CN106349971A - Natural environment-friendly mildew-proof and damp-proof glutinous rice glue and preparation process thereof - Google Patents

Natural environment-friendly mildew-proof and damp-proof glutinous rice glue and preparation process thereof Download PDF

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CN106349971A
CN106349971A CN201610735429.4A CN201610735429A CN106349971A CN 106349971 A CN106349971 A CN 106349971A CN 201610735429 A CN201610735429 A CN 201610735429A CN 106349971 A CN106349971 A CN 106349971A
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parts
proof
oryza glutinosa
starch
water
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吴通明
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Tongxiang Jialifeng Industry Co Ltd
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Tongxiang Jialifeng Industry Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J103/00Adhesives based on starch, amylose or amylopectin or on their derivatives or degradation products
    • C09J103/02Starch; Degradation products thereof, e.g. dextrin
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/06Non-macromolecular additives organic
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/08Stabilised against heat, light or radiation or oxydation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Organic Chemistry (AREA)
  • Medicinal Preparation (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses natural environment-friendly mildew-proof and damp-proof glutinous rice glue and a preparation process thereof. The natural environment-friendly mildew-proof and damp-proof glutinous rice glue comprises, by weight, 20-38 parts of glutinous rice, 22-30 parts of non-glutinous rice, 17-23 parts of carboxymethyl modified starch, 16-20 parts of oxidative modified starch, 18-22 parts of salix leaves, 15-20 parts of fructus kochiae, 12-18 parts of thymus mongolicus, 8-13 parts of galla chinensis, 9-15 parts of cortex cinnamomi, 9-14 parts of cacumen biotae, 5-8 parts of cyrtomium fortune, 5-9 parts of elm barks and 13-18 parts of water-soluble colophony. The natural environment-friendly mildew-proof and damp-proof glutinous rice glue has good killing and inhibiting effects on normal mucedine of wallpaper, has a good mildew proofing effect after being placed in damp air for twelve months, can be used for a long term, and is high in gluing property and superior to other glutinous rice glue products in markets. And on the other hand, the natural environment-friendly mildew-proof and damp-proof glutinous rice glue made of natural plants has no toxic and side effects on human bodies and no pollution to environment, and is a natural environment-friendly mildew-proof and damp-proof product.

Description

A kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue and its preparation technology
Technical field
The present invention relates to a kind of Oryza glutinosa glue is and in particular to a kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue and its preparation technology, Belong to technical field of fine.
Background technology
Oryza glutinosa glue is with pure natural Oryza glutinosa or glutinous rice as raw material, is formed through 12 procedures such as purification, grinding, dryings Environment-protective adhesive.Oryza glutinosa glue source is natural, environment friendly and pollution-free, but existing Oryza glutinosa glue mildew resistant moistureproof effect general it is impossible to Meet the demand of life-time service.Generally antimildew function is realized by the method adding antifungus agent in prior art.
Fungal contamination brings serious harm to all many-sides of human lives.Wherein, mycete is not formed in funguses Whole hyphomycetes of big sporophore, often colonize in and carry out flourish on animal and plant body.There is many due in air Fungal spore, after falling within body surface, sprouts for mycelia, thus secreting out of enzyme to carry out corrosion under suitable temperature and humidity Object, so that rotten go rotten, the internal component of object also can change.
The a certain link that conventional chemical anti mildew agent is often optionally directed to mycete biological metabolism produces inhibitory action, Thus easily cause the formation and development of microbial resistance.Many studies demonstrate that most of mycete is to existing chemical anti mildew agent Create resistance.And, a large amount of use of chemical anti mildew agent brings serious ecological environmental pollution problem to the whole world, Its residual toxicity has also become the hidden trouble of Environmental security simultaneously.In addition, can antifungus agent uniformly be mixed with Oryza glutinosa glue itself It is also a problem that must take into.
Content of the invention
The purpose of the present invention is for overcoming above-mentioned the deficiencies in the prior art, providing a kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa Glue.
Present invention also offers a kind of preparation technology of described mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue.
For achieving the above object, the present invention adopts following technical proposals:
A kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, is to be made up of the component of following weight portion: 20~38 parts of Oryza glutinosa, round-grained rice 22~30 parts of rice, 17~23 parts of carboxymethyl modified starch, 16~20 parts of oxidation modification starch, 18~22 parts of Folium Salicis Babylonicae, the Fructus Kochiae 15 ~20 parts, 12~18 parts of Herba thymi vulgariss, 8~13 parts of Galla Chinensiss, 9~15 parts of Cortex Cinnamomi, 9~14 parts of Cacumen Platycladi, 5~8 parts of Rhizoma Osmundae, elm 5~9 parts of skin, 13~18 parts of water-soluble rosin.
Preferably, it is to be made up of the component of following weight portion: 22~35 parts of Oryza glutinosa, 24~28 parts of Semen oryzae sativae, carboxymethyl changes 19~22 parts of starch of property, 17~19 parts of oxidation modification starch, 19~21 parts of Folium Salicis Babylonicae, 16~19 parts of the Fructus Kochiae, Herba thymi vulgariss 13~17 Part, 9~12 parts of Galla Chinensiss, 10~14 parts of Cortex Cinnamomi, 10~13 parts of Cacumen Platycladi, 6~7 parts of Rhizoma Osmundae, 6~8 parts of Cortex ulmi pumilae, water solublity pine Fragrant 14~17 parts.
It is further preferred that being to be made up of the component of following weight portion: 30 parts of Oryza glutinosa, 27 parts of Semen oryzae sativae, carboxymethyl modified 21 parts of starch, 18 parts of oxidation modification starch, 20 parts of Folium Salicis Babylonicae, 18 parts of the Fructus Kochiae, 15 parts of Herba thymi vulgariss, 10 parts of Galla Chinensiss, 12 parts of Cortex Cinnamomi, 11 parts of Cacumen Platycladi, 7 parts of Rhizoma Osmundae, 7 parts of Cortex ulmi pumilae, 16 parts of water-soluble rosin.
Preferably, described carboxymethyl modified starch is to be carried out with Rhizoma Dioscoreae esculentae, Semen phaseoli radiati, Pedicellus et Pericarpium Trapae, Rhizoma Nelumbiniss or Corm Eleocharitis starch for raw material Carboxymethyl modified obtain;Oxidation modification starch is to carry out oxidation with Rhizoma Dioscoreae esculentae, Semen phaseoli radiati, Pedicellus et Pericarpium Trapae, Rhizoma Nelumbiniss or Corm Eleocharitis starch for raw material to change Property obtains.
A kind of preparation technology of above-mentioned mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, including step:
(1) preparation of extracting solution: weigh the Folium Salicis Babylonicae of formula ratio, the Fructus Kochiae, Herba thymi vulgariss, Galla Chinensiss, Cortex Cinnamomi, Cacumen Platycladi, pass through Crowd and Cortex ulmi pumilae, add the water of 4~6 times of weight, soak 2~3 hours, boil by intense fire, continue boiling by slow fire afterwards 2~3 hours, Filter, take filtrate, standby;
(2) weigh Oryza glutinosa and the Semen oryzae sativae of formula ratio, soaked 12~24 hours with the water of 3~5 times of weight, defibrination, 100~ 120 eye mesh screen screening and filterings, 90~120 DEG C of gelatinizings;
(3) carboxymethyl modified starch and the oxidation modification starch of formula ratio are added, 40~60 DEG C are stirred steaming and decocting 3~5 hours, Sequentially add water-soluble rosin and step (1) gained extracting solution, 70~80 DEG C are stirred steaming and decocting 6~8 hours, obtain final product.
Preferably, the water in step (1) and step (2) is deionized water or distilled water.
Preferably, the gelatinizing in step (2) adopts vapor or oil bath heating.
Beneficial effects of the present invention:
The Oryza glutinosa glue of the present invention is used with Oryza glutinosa and Semen oryzae sativae collocation, meets basic viscosity requirement, adds carboxymethyl modified shallow lake Powder and oxidation modification starch, strengthen caking property, and add Folium Salicis Babylonicae, the Fructus Kochiae, Herba thymi vulgariss, Galla Chinensiss, Cortex Cinnamomi, Cacumen Platycladi, pass through The composition such as crowd and Cortex ulmi pumilae, by the coordinated of each composition, is allowed to there is good mildew resistant moistureproof effect, in conjunction with water solublity pine Perfume is so that aforementioned each component can be sufficiently mixed obtains the good product of homogeneity.
To wallpaper, common mycete has preferable killing inhibitory action to the Oryza glutinosa glue of the present invention, and puts in humid air After putting 12 months, still there is preferable anti-mold effect, can be with life-time service.The gluing angle value of Oryza glutinosa of the present invention exists More than 90000mpa s, up to 110000mpa s, have preferable caking property, and the Oryza glutinosa glue far superior on market produces Product.And, the present invention is with natural plants as raw material, without any side effects to human body, free from environmental pollution, can make safely With being a kind of natural environmental-protective product of mildew resistant moistureproof.
Specific embodiment
With reference to embodiment the present invention will be further elaborated it should explanation, the description below merely to Explain the present invention, its content is not defined.
The water-soluble rosin of the present invention, purchased from Guangzhou Song Bao Chemical Co., Ltd..
Embodiment 1:
A kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, is made up of following components: Oryza glutinosa 20kg, Semen oryzae sativae 22kg, carboxylic first Base modified starch 17kg, oxidation modification starch 16kg, Folium Salicis Babylonicae 18kg, Fructus Kochiae 15kg, Herba thymi vulgariss 12kg, Galla Chinensiss 8kg, Cortex Cinnamomi 9kg, Cacumen Platycladi 9kg, Rhizoma Osmundae 5kg, Cortex ulmi pumilae 5kg, water-soluble rosin 13kg.
Wherein, described carboxymethyl modified starch and oxidation modification starch are to carry out carboxymethyl with sweet potato starch respectively for raw material Obtain with oxidation modification.
A kind of preparation technology of above-mentioned mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, including step:
(1) preparation of extracting solution: weigh the Folium Salicis Babylonicae of formula ratio, the Fructus Kochiae, Herba thymi vulgariss, Galla Chinensiss, Cortex Cinnamomi, Cacumen Platycladi, pass through Crowd and Cortex ulmi pumilae, add the deionized water of 4 times of weight, soak 2 hours, boil by intense fire, continue boiling by slow fire 2 hours afterwards, mistake Filter, takes filtrate, standby;
(2) weigh Oryza glutinosa and the Semen oryzae sativae of formula ratio, soaked 12 hours with the deionized water of 3 times of weight, defibrination, 100 mesh sieves Net screening and filtering, heats 90 DEG C of gelatinizings using vapor;
(3) add the carboxymethyl modified starch of formula ratio and oxidation modification starch, 40 DEG C of stirring steaming and decoctings 3 hours, successively plus Enter water-soluble rosin and step (1) gained extracting solution, 70 DEG C are stirred steaming and decocting 6 hours, obtain final product.
Embodiment 2:
A kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, is made up of following components: Oryza glutinosa 38kg, Semen oryzae sativae 30kg, carboxylic first Base modified starch 23kg, oxidation modification starch 20kg, Folium Salicis Babylonicae 22kg, Fructus Kochiae 20kg, Herba thymi vulgariss 18kg, Galla Chinensiss 13kg, meat Osmanthus 15kg, Cacumen Platycladi 14kg, Rhizoma Osmundae 8kg, Cortex ulmi pumilae 9kg, water-soluble rosin 18kg.
Wherein, described carboxymethyl modified starch and oxidation modification starch are to carry out carboxymethyl with green starch respectively for raw material Obtain with oxidation modification.
A kind of preparation technology of above-mentioned mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, including step:
(1) preparation of extracting solution: weigh the Folium Salicis Babylonicae of formula ratio, the Fructus Kochiae, Herba thymi vulgariss, Galla Chinensiss, Cortex Cinnamomi, Cacumen Platycladi, pass through Crowd and Cortex ulmi pumilae, add the distilled water of 6 times of weight, soak 3 hours, boil by intense fire, continue boiling by slow fire afterwards 3 hours, filter, Take filtrate, standby;
(2) Oryza glutinosa and the Semen oryzae sativae of formula ratio are weighed, with the distilled water immersion 24 hours of 5 times of weight, defibrination, 120 eye mesh screens Screening and filtering, using 120 DEG C of gelatinizings of oil bath heating;
(3) add the carboxymethyl modified starch of formula ratio and oxidation modification starch, 60 DEG C of stirring steaming and decoctings 5 hours, successively plus Enter water-soluble rosin and step (1) gained extracting solution, 80 DEG C are stirred steaming and decocting 8 hours, obtain final product.
Embodiment 3:
A kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, is made up of following components: Oryza glutinosa 22kg, Semen oryzae sativae 24kg, carboxylic first Base modified starch 19kg, oxidation modification starch 17kg, Folium Salicis Babylonicae 19kg, Fructus Kochiae 16kg, Herba thymi vulgariss 13kg, Galla Chinensiss 9kg, Cortex Cinnamomi 10kg, Cacumen Platycladi 10kg, Rhizoma Osmundae 6kg, Cortex ulmi pumilae 6kg, water-soluble rosin 14kg.
Wherein, described carboxymethyl modified starch and oxidation modification starch are to carry out carboxymethyl with water caltrop starch respectively for raw material Obtain with oxidation modification.
A kind of preparation technology of above-mentioned mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, including step:
(1) preparation of extracting solution: weigh the Folium Salicis Babylonicae of formula ratio, the Fructus Kochiae, Herba thymi vulgariss, Galla Chinensiss, Cortex Cinnamomi, Cacumen Platycladi, pass through Crowd and Cortex ulmi pumilae, add the deionized water of 4 times of weight, soak 3 hours, boil by intense fire, continue boiling by slow fire 2 hours afterwards, mistake Filter, takes filtrate, standby;
(2) weigh Oryza glutinosa and the Semen oryzae sativae of formula ratio, soaked 12 hours with the deionized water of 5 times of weight, defibrination, 120 mesh sieves Net screening and filtering, heats 90 DEG C of gelatinizings using vapor;
(3) add the carboxymethyl modified starch of formula ratio and oxidation modification starch, 60 DEG C of stirring steaming and decoctings 3 hours, successively plus Enter water-soluble rosin and step (1) gained extracting solution, 80 DEG C are stirred steaming and decocting 6 hours, obtain final product.
Embodiment 4:
A kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, is made up of following components: Oryza glutinosa 35kg, Semen oryzae sativae 28kg, carboxylic first Base modified starch 22kg, oxidation modification starch 19kg, Folium Salicis Babylonicae 21kg, Fructus Kochiae 19kg, Herba thymi vulgariss 17kg, Galla Chinensiss 12kg, meat Osmanthus 14kg, Cacumen Platycladi 13kg, Rhizoma Osmundae 7kg, Cortex ulmi pumilae 8kg, water-soluble rosin 17kg.
Wherein, described carboxymethyl modified starch and oxidation modification starch are to carry out carboxymethyl with Lotus Root Starch respectively for raw material Obtain with oxidation modification.
A kind of preparation technology of above-mentioned mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, including step:
(1) preparation of extracting solution: weigh the Folium Salicis Babylonicae of formula ratio, the Fructus Kochiae, Herba thymi vulgariss, Galla Chinensiss, Cortex Cinnamomi, Cacumen Platycladi, pass through Crowd and Cortex ulmi pumilae, add the distilled water of 6 times of weight, soak 2 hours, boil by intense fire, continue boiling by slow fire afterwards 3 hours, filter, Take filtrate, standby;
(2) Oryza glutinosa and the Semen oryzae sativae of formula ratio are weighed, with the distilled water immersion 12 hours of 5 times of weight, defibrination, 100~120 mesh Screen cloth screening and filtering, using 120 DEG C of gelatinizings of oil bath heating;
(3) add the carboxymethyl modified starch of formula ratio and oxidation modification starch, 40 DEG C of stirring steaming and decoctings 5 hours, successively plus Enter water-soluble rosin and step (1) gained extracting solution, 70 DEG C are stirred steaming and decocting 8 hours, obtain final product.
Embodiment 5:
A kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, is made up of following components: Oryza glutinosa 30kg, Semen oryzae sativae 27kg, carboxylic first Base modified starch 21kg, oxidation modification starch 18kg, Folium Salicis Babylonicae 20kg, Fructus Kochiae 18kg, Herba thymi vulgariss 15kg, Galla Chinensiss 10kg, meat Osmanthus 12kg, Cacumen Platycladi 11kg, Rhizoma Osmundae 7kg, Cortex ulmi pumilae 7kg, water-soluble rosin 16kg.
Wherein, described carboxymethyl modified starch and oxidation modification starch are purchased from National Starch industry (Shanghai) Co., Ltd..
A kind of preparation technology of above-mentioned mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue, including step:
(1) preparation of extracting solution: weigh the Folium Salicis Babylonicae of formula ratio, the Fructus Kochiae, Herba thymi vulgariss, Galla Chinensiss, Cortex Cinnamomi, Cacumen Platycladi, pass through Crowd and Cortex ulmi pumilae, add the deionized water of 5 times of weight, soak 2 hours, boil by intense fire, continue boiling by slow fire 3 hours afterwards, mistake Filter, takes filtrate, standby;
(2) weigh Oryza glutinosa and the Semen oryzae sativae of formula ratio, soaked 20 hours with the deionized water of 4 times of weight, defibrination, 110 mesh sieves Net screening and filtering, heats 100 DEG C of gelatinizings using vapor;
(3) add the carboxymethyl modified starch of formula ratio and oxidation modification starch, 50 DEG C of stirring steaming and decoctings 4 hours, successively plus Enter water-soluble rosin and step (1) gained extracting solution, 70 DEG C are stirred steaming and decocting 7 hours, obtain final product.
Test example
Mould proof test:
Screen mycete from wallpaper, carry out purifying agaric, analyze fungal species, from wherein selecting three kinds of mycetes, be respectively Chaetomium globosum (chaetomium qlobosum), aspergillus terreus (asperqillus terreus), Aspergillus fumigatus (aspergillus fumigatus), cultivates three kinds of mycetes according to normal experiment method culture dish, often in constant incubator Plant mycete and cultivate 6 groups respectively, be divided into matched group and 1~5 group of embodiment, three kinds of mycetes are placed in constant incubator and cultivate two days Afterwards, count the clump count of matched group and 1~5 group of embodiment and record, afterwards matched group and 1~5 group of embodiment are respectively placed in 6 Cultivate in individual incubator, wherein in the incubator of 1~5 group of embodiment, place the Oryza glutinosa glue being obtained in embodiment 1~5 respectively, right Do not put according in group incubator, the growing state of every group of mycete is observed and recorded in culture after 36 hours, the results are shown in Table 1.
The anti-mold effect of table 1. Oryza glutinosa glue
Conclusion as can be drawn from Table 1, to wallpaper, common mycete has preferable killing inhibitory action to the Oryza glutinosa glue of the present invention.
Mould proof effect duration test:
By antifungus agent in embodiment 1~5 respectively in the humid air of humidity 60%rh place three months, six months, ten After two months, according to the anti-mold effect to three kinds of mycetes for the aforesaid mould proof test method detection, the results are shown in Table 2.
Table 2. mould proof effect duration tests
From table 2 it can be seen that the Oryza glutinosa glue of the present invention still have after placing 12 months in humid air preferably anti- Mould effect, can be with life-time service.
Viscosity measurements are tested:
Applicant determines the viscosity of embodiment 1~5 Oryza glutinosa glue according to gb/t 2794-1995, and concrete data is shown in Table 3.
The viscosity data of table 3. Oryza glutinosa glue
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5
Viscosity (mpa s) 90000 90000 100000 100000 110000
Oryza glutinosa adhesiveness on market is typically in more than 50000mpa s, and the viscosity number of embodiment 1~5 exists More than 90000mpa s, up to 110000mpa s, have preferable caking property.
Although the above-mentioned specific embodiment to the present invention is described, not the limit to the scope of the present invention System, on the basis of technical scheme, those skilled in the art do not need to pay that creative work can make is each Plant modification or deformation still within protection scope of the present invention.

Claims (7)

1. a kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue is it is characterised in that be to be made up of the component of following weight portion: Oryza glutinosa 20 ~38 parts, 22~30 parts of Semen oryzae sativae, 17~23 parts of carboxymethyl modified starch, 16~20 parts of oxidation modification starch, 18~22 parts of Folium Salicis Babylonicae, 15~20 parts of the Fructus Kochiae, 12~18 parts of Herba thymi vulgariss, 8~13 parts of Galla Chinensiss, 9~15 parts of Cortex Cinnamomi, 9~14 parts of Cacumen Platycladi, Rhizoma Osmundae 5~ 8 parts, 5~9 parts of Cortex ulmi pumilae, 13~18 parts of water-soluble rosin.
2. a kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue according to claim 1 is it is characterised in that be by following weight portion Component make: 22~35 parts of Oryza glutinosa, 24~28 parts of Semen oryzae sativae, 19~22 parts of carboxymethyl modified starch, oxidation modification starch 17 ~19 parts, 19~21 parts of Folium Salicis Babylonicae, 16~19 parts of the Fructus Kochiae, 13~17 parts of Herba thymi vulgariss, 9~12 parts of Galla Chinensiss, 10~14 parts of Cortex Cinnamomi, 10~13 parts of Cacumen Platycladi, 6~7 parts of Rhizoma Osmundae, 6~8 parts of Cortex ulmi pumilae, 14~17 parts of water-soluble rosin.
3. a kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue according to claim 1 is it is characterised in that be by following weight portion Component make: 30 parts of Oryza glutinosa, 27 parts of Semen oryzae sativae, 21 parts of carboxymethyl modified starch, 18 parts of oxidation modification starch, 20 parts of Folium Salicis Babylonicae, 18 parts of the Fructus Kochiae, 15 parts of Herba thymi vulgariss, 10 parts of Galla Chinensiss, 12 parts of Cortex Cinnamomi, 11 parts of Cacumen Platycladi, 7 parts of Rhizoma Osmundae, 7 parts of Cortex ulmi pumilae, water solublity 16 parts of Colophonium.
4. a kind of mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue according to any one of claims 1 to 3 is it is characterised in that institute Stating carboxymethyl modified starch is to carry out carboxymethyl modified obtaining with Rhizoma Dioscoreae esculentae, Semen phaseoli radiati, Pedicellus et Pericarpium Trapae, Rhizoma Nelumbiniss or Corm Eleocharitis starch for raw material;Oxygen Changing modified starch is to carry out oxidation modification with Rhizoma Dioscoreae esculentae, Semen phaseoli radiati, Pedicellus et Pericarpium Trapae, Rhizoma Nelumbiniss or Corm Eleocharitis starch for raw material to obtain.
5. the preparation technology of the mildew resistant moistureproof natural environmental-protective Oryza glutinosa glue any one of a kind of claims 1 to 3, its feature exists In including step:
(1) preparation of extracting solution: weigh the Folium Salicis Babylonicae of formula ratio, the Fructus Kochiae, Herba thymi vulgariss, Galla Chinensiss, Cortex Cinnamomi, Cacumen Platycladi, Rhizoma Osmundae and Cortex ulmi pumilae, adds the water of 4~6 times of weight, soaks 2~3 hours, boils by intense fire, continue boiling by slow fire 2~3 hours afterwards, mistake Filter, takes filtrate, standby;
(2) weigh Oryza glutinosa and the Semen oryzae sativae of formula ratio, soaked 12~24 hours with the water of 3~5 times of weight, defibrination, 100~120 mesh Screen cloth screening and filtering, 90~120 DEG C of gelatinizings;
(3) carboxymethyl modified starch and the oxidation modification starch of formula ratio are added, 40~60 DEG C are stirred steaming and decocting 3~5 hours, successively Add water-soluble rosin and step (1) gained extracting solution, 70~80 DEG C are stirred steaming and decocting 6~8 hours, obtain final product.
6. preparation technology according to claim 5 is it is characterised in that the water in step (1) and step (2) is deionized water Or distilled water.
7. preparation technology according to claim 5 is it is characterised in that the gelatinizing in step (2) adopts vapor or oil bath Heating.
CN201610735429.4A 2016-08-26 2016-08-26 Natural environment-friendly mildew-proof and damp-proof glutinous rice glue and preparation process thereof Pending CN106349971A (en)

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CN108047990A (en) * 2018-01-24 2018-05-18 合肥市大卓电力有限责任公司 A kind of novel antibacterial glutinous rice glue and preparation method thereof

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