CN106281026A - A kind of fire-retardant uvioresistant ointment waterproof coating material and preparation method thereof - Google Patents

A kind of fire-retardant uvioresistant ointment waterproof coating material and preparation method thereof Download PDF

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Publication number
CN106281026A
CN106281026A CN201610741916.1A CN201610741916A CN106281026A CN 106281026 A CN106281026 A CN 106281026A CN 201610741916 A CN201610741916 A CN 201610741916A CN 106281026 A CN106281026 A CN 106281026A
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Prior art keywords
fire
colophonium
retardant
parts
ointment
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CN201610741916.1A
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Inventor
张金根
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Anhui Wuxing Kaihong Waterproof Building Materials Technology Co Ltd
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Anhui Wuxing Kaihong Waterproof Building Materials Technology Co Ltd
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Priority to CN201610741916.1A priority Critical patent/CN106281026A/en
Publication of CN106281026A publication Critical patent/CN106281026A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/02—Flame or fire retardant/resistant
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a kind of fire-retardant uvioresistant ointment waterproof coating material and preparation method thereof, described preparation method includes following step: step 1: open blender, raising blender temperature is 130 150 DEG C, take 10# Colophonium, 70# Colophonium, mineral oil, styrene butadiene styrene block copolymer, butadiene-styrene rubber, PP GRANULES the most respectively, after stirring 30min, rising high-temperature is 190 DEG C of insulation 3h；Step 2: reduction temperature, to 160 170 DEG C, adds fire retardant, antimony oxide, 2 hydroxyl 4 methoxy benzophenones, superfine talcum powder, stirs 1h；Step 3: by the mixture of step 2 circular grinding 1 3h in colloid mill, discharging after being cooled to 150 DEG C.The coating of preparation has good fire prevention, uvioresistant and waterproof intensity.

Description

A kind of fire-retardant uvioresistant ointment waterproof coating material and preparation method thereof
Technical field
The invention belongs to paint field, relate to a kind of fire-retardant uvioresistant ointment waterproof coating material and preparation method thereof.
Background technology
Water-repellent paint, according to the liquid type of coating, can be divided into solvent-borne type, emulsion type, response type three kinds water-repellent paint. Initial waterproof material is tar asphalt and oil green grass or young crops asphalt paper, originates from Europe, the twenties in 20th century incoming China.Along with The progress of science and technology, modern waterproof material develops rapidly, it is seen that 20 century 70s, various high polymer waterproof materials are come out one after another. China's waterproof material gradually forms coiled material, coating, the big series of encapsulant three.
Synthesis high polymer waterproof material is with synthetic rubber or contract resin as main film forming substance, adds other auxiliary materials The waterproof coating material expected and be configured to.The brand of synthetic molecules waterproof material is varied, as polyurethane, acrylic acid and they Mixture etc..Although the application of coating is more and more extensive, in addition to excellent water resistance, the also uvioresistant to coating Higher requirement is it is also proposed with fire-retardant intensity.
Summary of the invention
Solve the technical problem that: conventional its waterproof strength of water-repellent paint is poor, be easily generated the phenomenon leaked, and easily Combustion, causes job site potential safety hazard；Loss of properties on aging, embrittlement under long-time action of ultraviolet radiation, cause waterproof failure, this Bright purpose is to provide a kind of water-repellent paint and preparation method thereof, improves the water resistance of coating, uvioresistant performance and anti-flammability Energy.
Technical scheme: in order to solve the problems referred to above, the invention discloses a kind of fire-retardant uvioresistant ointment waterproof coating material, institute The coating stated includes the composition of following weight parts:
10# Colophonium: 3-10 part, 70# Colophonium: 40-50 part, mineral oil: 12-20 part, s-B-S are embedding Section copolymer: 3-10 part, butadiene-styrene rubber: 1-4 part, PP GRANULES: 5-15 part, fire retardant: 3-8 part, antimony oxide: 3-8 Part, ESCALOL 567: 2-8 part, superfine talcum powder: 10-15 part.
Preferably, described coating includes the composition of following weight parts:
10# Colophonium: 3-10 part, 70# Colophonium: 40-50 part, mineral oil: 12-20 part, s-B-S are embedding Section copolymer: 3-10 part, butadiene-styrene rubber: 1-4 part, PP GRANULES: 5-15 part, fire retardant: 3-8 part, antimony oxide: 3-8 Part, ESCALOL 567: 2-8 part, superfine talcum powder: 10-15 part, lactoprene: 2-5 part, the poly-fourth of terminal hydroxy group Diene: 3-6 part.
Preferably, described fire retardant is ethyl phosphonic acid diethylester, APP, isopropylated triphenyl phosphates, season penta One or more in tetrol phosphate ester.
A kind of preparation method of fire-retardant uvioresistant ointment waterproof coating material, the step including following:
Step 1: open blender, raise blender temperature be 130-150 DEG C, take the most respectively 10# Colophonium 3-10 part, 70# Colophonium 40-50 part, mineral oil 12-20 part, styrene butadiene styrene block copolymer (SBS) 3-10 part, butadiene-styrene rubber 1-4 Part, PP GRANULES 5-15 part, after stirring 30min, rising high-temperature is 190 DEG C of insulation 3h；
Step 2: reduction temperature, to 160-170 DEG C, adds fire retardant 3-8 part, antimony oxide 3-8 part, 2-hydroxyl-4-first Epoxide benzophenone 2-8 part, superfine talcum powder 10-15 part, stir 1h；
Step 3: by the mixture of step 2 circular grinding 1-3h in colloid mill, discharging after being cooled to 150 DEG C.
Preferably, raising blender temperature in described step 1 is 140 DEG C.
Preferably, circular grinding 2h in described step 3.
Beneficial effect: the coating of the present invention has bigger different from the preparation technology of conventional coating and compositing formula, The water-repellent paint that the preparation method of the present invention prepares has possessed preferable water resistance, fire resistance and uvioresistant performance. Its water resistance is significantly better than the coating of routine, and also has higher adhesion strength.
Detailed description of the invention
Embodiment 1
Step 1: open blender, raising blender temperature is 150 DEG C, takes 10# Colophonium 3 parts, 70# Colophonium the most respectively 50 parts, 12 parts of mineral oil, styrene butadiene styrene block copolymer (SBS) 3 parts, 4 parts of butadiene-styrene rubber, PP GRANULES 5 parts, After stirring 30min, rising high-temperature is 190 DEG C of insulation 3h；
Step 2: reduction temperature, to 170 DEG C, adds fire retardant 8 parts, antimony oxide 3 parts, 2-hydroxyl-4-methoxyl group hexichol Ketone 8 parts, superfine talcum powder 10 parts, stir 1h；
Step 3: by the mixture of step 2 circular grinding 3h in colloid mill, discharging after being cooled to 150 DEG C.
Embodiment 2
Step 1: open blender, raising blender temperature is 130 DEG C, takes 10# Colophonium 10 parts, 70# drip the most respectively Green grass or young crops 40 parts, 20 parts of mineral oil, styrene butadiene styrene block copolymer (SBS) 10 parts, 1 part of butadiene-styrene rubber, PP GRANULES 15 Part, after stirring 30min, rising high-temperature is 190 DEG C of insulation 3h；
Step 2: reduction temperature, to 160 DEG C, adds fire retardant 3 parts, antimony oxide 8 parts, 2-hydroxyl-4-methoxyl group hexichol Ketone 2 parts, superfine talcum powder 15 parts, stir 1h；
Step 3: by the mixture of step 2 circular grinding 1h in colloid mill, discharging after being cooled to 150 DEG C.
Embodiment 3
Step 1: open blender, raising blender temperature is 140 DEG C, takes 10# Colophonium 6 parts, 70# Colophonium the most respectively 46 parts, 16 parts of mineral oil, styrene butadiene styrene block copolymer (SBS) 6 parts, 2 parts of butadiene-styrene rubber, PP GRANULES 10 parts, After stirring 30min, rising high-temperature is 190 DEG C of insulation 3h；
Step 2: reduction temperature, to 170 DEG C, adds fire retardant 5 parts, antimony oxide 5 parts, 2-hydroxyl-4-methoxyl group hexichol Ketone 5 parts, superfine talcum powder 13 parts, stir 1h；
Step 3: by the mixture of step 2 circular grinding 2h in colloid mill, discharging after being cooled to 150 DEG C.
Embodiment 4
Step 1: open blender, raising blender temperature is 140 DEG C, takes 10# Colophonium 6 parts, 70# Colophonium the most respectively 46 parts, 16 parts of mineral oil, styrene butadiene styrene block copolymer (SBS) 6 parts, 2 parts of butadiene-styrene rubber, PP GRANULES 10 parts, After stirring 30min, rising high-temperature is 190 DEG C of insulation 3h；
Step 2: reduction temperature, to 170 DEG C, adds fire retardant 5 parts, antimony oxide 5 parts, 2-hydroxyl-4-methoxyl group hexichol Ketone 5 parts, superfine talcum powder 13 parts, lactoprene 5 parts, end hydroxy butadiene 3 parts, stir 1h；
Step 3: by the mixture of step 2 circular grinding 2h in colloid mill, discharging after being cooled to 150 DEG C.
Embodiment 5
Step 1: open blender, raising blender temperature is 140 DEG C, takes 10# Colophonium 6 parts, 70# Colophonium the most respectively 46 parts, 16 parts of mineral oil, styrene butadiene styrene block copolymer (SBS) 6 parts, 2 parts of butadiene-styrene rubber, PP GRANULES 10 parts, After stirring 30min, rising high-temperature is 190 DEG C of insulation 3h；
Step 2: reduction temperature, to 170 DEG C, adds fire retardant 5 parts, antimony oxide 5 parts, 2-hydroxyl-4-methoxyl group hexichol Ketone 5 parts, superfine talcum powder 13 parts, lactoprene 2 parts, end hydroxy butadiene 6 parts, stir 1h；
Step 3: by the mixture of step 2 circular grinding 2h in colloid mill, discharging after being cooled to 150 DEG C.
Comparative example 1
Step 1: open blender, raising blender temperature is 150 DEG C, takes 10# Colophonium 3 parts, 70# Colophonium the most respectively 50 parts, 12 parts of mineral oil, PP GRANULES 5 parts, stirring 30min after, rise high-temperature be 190 DEG C insulation 3h；
Step 2: reduction temperature, to 170 DEG C, adds fire retardant 8 parts, antimony oxide 3 parts, 2-hydroxyl-4-methoxyl group hexichol Ketone 8 parts, superfine talcum powder 10 parts, stir 1h；
Step 3: by the mixture of step 2 circular grinding 3h in colloid mill, discharging after being cooled to 150 DEG C.
Comparative example 2
Step 1: open blender, raising blender temperature is 150 DEG C, takes 10# Colophonium 3 parts, 70# Colophonium the most respectively 50 parts, 12 parts of mineral oil, PP GRANULES 5 parts, stirring 30min after, rise high-temperature be 190 DEG C insulation 3h；
Step 2: reduction temperature, to 170 DEG C, adds superfine talcum powder 10 parts, stirs 1h；
Step 3: by the mixture of step 2 circular grinding 3h in colloid mill, discharging after being cooled to 150 DEG C.
Determine embodiment 1 to 5, the water resistance of coating of comparative example 1 and 2, adhesion strength, fire resistance, ageing-resistant The performance test results is as follows:
Water resistance Adhesion strength (MPa)
Embodiment 1 0.3MPa, 60min are without infiltration 3.1
Embodiment 2 0.3MPa, 60min are without infiltration 3.2
Embodiment 3 0.3MPa, 90min are without infiltration 3.6
Embodiment 4 0.3MPa, 120min are without infiltration 4.5
Embodiment 5 0.3MPa, 120min are without infiltration 4.8
Comparative example 1 0.3MPa, 30min are without infiltration 2.7
Comparative example 2 0.3MPa, 30min permeate 2.0

Claims (6)

1. a fire-retardant uvioresistant ointment waterproof coating material, it is characterised in that described coating includes the composition of following weight parts:
10# Colophonium: 3-10 part, 70# Colophonium: 40-50 part, mineral oil: 12-20 part, s-B-S block are altogether Polymers: 3-10 part, butadiene-styrene rubber: 1-4 part, PP GRANULES: 5-15 part, fire retardant: 3-8 part, antimony oxide: 3-8 part, 2- Hydroxyl-4-methoxy benzophenone: 2-8 part, superfine talcum powder: 10-15 part.
One the most according to claim 1 fire-retardant uvioresistant ointment waterproof coating material, it is characterised in that described coating bag Include the composition of following weight parts:
10# Colophonium: 3-10 part, 70# Colophonium: 40-50 part, mineral oil: 12-20 part, s-B-S block are altogether Polymers: 3-10 part, butadiene-styrene rubber: 1-4 part, PP GRANULES: 5-15 part, fire retardant: 3-8 part, antimony oxide: 3-8 part, 2- Hydroxyl-4-methoxy benzophenone: 2-8 part, superfine talcum powder: 10-15 part, lactoprene: 2-5 part, end hydroxy butadiene: 3-6 part.
3. according to the fire-retardant uvioresistant ointment waterproof coating material of the one described in claims 1 or 2, it is characterised in that described Fire retardant is the one in ethyl phosphonic acid diethylester, APP, isopropylated triphenyl phosphates, pentaerythritol phosphate or several Kind.
4. the preparation method of a fire-retardant uvioresistant ointment waterproof coating material, it is characterised in that under described preparation method includes The step stated:
Step 1: open blender, raises blender temperature and is 130-150 DEG C, take 10# Colophonium 3-10 part, 70# the most respectively Colophonium 40-50 part, mineral oil 12-20 part, styrene butadiene styrene block copolymer (SBS) 3-10 part, butadiene-styrene rubber 1-4 part, PP GRANULES 5-15 part, after stirring 30min, rising high-temperature is 190 DEG C of insulation 3h；
Step 2: reduction temperature, to 160-170 DEG C, adds fire retardant 3-8 part, antimony oxide 3-8 part, 2-hydroxyl-4-methoxyl group Benzophenone 2-8 part, superfine talcum powder 10-15 part, stir 1h；
Step 3: by the mixture of step 2 circular grinding 1-3h in colloid mill, discharging after being cooled to 150 DEG C.
The preparation method of a kind of fire-retardant uvioresistant ointment waterproof coating material the most according to claim 4, it is characterised in that institute Raising blender temperature in the step 1 stated is 140 DEG C.
The preparation method of a kind of fire-retardant uvioresistant ointment waterproof coating material the most according to claim 4, it is characterised in that institute Circular grinding 2h in the step 3 stated.
CN201610741916.1A 2016-08-26 2016-08-26 A kind of fire-retardant uvioresistant ointment waterproof coating material and preparation method thereof Pending CN106281026A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107629559A (en) * 2017-09-22 2018-01-26 深圳市晟腾企业管理有限公司 A kind of building coating with flameproof effect and preparation method thereof
CN109735232A (en) * 2018-11-22 2019-05-10 贾世艇 A kind of pitch environment-friendly building coating and preparation method thereof
CN114477854A (en) * 2022-01-21 2022-05-13 广东广基建设集团有限公司 Foamed asphalt mixture and preparation method thereof
CN115197644A (en) * 2022-08-16 2022-10-18 福建中意铁科新型材料有限公司 Cold-coating non-curing rubber asphalt waterproof coating, preparation and construction

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* Cited by examiner, † Cited by third party
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JP2003255076A (en) * 2002-02-28 2003-09-10 Hitachi Ltd Underwater paint film-repairing method and apparatus
CN104312239A (en) * 2014-11-07 2015-01-28 南京溧水振兴船舶附件有限公司 Anti-corrosion and flame-retardant coating for ships, and preparation method thereof
CN104592846A (en) * 2015-02-16 2015-05-06 北京卓越金控高科技有限公司 High-strength waterproof flame-retardant seal coating and preparation method thereof
CN104945989A (en) * 2015-07-10 2015-09-30 常州市宏硕电子有限公司 Flame retardant high-sotactic polybutylene coating and preparation technology thereof
CN105238271A (en) * 2015-09-24 2016-01-13 天长市金牛防水防腐材料有限公司 Smoke-suppression non-cured rubber bitumen waterproof coating material
CN105238270A (en) * 2015-09-24 2016-01-13 天长市金牛防水防腐材料有限公司 Flame-retardant and smoke-inhibition type non-cured rubber asphalt waterproof coating material

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003255076A (en) * 2002-02-28 2003-09-10 Hitachi Ltd Underwater paint film-repairing method and apparatus
CN104312239A (en) * 2014-11-07 2015-01-28 南京溧水振兴船舶附件有限公司 Anti-corrosion and flame-retardant coating for ships, and preparation method thereof
CN104592846A (en) * 2015-02-16 2015-05-06 北京卓越金控高科技有限公司 High-strength waterproof flame-retardant seal coating and preparation method thereof
CN104945989A (en) * 2015-07-10 2015-09-30 常州市宏硕电子有限公司 Flame retardant high-sotactic polybutylene coating and preparation technology thereof
CN105238271A (en) * 2015-09-24 2016-01-13 天长市金牛防水防腐材料有限公司 Smoke-suppression non-cured rubber bitumen waterproof coating material
CN105238270A (en) * 2015-09-24 2016-01-13 天长市金牛防水防腐材料有限公司 Flame-retardant and smoke-inhibition type non-cured rubber asphalt waterproof coating material

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107629559A (en) * 2017-09-22 2018-01-26 深圳市晟腾企业管理有限公司 A kind of building coating with flameproof effect and preparation method thereof
CN109735232A (en) * 2018-11-22 2019-05-10 贾世艇 A kind of pitch environment-friendly building coating and preparation method thereof
CN114477854A (en) * 2022-01-21 2022-05-13 广东广基建设集团有限公司 Foamed asphalt mixture and preparation method thereof
CN115197644A (en) * 2022-08-16 2022-10-18 福建中意铁科新型材料有限公司 Cold-coating non-curing rubber asphalt waterproof coating, preparation and construction

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Application publication date: 20170104