CN106214622A - Moisturizing maintenance cosmetic water and preparation method thereof - Google Patents
Moisturizing maintenance cosmetic water and preparation method thereof Download PDFInfo
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- CN106214622A CN106214622A CN201610786158.5A CN201610786158A CN106214622A CN 106214622 A CN106214622 A CN 106214622A CN 201610786158 A CN201610786158 A CN 201610786158A CN 106214622 A CN106214622 A CN 106214622A
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
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Abstract
The present invention relates to a kind of moisturizing maintenance cosmetic water and preparation method thereof, to the north of moisturizing maintenance cosmetic water, U.S. hamamelis extract, Rhizoma Polygonati Odorati extract and Rhizoma Polygonati extract are primary raw material, and yeast extract, wetting agent, preservative, solubilizing agent and the quintessence oil etc. that add protein content higher make finished product；In preparation process, use the technique such as leach at low temperature and lyophilization to make Rhizoma Polygonati Odorati extract and Rhizoma Polygonati extract, then be mixed and made into cosmetic water semi-finished product by multistep, finally use the modern chemical industry technologies such as emulsifying, homogenizing and microfiltration to make finished product.The invention have the benefit that the moisturizing maintenance cosmetic water of the present invention has crease-resistant, defying age, moisturizing, profit flesh and effect of maintenance skin, it, to skin safe, non-stimulated, is more easy to infiltrate into skin internal layer；Make skin become soft and smooth, compact, recover elastic；Preparation method is safe and environment-friendly, and cost of manufacture is low.
Description
Technical field
The invention belongs to cosmetics manufacture field, be specifically related to a kind of moisturizing maintenance cosmetic water and preparation method thereof.
Background technology
Cosmetic water is also referred to as firming lotion, astringent etc., and its effect is that the pH-value again cleaning to recover skin surface,
And nurse one's health horny layer, make skin preferably absorb, and prepare for application maintenance product.Therefore, accepted by increasing people
And use.Cosmetic water on market often adds substantial amounts of denatured alcohol, very big to the zest of skin, results even in skin
The phenomenons such as skin comes off occur.
Hamamelis virginiana is a kind of big shrub of falling leaves, and stem is grown by plant base portion, the close life of branch, and plant height can be given birth to
Long to six meters high, only a few individuality can be grown sometimes to about ten meters.Bark is light brown, and surface smooths, and bark squamous is split, and peels off
Time be flakey, endothelium reddish violet.The extract of branch, leaf and bark can be used for medicinal purpose, and is mainly used to treat acne, injury with blood-stasis
And swelling, but the application that its extract is in cosmetics is actually rare.
Summary of the invention
In order to solve the problems referred to above that prior art exists, the invention provides a kind of moisturizing maintenance cosmetic water and preparation thereof
Method, the moisturizing maintenance cosmetic water of preparation has crease-resistant, defying age, moisturizing, profit flesh and effect of maintenance skin.
The technical solution adopted in the present invention is: a kind of moisturizing maintenance cosmetic water, including the raw material of following weight portion: fourth two
Alcohol 0.1-0.5 part；Methyl hydroxybenzoate 0.2-0.6 part；Carbomer 2-6 part；Glycerol 0.1-0.5 part；Ethoxy urea 0.1-0.3 part；Second
Edetate disodium 0.3-1.5 part；Hamamelis virginiana extract 3-5 part；Water soluble vitamins 0.4-0.8 part；Triethanolamine
0.2-0.5 part；Yeast extract 1-5 part；Cremophor RH40 0.1-0.5 part；Rhizoma Polygonati Odorati extract 0.8-1.2 part；Rhizoma Polygonati
Extract 0.8-1.2 part；Quintessence oil 0.1-0.2 part and imidazolidinyl urea 0.1-0.2 part.
Further, including the raw material of following weight portion: butanediol 0.1 part；Methyl hydroxybenzoate 0.2 part；Carbomer 2 parts；Sweet
Oil 0.1 part；Ethoxy urea 0.1 part；Edetate disodium 0.3 part；Hamamelis virginiana extract 3 parts；Water soluble vitamins 0.6
Part；Triethanolamine 0.2 part；Yeast extract 1 part；Cremophor RH40 0.1 part；Rhizoma Polygonati Odorati extract 1.0 parts；Rhizoma Polygonati extracts
Thing 1.0 parts；Quintessence oil 0.1 part and imidazolidinyl urea 0.1 part.
Further, any two kinds or three during described water soluble vitamins is vitamin B3, vitamin B5 and vitamin C
Plant the compound vitamin of composition.
The preparation method of a kind of described moisturizing maintenance cosmetic water, comprises the following steps:
(1) preparation of Rhizoma Polygonati Odorati extract: pulverized by raw material Rhizoma Polygonati Odorati, adds 3-5 times of boiling water leaching of described raw material Rhizoma Polygonati Odorati weight
Steep 2-5 minute, take out and the water of 15-20 times that Rhizoma Polygonati Odorati places into described raw material Rhizoma Polygonati Odorati weight carries out extraction 3-6 hour, obtain jade
Bamboo lixiviating solution concentrates, and then adds the ethanol that concentration is 80-95% in Rhizoma Polygonati Odorati concentrated solution and carries out precipitate with ethanol process 2-3 hour,
Supernatant discarded alcohol liquid, obtains Rhizoma Polygonati Odorati extractum, carries out lyophilization, obtains Rhizoma Polygonati Odorati extract；
(2) preparation of Rhizoma Polygonati extract: the raw material Rhizoma Polygonati gathered autumn is pulverized, and adds the 3-of described raw material Rhizoma Polygonati weight
5 times of boiling water soak 2-5 minute, take out that to carry out extraction 3-6 in the water of 15-20 times that Rhizoma Polygonati places into described raw material Rhizoma Polygonati weight little
Time, obtain polygonatum sibiricum red juice and concentrate, in Rhizoma Polygonati concentrated solution, then add the ethanol that concentration is 80-95% carry out at precipitate with ethanol
Manage 2-3 hour, supernatant discarded alcohol liquid, obtain Rhizoma Polygonati extractum, carry out lyophilization, obtain Rhizoma Polygonati extract；
(3) preparation of cosmetic water semi-finished product: described Rhizoma Polygonati Odorati extract, described Rhizoma Polygonati extract and yeast extract are carried out
Mixing, mix homogeneously obtains mixture A, Hamamelis virginiana extract, ethoxy urea is mixed with water soluble vitamins, mixed
Close and uniformly obtain mixture B, described mixture A is mixed with described mixture B, obtains one-level premix material；By imidazolidine
Base urea mixes with methyl hydroxybenzoate, and mix homogeneously obtains mixing preservative, and with described, described one-level premix material is mixed anticorrosion
Agent mixes, and mix homogeneously obtains two grades of premix material；Described two grades of premix material, edetate disodium are entered with triethanolamine
Row mixing, mix homogeneously obtains three grades of premix material；Three grades of premix material are mixed with deionized water or ultrafiltration water, mix homogeneously
Obtain cosmetic water semi-finished product；
(4) preparation of finished product: mixed with butanediol by Cremophor RH40, mix homogeneously obtains mixing solubilising
Agent, after described cosmetic water semi-finished product, described mixed solubilizers, glycerol, quintessence oil are mixed with carbomer with deionized water or
Ultrafiltration water dilutes, reemulsification, then carries out homogenizing, finally uses membrane filtration to obtain finished product.
Further, precipitate with ethanol described in step (1) is processed as adding described Rhizoma Polygonati Odorati concentrated solution in described Rhizoma Polygonati Odorati concentrated solution
The concentration of 2-3 times of weight be 90% ethanol carry out precipitate with ethanol process 3 hours, supernatant discarded alcohol liquid, obtain Rhizoma Polygonati Odorati extractum.
Further, precipitate with ethanol described in step (2) is processed as adding described Rhizoma Polygonati concentrated solution in described Rhizoma Polygonati concentrated solution
The concentration of 1-2 times of weight be 95% ethanol carry out for the first time precipitate with ethanol and process 2 hours, supernatant discarded alcohol liquid；Add described
The ethanol that concentration is 80% of 1-2 times of Rhizoma Polygonati concentrated solution weight carries out second time precipitate with ethanol and processes 1 hour, supernatant discarded alcohol liquid,
Obtain Rhizoma Polygonati extractum.
Further, concentrating and be concentrating under reduced pressure described in step (1) and step (2), the temperature of described concentrating under reduced pressure is
Less than 70 DEG C；Rhizoma Polygonati Odorati lixiviating solution described in step (1) is 2-5 times of the weight of Rhizoma Polygonati Odorati concentrated solution；Rhizoma Polygonati described in step (2) soaks
Extract is 2-5 times of the weight of Rhizoma Polygonati concentrated solution.
Further, described in step (1) and step (2), the temperature of extraction is 50-70 DEG C.
Further, described in step (4), the temperature of emulsifying is 50-60 DEG C, and the time of described emulsifying is 3-5 minute；Institute
Stating homogenizing and carry out homogenizing for employing homogenizer, the time of described homogenizing is 5-8 minute.
Further, described in step (4), the aperture of filter membrane is 0.2-0.4 μm.
Below the raw material used in the present invention is described in detail:
Butanediol is the most common in cosmetics, and another name is named again 1, and 3-dihydroxy butane, is the one of polyhydric alcohol, at cosmetics
In often do wetting agent and solvent and use, in terms of moisturizing, owing to butanediol is little molecule moisturizing composition, so grabbing water ratio very
Little, also there is certain bacteriostasis simultaneously.
Methyl hydroxybenzoate, also known as methyl parahydroxybenzoate.White crystalline powder or colourless crystallization, be soluble in alcohol, ether and third
Ketone, atomic is dissolved in water.It is mainly used as organic synthesis, food, cosmetics, the sterilization antiseptic of medicine.
Carbomer is acrylic acid bonding allyl sucrose or the high molecular polymer of tetramethylolmethane allyl ether, and cosmetics are commonly used
Thickening agent, is a very important rheology control agent of class, has the important use such as thickening, suspension, and technique is simple, good stability, extensively
General it is applied in emulsion, cream, gel.
Ethoxy urea, also known as hydroxyethyl urea, is a kind of wetting agent, is used in cosmetics, plays moisture-keeping efficacy.Ethoxy
Urea is permeable to be entered in horny layer, increases moisture content of skin, alleviates and be dried, fills up microgroove, increases skin elasticity, and provides happy
Use sensation.Can how many material combinations the biggest with cosmetics, there is the PH scope of application widely.Even if with glycerol, the third two
Alcohol is in main basic components, and hydroxyethyl urea can also be by reducing the consumption of the component of other influences cream outward appearance (such as silicon
Oil), reach more preferably moistening effect, more smooth coating sensation, identical even lower formulation cost.
Disodiumedetate is called again EDTA-2Na, is a kind of good compounding ingredient in chemistry, and it has six coordinations
Atom, the coordination compound of formation is called sequestration thing；For tasteless odorless or micro-salty white or creamy white crystals or particulate powder；Molten
Yu Shui, insoluble in ethanol, ether；Make heavy metal detoxification medicine, chelating agent, antioxidant synergist, stabilizer and softening agent etc.；A kind of weight
Want chelating agent, for complexation of metal ions and separation metal.
Hamamelis virginiana extract is leaf and the bark extracting from Hamamelis virginiana, and the main component of extract includes
Tannic acid, gallic acid, catechin, procyanidin, Protoapigenone (kaempferol, Quercetin), quintessence oil (carvacrol, eugenol, oneself
Enol), choline and Saponin；It is the strongest a kind of antioxidant and astringent, there is releiving, the function spy restraining control oil, sterilizing
Property, be used for treat during comedo highly effective, it is possible to be used for treat chronic eczema, eczema, laceration of skin or get blister, mosquito bite,
The disease such as varicosis and hemorrhoid, for skin cuts, abrades and tans severely the most effective in cure；In cosmetics, it is used for antiinflammatory, can delay
Skin with irriate, it is possible to make the cleaning of deeper, makes the younger cunning of skin beautiful, with the moisturizing composition such as ethoxy urea, multiple
The nutritional labeling cooperations such as Heshui dissolubility vitamin apply in hydrosol, have the tender white effect of moisturizing to skin, effectively help skin
The regeneration capacity at night, also has the most excellent effect to removing eye pouch etc..
Triethanolamine can regard the trihydroxy substituent of triethylamine as, for colourless to pale yellow transparent thick liquid,
Cosmetics are used as emulsifying agent, wetting agent or pH poising agent.
Yeast extract also known as yeast extraction, uses with the edible yeast of rich in protein as raw material, use self-dissolving,
Enzymolysis, separate, the modern biotechnology new and high technology such as concentration, after the protein in yeast cells, nucleic acid etc. are degraded refined and
A kind of brown color solubility paste become or slight yellow powdery natural product；It is applied to the yeast extract mark of cosmetic field
Standard is higher, and preparation technology is the most complicated, and cost is the highest, rich in natural activities such as the aminoacid of little molecule, peptide, nucleotide, vitamin
Composition；Aminoacid is the main component of natural Moisture factor (NMF) in keratodermatitis, is easily absorbed by the skin, makes aging table
Skin recovers elasticity, delay skin aging.Nucleic acid and nucleotide are the central genetic materials of human body, have and enhance metabolism, carry
High protein aggregate velocities etc. act on, and strengthen immune function, enhancement of SOD activity, improve skin antiradical activities.Additionally, produce
The nutrients such as vitamin a small amount of in product and mineral can also provide the nutrition of abundance for skin.Yeast extract is being made up
Product have moisturizing, composes effects such as living.
Cremophor RH40 initiation material comes from natural plants--castor oil hydrogenated, be colourless thick liquid or
Mastic, a kind of conventional efficient solubilizing agents, the oily matters such as essence, quintessence oil can be evenly dispersed in water, formed stably,
Transparent solution.Cremophor RH40 adds a small amount of butanediol, and solubilized is better；Be applicable to food, medicine or
Cosmetics.
Quintessence oil is from the flower of plant, leaf, stem, root or fruit, by steam distillation, squeezing and pressing method, cold-maceration or molten
Agent extraction method refines the volatile flavor of extraction.Quintessence oil of the present invention is Flos Jasmini Sambac quintessence oil, rose ethereal oil or smokes
Clothing grass quintessence oil.
Imidazolidinyl urea is a kind of white powder material, to skin avirulence, without allergy, nonirritant, is generally used as
Cosmetics preservative.Almost can with cosmetics all component interworkings.
Rhizoma Polygonati Odorati extract derives from the rhizome of liliaceous plant Rhizoma Polygonati Odorati, faint yellow fine powder, has nourishing YIN to relieve dryness, promotes the production of body fluid
The effect quenched the thirst.Its there is with Rhizoma Polygonati extract synergism, Rhizoma Polygonati Odorati extract and Rhizoma Polygonati extract mixing after external to skin
There is effect of moisturizing, defying age.
Rhizoma Polygonati extract derives from the rhizome of Liliaceae Rhizoma Polygonati, has boosting qi and nourishing yin, spleen invigorating, effect of lung moistening.North America gold
Prunus mume extract, Rhizoma Polygonati Odorati extract and Rhizoma Polygonati extract have a synergism in detail, shared then have defying age, moisturizing, profit flesh and repair
The effect protected.
Ultrafiltration water is a kind of new water technology, is mainly used in removing the micro-content organism in water and metal ion, it
Essence is a kind of new technique surfactant and ultrafilter membrane combined.Its ultimate principle is, when the table put in water
When face surfactant concentration exceedes the critical micelle concentration of surfactant, remaining surfactant molecule will be cohesion at solution
Collection, forms the aggregation that hydrophobic group is inside, hydrophilic group is outside, i.e. micelle.If water has dissolved other chemical mechanical and character
Organic substance similar to the hydrophobic group of surfactant molecule, according to the similar principle that mixes, this Organic substance will be dissolved in micelle
Or the hydrophilic group of Organic substance and surfactant can form hydrogen and be good for, Organic substance also can be transferred to micelle from aqueous phase, when they lead to
When crossing ultrafilter membrane, then carry organic micelle because not being trapped through film, water and a small amount of surfactant monomer and not
The Organic substance forming micelle can freely pass through film, thus realizes efficiently separating of most organic and water.
The moisturizing maintenance cosmetic water of the present invention be to the north of U.S. hamamelis extract, Rhizoma Polygonati Odorati extract and Rhizoma Polygonati extract be main
Wanting raw material, yeast extract, wetting agent, preservative, solubilizing agent and the quintessence oil etc. that add protein content higher make finished product；Rhizoma Polygonati Odorati
Extract and Rhizoma Polygonati extract use the technique such as leach at low temperature and lyophilization to ensure that in Rhizoma Polygonati Odorati and Rhizoma Polygonati in preparation process
Effective ingredient be not destroyed；Mixed process first employs mixing is dry mixed, it is to avoid there is use limitation especially water-sensitive
Each bioactive substance of sense directly contacts and Long contact time with water and air, has been effectively retained each bioactive substance
Biological activity；First Rhizoma Polygonati Odorati extract and Rhizoma Polygonati extract are mixed, then with Hamamelis virginiana extract, ethoxy urea and water
The mixture B of what soluble vitamin mixed the have tender white effect of moisturizing carries out mixing and has preferably played Hamamelis virginiana and carry
Take thing, Rhizoma Polygonati Odorati extract and Rhizoma Polygonati extract and share defying age, moisturizing profit flesh and the effect of maintenance being had；Finally use breast
Change, the modern chemical industry technology such as homogenizing and microfiltration, make that the moisturizing maintenance cosmetic water prepared is finer and smoother, lubrication, be more easy to infiltrate into
Skin internal layer, promotes the absorption of nutritional labeling, gives full play to its effect.
Data from investigation and result thereof
Investigation time: 2012-2015；Target of investication and study: there is the colony of skin puzzlement；Investigation age bracket: 18-45 year；
Finding: investigating 30 example triers altogether, wherein the skin of 25 example user is thoroughly improved；The skin of 2 example triers rises
To remarkable result, the skin of 3 example triers has certain effect.
Zhang, 21 years old, man, university students, pachylosis and secretion oils and fats were too much, the moisturizing maintenance cosmetic water of trial edition invention
1 month, facial skin was smooth and oils and fats balances；
Lee, 33 years old, female, white collar, the colour of skin was dark yellow, and there are microgroove, the moisturizing maintenance cosmetic water 2 of trial edition invention in face
Month, skin has smoothness, microgroove substantially to disappear；
Wang, 45 years old, female, profession, facial skin was coarse and has wrinkle, the moisturizing maintenance cosmetic water of trial edition invention
3 wheat harvesting periods, skin is glossy, and wrinkle fades away.
The invention have the benefit that the moisturizing maintenance cosmetic water of the present invention have crease-resistant, defying age, moisturizing, profit flesh and
Effect of maintenance skin, it, to skin safe, non-stimulated, has been sufficiently reserved Rhizoma Polygonati Odorati extract, Rhizoma Polygonati extract and north in finished product
Various effective ingredient in U.S. hamamelis extract；By adding the raw material such as solubilizing agent and emulsifying agent, and by emulsifying, homogenizing
Deng modern chemical industry technology, various raw materials are sufficiently mixed so that finished product is finer and smoother, lubrication, is more easy to infiltrate into skin internal layer,
Promote the absorption of nutritional labeling, give full play to its effect；Make skin become soft and smooth, compact, recover elastic；Preparation method safety,
Environmental protection, cost of manufacture is low.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme and effect are described in further details.
As without unexpected especially explanation, each raw material used in the present invention is all industry universal raw material.
Embodiment 1
A kind of moisturizing maintenance cosmetic water, is made up of following raw material: butanediol 0.1kg；Methyl hydroxybenzoate 0.6kg；Carbomer
6kg；Glycerol 0.1kg；Ethoxy urea 0.3kg；Disodiumedetate 1.5kg；Hamamelis virginiana extract 5kg；Vitamin C
And vitamin B5Compound vitamin 0.8kg；Triethanolamine 0.2kg；Yeast extract 5kg；Cremophor RH40
0.1kg；Rhizoma Polygonati Odorati extract 1.2kg；Rhizoma Polygonati extract 0.8kg；Quintessence oil 0.1kg and imidazolidinyl urea 0.2kg.
Its preparation method, comprises the following steps:
(1) preparation of Rhizoma Polygonati Odorati extract: pulverized by raw material Rhizoma Polygonati Odorati, the 4 times of boiling water adding raw material Rhizoma Polygonati Odorati weight soak 3 points
Clock, takes out in the water of 18 times that Rhizoma Polygonati Odorati places into raw material Rhizoma Polygonati Odorati weight and carries out extracting at 60 DEG C 4 hours, obtain Rhizoma Polygonati Odorati lixiviating solution
Carrying out the concentrating under reduced pressure below 70 DEG C is Rhizoma Polygonati Odorati lixiviating solution 1/4, then adds Rhizoma Polygonati Odorati concentrated solution weight in Rhizoma Polygonati Odorati concentrated solution
2.5 times 90% ethanol carry out precipitate with ethanol and process 2.5 hours, supernatant discarded alcohol liquid, obtain Rhizoma Polygonati Odorati extractum, carry out freezing dry
Dry, obtain Rhizoma Polygonati Odorati extract；
(2) preparation of Rhizoma Polygonati extract: the raw material Rhizoma Polygonati gathered autumn is pulverized, adds 3-5 times of raw material Rhizoma Polygonati weight
Boiling water soaks 2-5 minute, takes out in the water of 18 times that Rhizoma Polygonati places into raw material Rhizoma Polygonati weight and carries out extracting at 60 DEG C 4 hours,
Obtaining polygonatum sibiricum red juice and carrying out concentrating under reduced pressure below 70 DEG C is polygonatum sibiricum red juice 1/3, then adds 1.5 in Rhizoma Polygonati concentrated solution
The ethanol of 95% again carries out precipitate with ethanol for the first time and processes 2 hours, supernatant discarded alcohol liquid；Add Rhizoma Polygonati concentrated solution weight 1.5 times
80% ethanol carry out second time precipitate with ethanol process 1 hour, supernatant discarded alcohol liquid, obtain Rhizoma Polygonati extractum, carry out lyophilization,
To Rhizoma Polygonati extract；
(3) preparation of cosmetic water semi-finished product: Rhizoma Polygonati Odorati extract, Rhizoma Polygonati extract and yeast extract are mixed, mixed
Close and uniformly obtain mixture A, Hamamelis virginiana extract, ethoxy urea are mixed with water soluble vitamins, mix homogeneously
Obtain mixture B, mixture A is mixed with mixture B, obtain one-level premix material；By imidazolidinyl urea and methyl hydroxybenzoate
Mixing, mix homogeneously obtains mixing preservative, one-level premix material is mixed with mixing preservative, and mix homogeneously obtains
Two grades of premix material；Two grades of premix material, edetate disodium being mixed with triethanolamine, mix homogeneously obtains three grades of premixs
Material；Three grades of premix material being mixed with deionized water or ultrafiltration water, mix homogeneously obtains cosmetic water semi-finished product；
(4) preparation of finished product: mixed with butanediol by Cremophor RH40, mix homogeneously obtains mixing solubilising
Agent, dilute with deionized water or ultrafiltration water after cosmetic water semi-finished product, mixed solubilizers, glycerol, quintessence oil are mixed with carbomer
Release, more emulsified 4 minutes at 55 DEG C, then use homogenizer to carry out homogenizing 6 minutes, the filter membrane finally using aperture to be 0.3 μm
Carry out being filtrated to get finished product.
Embodiment 2
A kind of moisturizing maintenance cosmetic water, is made up of following raw material:
Butanediol 0.5kg；Methyl hydroxybenzoate 0.2kg；Carbomer 2kg；Glycerol 0.5kg；Ethoxy urea 0.1kg；Ethylenediamine tetraacetic
Acetic acid disodium 0.3kg；Hamamelis virginiana extract 3kg；Vitamin B3With ascorbic compound vitamin 0.4kg；Triethanolamine
0.5kg；Yeast extract 1kg；Cremophor RH40 0.5kg；Rhizoma Polygonati Odorati extract 0.8kg；Rhizoma Polygonati extract 1.2kg；Essence
Oil 0.2kg and imidazolidinyl urea 0.1kg.
Its preparation method, comprises the following steps:
(1) preparation of Rhizoma Polygonati Odorati extract: pulverized by raw material Rhizoma Polygonati Odorati, the 3 times of boiling water adding raw material Rhizoma Polygonati Odorati weight soak 5 points
Clock, takes out in the water of 20 times that Rhizoma Polygonati Odorati places into raw material Rhizoma Polygonati Odorati weight and carries out extracting at 50 DEG C 6 hours, obtain Rhizoma Polygonati Odorati lixiviating solution
Carry out below 70 DEG C that concentrating under reduced pressure is Rhizoma Polygonati Odorati lixiviating solution 1/2, then adds the 2 of Rhizoma Polygonati Odorati concentrated solution weight in Rhizoma Polygonati Odorati concentrated solution
The ethanol of 95% again carries out precipitate with ethanol and processes 2 hours, and supernatant discarded alcohol liquid obtains Rhizoma Polygonati Odorati extractum, carries out lyophilization, obtain jade
Bamboo extract；
(2) preparation of Rhizoma Polygonati extract: the raw material Rhizoma Polygonati gathered autumn is pulverized, adds 3-5 times of raw material Rhizoma Polygonati weight
Boiling water soaks 2 minutes, takes out in the water of 20 times that Rhizoma Polygonati places into raw material Rhizoma Polygonati weight and carries out extracting at 50 DEG C 6 hours,
Carrying out less than 70 DEG C concentrating under reduced pressure to polygonatum sibiricum red juice is polygonatum sibiricum red juice 1/2, then adds 1 times in Rhizoma Polygonati concentrated solution
The ethanol of 95% carries out precipitate with ethanol for the first time and processes 2 hours, supernatant discarded alcohol liquid；Add 2 times of Rhizoma Polygonati concentrated solution weight
The ethanol of 80% carries out second time precipitate with ethanol and processes 1 hour, and supernatant discarded alcohol liquid obtains Rhizoma Polygonati extractum, carries out lyophilization, obtain
Rhizoma Polygonati extract；
(3) preparation of cosmetic water semi-finished product: Rhizoma Polygonati Odorati extract, Rhizoma Polygonati extract and yeast extract are mixed, mixed
Close and uniformly obtain mixture A, Hamamelis virginiana extract, ethoxy urea are mixed with water soluble vitamins, mix homogeneously
Obtain mixture B, mixture A is mixed with mixture B, obtain one-level premix material；By imidazolidinyl urea and methyl hydroxybenzoate
Mixing, mix homogeneously obtains mixing preservative, one-level premix material is mixed with mixing preservative, and mix homogeneously obtains
Two grades of premix material；Two grades of premix material, edetate disodium being mixed with triethanolamine, mix homogeneously obtains three grades of premixs
Material；Three grades of premix material being mixed with deionized water or ultrafiltration water, mix homogeneously obtains cosmetic water semi-finished product；
(4) preparation of finished product: mixed with butanediol by Cremophor RH40, mix homogeneously obtains mixing solubilising
Agent, dilute with deionized water or ultrafiltration water after cosmetic water semi-finished product, mixed solubilizers, glycerol, quintessence oil are mixed with carbomer
Release, more emulsified 5 minutes at 50 DEG C, then use homogenizer to carry out homogenizing 5 minutes, the filter membrane finally using aperture to be 0.4 μm
It is filtrated to get finished product.
Embodiment 3
A kind of moisturizing maintenance cosmetic water, is made up of following raw material:
Butanediol 0.1kg；Methyl hydroxybenzoate 0.2kg；Carbomer 2kg；Glycerol 0.1kg；Ethoxy urea 0.1kg；Diamidogen tetrem
Acid disodium 0.3kg；Hamamelis virginiana extract 3kg；Vitamin B3And vitamin B5Compound vitamin 0.6kg；Triethanolamine
0.2kg；Yeast extract 1kg；Cremophor RH40 0.1kg；Rhizoma Polygonati Odorati extract 1.0kg；Rhizoma Polygonati extract 1.0kg；Essence
Oil 0.1kg and imidazolidinyl urea 0.1kg.
Its preparation method, comprises the following steps:
(1) preparation of Rhizoma Polygonati Odorati extract: pulverized by raw material Rhizoma Polygonati Odorati, the 5 times of boiling water adding raw material Rhizoma Polygonati Odorati weight soak 2 points
Clock, takes out in the water of 15 times that Rhizoma Polygonati Odorati places into raw material Rhizoma Polygonati Odorati weight and carries out extracting at 70 DEG C 3 hours, obtain Rhizoma Polygonati Odorati lixiviating solution
Carry out below 70 DEG C that concentrating under reduced pressure is Rhizoma Polygonati Odorati lixiviating solution 1/5, then adds the 3 of Rhizoma Polygonati Odorati concentrated solution weight in Rhizoma Polygonati Odorati concentrated solution
The ethanol of 80% again carries out precipitate with ethanol and processes 3 hours, and supernatant discarded alcohol liquid obtains Rhizoma Polygonati Odorati extractum, carries out lyophilization, obtain jade
Bamboo extract；
(2) preparation of Rhizoma Polygonati extract: the raw material Rhizoma Polygonati gathered autumn is pulverized, adds 3-5 times of raw material Rhizoma Polygonati weight
Boiling water soaks 5 minutes, takes out in the water of 15 times that Rhizoma Polygonati places into raw material Rhizoma Polygonati weight and carries out extracting at 70 DEG C 3 hours,
Carrying out less than 70 DEG C concentrating under reduced pressure to polygonatum sibiricum red juice is polygonatum sibiricum red juice 1/5, then adds 2 times in Rhizoma Polygonati concentrated solution
The ethanol of 95% carries out precipitate with ethanol for the first time and processes 2 hours, supernatant discarded alcohol liquid；Add 1 times of Rhizoma Polygonati concentrated solution weight
The ethanol of 80% carries out second time precipitate with ethanol and processes 1 hour, and supernatant discarded alcohol liquid obtains Rhizoma Polygonati extractum, carries out lyophilization, obtain
Rhizoma Polygonati extract；
(3) preparation of cosmetic water semi-finished product: Rhizoma Polygonati Odorati extract, Rhizoma Polygonati extract and yeast extract are mixed, mixed
Close and uniformly obtain mixture A, Hamamelis virginiana extract, ethoxy urea are mixed with water soluble vitamins, mix homogeneously
Obtain mixture B, mixture A is mixed with mixture B, obtain one-level premix material；By imidazolidinyl urea and methyl hydroxybenzoate
Mixing, mix homogeneously obtains mixing preservative, one-level premix material is mixed with mixing preservative, and mix homogeneously obtains
Two grades of premix material；Two grades of premix material, edetate disodium being mixed with triethanolamine, mix homogeneously obtains three grades of premixs
Material；Three grades of premix material being mixed with deionized water or ultrafiltration water, mix homogeneously obtains cosmetic water semi-finished product；
(4) preparation of finished product: mixed with butanediol by Cremophor RH40, mix homogeneously obtains mixing solubilising
Agent, dilute with deionized water or ultrafiltration water after cosmetic water semi-finished product, mixed solubilizers, glycerol, quintessence oil are mixed with carbomer
Release, more emulsified 3 minutes at 60 DEG C, then use homogenizer to carry out homogenizing 8 minutes, the filter membrane finally using aperture to be 0.2 μm
It is filtrated to get finished product.
The present invention is not limited to above-mentioned preferred forms, and anyone can show that under the enlightenment of the present invention other are various
The product of form, no matter but in its shape or structure, make any change, every have same as the present application or akin skill
Art scheme, within all falling within protection scope of the present invention.
Claims (10)
1. a moisturizing maintenance cosmetic water, it is characterised in that include the raw material of following weight portion: butanediol 0.1-0.5 part；Oxybenzene
Methyl ester 0.2-0.6 part；Carbomer 2-6 part；Glycerol 0.1-0.5 part；Ethoxy urea 0.1-0.3 part；Disodiumedetate
0.3-1.5 part；Hamamelis virginiana extract 3-5 part；Water soluble vitamins 0.4-0.8 part；Triethanolamine 0.2-0.5 part；Yeast
Extract 1-5 part；Cremophor RH40 0.1-0.5 part；Rhizoma Polygonati Odorati extract 0.8-1.2 part；Rhizoma Polygonati extract 0.8-1.2
Part；Quintessence oil 0.1-0.2 part and imidazolidinyl urea 0.1-0.2 part.
Moisturizing maintenance cosmetic water the most according to claim 1, it is characterised in that include the raw material of following weight portion: fourth two
Alcohol 0.1 part；Methyl hydroxybenzoate 0.2 part；Carbomer 2 parts；Glycerol 0.1 part；Ethoxy urea 0.1 part；Edetate disodium 0.3 part；
Hamamelis virginiana extract 3 parts；Water soluble vitamins 0.6 part；Triethanolamine 0.2 part；Yeast extract 1 part；PEG-40 hydrogenates
Oleum Ricini 0.1 part；Rhizoma Polygonati Odorati extract 1.0 parts；Rhizoma Polygonati extract 1.0 parts；Quintessence oil 0.1 part and imidazolidinyl urea 0.1 part.
Moisturizing maintenance cosmetic water the most according to claim 1, it is characterised in that described water soluble vitamins is vitamin B3、
Vitamin B5Compound vitamin with any two or three composition in vitamin C.
4. the preparation method of the moisturizing maintenance cosmetic water as according to any one of claim 1,2 and 3, it is characterised in that
Comprise the following steps:
(1) preparation of Rhizoma Polygonati Odorati extract: pulverized by raw material Rhizoma Polygonati Odorati, the 3-5 times of boiling water adding described raw material Rhizoma Polygonati Odorati weight soaks 2-5
Minute, take out and the water of 15-20 times that Rhizoma Polygonati Odorati places into described raw material Rhizoma Polygonati Odorati weight carries out extraction 3-6 hour, obtain Rhizoma Polygonati Odorati leaching
Extract concentrates, and then adds the ethanol that concentration is 80-95% in Rhizoma Polygonati Odorati concentrated solution and carries out precipitate with ethanol process 2-3 hour, abandons
Remove pure liquid, obtain Rhizoma Polygonati Odorati extractum, carry out lyophilization, obtain Rhizoma Polygonati Odorati extract；
(2) preparation of Rhizoma Polygonati extract: the raw material Rhizoma Polygonati gathered autumn is pulverized, and adds 3-5 times of described raw material Rhizoma Polygonati weight
Boiling water soaks 2-5 minute, takes out and carries out extraction 3-6 hour in the water of 15-20 times that Rhizoma Polygonati places into described raw material Rhizoma Polygonati weight,
Obtain polygonatum sibiricum red juice to concentrate, in Rhizoma Polygonati concentrated solution, then add the ethanol that concentration is 80-95% carry out precipitate with ethanol process
2-3 hour, supernatant discarded alcohol liquid, obtain Rhizoma Polygonati extractum, carry out lyophilization, obtain Rhizoma Polygonati extract；
(3) preparation of cosmetic water semi-finished product: described Rhizoma Polygonati Odorati extract, described Rhizoma Polygonati extract and yeast extract are mixed
Closing, mix homogeneously obtains mixture A, Hamamelis virginiana extract, ethoxy urea is mixed with water soluble vitamins, mixing
Uniformly obtain mixture B, described mixture A is mixed with described mixture B, obtains one-level premix material；By imidazolidinyl
Urea mixes with methyl hydroxybenzoate, and mix homogeneously obtains mixing preservative, and with described, described one-level premix material is mixed preservative
Mixing, mix homogeneously obtains two grades of premix material；Described two grades of premix material, edetate disodium are carried out with triethanolamine
Mixing, mix homogeneously obtains three grades of premix material；Three grades of premix material being mixed with deionized water or ultrafiltration water, mix homogeneously obtains
To cosmetic water semi-finished product；
(4) preparation of finished product: being mixed with butanediol by Cremophor RH40, mix homogeneously obtains mixed solubilizers,
With deionized water or ultrafiltration after described cosmetic water semi-finished product, described mixed solubilizers, glycerol, quintessence oil are mixed with carbomer
Water dilutes, reemulsification, then carries out homogenizing, finally uses membrane filtration to obtain finished product.
The preparation method of moisturizing maintenance cosmetic water the most according to claim 4, it is characterised in that alcohol described in step (1)
The ethanol that concentration is 90% of heavy be processed as adding described Rhizoma Polygonati Odorati concentrated solution weight in described Rhizoma Polygonati Odorati concentrated solution 2-3 times is carried out
Precipitate with ethanol processes 3 hours, and supernatant discarded alcohol liquid obtains Rhizoma Polygonati Odorati extractum.
The preparation method of moisturizing maintenance cosmetic water the most according to claim 4, it is characterised in that alcohol described in step (2)
The ethanol that concentration is 95% of heavy be processed as adding described Rhizoma Polygonati concentrated solution weight in described Rhizoma Polygonati concentrated solution 1-2 times is carried out
Precipitate with ethanol processes 2 hours for the first time, supernatant discarded alcohol liquid；The concentration of add described Rhizoma Polygonati concentrated solution weight 1-2 times is 80%
Ethanol carry out second time precipitate with ethanol process 1 hour, supernatant discarded alcohol liquid, obtain Rhizoma Polygonati extractum.
The preparation method of moisturizing maintenance cosmetic water the most according to claim 4, it is characterised in that step (1) and step (2)
Described in concentrate be concentrating under reduced pressure, the temperature of described concentrating under reduced pressure is less than 70 DEG C；Described in step (1), Rhizoma Polygonati Odorati lixiviating solution is
2-5 times of the weight of Rhizoma Polygonati Odorati concentrated solution；Polygonatum sibiricum red juice described in step (2) is 2-5 times of the weight of Rhizoma Polygonati concentrated solution.
The preparation method of moisturizing maintenance cosmetic water the most according to claim 4, it is characterised in that step (1) and step (2)
Described in extraction temperature be 50-70 DEG C.
The preparation method of moisturizing maintenance cosmetic water the most according to claim 4, it is characterised in that breast described in step (4)
The temperature changed is 50-60 DEG C, and the time of described emulsifying is 3-5 minute；Described homogenizing for using homogenizer to carry out homogenizing, described all
The time of matter is 5-8 minute.
The preparation method of moisturizing maintenance cosmetic water the most according to claim 4, it is characterised in that filter described in step (4)
The aperture of film is 0.2-0.4 μm.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106667848A (en) * | 2017-02-22 | 2017-05-17 | 广州市聚吉科绿色化学共性技术研究院有限公司 | Toner |
| CN115252533A (en) * | 2022-08-18 | 2022-11-01 | 广州瑞誉化工科技有限公司 | Moisturizing and repairing composition and preparation method and application thereof |
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| CN104173232A (en) * | 2014-08-06 | 2014-12-03 | 金玲 | Method for preparing beautifying fluid capable of promoting skin resistance and repairing small-invasive skin |
| CN105078818A (en) * | 2015-07-27 | 2015-11-25 | 深圳市零重力科技有限公司 | Massaging conditioning water applied after cleansing face and preparation method of massaging conditioning water |
| CN105267084A (en) * | 2015-09-23 | 2016-01-27 | 嘉兴市蝶柔化妆品有限公司 | Moisturizer |
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| CN102232911A (en) * | 2010-04-22 | 2011-11-09 | 车芳芳 | Balance moisture toner |
| CN104173232A (en) * | 2014-08-06 | 2014-12-03 | 金玲 | Method for preparing beautifying fluid capable of promoting skin resistance and repairing small-invasive skin |
| CN105078818A (en) * | 2015-07-27 | 2015-11-25 | 深圳市零重力科技有限公司 | Massaging conditioning water applied after cleansing face and preparation method of massaging conditioning water |
| CN105267084A (en) * | 2015-09-23 | 2016-01-27 | 嘉兴市蝶柔化妆品有限公司 | Moisturizer |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106667848A (en) * | 2017-02-22 | 2017-05-17 | 广州市聚吉科绿色化学共性技术研究院有限公司 | Toner |
| CN115252533A (en) * | 2022-08-18 | 2022-11-01 | 广州瑞誉化工科技有限公司 | Moisturizing and repairing composition and preparation method and application thereof |
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Application publication date: 20161214 |