CN106280711A - The preparation method of photosensitive colour-changing anti-forgery ink - Google Patents
The preparation method of photosensitive colour-changing anti-forgery ink Download PDFInfo
- Publication number
- CN106280711A CN106280711A CN201610711566.4A CN201610711566A CN106280711A CN 106280711 A CN106280711 A CN 106280711A CN 201610711566 A CN201610711566 A CN 201610711566A CN 106280711 A CN106280711 A CN 106280711A
- Authority
- CN
- China
- Prior art keywords
- parts
- ink
- wax powder
- stirring
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/50—Sympathetic, colour changing or similar inks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/104—Polyesters
- C09D11/105—Alkyd resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses the preparation method of a kind of photosensitive colour-changing anti-forgery ink, including: weigh, weighing material according to formulation weight standby, ink comprises the composition of following mass fraction: acrylic emulsion 40 ~ 45 parts, alkyd resin 10 ~ 15 parts, photochromic crystallization pigment 5 ~ 8 parts, filler 3 ~ 5 parts, ethanol 10 ~ 15 parts, 10 ~ 15 parts of water, plasticizer 0.5 ~ 1 part, adhesion promoter 1 ~ 2 part, drier 0.5 ~ 1 part, levelling agent 1 ~ 2 part and 1 ~ 2 part of wax powder；Stirring, stirs acrylic emulsion, alkyd resin with ethanol, adds wax powder and whole fillers, the water of half quality, stirring；Grind, the material after stirring is passed through grinding machine for grinding, until particle diameter is not more than 10 μm;Quenched, material after grinding is added remaining wax powder, photochromic crystallization pigment, plasticizer, adhesion promoter, drier and levelling agent, stirring, obtains finished product ink.The preparation process of the present invention is easy, and condition controllability is preferable, and the ink prepared can be applicable to the article that various sensitive color change is false proof.
Description
Technical field
The present invention relates to ink preparing technical field, particularly relate to the preparation method of a kind of photosensitive colour-changing anti-forgery ink.
Background technology
Ink is the important materials for packaging material printing, and it is by printing by pattern, literal table the most on the substrate.
Ink includes main component and auxiliary element, and they mix uniformly and form a kind of viscosity colloidal fluid through repeat-rolling.
It is made up of pigment, link stuff, auxiliary agent and solvent.For various printings such as books and periodicals, packing and decorating, building decorations.Along with society needs
Ask increase, ink kind and yield also respective extension and growth.
The sensitization discoloration definition of existing ink is inadequate, because the condition impacts such as season, humidity, temperature are very big, and its
In a lot of compositions there is the material to human body or environmental pollution.
Summary of the invention
The technical problem that present invention mainly solves is to provide the preparation method of a kind of photosensitive colour-changing anti-forgery ink.
For solving above-mentioned technical problem, the technical scheme that the present invention uses is:
The preparation method of a kind of photosensitive colour-changing anti-forgery ink is provided, comprises the steps:
1) weighing, weigh material according to formulation weight standby, described photosensitive colour-changing anti-forgery ink is by the one-tenth of following mass fraction
Point it is prepared from: acrylic emulsion 40 ~ 45 parts, alkyd resin 10 ~ 15 parts, photochromic crystallization pigment 5 ~ 8 parts, filler 3 ~ 5
Part, ethanol 10 ~ 15 parts, 10 ~ 15 parts of water, plasticizer 0.5 ~ 1 part, adhesion promoter 1 ~ 2 part, drier 0.5 ~ 1 part, levelling agent
1 ~ 2 part and 1 ~ 2 part of wax powder；
2) stirring, stirs acrylic emulsion, alkyd resin with ethanol, stirs 30min under the rotating speed of 400r/min, then
Add wax powder and whole fillers, the water of half quality, continue stirring 1h；
3) grind, by step 2) stirring after material be passed through grinding machine for grinding, until particle diameter is not more than 10 μm;
4) quenched, material after the grinding in step 3) is added remaining wax powder, photochromic crystallization pigment, plasticizer, attachment
Power accelerator, drier and levelling agent, stir 30min under the rotating speed of 800r/min, obtain finished product ink.
In a preferred embodiment of the present invention, described wax powder is polyethylene wax powder.
In a preferred embodiment of the present invention, described filler is nano silicon.
In a preferred embodiment of the present invention, described photosensitive colour-changing anti-forgery ink is by the composition system of following mass fraction
Standby: acrylic emulsion 42 parts, alkyd resin 15 parts, photochromic crystallization pigment 6 parts, filler 3 parts, ethanol 15 parts, water
12 parts, plasticizer 0.5 part, adhesion promoter 1.5 parts, drier 0.8 part, levelling agent 1.5 parts and 1.5 parts of wax powder.
The invention has the beneficial effects as follows: the preparation method of photosensitive colour-changing anti-forgery ink of the present invention, use acrylic emulsion, alcohol
Acid resin, as link stuff, uses light-induced variable crystallization pigment, and second alcohol and water is as solvent, adds wax powder, filler and auxiliary agent,
To the light-induced variable anti-forgery ink reversible, variable color is sensitive.The preparation process of the present invention is easy, and condition controllability is preferable, is prepared into
To ink can be applicable to the article that various sensitive color change is false proof.
Detailed description of the invention
Below presently preferred embodiments of the present invention is described in detail so that advantages and features of the invention can be easier to by
It will be appreciated by those skilled in the art that thus protection scope of the present invention is made apparent clear and definite defining.
The preparation method of a kind of photosensitive colour-changing anti-forgery ink, comprises the steps:
1) weighing, weigh material according to formulation weight standby, described photosensitive colour-changing anti-forgery ink is by the one-tenth of following mass fraction
Point it is prepared from: acrylic emulsion 42 parts, alkyd resin 15 parts, photochromic crystallization pigment 6 parts, filler 3 parts, ethanol 15
Part, 12 parts of water, plasticizer 0.5 part, adhesion promoter 1.5 parts, drier 0.8 part, levelling agent 1.5 parts and 1.5 parts of wax powder；
2) stirring, stirs acrylic emulsion, alkyd resin with ethanol, stirs 30min under the rotating speed of 400r/min, then
Add wax powder and whole fillers, the water of half quality, continue stirring 1h；
3) grind, by step 2) stirring after material be passed through grinding machine for grinding, until particle diameter is not more than 10 μm;
4) quenched, material after the grinding in step 3) is added remaining wax powder, photochromic crystallization pigment, plasticizer, attachment
Power accelerator, drier and levelling agent, stir 30min under the rotating speed of 800r/min, obtain finished product ink.
Described wax powder is polyethylene wax powder, and described filler is nano silicon.
The foregoing is only embodiments of the invention, not thereby limit the scope of the claims of the present invention, every utilize this
Equivalent structure or equivalence flow process that bright description is made convert, or are directly or indirectly used in other relevant technology necks
Territory, is the most in like manner included in the scope of patent protection of the present invention.
Claims (4)
1. the preparation method of a photosensitive colour-changing anti-forgery ink, it is characterised in that comprise the steps:
1) weighing, weigh material according to formulation weight standby, described photosensitive colour-changing anti-forgery ink is by the one-tenth of following mass fraction
Point it is prepared from: acrylic emulsion 40 ~ 45 parts, alkyd resin 10 ~ 15 parts, photochromic crystallization pigment 5 ~ 8 parts, filler 3 ~ 5
Part, ethanol 10 ~ 15 parts, 10 ~ 15 parts of water, plasticizer 0.5 ~ 1 part, adhesion promoter 1 ~ 2 part, drier 0.5 ~ 1 part, levelling agent
1 ~ 2 part and 1 ~ 2 part of wax powder；
2) stirring, stirs acrylic emulsion, alkyd resin with ethanol, stirs 30min under the rotating speed of 400r/min, then
Add wax powder and whole fillers, the water of half quality, continue stirring 1h；
3) grind, by step 2) stirring after material be passed through grinding machine for grinding, until particle diameter is not more than 10 μm;
4) quenched, material after the grinding in step 3) is added remaining wax powder, photochromic crystallization pigment, plasticizer, attachment
Power accelerator, drier and levelling agent, stir 30min under the rotating speed of 800r/min, obtain finished product ink.
The preparation method of photosensitive colour-changing anti-forgery ink the most according to claim 1, it is characterised in that described wax powder is poly-second
Alkene wax powder.
The preparation method of photosensitive colour-changing anti-forgery ink the most according to claim 1, it is characterised in that described filler is nanometer
Silicon dioxide.
The preparation method of photosensitive colour-changing anti-forgery ink the most according to claim 1, it is characterised in that described photosensitive colour-changing is prevented
Pseudo-ink is to be prepared from by the composition of following mass fraction: acrylic emulsion 42 parts, alkyd resin 15 parts, photochromic knot
Brilliant pigment 6 parts, filler 3 parts, ethanol 15 parts, 12 parts of water, plasticizer 0.5 part, adhesion promoter 1.5 parts, drier 0.8 part,
Levelling agent 1.5 parts and 1.5 parts of wax powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610711566.4A CN106280711A (en) | 2016-08-24 | 2016-08-24 | The preparation method of photosensitive colour-changing anti-forgery ink |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610711566.4A CN106280711A (en) | 2016-08-24 | 2016-08-24 | The preparation method of photosensitive colour-changing anti-forgery ink |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106280711A true CN106280711A (en) | 2017-01-04 |
Family
ID=57614838
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610711566.4A Pending CN106280711A (en) | 2016-08-24 | 2016-08-24 | The preparation method of photosensitive colour-changing anti-forgery ink |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106280711A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107828283A (en) * | 2017-12-21 | 2018-03-23 | 宝艺新材料股份有限公司 | Cardboard printing aqueous anti-counterfeiting ink and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1375528A (en) * | 2001-03-19 | 2002-10-23 | 樊官保 | Photochromic ink compound and its application |
| CN102964917A (en) * | 2012-11-23 | 2013-03-13 | 东莞市佳烨化工科技有限公司 | Water-based offset print anti-forgery ink and method for preparing same |
| CN104194491A (en) * | 2014-09-26 | 2014-12-10 | 苏州中亚油墨有限公司 | Method for preparing novel aqueous ink |
| CN104419250A (en) * | 2013-09-10 | 2015-03-18 | 南雄市连邦化工石油科技有限公司 | Preparation method of water-based black scratch ink |
| CN105567016A (en) * | 2016-03-08 | 2016-05-11 | 中钞油墨有限公司 | Preparation and production method of optical variable anti-counterfeiting printing ink for sculpture gravure |
-
2016
- 2016-08-24 CN CN201610711566.4A patent/CN106280711A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1375528A (en) * | 2001-03-19 | 2002-10-23 | 樊官保 | Photochromic ink compound and its application |
| CN102964917A (en) * | 2012-11-23 | 2013-03-13 | 东莞市佳烨化工科技有限公司 | Water-based offset print anti-forgery ink and method for preparing same |
| CN104419250A (en) * | 2013-09-10 | 2015-03-18 | 南雄市连邦化工石油科技有限公司 | Preparation method of water-based black scratch ink |
| CN104194491A (en) * | 2014-09-26 | 2014-12-10 | 苏州中亚油墨有限公司 | Method for preparing novel aqueous ink |
| CN105567016A (en) * | 2016-03-08 | 2016-05-11 | 中钞油墨有限公司 | Preparation and production method of optical variable anti-counterfeiting printing ink for sculpture gravure |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107828283A (en) * | 2017-12-21 | 2018-03-23 | 宝艺新材料股份有限公司 | Cardboard printing aqueous anti-counterfeiting ink and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103992690B (en) | Compound oil ink is printed in novel environment friendly high speed | |
| CN101879819B (en) | Production method of hot stamping foil | |
| CN104177917A (en) | Alcohol-soluble environment-friendly high-speed surface printing ink and preparation method thereof | |
| CN102675981A (en) | White ink suitable for solvent-free glue compositing and preparation method thereof | |
| CN110845924A (en) | Preparation method of inorganic modified water-based multicolor paint | |
| CN104277585A (en) | Environment-friendly colorful printing ink for handkerchief paper packages and preparation method thereof | |
| CN103183831B (en) | Universal binder resin for water-based plastic surface printing ink, preparation method thereof and printing ink using binder resin | |
| CN113897095A (en) | Thermochromic ink and preparation method thereof | |
| CN102321405A (en) | Environmentally-friendly surface printing plastic white ink and preparation method thereof | |
| CN104277584A (en) | Preparation method of environmental-friendly water-based paper ink | |
| CN106318023A (en) | Environment-friendly and quick-drying water-based ink | |
| CN105440778A (en) | Novel environment-friendly printing ink | |
| CN106280711A (en) | The preparation method of photosensitive colour-changing anti-forgery ink | |
| CN106147401A (en) | A kind of preparation method of heat-sensitive colour-changing ink | |
| CN104177914B (en) | Benzene-free ketone-free single solvent ink and preparation method thereof | |
| CN105949978A (en) | Antiaging high-covering-power matte gloss oil | |
| CN105907171B (en) | A kind of UV resistant heat resistance accessory and the base gravure ink composition for layer of PVC comprising it | |
| CN104817876A (en) | Color-variable printing ink and preparation method thereof | |
| CN102875822A (en) | Preparation method of photochromic latex emulsion | |
| CN105440777A (en) | Preparation method of novel environment-friendly printing ink | |
| CN106147399A (en) | Photosensitive colour-changing anti-forgery ink | |
| CN109517458A (en) | A kind of preparation method of the light laminated type multicolor finish of material-saving | |
| CN106221360A (en) | High speed printing adaptive rub resistance environment-friendly ink | |
| CN106147402A (en) | A kind of heat-sensitive colour-changing ink | |
| CN102732097B (en) | Method for preparing aluminum foil ink |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170104 |
|
| RJ01 | Rejection of invention patent application after publication |