CN106367957B - Tea contaminates the preparation method of garment material - Google Patents
Tea contaminates the preparation method of garment material Download PDFInfo
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- CN106367957B CN106367957B CN201610759046.0A CN201610759046A CN106367957B CN 106367957 B CN106367957 B CN 106367957B CN 201610759046 A CN201610759046 A CN 201610759046A CN 106367957 B CN106367957 B CN 106367957B
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Abstract
The invention discloses the preparation methods that a plant tea contaminates garment material, the infiltration of water is accelerated using fatty alcohol polyoxyethylene ether, sodium citrate, hydroxypropyl methyl cellulose, ethylmaltol, 2 hydracrylic acids, so that tea polyphenols is quickly entered in water, saves extraction time；2 phosphonobutane, 1,2,4 tricarboxylic acids sodium salt, sodium tetraphenylborate, 1,2,3,4,5, bis- (the 2 amino-ethyl ether) tetraacethyls of 6 hexamethylene hexacarboxylic acid sodium salts, sorbierite, ethylene glycol enhance tealeaves level dyeing, keep even dyeing consistent, while improving the moisture-proof rubbing fastness of tealeaves；Guar hydroxypropyltrimonium ammonium chloride, trehalose, Glucosamine Sulphate, 2,4,6 trichlorobenzoic acids, 4 hydroxyphenethylamines enhance the antibiotic property of chitosan, and contribute to colorfastness；Disodium ethylene diamine tetraacetate, L cysteines, 4 hydroxyl phenyl boric acids, the colour fixation that tea dyestuff is enhanced to methoxyphenylboronic acid, hexamethylolmelamine, so that dyefastness is enhanced, prepares a kind of garment material with good washing fastness, antibiotic property and Bearable dry and wet wipe.
Description
Technical field
The present invention relates to the preparation methods that tea contaminates garment material, especially with Bearable dry and wet wipe, water-fastness and with good
Dye easily color fastness tea dye garment material preparation method.
Background technology
China is that plant tea, tea making in the world and earliest country of drinking tea, tea tree planting area and yield occupy first place in the world.Tea
The physiological activator that leaf is rich in --- tea polyphenols, content account for about the 20-35% of its dry weight, and main component catechin is easily by oxygen
It is melted into the Tea Pigment for having and removing the physiological functions such as free radical, anti-oxidant, anti-mutation, anti-bacteria and anti-virus.But at present both at home and abroad
Develop that dark brown cellulose product is rare, the deep processed product researched and developed using fresh tea leaves as raw material is more rare.
Tea dye is the one kind belonged in plant dyeing technique.Tea dye, plant dye, are a life-stylize art.But in recent years
The general mood for advocating nature life is risen or the color of plant dye is naturally resistance to be seen.Plant dye truly has unique glamour, in addition to tool
There are natural colored, finished product to contain plant Shen Jing, soft, stable makings again, people wear the clothing of plant dye, distribute plant
Fragrance, not only without chemical stain composition, it might even be possible to protect skin；Tea dye is to be dyed with millet paste.With native annulus
It protects, the effect recovered one's original simplicity.Millet paste is dyed cloth, antique.Various thought-provoking clothes are dyed with various tea-drinking.Today,
As more and more people focus more on the health of itself, pursues " green product " and " green, which disappears, has become a kind of important need.
People are again dense to the interest of natural dye.Why natural dye has been favored by people, and is because natural
The colors such as dyestuff institute dyeing and weaving object, dress ornament are natural, graceful, rough, and have the breath of natural fragrance, while also having one
Fixed antibiotic health care and other effects.Natural dye is derived from naturally, be harmful to human health simultaneously, good with environment compatibility, is not polluted
Environment, it is biodegradable, assign people physiologically with psychological comfort.The growing, living standard of science and technology not
Disconnected abundant today, requirement of the people to food, clothing, housing and transportation are also improved constantly.It is growing day by day to the attention of environmental protection, health,
People more pursue clothing it is beautiful and comfortable, more focus on healthcare function.
The correlative study of upper dye mechanism about tea dyestuff is less, since its main component is the compound of polyphenol structure,
The combination of it and cotton fiber relies primarily on hydrogen bond and Van der Waals force, but this combination is not secured enough, causes dye-uptake low, color jail
Degree is poor, and the common method by the way that metal salt mordant is added can improve the dye-uptake of tea dyestuff, but not meet green ring
Factoring is read, and the defects of reproducibility is poor, fastness to washing is poor is existed simultaneously.
Invention content
, reproducibility poor with fastness to washing low defect low for dye-uptake existing for tradition, the present invention utilize free
Material improvement drawbacks described above.
1 tea contaminates the preparation method of garment material, it is characterised in that：
（1）By the 50g tealeaves crushed and 1g fatty alcohol polyoxyethylene ether, it is added in 900ml tap water, is warming up to 98
DEG C, during which extraction time control supplements clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution in 3h
The tea dye solution for being 3% to mass fraction；
（2）Prepare dressing liquid：
The glacial acetic acid solution 100g that mass concentration is 4% is gradually added into chitosan powder 15g and guar gum hydroxypropyl trimethylammonium
In ammonium chloride 2.6g, while after stirring evenly, water 100g is added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid；60g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 3 min are dried under 65 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, and the bath raio of tea dyeing is 1：5,2- is added
Phosphonobutane -1,2,4- tricarboxylic acids sodium salt, dye bath pH values be 8, at 45 DEG C, dyeing time control exists for dye bath temperature control
Disodium ethylene diamine tetraacetate is added in 1.0h, after dry 3 min under 75 DEG C of environment temperature, obtain tea dye garment material.
2 tea contaminate the preparation method of garment material, it is characterised in that：
（1）It by the 60g tealeaves crushed and sodium citrate 2g, is added in 1000ml tap water, is warming up to 98 DEG C, when extraction
Between control in 3h, during which supplement clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution to mass fraction
For 5% tea dye solution；
（2）Prepare dressing liquid：
The glacial acetic acid solution 200g that mass concentration is 4% is gradually added into chitosan powder 18g and 3.6g trehalose, simultaneously
After stirring evenly, water 150g is added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid；70g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 3 min are dried under 75 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, and the bath raio of tea dyeing is 1：4, it is added four
Phenylboric acid sodium, dye bath pH values be 8, at 55 DEG C, half Guang ammonia of L- is added in 1.5h in dyeing time control for dye bath temperature control
Acid, after dry 5 min under 75 DEG C of environment temperature, obtain tea dye garment material.
3 tea contaminate the preparation method of garment material, it is characterised in that：
（1）By the 70g tealeaves crushed and hydroxypropyl methyl cellulose 1.4g, it is added in 1200ml tap water, is warming up to
98 DEG C, during which extraction time control supplements clear water to keep total liquid measure constant in 4h, extraction terminates filtration residue, and concentration is molten
The tea dye solution that liquid is 4% to mass fraction；
（2）Prepare dressing liquid：
The glacial acetic acid solution 200g that mass concentration is 4% is gradually added into chitosan powder 20g and Glucosamine Sulphate 3.6g
In, while after stirring evenly, water 100g being added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid；60g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 4 min are dried under 75 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, and the bath raio of tea dyeing is 1：4, dye bath
PH values are 8,1,2,3,4,5,6- hexamethylene hexacarboxylic acid sodium salts, dye bath temperature control are added at 45 DEG C, dyeing time control exists
4- hydroxyl phenyl boric acids are added in 1.0h, after dry 5 min under 75 DEG C of environment temperature, obtain tea dye garment material.
4 tea contaminate the preparation method of garment material, it is characterised in that：
（1）It is added to the 80g tealeaves crushed and ethylmaltol 1.6g in 900ml tap water, is warming up to 98 DEG C, leaching
Time control is put forward in 2h, during which supplements clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution to quality
The tea dye solution that score is 3%；
（2）Prepare dressing liquid：
The glacial acetic acid solution 120g that mass concentration is 4% is gradually added into chitosan powder 12g and 2,4,6- trichlorobenzoic acid
In 4.6g, while after stirring evenly, water 100g is added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid；80g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 5 min are dried under 75 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, and the bath raio of tea dyeing is 1：6, dye bath
PH values are 8, and the control of sorbierite dye bath temperature is added at 50 DEG C, and dyeing time control is added in 1.5h to methoxyphenylboronic acid,
After dry 5min under 75 DEG C of environment temperature, obtain tea dye garment material.
5 tea contaminate the preparation method of garment material, it is characterised in that：
（1）It is added to the 90g tealeaves crushed and 2 hydroxy propanoic acid 1.8g in 900ml tap water, is warming up to 98 DEG C, leaching
Time control is put forward in 1h, during which supplements clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution to quality
The tea dye solution that score is 3%；
（2）Prepare dressing liquid：
The glacial acetic acid solution 100g that mass concentration is 4% is gradually added into chitosan powder 16g and 4- hydroxyphenethylamine 1.8g
In, while after stirring evenly, water 100g being added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid；60g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 3 min are dried under 65 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, and the bath raio of tea dyeing is 1：5, dye bath
PH values are 8, bis- (the 2- amino-ethyls ether) tetraacethyls of ethylene glycol, dye bath temperature control are added at 45 DEG C, dyeing time control exists
Hexamethylolmelamine is added in 1.0h, after dry 4min under 85 DEG C of environment temperature, obtain tea dye garment material.
The compare advantage of the prior art of the present invention is：
（1）Fatty alcohol polyoxyethylene ether, sodium citrate, hydroxypropyl methyl cellulose, ethylmaltol, 2 hydroxy propanoic acid add
The speed infiltration of water, enables tea polyphenols to quickly enter in water, has saved extraction time；
（2）2- phosphonobutane -1,2,4- tricarboxylic acids sodium salt, sodium tetraphenylborate, 1,2,3,4,5,6- hexamethylene hexacarboxylic acids
Bis- (the 2- amino-ethyls ether) tetraacethyls of sodium salt, sorbierite, ethylene glycol enhance tealeaves level dyeing, keep even dyeing consistent, improve simultaneously
The moisture-proof rubbing fastness of tealeaves；
（3）Guar hydroxypropyltrimonium ammonium chloride, trehalose, Glucosamine Sulphate, 2,4,6- trichlorobenzoic acids, 4-
Hydroxyphenethylamine enhances the antibiotic property of chitosan, and contributes to colorfastness；
（4）Disodium ethylene diamine tetraacetate, L-cysteine, 4- hydroxyls phenyl boric acid, to methoxyphenylboronic acid, hexamethylol three
Poly cyanamid enhances the colour fixation of tea dyestuff, and dyefastness is made to enhance；
（5）Raw material sources of the present invention are extensive, are easy to get, and wherein tealeaves comes from green tea, but the actual effect of the present invention
It is not limited to green tea；
（6）3,4,5-trihydroxy benzoic acid, succimide increase its washing fastness.
Specific implementation mode
Example 1
（1）By the 50g tealeaves crushed and 1g fatty alcohol polyoxyethylene ether, it is added in 900ml tap water, is warming up to 98
DEG C, during which extraction time control supplements clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution in 3h
The tea dye solution for being 3% to mass fraction；
（2）Prepare dressing liquid
The glacial acetic acid aqueous solution 100g that mass concentration is 4% is gradually added into chitosan powder 15g and guar gum hydroxypropyl trimethylammonium
In ammonium chloride 2.6g, while after stirring evenly, water 100g is added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid：60g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 3 min are dried under 65 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes：By step（3）Middle 60g pure cotton fabrics are added to
Step（1）In the tea dye solution of gained 3%, 2- phosphonobutanes -1,2,4- tricarboxylic acids sodium salt 5g, dye is added to tea dye solution
The pH values of bath are 8, and at 45 DEG C, disodium ethylene diamine tetraacetate 3g is added in 1.0h in dyeing time control for dye bath temperature control, 45
DEG C control reaction 20min, after dry 3 min under 75 DEG C of environment temperature, obtain tea dye garment material.
Example 2
（1）It by the 60g tealeaves crushed and sodium citrate 2g, is added in 1000ml tap water, is warming up to 98 DEG C, when extraction
Between control in 3h, during which supplement clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution to mass fraction
For 5% tea dye solution；
（2）Prepare dressing liquid
The glacial acetic acid solution 200g that mass concentration is 4% is gradually added into chitosan powder 18g and 3.6g trehalose, simultaneously
After stirring evenly, water 150g is added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid：70g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 3 min are dried under 75 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, step（3）Middle 70g pure cotton fabrics are added to step
Suddenly（1）Sodium tetraphenylborate 3.2g is added to tea dye solution in the tea dye solution tea dyestuff of gained 5%, and the pH values of dye bath are
8, at 55 DEG C, L-cysteine 2.4g, 45 DEG C of control reactions are added in 1.5h in dyeing time control for dye bath temperature control
30min, after dry 5 min under 75 DEG C of environment temperature, obtain tea dye garment material.
Example 3
（1）By the 70g tealeaves crushed and hydroxypropyl methyl cellulose 1.4g, it is added in 1200ml tap water, is warming up to
98 DEG C, during which extraction time control supplements clear water to keep total liquid measure constant in 4h, extraction terminates filtration residue, and concentration is molten
The tea dye solution that liquid is 4% to mass fraction；
（2）Prepare dressing liquid
The glacial acetic acid solution 200g that mass concentration is 4% is gradually added into chitosan powder 20g and Glucosamine Sulphate 3.6g
In, while after stirring evenly, water 100g being added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid；60g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 4 min are dried under 75 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes：Step（3）Middle 60g pure cotton fabrics are added to step
Suddenly（1）The pH values of the tea dye solution of gained 4%, dye bath are 8, and 1,2,3,4,5,6- hexamethylene, six carboxylic is added to tea dye solution
At 45 DEG C, 4- hydroxyl phenyl boric acids 4.2g, 45 DEG C of controls are added in 1.0h in dyeing time control for acid sodium-salt 2.5g, dye bath temperature control
System reaction, 15min, after dry 5 min under 75 DEG C of environment temperature, obtain tea dye garment material.
Example 4
（1）It is added to the 80g tealeaves crushed and ethylmaltol 1.6g in 900ml tap water, is warming up to 98 DEG C, leaching
Time control is put forward in 2h, during which supplements clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution to quality
The tea dye solution that score is 3%；
（2）Prepare dressing liquid
The glacial acetic acid solution 120g that mass concentration is 4% is gradually added into chitosan powder 12g and 2,4,6- trichlorobenzoic acid
In 4.6g, while after stirring evenly, water 100g is added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid：80g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 5 min are dried under 75 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes：By step（3）Middle 80g pure cotton fabrics are added to
Step（1）Sorbierite 5.2g is added to tea dye solution in the tea dye solution of gained 3%, and dye bath temperature control is at 50 DEG C, dye bath
PH values be 8, dyeing time control is added to methoxyphenylboronic acid 2.3g and Gallic Acid 0.8g in 1.5h,
45 DEG C of control reaction 20min, after dry 5min under 75 DEG C of environment temperature, obtain tea dye garment material.
Example 5
（1）It is added to the 90g tealeaves crushed and 2 hydroxy propanoic acid 1.8g in 900ml tap water, is warming up to 98 DEG C, leaching
Time control is put forward in 1h, during which supplements clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution to quality
The tea dye solution that score is 3%；
（2）Prepare dressing liquid
The glacial acetic acid solution 100g that mass concentration is 4% is gradually added into chitosan powder 16g and 4- hydroxyphenethylamine 1.8g
In, while after stirring evenly, water 100g being added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid：60g pure cotton knitted fabrics are padded into step
（2）Dressing liquid, two leaching two roll after, 3 min are dried under 65 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes：By step（3）Middle 60g pure cotton fabrics are added to
Step（1）Bis- (2- amino-ethyls ether) the tetraacethyl 4.3g of ethylene glycol, dye is added to tea dye solution in the tea dye solution of gained 3%
The pH values of bath are 8, and at 45 DEG C, hexamethylolmelamine 2.1g is added in 1.0h in dyeing time control for dye bath temperature control
With succimide 1.5g, 45 DEG C of control reaction 20min, after dry 4min under 85 DEG C of environment temperature, obtain tea dye clothes
Fill fabric.
Foundation：Anti-microbial property is detected by GB/15979-2002 methods, and washable aqueous and colour fastness to rubbing presses GB/ respectively
T3921-2008 and GB/T3920-2008 methods measure.
1 antibiotic property test data of table（Antibiotic rate）
| Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | |
| Staphylococcus aureus（%） | 99 | 99 | 99 | 98 | 99 |
| Escherichia coli（%） | 98 | 98 | 99 | 98 | 98 |
The color fastness of 2 present invention of table
| Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | |
| Washing fastness（Grade） | 4 | 3-4 | 4 | 4 | 4 |
| Colour fastness to rubbing（Grade） | 4 | 4 | 3-4 | 4-5 | 4-5 |
Claims (4)
1. tea contaminates the preparation method of garment material, it is characterised in that：
（1）It is added to the 50g tealeaves crushed and 1g fatty alcohol polyoxyethylene ether in 900ml tap water, is warming up to 98 DEG C, leaching
Time control is put forward in 3h, during which supplements clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution to quality
The tea dye solution that score is 3%；
（2）Prepare dressing liquid
The glacial acetic acid solution 100g that mass concentration is 4% is gradually added into chitosan powder 15g and guar hydroxypropyltrimonium chlorine
Change in ammonium 2.6g, while after stirring evenly, water 100g is added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid；60g pure cotton knitted fabrics are padded into step（2）'s
Dressing liquid dries 3 min after two leachings two are rolled under 65 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, and the bath raio of tea dyeing is 1：5,2- phosphines are added
Sour butane -1,2,4- tricarboxylic acids sodium salt, dye bath pH values be 8, at 45 DEG C, dyeing time is controlled in 1.0h for dye bath temperature control
, disodium ethylene diamine tetraacetate is added, after dry 3 min under 75 DEG C of environment temperature, obtain tea dye garment material.
2. tea contaminates garment material preparation method, it is characterised in that：
（1）By the 70g tealeaves crushed and hydroxypropyl methyl cellulose 1.4g, it is added in 1200ml tap water, is warming up to 98
DEG C, during which extraction time control supplements clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution in 4h
The tea dye solution for being 4% to mass fraction；
（2）Prepare dressing liquid：
The glacial acetic acid solution 200g that mass concentration is 4% is gradually added into chitosan powder 20g and Glucosamine Sulphate 3.6g,
After stirring evenly simultaneously, water 100g is added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid；60g pure cotton knitted fabrics are padded into step（2）'s
Dressing liquid dries 4 min after two leachings two are rolled under 75 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, and the bath raio of tea dyeing is 1：4, the pH of dye bath
Value is 8,1,2,3,4,5,6- hexamethylene hexacarboxylic acid sodium salts, dye bath temperature control is added at 45 DEG C, dyeing time is controlled in 1.0h
, 4- hydroxyl phenyl boric acids are added, after dry 5 min under 75 DEG C of environment temperature, obtain tea dye garment material.
3. tea contaminates the preparation method of garment material, it is characterised in that：
（1）It by the 80g tealeaves crushed and ethylmaltol 1.6g, is added in 900ml tap water, is warming up to 98 DEG C, when extraction
Between control in 2h, during which supplement clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution to mass fraction
For 3% tea dye solution；
The glacial acetic acid solution 120g that mass concentration is 4% is gradually added into chitosan powder 12g and 2,4,6- trichlorobenzoic acid 4.6g
In, while after stirring evenly, water 100g being added to mix well to obtain dressing liquid；
（3）Pure cotton knitted fabric is arranged using padding method using dressing liquid；80g pure cotton knitted fabrics are padded into step（2）'s
Dressing liquid dries 5 min after two leachings two are rolled under 75 DEG C of environment temperature；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, and the bath raio of tea dyeing is 1：6, the pH of dye bath
Value is 8, the control of sorbierite dye bath temperature is added at 50 DEG C, dyeing time control is added, in 1.5h to methoxyphenylboronic acid, knot
5min is dried under 75 DEG C of environment temperature after beam, obtains tea dye garment material.
4. tea contaminates the preparation method of garment material, it is characterised in that：
（1）It by the 90g tealeaves crushed and 2 hydroxy propanoic acid 1.8g, is added in 900ml tap water, is warming up to 98 DEG C, when extraction
Between control in 1h, during which supplement clear water to keep total liquid measure constant, extraction terminates filtration residue, concentrate solution to mass fraction
For 3% tea dye solution；
The glacial acetic acid solution 100g that mass concentration is 4% is gradually added into chitosan powder 16g and 4- hydroxyphenethylamine 1.8g, together
When stir evenly after, add water 100g to mix well to obtain dressing liquid；
（4）Pure cotton knitted fabric after being arranged to collated liquid dyes, and the bath raio of tea dyeing is 1：5, the pH of dye bath
Value is 8, bis- (the 2- amino-ethyls ether) tetraacethyls of ethylene glycol, dye bath temperature control is added at 45 DEG C, dyeing time is controlled in 1.0h
, hexamethylolmelamine is added, after dry 4min under 85 DEG C of environment temperature, obtain tea dye garment material.
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| CN111979794B (en) * | 2020-07-31 | 2022-01-04 | 盐城工学院 | Functional modification method for improving dyeing effect of natural dye alkaline bath for fabric |
| CN111996815B (en) * | 2020-08-26 | 2021-08-17 | 盐城工学院 | Preparation and dyeing of boron/silicon-containing hybrid functional protein fiber |
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|---|---|---|---|---|
| CN101851869A (en) * | 2010-06-09 | 2010-10-06 | 五邑大学 | Accelerant of active dye |
| CN103451963A (en) * | 2013-08-09 | 2013-12-18 | 常州纺织服装职业技术学院 | Method for dyeing cotton fabric with tea dye and finishing liquor used by method |
| CN104087020A (en) * | 2014-07-01 | 2014-10-08 | 常州大学 | Preparation method and application of chitosan-natural plant pigment macromolecular dye solution |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101851869A (en) * | 2010-06-09 | 2010-10-06 | 五邑大学 | Accelerant of active dye |
| CN103451963A (en) * | 2013-08-09 | 2013-12-18 | 常州纺织服装职业技术学院 | Method for dyeing cotton fabric with tea dye and finishing liquor used by method |
| CN104087020A (en) * | 2014-07-01 | 2014-10-08 | 常州大学 | Preparation method and application of chitosan-natural plant pigment macromolecular dye solution |
Non-Patent Citations (1)
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| 王登良等."提高红碎茶水溶性多酚类保留量实验".《茶业科学》.1998,第18卷(第1期), * |
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