CN106226189B - Rotary disc type multi-degree-of-freedom barium sulfate sulfur measuring device - Google Patents
Rotary disc type multi-degree-of-freedom barium sulfate sulfur measuring device Download PDFInfo
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- CN106226189B CN106226189B CN201610673229.0A CN201610673229A CN106226189B CN 106226189 B CN106226189 B CN 106226189B CN 201610673229 A CN201610673229 A CN 201610673229A CN 106226189 B CN106226189 B CN 106226189B
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- barium sulfate
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N5/00—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
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Abstract
The invention discloses a turntable type multi-degree-of-freedom barium sulfate sulfur measuring device, which is characterized in that test running in an idle state is carried out before work, whether a movement mechanism works normally is checked, then a worker manufactures a moxa sample, the sample is placed in a combustion furnace to combust impurities, then the sample is prepared into solution to be stirred, chloride ions are removed through a first stirring device and a second stirring device, weighing of barium sulfate is started after ashing of filter paper, a weighing bottle is conveyed forwards under the action of a spiral feeder, then a bottle pushing cylinder drives a material pushing claw to move the weighing bottle forwards, then a weighing bottle driving mechanism places the weighing bottle on an electronic analysis balance to be weighed and then places the weighing bottle on a conveyor belt to be conveyed away, so that the device finishes one work cycle, and starts test work of barium sulfate in the next group of weighing bottles, and the device can automatically finish the measurement work of barium sulfate, the device is favorable for improving the measurement quality and reducing the physical effort of operators.
Description
Technical Field
The invention mainly relates to the field of automatic measuring equipment for the sulfur content of barium sulfate, in particular to an Eschka sulfur measuring device capable of automatically weighing barium sulfate.
Background
Sulfur is very harmful to coal coking, gasification, and combustion and needs to be measured accurately. In order to accurately and rapidly measure the sulfur content of sulfur element in coal, a sulfur determinator or a sulfur detector is generally used as a commonly used measuring device. In the prior art, a coulometry sulfur method is adopted. The coulometric sulfur method needs a pump as a power source and adopts a continuous air extraction and continuous measurement mode for measurement. Since the sulfur concentration in the gas varies with time, the sulfur content is difficult to measure accurately, and the pump life is shortened due to load imbalance. The classic Eschka sulfur measurement method is a standard method for measuring the total sulfur content in coal commonly used in various countries at present, and has the advantages of high accuracy, batch measurement and the like. The last step of measuring sulfur by the Israel method is as follows: the crucible containing the ashed filter paper and barium sulfate was taken out of the muffle furnace, slightly cooled in air, and then placed in a desiccator to be cooled to room temperature (about 25 to 30min), and the mass of barium sulfate was measured. One step in the prior art is mostly in a manual mode, and completely automatic Eschka sulfur measuring equipment is rarely used abroad.
The skilled person is constantly improving the production technology and production equipment of barium sulfate. Related technical documents in existing sulfur measuring apparatuses include patent documents [ application No.: 201510531466.9 discloses a sulfur detector with automatic weighing function, which is mainly fixed on a bottom plate and comprises an Aishi sample making device, a combustion furnace, a solution stirring device, a first filtering device, a second filtering device, a chloride ion removing device, a filter paper ashing device and a barium sulfate weighing device; the barium sulfate weighing device comprises a weighing disc arranged at the top of the rotating shaft, a weighing rod arranged on the digital balance, a bearing frame, a rotating motor, a main support, an upper support, a lower support, a lifting motor frame, a ball screw, a guide rail, a sliding block, a rolling nut and a lifting motor. The device structure is fairly simple, can alleviate barium sulfate to a certain extent and contain the big and inefficiency problem of the sulphur content test degree of difficulty, but its sulphur content that can only measure a barium sulfate container at every turn, consequently measurement of efficiency is not high, and the action process also lacks the flow nature, has consequently restricted its application range.
In conclusion, the traditional barium sulfate measuring method has the defects of low measuring efficiency, lack of flow property in the action process, insufficient consideration of details, overlarge labor intensity of workers and the like.
Disclosure of Invention
The invention provides a rotating disc type multi-degree-of-freedom barium sulfate sulfur measuring device which can accurately control the retention time of a calcined substance, ensures that the calcined substance is uniformly heated, has stable long-term operation, low cloth bag resistance and long service life, and is convenient and safe to operate and good in process capability.
The utility model provides a carousel formula multi freedom barium sulfate sulphur measurement device, ejection of compact supporting seat and pan feeding supporting seat are fixed in subaerially, the preceding curb plate has been installed to the mesa one end of pan feeding supporting seat, and the slide rail is then installed to the other end be the bottom plate between slide rail and the preceding curb plate, the top of bottom plate be the spiral feeder between slide rail and the preceding curb plate promptly, and spiral feeder drive weighing bottle moves forward, gets into weighing bottle actuating mechanism until the weighing bottle, and weighing bottle actuating mechanism spanes ejection of compact supporting seat and pan feeding supporting seat, the upside installation guide rail frame of ejection of compact supporting seat is one, then installed the conveyer belt between the guide rail frame one. A servo motor is arranged below the discharging supporting seat and connected with a speed reducer, the speed reducer drives a cam to rotate, the cam is in contact with a push rod, and the push rod drives a turntable to move up and down.
The weighing bottle driving mechanism comprises a turntable, an L-shaped rod, a pushing claw, a pushing cylinder, a baffle, a sliding rail and a handle, wherein the side plate is installed on one side of the sliding rail, the pushing cylinder is installed on the upper side of the side plate and drives the pushing claw to move, the baffle is located in front of the pushing claw, and what needs to be described is that the baffle can move up and down as required. The rotary table is arranged on the table top of the discharging support seat, four L-shaped rods are arranged in the circumferential direction of the rotary table, and the lower ends of the L-shaped rods are connected with handles of a proper amount.
The turntable can move up and down while rotating, and moves up and down once every 1/4 weeks of rotation.
The pitch of the screw feeder is equal to the diameter of the weighing bottle, and the height of the spiral line at the leading end is gradually changed from small to large. The front end of the material pushing claw is fork-shaped, and the width of each fork is equal to the diameter of the weighing bottle.
The invention has the following remarkable effects:
1. the invention has simple structure and working principle, easy realization and low personnel participation level, is used for barium sulfate production enterprises to determine the quality of the finished barium sulfate product and is convenient for realizing the automatic production of factories; can realize real-time pause and start, quantity control is accurate, and position location degree is high, measures a plurality of weighing bottles simultaneously, consequently has very outstanding reliability and high efficiency.
2. The spiral feeder can realize easy regulation to the rotational speed thereof through being connected with programmable driver, can realize the transport and the weighing of weighing bottle through the chronogenesis cooperation of cam, gear, spiral feeder motion, measure the barium sulfate content of a plurality of weighing bottle insides simultaneously in addition, the work efficiency of system is easily adjusted.
Drawings
FIG. 1 is a schematic assembly of the present invention. Wherein: 1-discharging supporting seat; 2-a guide rail bracket I; 3-a conveyor belt; 4-a screw feeder; 5-front side plate; 6-feeding a supporting seat; 7-a bottom plate; 8-erecting a rod; 9-gear; 10-a push rod; 11-a cam; 12-a reducer; 13-a servo motor; 14-L-shaped rods; 15-a turntable; 16-a pushing claw; 17-a material pushing cylinder; 18-weighing bottle; 19-a baffle plate; 20-a slide rail; 21-electronic analytical balance; 22-handle, 23-side plate; 24-Aishi sample preparation device, 25-combustion furnace, 26-solution stirring device, 27-first filtering device, 28-second filtering device, 29-chloride ion removing device and 30-filter paper ashing device.
FIG. 2 is a schematic diagram of the direction of the station of the present invention, wherein B is the sign of the direction of movement of the weighing bottle, C is the sign of the direction of movement of the bottle pushing, and D is the sign of the direction of movement of the turntable.
FIG. 3 is a schematic view of the weigh bottle drive mechanism of the present invention at section A.
FIG. 4 is a schematic plan view of an Eschka sulfur measuring apparatus with automatic weighing of barium sulfate according to the present invention.
Detailed Description
The following description is made with reference to fig. 1 to 4, where the requirement of the device on the motion sequence is relatively high, the motion condition of each component should be checked before the device works, and especially, it is important to check that the baffle 19 can move down in time when the screw feeder 4 conveys four weighing bottles 18 to the position right in front of the baffle 19, the pushing cylinder 17 drives the pushing claw 16 to place the weighing bottles 18 right below the handle 22, the turntable 15 moves down, the handle 22 holds the weighing bottles 18, the turntable 15 moves up and continues to rotate, and then the weighing bottles 18 are placed on the electronic analytical balance 21, so as to complete the transfer process of the weighing bottles 18.
When the device works, an Aishi sample is prepared and then placed on a combustion furnace 25 for calcination, so that non-barium sulfate substances are oxidized and denatured into water-soluble substances, then the water-soluble substances are prepared into a solution and stirred by a solution stirring device 26, chlorine ions are removed by a chlorine ion removal device 29 after the barium sulfate is filtered by a first filtering device 27 and a second filtering device 28, all barium sulfate to be weighed after filter paper in a container is ashed are placed in a weighing bottle 18, then the weighing bottle 18 to be weighed is placed on the upper side of a feeding support seat 6 and continuously moves forwards under the action of a spiral feeder 4, after a specified number of weighing bottles 18 move to a position between a pushing claw 16 and a baffle 19, the baffle 19 moves downwards in time, meanwhile, the pushing cylinder 17 acts to drive the pushing claw 16 to move forwards, the front end of the pushing claw 16 clamps the weighing bottle 18 and then places the weighing bottle 18 under a handle 22, then the handle 22 grips the weighing bottle 18 tightly, and with the lifting and indexing of the turntable 15, the weighing bottle 18 is placed on the electronic analytical balance 21, the electronic analytical balance 21 records the mass of the barium sulfate (the weighing bottle 18 is peeled), the hand 22 moves downwards to hold the weighing bottle 18, then the weighing bottle 18 is placed on the conveyor belt 3, meanwhile, the hand 22 on the other side places the weighing bottle 18 to be weighed on the electronic analytical balance 21, so that the device completes one working cycle, and then the next group of weighing bottles 18 goes through the same action process.
Claims (3)
1. The utility model provides a carousel formula multi freedom barium sulfate sulphur device, ejection of compact supporting seat (1) and pan feeding supporting seat (6) are fixed in subaerially, preceding curb plate (5) have been installed to the mesa one end of pan feeding supporting seat (6), and slide rail (20) are then installed to the other end be the bottom plate between slide rail (20) and preceding curb plate (5), its characterized in that: a spiral feeder (4) is arranged above the bottom plate (7), namely between the sliding rail (20) and the front side plate (5), the spiral feeder (4) drives the weighing bottle (18) to move forwards until the weighing bottle (18) enters a weighing bottle driving mechanism, the weighing bottle driving mechanism stretches across the discharging supporting seat (1) and the feeding supporting seat (6), a first guide rail frame (2) is arranged on the upper side of the discharging supporting seat (1), a conveying belt (3) is arranged between the first guide rail frames (2), a servo motor (13) is arranged below the discharging supporting seat (1), the servo motor (13) is connected with a speed reducer (12), the speed reducer (12) drives the cam (11) to rotate, the cam (11) is in contact with the push rod (10), and the push rod (10) drives the rotary table (15) to move up and down;
the weighing bottle driving mechanism comprises a turntable (15), an L-shaped rod (14), a material pushing claw (16), a material pushing cylinder (17), a baffle plate (19) and a handle (22), a side plate (23) is mounted on one side of a sliding rail (20), the material pushing cylinder (17) is mounted on the upper side of the side plate (23), the material pushing cylinder (17) drives the material pushing claw (16) to move, the baffle plate (19) is located in front of the material pushing claw (16), and it needs to be noted that the baffle plate (19) can move up and down as required; the rotary table (15) is arranged on the table top of the discharging support base (1), four L-shaped rods (14) are arranged on the periphery of the rotary table (15), and the lower ends of the L-shaped rods (14) are connected with a corresponding number of handles (22);
the turntable (15) can move up and down while rotating, and moves up and down once every 1/4 weeks of rotation.
2. The rotating disc type multi-degree-of-freedom barium sulfate sulfur measuring device as claimed in claim 1, wherein: the front end of the material pushing claw (16) is fork-shaped, and the width of each fork is equal to the diameter of the weighing bottle (18).
3. The rotating disc type multi-degree-of-freedom barium sulfate sulfur measuring device as claimed in claim 1, wherein: the pitch of the screw feeder (4) is equal to the diameter of the weighing bottle (18), and the height of the screw line at the leading-in end is gradually changed from small to large.
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CN201610673229.0A CN106226189B (en) | 2016-08-16 | 2016-08-16 | Rotary disc type multi-degree-of-freedom barium sulfate sulfur measuring device |
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CN201610673229.0A CN106226189B (en) | 2016-08-16 | 2016-08-16 | Rotary disc type multi-degree-of-freedom barium sulfate sulfur measuring device |
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CN106226189B true CN106226189B (en) | 2022-04-01 |
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CN115266890B (en) * | 2022-07-09 | 2023-08-04 | 江苏地质矿产设计研究院(中国煤炭地质总局检测中心) | Full-automatic coulomb integrator capable of automatically changing sample based on sulfur measurement |
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JP2001073200A (en) * | 1999-08-30 | 2001-03-21 | Ebara Corp | Plating liquid management method and management apparatus therefor |
CN2520510Y (en) * | 2002-01-31 | 2002-11-13 | 国电环境保护研究所 | Instrument for quick analysis of total sulfur of coal |
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CN105092355A (en) * | 2015-08-25 | 2015-11-25 | 常州大学 | Aicardi sulfur detector with burning substance stirring and mashing function |
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JPH06160263A (en) * | 1992-11-24 | 1994-06-07 | Shimadzu Corp | Automatic measuring equipment of variation of mass |
CN103969147B (en) * | 2014-04-17 | 2016-05-25 | 广州特种承压设备检测研究院 | A kind of full-automatic petroleum ash content determinator |
CN204286565U (en) * | 2014-12-19 | 2015-04-22 | 湖南三德科技股份有限公司 | For the efficient poidometer of coal sample test |
CN105053291B (en) * | 2015-08-18 | 2018-05-04 | 云南韵和机械科技有限公司 | A kind of tealeaves automates press device |
CN105352841A (en) * | 2015-10-24 | 2016-02-24 | 常州大学 | Balance elevating linear parallel weighing apparatus used for Eschka sulphur meter |
CN205981976U (en) * | 2016-08-16 | 2017-02-22 | 广西联壮科技股份有限公司 | Sulphur device is surveyed to carousel formula multi freedom barium sulfate |
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2001073200A (en) * | 1999-08-30 | 2001-03-21 | Ebara Corp | Plating liquid management method and management apparatus therefor |
CN2520510Y (en) * | 2002-01-31 | 2002-11-13 | 国电环境保护研究所 | Instrument for quick analysis of total sulfur of coal |
KR20120044197A (en) * | 2010-10-27 | 2012-05-07 | (주)바이오니아 | Automatic realtime pcr system for the various analysis of biological sample, method for automatic nucleic acid purification and realtime quantification of gene amplification, method for automatic viable cell count of pathogenic bacteria using realtime quantitative pcr, method for automatically getting antigene density using quantitative immunity pcr |
CN105092355A (en) * | 2015-08-25 | 2015-11-25 | 常州大学 | Aicardi sulfur detector with burning substance stirring and mashing function |
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