.005-0.02%；
EDTA-2Na 0.05-0.2%；
Cocamido propyl betaine 2-8%；
Fatty alcohol polyoxyethylene ether sulfate 10-20%；
Ammonium lauryl sulfate 1-5%；
Alkyl androstanediol 0.1-1%；
PEG-7 glyceryl cocoate 0.5-2%；
Component C includes following raw material by weight percentage：
Essence 0.1-0.5%；
Refined salt 1-3%.
2. contain as claimed in claim 1 the shampoo Compositions of tea seed cake extract it is characterised in that described tea seed cake water extraction
Thing is obtained by following extracting method：
（1）Pulverize：Weigh quantitative tea seed cake, break into pieces, be subsequently adding Universalpulverizer and pulverized, obtain the tea of 20 ~ 50 mesh
Seedcake powder；
（2）Extract：Add water, heated and boiled 50 ~ 90min in tea seed cake powder, filter, obtain filtrate；
（3）Refined：Under 75 DEG C of temperature conditionss to filtrate in be separately added into weight be filtrate volume 0.4 ~ 0.8 ‰ ZTC- plant carry
Clarifier B group and the ZTC- that weight is filtrate volume 0.2 ~ 0.4 ‰ plant and put forward clarifier A group, stir, stand to room temperature, take
Supernatant, filters, obtains refined liquid；
（4）Concentrate：Using fine vacuum heat pump dual-effect concentrator, refined liquid is carried out being concentrated into the concentrated solution of solid contents >=30%
Body；
（5）It is dried：Concentrated liquid spray dryer is dried, obtains dry powdered tea seed cake extract.
3. contain as claimed in claim 1 the shampoo Compositions of tea seed cake extract it is characterised in that the pure water of described component A
For 45 DEG C of pure water.
4. contain as claimed in claim 1 the shampoo Compositions of tea seed cake extract it is characterised in that by component A, B component and C
Component is made；
Component A includes following raw material by weight percentage：
Tea seed cake water extract 0.5-1%；
Kazon 0.08%；
Pure water 4-6%；
B component includes following raw material by weight percentage：
Pure water 65-68%；
Cation guar gum 0.3-0.6%；
Citric acid 0.01-0.015%；
EDTA-2Na 0.1-0.2%；
Cocamido propyl betaine 3-6%；
Fatty alcohol polyoxyethylene ether sulfate 15-18%；
Ammonium lauryl sulfate 2-5%；
Alkyl androstanediol 0.3-0.8%；
PEG-7 glyceryl cocoate 0.5-1.5%；
Component C includes following raw material by weight percentage：
Essence 0.2-0.4%；
Refined salt 1-2%.
5. a kind of preparation method containing the shampoo Compositions of tea seed cake extract as claimed in claim 1 is it is characterised in that wrap
Include following steps：
Step 1：By weight percentage the tea seed cake water extract of component A, Kazon are added to dissolving in pure water, stir,
Filtrate after filtration is expected stand-by as A；
Step 2：By weight percentage the pure water of B component, cation guar gum are added in pot, quick dispersed with stirring is uniform,
Add citric acid, after being warming up to 65 ~ 75 DEG C, be incubated 15 minutes；
Step 3：Add EDTA-2Na to stir, sequentially add cocamido propyl betaine, fatty alcohol-polyoxyethylene ether
Sulfate, ammonium lauryl sulfate, temperature is maintained at 65 ~ 75 DEG C and stirs to being completely dissolved, and is incubated 10 minutes；
Step 4：It is cooled to less than 65 DEG C, adds alkyl androstanediol, PEG-7 glyceryl cocoate, stir, obtain B material；
Step 5：It is cooled to less than 55 DEG C, A is expected to add in B material, stirs, obtain compound；
Step 6：Successively the essence of component C, refined salt are added in compound by weight percentage, stir；
Step 7：Sampling test control, Visual appearance state, survey pH value, viscosity, qualified rear shutdown discharging, obtain described shampoo
Compositionss.
6. contain as claimed in claim 5 the preparation method of the shampoo Compositions of tea seed cake extract it is characterised in that described step
The filter cloth aperture filtering selection in rapid 1 is 350-450 mesh.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107468597A (en) * | 2017-10-09 | 2017-12-15 | 三江县稻香山茶油生态发展有限公司 | One plant tea bran shampoo and preparation method thereof |
| CN111449090A (en) * | 2020-04-13 | 2020-07-28 | 湖南润农生态茶油有限公司 | Preparation method of tea seed cake extract |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1754883A (en) * | 2004-10-01 | 2006-04-05 | 南华大学 | Production process for extracting tea saponin from tea-oil tree cake by using water as dissoluent |
| CN104055703A (en) * | 2014-06-18 | 2014-09-24 | 中山职业技术学院 | Dandruff-removing itching-relieving liquid shampoo and preparation method thereof |
| CN104940094A (en) * | 2015-07-23 | 2015-09-30 | 河源市西罗茶油开发有限公司 | Natural environment-friendly camellia cake shampoo and preparation method thereof |
| KR20160059263A (en) * | 2014-11-18 | 2016-05-26 | 정석훈 | Bubble type waterless shampoo composition |
-
2016
- 2016-10-14 CN CN201610896888.0A patent/CN106377458A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1754883A (en) * | 2004-10-01 | 2006-04-05 | 南华大学 | Production process for extracting tea saponin from tea-oil tree cake by using water as dissoluent |
| CN104055703A (en) * | 2014-06-18 | 2014-09-24 | 中山职业技术学院 | Dandruff-removing itching-relieving liquid shampoo and preparation method thereof |
| KR20160059263A (en) * | 2014-11-18 | 2016-05-26 | 정석훈 | Bubble type waterless shampoo composition |
| CN104940094A (en) * | 2015-07-23 | 2015-09-30 | 河源市西罗茶油开发有限公司 | Natural environment-friendly camellia cake shampoo and preparation method thereof |
Non-Patent Citations (2)
| Title |
|---|
| 孔令义: "《中药制药化学》", 30 April 2007, 中国医药科技出版社 * |
| 成本诚 等: "《新编实用化工小商品配方与生产(三)》", 30 June 1994, 中南工业大学出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107468597A (en) * | 2017-10-09 | 2017-12-15 | 三江县稻香山茶油生态发展有限公司 | One plant tea bran shampoo and preparation method thereof |
| CN111449090A (en) * | 2020-04-13 | 2020-07-28 | 湖南润农生态茶油有限公司 | Preparation method of tea seed cake extract |
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