CN106182248A - A kind of method promoting wicker products decay resistance - Google Patents

A kind of method promoting wicker products decay resistance Download PDF

Info

Publication number
CN106182248A
CN106182248A CN201610551270.0A CN201610551270A CN106182248A CN 106182248 A CN106182248 A CN 106182248A CN 201610551270 A CN201610551270 A CN 201610551270A CN 106182248 A CN106182248 A CN 106182248A
Authority
CN
China
Prior art keywords
temperature
wicker
parts
puts
standby
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610551270.0A
Other languages
Chinese (zh)
Other versions
CN106182248B (en
Inventor
李明
李东猛
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
FUNAN COUNTY MENGFA ARTS & CRAFTS Co Ltd
Original Assignee
FUNAN COUNTY MENGFA ARTS & CRAFTS Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by FUNAN COUNTY MENGFA ARTS & CRAFTS Co Ltd filed Critical FUNAN COUNTY MENGFA ARTS & CRAFTS Co Ltd
Priority to CN201610551270.0A priority Critical patent/CN106182248B/en
Publication of CN106182248A publication Critical patent/CN106182248A/en
Application granted granted Critical
Publication of CN106182248B publication Critical patent/CN106182248B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27JMECHANICAL WORKING OF CANE, CORK, OR SIMILAR MATERIALS
    • B27J3/00Peeling osier rods
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27JMECHANICAL WORKING OF CANE, CORK, OR SIMILAR MATERIALS
    • B27J1/00Mechanical working of cane or the like
    • B27J1/02Braiding, e.g. basket-making
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/0207Pretreatment of wood before impregnation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/08Impregnating by pressure, e.g. vacuum impregnation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/16Inorganic impregnating agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/34Organic impregnating agents
    • B27K3/50Mixtures of different organic impregnating agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/52Impregnating agents containing mixtures of inorganic and organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/0005Cryogenic treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/001Heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/003Treating of wood not provided for in groups B27K1/00, B27K3/00 by using electromagnetic radiation or mechanical waves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/06Softening or hardening of wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K9/00Chemical or physical treatment of reed, straw, or similar material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment
    • B27K2240/20Removing fungi, molds or insects

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Forests & Forestry (AREA)
  • Wood Science & Technology (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)

Abstract

The invention discloses a kind of method promoting wicker products decay resistance, comprise the steps: the peeling of (1) wicker, the braiding of (2) sofening treatment, (3) wicker, (4) preservative treatment.The collocation of the inventive method each step is scientific and reasonable, the wicker products insect protected, mildew-resistant, the corrosion resistant effect that prepare are preferable, case hardness is higher, compared with prior art, its case hardness can improve about 25%, use under stronger acid-base condition, its anticorrosion time can reach 4 ~ 5 times of original anticorrosion time, service life under normal service condition can extend about 30%, service life under high humidity conditions can extend more than 40%, and stability in use is preferable, and anti-deformation ability is stronger, decay resistance is good, and use value is higher.

Description

A kind of method promoting wicker products decay resistance
Technical field
The invention belongs to wicker plaiting article manufacture field, be specifically related to a kind of method promoting wicker products decay resistance.
Background technology
Wicker plaiting article is China's one traditional technology, and present wicker products is commercially popular, and the kind of wicker products is numerous Many, the polytypes such as seat, basket, basket, dustpan, round-bottomed basket, crate, shallow basket made of wicker or thin bamboo strips, the gaily decorated basket, bamboo strainer, food dish are had at domestic aspect.Export trade side Face, has formed buck basket, flower pot coat, picnic tableware basket, hanging basket, lampshade, kennel, cat litter, Bird's Nest etc. through developing and design many Kind, foreign trade is formed the appreciation effect that low-grade goods become high-grade, very popular.But, wicker plaiting article belongs to organic fibre Dimension material, weatherability is poor, is susceptible to degrade aging, needs to be processed by surface to protect it, extends the use longevity Life, retains its natural beauty simultaneously.Conventional oily treating agent causes environment pollution and endangers and cost height, and aqueous treatment The poor-performings such as the adhesive force of agent, resistance to blocking, resistance to water, stability.The hardness of film that common water borne inorganic agent is formed is relatively low, Pliability is poor, and poor corrosion resistance, and protective effect is bad.Additionally, aforesaid way is all to process wicker surface, one There is damage in denier surface, and its protected effect will be greatly reduced.
Summary of the invention
In order to solve the problems referred to above, the invention provides a kind of method promoting wicker products decay resistance.
The present invention is achieved through the following technical solutions:
A kind of method promoting wicker products decay resistance, comprises the steps:
(1) wicker peeling: harvested wicker is carried out peeling operation, then puts it into the calcium chloride that mass fraction is 3.5% Soaking and washing 20min in solution, standby after being placed under the sun dry in the sun with clear water after being finally drawn off rinsing well 1 ~ 2 day;
(2) sofening treatment:
A. the wicker after dry in the sun is put into temperature be 160 ~ 170 DEG C, pressure be 7 ~ 8MPa, relative humidity be the vapor tight tank of 75 ~ 80% In, it is promptly restored to the state of normal temperature and pressure after heat-insulation pressure keeping 1h, puts into after taking-up and fill the compound enzyme water that mass fraction is 2% In solution, keeping aqueous temperature is 38 ~ 42 DEG C, puts it in vapor tight tank, by above-mentioned parameter bar after soaking enzymolysis 10min again Part processes, and this is a circulation, amounts to circulation operation 3 times;Containing cellulase, hemicellulose in described compound enzyme Enzyme, tannase, pectase, the weight ratio of four is 6:4:2:3;
B. the wicker after being processed by operation a is put in the acetum that mass fraction is 7%, and heating keeps solution temperature to be 50 DEG C, Immersion treatment 15min, puts it in the hydrochloric acid solution that mass fraction is 8% after taking-up, heating keeps solution temperature to be 65 DEG C, Immersion treatment 15min, puts it in the salpeter solution that mass fraction is 6% after taking-up, heating keeps solution temperature to be 70 DEG C, Immersion treatment 15min, puts in the sodium hydroxide solution that mass fraction is 8% after taking-up, heating keeps solution temperature to be 75 DEG C, Immersion treatment 15min, rinses well standby with clear water after finally taking out;
C. will operation b process after wicker put into bating liquor dries after immersion treatment 2h standby;Described bating liquor is by weighing as follows The material composition of amount part: 1 part of calcium superphosphate, 3 parts of olive oil, 1.5 parts of acrylic acid methyl ester .s, 2 parts of potassium sorbate, 1.5 parts of poly-diformazans Radical siloxane, 2 parts of polyoxyethylene lauryl ether, 70 parts of water;First wicker is carried out multiple high temp high pressure, enzymolysis processing, can be loose The organizational structure that wicker is overall, and tiny gap can be formed at wicker shallow-layer enzymolysis, and do not interfere with overall intensity, i.e. carry The high process of its pliability and bating effect, the most beneficially subsequent step, is carried out repeatedly it, different classes of soda acid the most again Processing, can effectively reduce the content of ashes in wicker, the content of ashes in wicker is about 2%, this type of material trichoderma just etc. The dependence composition of fungus existence, so reducing the viable conditions of the funguses such as trichoderma, improves the insect protected of wicker, fungicidal properties;
(3) wicker braiding:
Wicker after step (2) sofening treatment is woven, after braiding, obtains semi-finished product for standby;
(4) preservative treatment:
Weigh the material of following weight portion the most by weight: 4 parts of dimethylethanolamines, 5 parts of butyl glycol ether acetass, 3 part third Glycol butyl ether, 4 parts of sodium carboxymethyl cellulose, 3 parts of glyceryl monostearates, 8 parts of Polyethylene Glycol, 5 parts of Cacumen Platycladi extracts, 10 parts Nano zine oxide, 100 parts of water;
B. each composition in operation a is mixed jointly, obtain mixed liquor after stirring with the rotating speed of 2000 revs/min standby;
C. the semi-finished product after step (3) being processed are immersed in the mixed liquor of operation b gained, and then applying frequency is 35KHz's Ultrasound wave processes, and heating simultaneously keeps the water temperature of mixed liquor to be 50 ~ 55 DEG C, processes and takes out after 2h, place into temperature be 50 ~ It is 15 ~ 20% standby for being dried in the environment of 55 DEG C to water content;
D. will operation c process after semi-finished product put in alternating temperature case, arrange the highest temperature be 30 DEG C, lowest temperature be-10 DEG C, then from The highest temperature starts to lower the temperature with the speed of 4 DEG C per minute, when being down to lowest temperature, then heats up with the speed of 4 DEG C per minute To the highest temperature, this is a temperature varied cyclical, altogether temperature varied cyclical 4 times, i.e. obtains wicker products finished product after taking-up.
Further, the time that step (3) weaves is within 2 days.
Further, step (4) described Chinese mugwort Cacumen Platycladi extract is the water extract of Cacumen Platycladi.
There is advantages that
(1) processing semi-finished product wicker products with mixed liquor, the effective ingredient in mixed liquor is carried out with the material in wicker Combination reaction, improves the organizational structure of wicker, and the nano zine oxide of interpolation, under the effect of ultrasound wave, is well filled with soft Gap when change processes, enhances intensity and the wear resistence of entirety, and the Cacumen Platycladi extract of interpolation can assist to improve willow further The Vermins-proof mildew-proof characteristic of bar.
(2) the semi-finished product wicker products after being processed by mixed liquor is put in alternating temperature case, the intermittent warming being circulated, and utilizes Collapse effect, promote remaining effective ingredient of nano zine oxide and mixed liquor and wicker finer and close, deeper into combination, improve Its case hardness and corrosion resistant performance.
(3) collocation of the inventive method each step is scientific and reasonable, and the wicker products insect protected for preparing, mildew-resistant, corrosion resistant effect are preferable, Case hardness is higher, and compared with prior art, its case hardness can improve about 25%, uses under stronger acid-base condition, its The anticorrosion time can reach 4 ~ 5 times of original anticorrosion time, and the service life under normal service condition can extend about 30%, at height Service life under damp condition can extend more than 40%, and stability in use is preferable, and anti-deformation ability is relatively strong, and decay resistance is good, Use value is higher.
Detailed description of the invention
Embodiment 1
A kind of method promoting wicker products decay resistance, comprises the steps:
(1) wicker peeling: harvested wicker is carried out peeling operation, then puts it into the calcium chloride that mass fraction is 3.5% Soaking and washing 20min in solution, standby after being placed under the sun dry in the sun with clear water after being finally drawn off rinsing well 1 ~ 2 day;
(2) sofening treatment:
A. the wicker after dry in the sun is put into temperature be 165 DEG C, pressure be 8MPa, relative humidity be 78 ~ 80% vapor tight tank in, protect It is promptly restored to the state of normal temperature and pressure after temperature pressurize 1h, puts into after taking-up and fill the compound enzyme aqueous solution that mass fraction is 2% In, keeping aqueous temperature is 38 DEG C, puts it in vapor tight tank again, carry out by above-mentioned parameter condition after soaking enzymolysis 10min Processing, this is a circulation, amounts to circulation operation 3 times;Containing cellulase, hemicellulase, list in described compound enzyme Peaceful enzyme, pectase, the weight ratio of four is 6:4:2:3;
B. the wicker after being processed by operation a is put in the acetum that mass fraction is 7%, and heating keeps solution temperature to be 50 DEG C, Immersion treatment 15min, puts it in the hydrochloric acid solution that mass fraction is 8% after taking-up, heating keeps solution temperature to be 65 DEG C, Immersion treatment 15min, puts it in the salpeter solution that mass fraction is 6% after taking-up, heating keeps solution temperature to be 70 DEG C, Immersion treatment 15min, puts in the sodium hydroxide solution that mass fraction is 8% after taking-up, heating keeps solution temperature to be 75 DEG C, Immersion treatment 15min, rinses well standby with clear water after finally taking out;
C. will operation b process after wicker put into bating liquor dries after immersion treatment 2h standby;Described bating liquor is by weighing as follows The material composition of amount part: 1 part of calcium superphosphate, 3 parts of olive oil, 1.5 parts of acrylic acid methyl ester .s, 2 parts of potassium sorbate, 1.5 parts of poly-diformazans Radical siloxane, 2 parts of polyoxyethylene lauryl ether, 70 parts of water;
(3) wicker braiding:
Wicker after step (2) sofening treatment is woven, after braiding, obtains semi-finished product for standby;
(4) preservative treatment:
Weigh the material of following weight portion the most by weight: 4 parts of dimethylethanolamines, 5 parts of butyl glycol ether acetass, 3 part third Glycol butyl ether, 4 parts of sodium carboxymethyl cellulose, 3 parts of glyceryl monostearates, 8 parts of Polyethylene Glycol, 5 parts of Cacumen Platycladi extracts, 10 parts Nano zine oxide, 100 parts of water;
B. each composition in operation a is mixed jointly, obtain mixed liquor after stirring with the rotating speed of 2000 revs/min standby;
C. the semi-finished product after step (3) being processed are immersed in the mixed liquor of operation b gained, and then applying frequency is 35KHz's Ultrasound wave processes, and heating simultaneously keeps the water temperature of mixed liquor to be 53 DEG C, takes out after processing 2h, and placing into temperature is 55 DEG C It is 18 ~ 20% standby for being dried in environment to water content;
D. will operation c process after semi-finished product put in alternating temperature case, arrange the highest temperature be 30 DEG C, lowest temperature be-10 DEG C, then from The highest temperature starts to lower the temperature with the speed of 4 DEG C per minute, when being down to lowest temperature, then heats up with the speed of 4 DEG C per minute To the highest temperature, this is a temperature varied cyclical, altogether temperature varied cyclical 4 times, i.e. obtains wicker products finished product after taking-up.
Further, the time that step (3) weaves is within 2 days.
Further, step (4) described Chinese mugwort Cacumen Platycladi extract is the water extract of Cacumen Platycladi.
Comparative example 1
This comparative example 1 compared with Example 1, in preservative treatment step, does not contains nanometer in the mixed liquor composition of preparation Zinc oxide, method step in addition is the most identical.
Comparative example 2
This comparative example 2 compared with Example 1, in preservative treatment step, does not carry out operating d, method step in addition The most identical.
Matched group
Existing wicker products processing method.
In order to contrast using effect of the present invention, will process by above-mentioned four kinds of methods respectively with a collection of wicker product, enter The humidity mycete test experiments that row is special, specific as follows: the wicker products after processing is respectively put in proof box, Control experiment Temperature in case is 30 DEG C, normal pressure, and relative humidity is 100%, be inoculated with in proof box Trichoderma viride, aspergillus niger, aspergillus terreus, Green ochre penicillium sp and white rake teeth bacterium, statistics by fungal infection area by 5% time total duration of being experienced, represent with mildew-resistant duration, weigh Amount anti-mold effect;The case hardness of the wicker products after processing above-mentioned four kinds of methods is tested;At above-mentioned four kinds of methods Wicker products after reason carries out special alkaline test experiments, specific as follows: the wicker products after above-mentioned four kinds of methods being processed It is respectively put into immersion treatment in the sodium bicarbonate solution that concentration is 80g/L, adds up time when its pimple area reaches 3%, with This weighs decay resistance, and following table is the correction data of three experiments:
Embodiment 1 Comparative example 1 Comparative example 2 Matched group
Mildew-resistant duration (my god) 125 95 103 63
Case hardness 4H 3H 4H 2H
Corrosion resistant duration (h) 7 4.6 5.5 1.5

Claims (3)

1. the method promoting wicker products decay resistance, it is characterised in that comprise the steps:
(1) wicker peeling: harvested wicker is carried out peeling operation, then puts it into the calcium chloride that mass fraction is 3.5% Soaking and washing 20min in solution, standby after being placed under the sun dry in the sun with clear water after being finally drawn off rinsing well 1 ~ 2 day;
(2) sofening treatment:
A. the wicker after dry in the sun is put into temperature be 160 ~ 170 DEG C, pressure be 7 ~ 8MPa, relative humidity be the vapor tight tank of 75 ~ 80% In, it is promptly restored to the state of normal temperature and pressure after heat-insulation pressure keeping 1h, puts into after taking-up and fill the compound enzyme water that mass fraction is 2% In solution, keeping aqueous temperature is 38 ~ 42 DEG C, puts it in vapor tight tank, by above-mentioned parameter bar after soaking enzymolysis 10min again Part processes, and this is a circulation, amounts to circulation operation 3 times;Containing cellulase, hemicellulose in described compound enzyme Enzyme, tannase, pectase, the weight ratio of four is 6:4:2:3;
B. the wicker after being processed by operation a is put in the acetum that mass fraction is 7%, and heating keeps solution temperature to be 50 DEG C, Immersion treatment 15min, puts it in the hydrochloric acid solution that mass fraction is 8% after taking-up, heating keeps solution temperature to be 65 DEG C, Immersion treatment 15min, puts it in the salpeter solution that mass fraction is 6% after taking-up, heating keeps solution temperature to be 70 DEG C, Immersion treatment 15min, puts in the sodium hydroxide solution that mass fraction is 8% after taking-up, heating keeps solution temperature to be 75 DEG C, Immersion treatment 15min, rinses well standby with clear water after finally taking out;
C. will operation b process after wicker put into bating liquor dries after immersion treatment 2h standby;Described bating liquor is by weighing as follows The material composition of amount part: 1 part of calcium superphosphate, 3 parts of olive oil, 1.5 parts of acrylic acid methyl ester .s, 2 parts of potassium sorbate, 1.5 parts of poly-diformazans Radical siloxane, 2 parts of polyoxyethylene lauryl ether, 70 parts of water;
(3) wicker braiding:
Wicker after step (2) sofening treatment is woven, after braiding, obtains semi-finished product for standby;
(4) preservative treatment:
Weigh the material of following weight portion the most by weight: 4 parts of dimethylethanolamines, 5 parts of butyl glycol ether acetass, 3 part third Glycol butyl ether, 4 parts of sodium carboxymethyl cellulose, 3 parts of glyceryl monostearates, 8 parts of Polyethylene Glycol, 5 parts of Cacumen Platycladi extracts, 10 parts Nano zine oxide, 100 parts of water;
B. each composition in operation a is mixed jointly, obtain mixed liquor after stirring with the rotating speed of 2000 revs/min standby;
C. the semi-finished product after step (3) being processed are immersed in the mixed liquor of operation b gained, and then applying frequency is 35KHz's Ultrasound wave processes, and heating simultaneously keeps the water temperature of mixed liquor to be 50 ~ 55 DEG C, processes and takes out after 2h, place into temperature be 50 ~ It is 15 ~ 20% standby for being dried in the environment of 55 DEG C to water content;
D. will operation c process after semi-finished product put in alternating temperature case, arrange the highest temperature be 30 DEG C, lowest temperature be-10 DEG C, then from The highest temperature starts to lower the temperature with the speed of 4 DEG C per minute, when being down to lowest temperature, then heats up with the speed of 4 DEG C per minute To the highest temperature, this is a temperature varied cyclical, altogether temperature varied cyclical 4 times, i.e. obtains wicker products finished product after taking-up.
A kind of method promoting wicker products decay resistance the most according to claim 1, it is characterised in that step (3) The time of braiding is within 2 days.
A kind of method promoting wicker products decay resistance the most according to claim 1, it is characterised in that step (4) Described Chinese mugwort Cacumen Platycladi extract is the water extract of Cacumen Platycladi.
CN201610551270.0A 2016-07-13 2016-07-13 A kind of method for lifting wicker products decay resistance Active CN106182248B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610551270.0A CN106182248B (en) 2016-07-13 2016-07-13 A kind of method for lifting wicker products decay resistance

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610551270.0A CN106182248B (en) 2016-07-13 2016-07-13 A kind of method for lifting wicker products decay resistance

Publications (2)

Publication Number Publication Date
CN106182248A true CN106182248A (en) 2016-12-07
CN106182248B CN106182248B (en) 2018-01-23

Family

ID=57477368

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610551270.0A Active CN106182248B (en) 2016-07-13 2016-07-13 A kind of method for lifting wicker products decay resistance

Country Status (1)

Country Link
CN (1) CN106182248B (en)

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107127854A (en) * 2017-05-18 2017-09-05 阜南县星光工艺品有限公司 A kind of softening method of bark
CN107297803A (en) * 2017-05-18 2017-10-27 阜南县星光工艺品有限公司 A kind of softening mold-proof method of timber
CN107379176A (en) * 2017-09-07 2017-11-24 阜南县大自然工艺品有限公司 A kind of method of modifying of anti-corrosion crack resistence American elm plank
CN107457860A (en) * 2017-09-08 2017-12-12 安徽嘉美工艺品有限公司 A kind of high-quality colouring method of tables and chairs
CN107639708A (en) * 2017-10-10 2018-01-30 天津主流科技有限公司 A kind of softening method of bamboo fibre
CN108608543A (en) * 2018-04-24 2018-10-02 阜南县宇翔工艺品有限公司 A kind of wicker products novel mildew resistant method
CN108724400A (en) * 2018-05-31 2018-11-02 阜南县明强柳编工艺品有限公司 A kind of wicker products fungus-proof antisepsis treatment process
CN108748532A (en) * 2018-06-08 2018-11-06 阜南县永盛工艺品有限公司 A kind of dyeing treatment of levant cotton exocarp
CN108945804A (en) * 2018-04-21 2018-12-07 阜南县明强柳编工艺品有限公司 It is a kind of for holding the preparation method of the damping woven basket of eggs
CN111941566A (en) * 2020-08-11 2020-11-17 阜南县德盛隆工艺家具有限公司 Method for manufacturing wicker handicraft

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104400857A (en) * 2014-10-29 2015-03-11 阜南县宏泰工艺品有限公司 Processing technology of willow branch for willow artworks
CN104441131A (en) * 2014-11-04 2015-03-25 安徽阜南县万家和工艺品有限公司 Method for anticorrosive treatment of willow twigs
CN104441155A (en) * 2014-09-25 2015-03-25 阜南县猛发工艺品有限公司 Rattan treatment method
CN104488991A (en) * 2014-11-04 2015-04-08 安徽阜南县万家和工艺品有限公司 Anticorrosion reagent for processing wicker
CN104526801A (en) * 2014-12-08 2015-04-22 阜南佳利工艺品有限公司 Wicker treatment method
CN104589439A (en) * 2014-12-09 2015-05-06 安徽省阜南志峰工艺品有限公司 Mildew-resistant insect-preventing processing method for wicker
CN104924380A (en) * 2015-05-29 2015-09-23 阜南县猛发工艺品有限公司 Wicker mould and moth preventing treatment method
CN104960052A (en) * 2015-05-28 2015-10-07 阜南县金威工艺品有限公司 Wicker softening method
CN105599082A (en) * 2015-12-24 2016-05-25 安吉汉洲生物科技有限公司 Multifunctional preservative

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104441155A (en) * 2014-09-25 2015-03-25 阜南县猛发工艺品有限公司 Rattan treatment method
CN104400857A (en) * 2014-10-29 2015-03-11 阜南县宏泰工艺品有限公司 Processing technology of willow branch for willow artworks
CN104441131A (en) * 2014-11-04 2015-03-25 安徽阜南县万家和工艺品有限公司 Method for anticorrosive treatment of willow twigs
CN104488991A (en) * 2014-11-04 2015-04-08 安徽阜南县万家和工艺品有限公司 Anticorrosion reagent for processing wicker
CN104526801A (en) * 2014-12-08 2015-04-22 阜南佳利工艺品有限公司 Wicker treatment method
CN104589439A (en) * 2014-12-09 2015-05-06 安徽省阜南志峰工艺品有限公司 Mildew-resistant insect-preventing processing method for wicker
CN104960052A (en) * 2015-05-28 2015-10-07 阜南县金威工艺品有限公司 Wicker softening method
CN104924380A (en) * 2015-05-29 2015-09-23 阜南县猛发工艺品有限公司 Wicker mould and moth preventing treatment method
CN105599082A (en) * 2015-12-24 2016-05-25 安吉汉洲生物科技有限公司 Multifunctional preservative

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107127854A (en) * 2017-05-18 2017-09-05 阜南县星光工艺品有限公司 A kind of softening method of bark
CN107297803A (en) * 2017-05-18 2017-10-27 阜南县星光工艺品有限公司 A kind of softening mold-proof method of timber
CN107127854B (en) * 2017-05-18 2018-11-23 阜南县星光工艺品有限公司 A kind of softening method of bark
CN107379176A (en) * 2017-09-07 2017-11-24 阜南县大自然工艺品有限公司 A kind of method of modifying of anti-corrosion crack resistence American elm plank
CN107457860A (en) * 2017-09-08 2017-12-12 安徽嘉美工艺品有限公司 A kind of high-quality colouring method of tables and chairs
CN107457860B (en) * 2017-09-08 2018-12-21 安徽嘉美工艺品有限公司 A kind of high-quality colouring method of tables and chairs
CN107639708A (en) * 2017-10-10 2018-01-30 天津主流科技有限公司 A kind of softening method of bamboo fibre
CN108945804A (en) * 2018-04-21 2018-12-07 阜南县明强柳编工艺品有限公司 It is a kind of for holding the preparation method of the damping woven basket of eggs
CN108608543A (en) * 2018-04-24 2018-10-02 阜南县宇翔工艺品有限公司 A kind of wicker products novel mildew resistant method
CN108724400A (en) * 2018-05-31 2018-11-02 阜南县明强柳编工艺品有限公司 A kind of wicker products fungus-proof antisepsis treatment process
CN108748532A (en) * 2018-06-08 2018-11-06 阜南县永盛工艺品有限公司 A kind of dyeing treatment of levant cotton exocarp
CN111941566A (en) * 2020-08-11 2020-11-17 阜南县德盛隆工艺家具有限公司 Method for manufacturing wicker handicraft

Also Published As

Publication number Publication date
CN106182248B (en) 2018-01-23

Similar Documents

Publication Publication Date Title
CN106182248A (en) A kind of method promoting wicker products decay resistance
CN106003333A (en) Wicker product anti-pest and anti-mildew method capable of enhancing wicker knitting capacity
CN106182297A (en) A kind of method improving wicker products hardness
CN106182271A (en) A kind of processing method of wicker mildew and insect proof
CN101476164B (en) Method for processing oil palm fiber
CN106182241B (en) A kind of wicker for being used to weave does old antique imitation process
CN104029260A (en) Bamboo skin treating agent for wickers
CN107042566B (en) A kind of softening barking method of purple willow
CN110772597A (en) Nine-steaming and nine-sun characteristic processing technology for polygonatum kingianum
CN107932671A (en) A kind of processing method of rattan plaited rattan
CN104441159A (en) Reed processing method
CN107150390A (en) A kind of sofening treatment method of wicker
CN106182300A (en) A kind of processing method of mulberry shoot baskets craft
CN104441123A (en) Rattan processing method for willow artworks
CN105986475A (en) Antibacterial real silk scarf and manufacturing method
KR20170036170A (en) A natural dyeing method of fabric for increasing color fastness and the natural dyeing fabric
CN107263646A (en) A kind of drying Bracking-resistant method of rattan
CN105459243B (en) A kind of processing method with white rot bacterial plaque China fir Furniture panel
CN107471345A (en) A kind of preparation method of antibacterial and mouldproof raw bamboo handicraft
CN104308926A (en) Wicker treating agent
CN107351210A (en) A kind of method for extending willow-plaited process product service life
CN106217551A (en) A kind of bleaching processes weaving straw
CN107740194A (en) A kind of microbiological degumming method of corn wrapper fibre
CN108858561A (en) A method of prevent timber from going mouldy
CN105421041A (en) Method for producing washable antibacterial pure cotton cloth

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: Method for improving corrosion resistance of wicker products

Effective date of registration: 20190906

Granted publication date: 20180123

Pledgee: Funan SME financing Company limited by guarantee

Pledgor: FUNAN COUNTY MENGFA ARTS & CRAFTS CO., LTD.

Registration number: Y2019340000047

PE01 Entry into force of the registration of the contract for pledge of patent right