CN106192391A - A kind of water proof fire retardant canvas tent fabric and preparation method thereof - Google Patents

A kind of water proof fire retardant canvas tent fabric and preparation method thereof Download PDF

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Publication number
CN106192391A
CN106192391A CN201610680574.7A CN201610680574A CN106192391A CN 106192391 A CN106192391 A CN 106192391A CN 201610680574 A CN201610680574 A CN 201610680574A CN 106192391 A CN106192391 A CN 106192391A
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CN
China
Prior art keywords
fire retardant
tent fabric
fibre
water proof
colloidal sol
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610680574.7A
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Chinese (zh)
Inventor
龙小伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yingshang County Yida Tent Co Ltd
Original Assignee
Yingshang County Yida Tent Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yingshang County Yida Tent Co Ltd filed Critical Yingshang County Yida Tent Co Ltd
Priority to CN201610680574.7A priority Critical patent/CN106192391A/en
Publication of CN106192391A publication Critical patent/CN106192391A/en
Pending legal-status Critical Current

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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/74—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon or graphite; with carbides; with graphitic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
    • D06M13/2246—Esters of unsaturated carboxylic acids
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D06M15/11—Starch or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/10—Animal fibres
    • D06M2101/12—Keratin fibres or silk
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/18—Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/22—Polymers or copolymers of halogenated mono-olefins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16—Synthetic fibres, other than mineral fibres
    • D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32—Polyesters
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/30—Flame or heat resistance, fire retardancy properties

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a kind of water proof fire retardant canvas tent fabric, it is to be prepared by the raw material of following weight parts: polyster fibre 20 30, polytetrafluoroethylene fibre 20 30, polysulphonamide fiber 10 15, glass fibre 10 15, sepiolite powder 35, Firebrake ZB 12, tetramethylolmethane 35, dimethicone 24, Polyethylene Glycol Oleate 12, styrene-acrylic emulsion 5 10, modified starch colloidal sol 5 10.The canvas tent fabric of the present invention had both met basic use requirement, had again good moisture-penetrable ventilated property, coating stability and the uniformity high, difficult drop-off, cracking, exterior quality is good, has good fire retardant performance, can also play the most waterproof effect, security performance is good, practical.

Description

A kind of water proof fire retardant canvas tent fabric and preparation method thereof
Technical field
The present invention relates to tent material technical field, particularly relate to a kind of water proof fire retardant canvas tent fabric and preparation side thereof Method.
Background technology
Tent is a kind of textile with construction material function, isolates an individual secure in lowered in field environment Space.Tent has simplicity, light and handy feature, needs have Radix Saposhnikoviae, rainproof, snow defence, cold-proof, the basic function of mosquito proof. Recently as the development of tourist industry, the sales volume of tent is increased substantially, and market expands further, outside people are to tent See, the demand of performance improves the most further.Tent material is made up through surface dressing of base fabric, and its performance largely affects The serviceability of tent.Current most widely used tent material is polyester canvas, and its breathable moisture permeability is poor, serviceability The highest with surcharge, it is impossible to meet the potential demand of city's field alignment expensive goods.Rainwater can be contacted when tent uses in the wild Deng, therefore the water proofing property of tent material is particularly significant, and fire safety aspect also there is a need to simultaneously.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of water proof fire retardant canvas tent fabric and Preparation method.
The present invention is achieved by the following technical solutions:
A kind of water proof fire retardant canvas tent fabric, it is to be prepared by the raw material of following weight parts:
Polyster fibre 20-30, polytetrafluoroethylene fibre 20-30, polysulphonamide fiber 10-15, glass fibre 10-15, sepiolite powder 3-5, Firebrake ZB 1-2, tetramethylolmethane 3-5, dimethicone 2-4, Polyethylene Glycol Oleate 1-2, styrene-acrylic emulsion 5-10, modified shallow lake Powder colloidal sol 5-10；
Wherein modified starch colloidal sol is prepared by the raw materials in: corn starch 30-40, graphite powder 10-15, sodium nitrate 1- 2, potassium permanganate 2-4, acrylic acid 3-5, methyl methacrylate 6-8,15-20% concentration aqueous hydrogen peroxide solution 10-15, persulfuric acid Ammonium 0.5-1, sodium lauryl sulphate 0.5-1, water 200-300；The preparation method of modified starch colloidal sol is by solid-liquid by graphite powder Weight ratio 1:1.5-1:2 adds sodium nitrate, potassium permanganate, 40-50 DEG C of reaction after mixing with the concentrated sulphuric acid that mass fraction is 98% Water, corn starch and 15-20% concentration aqueous hydrogen peroxide solution 60-80 DEG C stirring 3-4h it is sequentially added into, in being adjusted to by pH after 0.5-1h Remaining raw material 70-80 DEG C reaction 1-2h is added, after cooling and get final product after property.
The preparation method of a kind of water proof fire retardant canvas tent fabric, comprises the following steps:
(1) by polyster fibre, polytetrafluoroethylene fibre, polysulphonamide fiber and glass fibre blending woven in proportion, canvas base is obtained Cloth；
(2) 40-50 DEG C of stirring 1-after styrene-acrylic emulsion, modified starch colloidal sol, Polyethylene Glycol Oleate and dimethicone being mixed 2h, adds remaining raw material co-ground to fineness≤50 μm, obtains coating agent after cooling；
(3) the canvas scrim surfaces that the coating agent in (2) is evenly applied in (1), prior to 80-90 DEG C of dry 4-6h, then at 120-140 DEG C of heat treatment 10-20min, i.e. obtains water proof fire retardant canvas tent fabric after cooling.
The invention have the advantage that
The present invention is compounded by raw materials such as modified starch colloidal sol and styrene-acrylic emulsions, and the coating agent of synthesis has with tent canvas base fabric Good associativity, generates in base fabric and has good adherence fastness, moisture-penetrable ventilated property and the film of mechanical property, makes final obtaining To canvas tent fabric both met basic use requirement, there is again good moisture-penetrable ventilated property, coating stability and uniformly Degree height, difficult drop-off, cracking, waterproof effect and exterior quality are good, have good fire retardant performance, and security performance is good, real Strong by property.
Detailed description of the invention
A kind of water proof fire retardant canvas tent fabric, it is to be prepared by the raw material of following weight parts:
Polyster fibre 20, polytetrafluoroethylene fibre 20, polysulphonamide fiber 10, glass fibre 10, sepiolite powder 3, Firebrake ZB 1, season Penta tetrol 3, dimethicone 2, Polyethylene Glycol Oleate 1, styrene-acrylic emulsion 5, modified starch colloidal sol 5；
Wherein modified starch colloidal sol is prepared by the raw materials in: corn starch 30, graphite powder 10, sodium nitrate 1, permanganic acid Potassium 2, acrylic acid 3, methyl methacrylate 6,15% concentration aqueous hydrogen peroxide solution 10, Ammonium persulfate. 0.5, sodium lauryl sulphate 0.5, water 200；Graphite powder is 98% by solid-liquid weight ratio 1:1.5 and mass fraction by the preparation method of modified starch colloidal sol Add sodium nitrate, potassium permanganate after concentrated sulphuric acid mixing, be sequentially added into water, corn starch and 15% concentration after 40 DEG C of reaction 0.5h double Oxygen water aqueous solution 60 DEG C stirring 3h, adds remaining raw material 70 DEG C reaction 1h, after cooling and get final product after pH is adjusted to neutrality.
The preparation method of a kind of water proof fire retardant canvas tent fabric, comprises the following steps:
(1) by polyster fibre, polytetrafluoroethylene fibre, polysulphonamide fiber and glass fibre blending woven in proportion, canvas base is obtained Cloth；
(2) by rear for the mixing of styrene-acrylic emulsion, modified starch colloidal sol, Polyethylene Glycol Oleate and dimethicone 40 DEG C of stirring 1h, cold Add remaining raw material co-ground the most afterwards to fineness≤50 μm, obtain coating agent；
(3) the canvas scrim surfaces being evenly applied in (1) by the coating agent in (2), prior to 80 DEG C of dry 4h, then at 120 DEG C Heat treatment 10min, i.e. obtains water proof fire retardant canvas tent fabric after cooling.
Above-mentioned prepared canvas tent fabric performance index test result is as follows:
Project Unit Index
Ultimate strength (warp-wise) N 2950
Ultimate strength (broadwise) N 2540
Vapor transfer rate g/m2d 1028
Burning char length mm 69
After flame time s 5
Water pressure resistance mm ≥1500

Claims (2)

1. a water proof fire retardant canvas tent fabric, it is characterised in that it is to be prepared by the raw material of following weight parts:
Polyster fibre 20-30, polytetrafluoroethylene fibre 20-30, polysulphonamide fiber 10-15, glass fibre 10-15, sepiolite powder 3-5, Firebrake ZB 1-2, tetramethylolmethane 3-5, dimethicone 2-4, Polyethylene Glycol Oleate 1-2, styrene-acrylic emulsion 5-10, modified shallow lake Powder colloidal sol 5-10；
Described modified starch colloidal sol is prepared by the raw materials in: corn starch 30-40, graphite powder 10-15, sodium nitrate 1-2, potassium permanganate 2-4, acrylic acid 3-5, methyl methacrylate 6-8,15-20% concentration aqueous hydrogen peroxide solution 10-15, over cure Acid ammonium 0.5-1, sodium lauryl sulphate 0.5-1, water 200-300；The preparation method of modified starch colloidal sol is by solid by graphite powder Liquid weight ratio 1:1.5-1:2 adds sodium nitrate, potassium permanganate, 40-50 DEG C of reaction after mixing with the concentrated sulphuric acid that mass fraction is 98% Water, corn starch and 15-20% concentration aqueous hydrogen peroxide solution 60-80 DEG C stirring 3-4h it is sequentially added into, in being adjusted to by pH after 0.5-1h Remaining raw material 70-80 DEG C reaction 1-2h is added, after cooling and get final product after property.
The preparation method of a kind of water proof fire retardant canvas tent fabric the most according to claim 1, it is characterised in that include with Lower step:
(1) by polyster fibre, polytetrafluoroethylene fibre, polysulphonamide fiber and glass fibre blending woven in proportion, canvas base is obtained Cloth；
(2) 40-50 DEG C of stirring 1-after styrene-acrylic emulsion, modified starch colloidal sol, Polyethylene Glycol Oleate and dimethicone being mixed 2h, adds remaining raw material co-ground to fineness≤50 μm, obtains coating agent after cooling；
(3) the canvas scrim surfaces that the coating agent in (2) is evenly applied in (1), prior to 80-90 DEG C of dry 4-6h, then at 120-140 DEG C of heat treatment 10-20min, i.e. obtains water proof fire retardant canvas tent fabric after cooling.
CN201610680574.7A 2016-08-17 2016-08-17 A kind of water proof fire retardant canvas tent fabric and preparation method thereof Pending CN106192391A (en)

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CN201610680574.7A CN106192391A (en) 2016-08-17 2016-08-17 A kind of water proof fire retardant canvas tent fabric and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201610680574.7A CN106192391A (en) 2016-08-17 2016-08-17 A kind of water proof fire retardant canvas tent fabric and preparation method thereof

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107558231A (en) * 2017-10-17 2018-01-09 苏州雨维斯纺织纤维有限公司 A kind of umbrella cloth and its manufacture method
CN107746699A (en) * 2017-09-29 2018-03-02 安徽东锦服饰有限公司 A kind of fabric is compound to use glue
CN108528059A (en) * 2018-03-08 2018-09-14 海宁天福经编涂层有限公司 A kind of preparation method of fire-retardant banner fabric
CN111663341A (en) * 2020-05-19 2020-09-15 宁波枫缘户外用品科技有限公司 Corrosion-resistant tent cloth and preparation method thereof
CN114103295A (en) * 2021-10-29 2022-03-01 安徽亿盈特纤新材料有限公司 Regenerated environment-friendly antibacterial fabric cloth and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104178011A (en) * 2014-08-27 2014-12-03 句容市石狮冲压件厂 Composite coating for outdoor tent and preparation method of composite coating
CN105129901A (en) * 2015-09-22 2015-12-09 陕西科技大学 Grafted modified starch flocculating absorbent for tanning sewage and preparation method of flocculating absorbent
CN105133335A (en) * 2015-09-23 2015-12-09 芜湖环瑞汽车内饰件有限公司 Fireproof flame-retardant sound-absorbing cotton and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104178011A (en) * 2014-08-27 2014-12-03 句容市石狮冲压件厂 Composite coating for outdoor tent and preparation method of composite coating
CN105129901A (en) * 2015-09-22 2015-12-09 陕西科技大学 Grafted modified starch flocculating absorbent for tanning sewage and preparation method of flocculating absorbent
CN105133335A (en) * 2015-09-23 2015-12-09 芜湖环瑞汽车内饰件有限公司 Fireproof flame-retardant sound-absorbing cotton and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107746699A (en) * 2017-09-29 2018-03-02 安徽东锦服饰有限公司 A kind of fabric is compound to use glue
CN107558231A (en) * 2017-10-17 2018-01-09 苏州雨维斯纺织纤维有限公司 A kind of umbrella cloth and its manufacture method
CN108528059A (en) * 2018-03-08 2018-09-14 海宁天福经编涂层有限公司 A kind of preparation method of fire-retardant banner fabric
CN111663341A (en) * 2020-05-19 2020-09-15 宁波枫缘户外用品科技有限公司 Corrosion-resistant tent cloth and preparation method thereof
CN114103295A (en) * 2021-10-29 2022-03-01 安徽亿盈特纤新材料有限公司 Regenerated environment-friendly antibacterial fabric cloth and preparation method thereof

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Application publication date: 20161207