CN106307605A - Cigarette essence capable of improving cigarette flavor and preparation method thereof - Google Patents
Cigarette essence capable of improving cigarette flavor and preparation method thereof Download PDFInfo
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- CN106307605A CN106307605A CN201610743907.6A CN201610743907A CN106307605A CN 106307605 A CN106307605 A CN 106307605A CN 201610743907 A CN201610743907 A CN 201610743907A CN 106307605 A CN106307605 A CN 106307605A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a cigarette essence capable of improving cigarette flavor and a preparation method thereof. The cigarette essence is prepared from the following raw materials in parts by weight: 16 to 20 parts of inula flower extract, 10 to 12 parts of bergamot essential oil, 8 to 10 parts of carrot seed essential oil, 5 to 7 parts of dendrobium officinale polysaccharide, 4 to 6 parts of maltol, 4 to 6 parts of isoamyl alcohol, 4 to 6 parts of geraniol, 3 to 5 parts of fennel oil, 3 to 5 parts of clove oil, 3 to 5 parts of cinnamaldehyde, and 2 to 4 parts of leaf alcohol. The cigarette essence has the advantages that the cigarette fragrance is effectively improved, the cigarette gas is softened, the irritation is decreased, and the mouth feel is improved; the inula flower has the effects of moistening lung and reliving cough, so that the effective ingredients of inula flower can be breathed into body in the smoking process, the functions of moistening lung, reducing phlegm and relieving cough are realized, the irritation of cigarette gas to respiratory mucosa is reduced, and the danger of cigarette is decreased.
Description
Technical field
The invention belongs to cigarette additive field, be specifically related to a kind of flavouring essence for tobacco improving cigarette smoke and preparation thereof
Method.
Background technology
Along with fast development, the formation of famous brand of tobacco industry, and Nicotiana tabacum L. category is the most perfect, to high-quality
The demand of tobacco aromatics using essence also grows with each passing day.Tobacco business use spices and essence can suppress the pungent zest of cigarette, cover
Miscellaneous QI, rectification are inhaled taste, are increased cigarette perfume.But traditional tobacco aromatics using essence uses chemical method to prepare, although price is low
Honest and clean, but chemicals sucked multipair smoker, and healthy meeting has a great impact, and also can not in purification process
That avoids also exists solvent and the problem of reactant residual.
There is abundant Chinese herbal medicine resource in China, from fragrant rich in extracting suitable cigarette the medicine-food two-purpose Chinese herbal medicine of fragrance
Material essence, can not only improve the pungent zest of cigarette, cover miscellaneous QI, and can give the local flavor that medicated cigarette is different, simultaneously because be
Extract from medicine food dual purpose plant and obtain, health of smokers is safe from harm, thus is welcome by market and consumer.
Flos Inulae has another name called Jin Fohua, Herba Inulae, belongs to Compositae, Inula herbaceos perennial, is distributed in Hunan, wide
The ground such as west, Guizhou and Yunnan.Flos Inulae is put down, and mildly bitter flavor has the therapeutic method to keep the adverse QI flowing downwards, Hang Shui, nourishing the lung to arrest cough, clearing away heat and expelling pathogen in the exterior, lowering the adverse-rising QI and dispelling phlegm
Etc. effect.At present, Flos Inulae is mainly used in Chinese crude drug field, cures mainly pertussis, bronchial asthma, the disease such as have a headache and fever, still
Not finding the report as tobacco aromatics using essence, the extraction to Flos Inulae active component mainly has soxhlet extraction, extraction, decocts
The methods such as cooking method, the Flos Inulae active component using existing method and technique to extract adds in Medicated cigarette, can bring muddy to flue gas
Turbid sense, and stimulation is big, oral cavity residual is serious, greatly reduces the quality of Medicated cigarette.
Summary of the invention
It is an object of the invention to provide a kind of flavouring essence for tobacco containing Flos Inulae extract, this essence adds in Medicated cigarette,
The fragrance of Medicated cigarette, soft flue gas can be increased, reduce stimulation, lifting mouthfeel, present invention also offers the preparation side of this flavouring essence for tobacco
Method.
The flavouring essence for tobacco that the present invention provides, is prepared from by the raw material of following weight portion: Flos Inulae extract 16～20 parts,
Bergamot 10～12 parts, carrot seed quintessence oil 8～10 parts, Dendrobium officinale polysaccharide 5～7 parts, maltol 4～6 parts, isoamyl alcohol 4
～6 parts, geraniol 4～6 parts, fennel oil 3～5 parts, Oleum Caryophylli 3～5 parts, cinnamic aldehyde 3～5 parts, folic alcohol 2～4 parts.
Applicant is devoted for years in the research and development of tobacco aromatics using essence, finds in great many of experiments, and Flos Inulae extract is used for
Flavouring essence for tobacco, can improve the flue gas of Medicated cigarette to a certain extent, reduces zest, further study show that, by Bergamot, recklessly
Radish seed quintessence oil, Dendrobium officinale polysaccharide, maltol, isoamyl alcohol, geraniol, fennel oil, Oleum Caryophylli, cinnamic aldehyde, folic alcohol and Flos Inulae
The flavouring essence for tobacco that extract is mixed with, is significantly improved effect to the flue gas tool of Medicated cigarette.
As preferably, described flavouring essence for tobacco, the raw material of following weight portion it is prepared from: Flos Inulae extract 18 parts,
Bergamot 11 parts, carrot seed quintessence oil 9 parts, Dendrobium officinale polysaccharide 6 parts, maltol 5 parts, isoamyl alcohol 5 parts, geraniol 5 parts,
Fennel oil 4 parts, Oleum Caryophylli 4 parts, cinnamic aldehyde 4 parts, folic alcohol 3 parts.
As preferably, the extracting method of described Flos Inulae extract is as follows:
(1) british inula root was pulverized 80 mesh sieves, obtained british inula root powder；
(2) british inula root powder is mixed by solid-liquid ratio 28～30g/L with ethanol, then in mixed liquor, add british inula root
The arabinose of powder quality 14%～20%, after mixed liquor mix homogeneously, uses ultrasonic extraction to obtain extracting solution；
(3) being filtered by extracting solution, filtrate is 1.25 through being concentrated in vacuo to relative density, obtains Flos Inulae extract.
The present invention uses ultrasonic extraction british inula root, can improve the extraction ratio of effective ingredient in british inula root, exists simultaneously
The arabinose of british inula root powder quality 14%～18% it is additionally added during extraction, anti-to carry out a certain degree of U.S. rad
Should.In this method, the addition controlling arabinose is abnormal crucial, if addition is less than 14%, then Flos Inulae extract does not has
Improving the effect of cigarette smoke, if addition is higher than 20%, then Flos Inulae extract not only can not improve cigarette smoke, makes on the contrary
Flue gas is more muddy, stimulates bigger.Wherein above-mentioned steps (3), concentrating the filtrate to relative density is 1.25, and measuring temperature is 30
℃。
As preferably, in above-mentioned steps (2), the temperature of ultrasonic extraction is 65～70 DEG C.Temperature not only affects Flos Inulae and carries
Taking the extraction ratio of thing, also can affect Maillard reaction, Extracting temperature is set to 65～70 DEG C, both can ensure higher extraction ratio,
Can also make to have through the Flos Inulae extract of Maillard reaction preferably to improve the effect of cigarette smoke.
As preferably, in above-mentioned steps (2), the time of ultrasonic extraction is 1.5～2h.
As preferably, in above-mentioned steps (2), the power of ultrasonic extraction is 500～700W.
As preferably, in above-mentioned steps (2), the volume fraction of ethanol is 65～70%.In ethanol, the content of moisture also can shadow
Ringing Maillard reaction, moisture is too high or too low all can be affected and extract the Flos Inulae extract that obtains and improve the effect of flue gas, this
The volume fraction of bright middle ethanol is most preferably 68%.
As preferably, in above-mentioned steps (2), arabinose addition is 17%.
Present invention also offers the preparation method of flavouring essence for tobacco as above, step is: first by maltol, isoamyl alcohol,
Geraniol, fennel oil, Oleum Caryophylli, cinnamic aldehyde and folic alcohol mixing, after stirring, then add Flos Inulae extract in mixed liquor
And Bergamot, carrot seed quintessence oil, Dendrobium officinale polysaccharide, mix homogeneously i.e. obtains flavouring essence for tobacco.
The invention has the beneficial effects as follows: the present invention provide flavouring essence for tobacco, can be effectively improved cigarette flavor, soft flue gas,
Reducing stimulation, promote mouthfeel, simultaneously because Flos Inulae has effect of nourishing the lung to arrest cough, in sucking process, Flos Inulae effectively becomes
Point can in suction body, play lung moistening, reduce phlegm, the effect of cough-relieving, thus alleviate the flue gas stimulation to respiratory mucosa, reduce Medicated cigarette
Harm.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme is described further.
If not raw material of the present invention and equipment refer in particular to, all it is commercially available or commonly used in the art, implements
Method in example, if no special instructions, is the conventional method of this area.
Embodiment 1
Flavouring essence for tobacco in the present embodiment is prepared from the following materials: Flos Inulae extract 18 parts, Bergamot 11
Part, carrot seed quintessence oil 9 parts, Dendrobium officinale polysaccharide 6 parts, maltol 5 parts, isoamyl alcohol 5 parts, geraniol 5 parts, fennel oil 4 parts,
Oleum Caryophylli 4 parts, cinnamic aldehyde 4 parts, folic alcohol 3 parts.
Wherein, the extracting method of Flos Inulae extract is:
(1) british inula root cleaned and dry is pulverized 80 mesh sieves, obtain british inula root powder；
(2) british inula root powder is mixed by solid-liquid ratio 29g/L with the ethanol that volume fraction is 68%, then in mixed liquor
Add the arabinose of british inula root powder quality 17%, after mixed liquor mix homogeneously, use ultrasonic extraction to obtain extracting solution,
Wherein, ultrasonic extraction condition is: temperature 68 DEG C, time 100min, power 600W；
(3) being filtered by extracting solution, it is 1.25 that filtrate is concentrated in vacuo to relative density at 30 DEG C of rotated evaporimeters, obtains rotation
Flos Inulae extract.
5g maltol, 5g isoamyl alcohol, 5g geraniol, 4g fennel oil, 4g Oleum Caryophylli, 4g cinnamic aldehyde and 3g folic alcohol are mixed,
And after stirring, then in mixed liquor, add Flos Inulae extract and the 11g Fructus Citri Sarcodactylis essence that the extraction of 18g said method obtains
Oil, 9g carrot seed quintessence oil, 6g Dendrobium officinale polysaccharide, mix homogeneously i.e. obtains flavouring essence for tobacco.
Embodiment 2
Flavouring essence for tobacco in the present embodiment is prepared from the following materials: Flos Inulae extract 16g, Bergamot 10g,
Carrot seed quintessence oil 8g, Dendrobium officinale polysaccharide 5g, maltol 4g, isoamyl alcohol 4g, geraniol 4g, fennel oil 3g, Oleum Caryophylli 3g,
Cinnamic aldehyde 3g, folic alcohol 2g.
Wherein, the extracting method of Flos Inulae extract is:
(1) british inula root cleaned and dry is pulverized 80 mesh sieves, obtain british inula root powder；
(2) british inula root powder is mixed by solid-liquid ratio 28g/L with the ethanol that volume fraction is 65%, then in mixed liquor
Add the arabinose of british inula root powder quality 14%, after mixed liquor mix homogeneously, use ultrasonic extraction to obtain extracting solution,
Wherein, ultrasonic extraction condition is: temperature 65 DEG C, time 90min, power 500W；
(3) being filtered by extracting solution, it is 1.25 that filtrate is concentrated in vacuo to relative density at 30 DEG C of rotated evaporimeters, obtains rotation
Flos Inulae extract.
4g maltol, 4g isoamyl alcohol, 4g geraniol, 3g fennel oil, 3g Oleum Caryophylli, 3g cinnamic aldehyde and 2g folic alcohol are mixed,
And after stirring, then in mixed liquor, add Flos Inulae extract and the 10g Fructus Citri Sarcodactylis essence that the extraction of 16g said method obtains
Oil, 8g carrot seed quintessence oil, 5g Dendrobium officinale polysaccharide, mix homogeneously i.e. obtains flavouring essence for tobacco.
Embodiment 3
Flavouring essence for tobacco in the present embodiment is prepared from the following materials: Flos Inulae extract 20g, Bergamot 12g,
Carrot seed quintessence oil 10g, Dendrobium officinale polysaccharide 7g, maltol 6g, isoamyl alcohol 6g, geraniol 6g, fennel oil 5g, Oleum Caryophylli 5g,
Cinnamic aldehyde 5g, folic alcohol 4g.
Wherein, the extracting method of Flos Inulae extract is:
(1) british inula root cleaned and dry is pulverized 80 mesh sieves, obtain british inula root powder；
(2) british inula root powder is mixed by solid-liquid ratio 30g/L with the ethanol that volume fraction is 70%, then in mixed liquor
Add the arabinose of british inula root powder quality 20%, after mixed liquor mix homogeneously, use ultrasonic extraction to obtain extracting solution,
Wherein, ultrasonic extraction condition is: temperature 70 C, time 120min, power 700W；
(3) being filtered by extracting solution, it is 1.25 that filtrate is concentrated in vacuo to relative density at 30 DEG C of rotated evaporimeters, obtains rotation
Flos Inulae extract.
6g maltol, 6g isoamyl alcohol, 6g geraniol, 5g fennel oil, 5g Oleum Caryophylli, 5g cinnamic aldehyde and 4g folic alcohol are mixed,
And after stirring, then in mixed liquor, add Flos Inulae extract and the 12g Fructus Citri Sarcodactylis essence that the extraction of 20g said method obtains
Oil, 10g carrot seed quintessence oil, 7g Dendrobium officinale polysaccharide, mix homogeneously i.e. obtains flavouring essence for tobacco.
Comparative example 1
In this comparative example, flavouring essence for tobacco is prepared from the following materials: Bergamot 11g, carrot seed quintessence oil 9g, ferrum
Skin dendrobium polysaccharide 6g, maltol 5g, isoamyl alcohol 5g, geraniol 5g, fennel oil 4g, Oleum Caryophylli 4g, cinnamic aldehyde 4g, folic alcohol 3g.This
Embodiment flavouring essence for tobacco is without Flos Inulae extract with the difference of embodiment 1.
Comparative example 2
In this comparative example, flavouring essence for tobacco only has Flos Inulae extract composition, the extracting method of Flos Inulae extract and enforcement
Example 1 is identical.
Comparative example 3～7
In comparative example 3, comparative example 4, comparative example 5, comparative example 6 and comparative example 7, the flavouring essence for tobacco of each comparative example by with
Lower raw material is prepared from: Flos Inulae extract 18g, Bergamot 11g, carrot seed quintessence oil 9g, Dendrobium officinale polysaccharide 6g, wheat
Bud phenol 5g, isoamyl alcohol 5g, geraniol 5g, fennel oil 4g, Oleum Caryophylli 4g, cinnamic aldehyde 4g, folic alcohol 3g.
Wherein, the flavouring essence for tobacco of each comparative example, its preparation method is all identical with embodiment 1, and difference is that Flos Inulae carries
Take the extraction conditions of thing, in comparative example 3, comparative example 4, comparative example 5, comparative example 6 and comparative example 7, during supersound extraction Flos Inulae,
The quality adding arabinose is respectively the 8% of british inula root powder quality, 12%, 24%, 30% and 40%, other condition phases
With.
Smoke panel test experiment
Being respectively used to prepare cigarette by the flavouring essence for tobacco of embodiment 1～3, comparative example 1～7 preparation, method is by tobacco shred matter
The 0.01% of amount is sprayed on tobacco shred equably with laryngeal spray, after placing 2 days in climatic chamber, with cigarette-roller by upper
Stating tobacco shred and be respectively prepared cigarette, be evaluated according to GB5606.4-2005 standard, evaluation criterion is shown in Table 1, embodiment 1～3 and right
The evaluation result of ratio 1～7 is shown in Table 2.
Be can be seen that by the smoking result of table 2, the total of embodiment 1～3 is divided more than 89, hence it is evident that higher than comparative example 1～7,
Illustrate that the flavouring essence for tobacco that the present invention provides is obvious to the improvement effect of cigarette smoke；The total of comparative example 1 divides only 74, illustrates
In the case of not adding Flos Inulae extract, other components are limited to the improvement effect of cigarette smoke, with embodiment 1～3 phase
Ratio, is mainly manifested in flue gas muddiness, stimulates greatly, especially stimulates throat big；The total of comparative example 2 divides also only 76, explanation
It is used alone Flos Inulae extract cigarette smoke to be had some improvement effect, but the use that effect can not meet Medicated cigarette is wanted
Asking, compared with comparative example 1, zest is less than normal, illustrates that Flos Inulae extract can effectively reduce the zest of flue gas；Comparative example
The total of 3～7 is divided and is followed successively by 80,82,80,78,77, illustrates when ultrasonic extraction Flos Inulae, the addition pair of arabinose
The essence influential effect of preparation is very big, and the addition of arabinose is on the low side, and the improvement of flue gas effect is substantially deteriorated, arabinose
Addition is on the high side, and the improvement of flue gas effect also can be deteriorated, and along with the further increase of addition, improves effect and also can enter one
Step is deteriorated.
Table 1 Sensory Quality of Cigarette evaluation criterion
The each embodiment of table 2 and the smoking result of comparative example flavouring essence for tobacco
Claims (9)
1. the flavouring essence for tobacco that can improve cigarette smoke, it is characterised in that be prepared from by the raw material of following weight portion: sheathed
Flower extract 16～20 parts, Bergamot 10～12 parts, carrot seed quintessence oil 8～10 parts, Dendrobium officinale polysaccharide 5～7 parts, wheat
Bud phenol 4～6 parts, isoamyl alcohol 4～6 parts, geraniol 4～6 parts, fennel oil 3～5 parts, Oleum Caryophylli 3～5 parts, cinnamic aldehyde 3～5 parts,
Folic alcohol 2～4 parts.
Flavouring essence for tobacco the most according to claim 1, it is characterised in that be prepared from by the raw material of following weight portion: sheathed
Flower extract 18 parts, Bergamot 11 parts, carrot seed quintessence oil 9 parts, Dendrobium officinale polysaccharide 6 parts, maltol 5 parts, isoamyl alcohol 5
Part, geraniol 5 parts, fennel oil 4 parts, Oleum Caryophylli 4 parts, cinnamic aldehyde 4 parts, folic alcohol 3 parts.
Flavouring essence for tobacco the most according to claim 1 and 2, it is characterised in that the extracting method of described Flos Inulae extract is such as
Under:
(1) british inula root was pulverized 80 mesh sieves, obtained british inula root powder；
(2) british inula root powder is mixed by solid-liquid ratio 28～30g/L with ethanol, then in mixed liquor, add british inula root powder
The arabinose of quality 14%～20%, after mixed liquor mix homogeneously, uses ultrasonic extraction to obtain extracting solution；
(3) being filtered by extracting solution, filtrate is 1.25 through being concentrated in vacuo to relative density, obtains Flos Inulae extract.
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2) temperature of ultrasonic extraction be 65～
70℃。
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2) time of ultrasonic extraction be 1.5～
2h。
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2) power of ultrasonic extraction be 500～
700W。
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2) volume fraction of ethanol be 65%～
70%.
Flavouring essence for tobacco the most according to claim 3, it is characterised in that in step (2), arabinose addition is 17%.
9. the preparation method of the flavouring essence for tobacco as described in any one of claim 1 to 8, it is characterised in that first by maltol,
Isoamyl alcohol, geraniol, fennel oil, Oleum Caryophylli, cinnamic aldehyde and folic alcohol mixing, after stirring, then add sheathed in mixed liquor
Flower extract and Bergamot, carrot seed quintessence oil, Dendrobium officinale polysaccharide, mix homogeneously i.e. obtains flavouring essence for tobacco.
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Cited By (3)
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| CN108158035A (en) * | 2018-01-11 | 2018-06-15 | 云南中烟工业有限责任公司 | A kind of wingceltis skin, sugarcane fiber composite paper filter material and its preparation method and application |
| CN112980579A (en) * | 2021-03-05 | 2021-06-18 | 吉林烟草工业有限责任公司 | Woody flower fragrance characteristic extract and preparation method and application thereof |
| CN113693262A (en) * | 2021-08-30 | 2021-11-26 | 深圳市真味生物科技有限公司 | Fruit-flavor electronic cigarette liquid solvent prepared from benzyl alcohol |
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| CN108158035A (en) * | 2018-01-11 | 2018-06-15 | 云南中烟工业有限责任公司 | A kind of wingceltis skin, sugarcane fiber composite paper filter material and its preparation method and application |
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| CN113693262A (en) * | 2021-08-30 | 2021-11-26 | 深圳市真味生物科技有限公司 | Fruit-flavor electronic cigarette liquid solvent prepared from benzyl alcohol |
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