CN106109263A - A kind of Longaacting fragrance-aretaining east floral type perfume and preparation method thereof - Google Patents
A kind of Longaacting fragrance-aretaining east floral type perfume and preparation method thereof Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A—HUMAN NECESSITIES
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/34—Alcohols
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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Abstract
One Longaacting fragrance-aretaining east of the present invention floral type perfume, calculates according to mass percent, east bouquet type composition by 10% 30%, the modified dextrins of 5% 20%, 10% 30%；Deionized water, the antioxidant of 0.1% 1%, the first ethanol composition of surplus.Additionally provide the preparation method of above-mentioned Longaacting fragrance-aretaining east floral type perfume, add modified dextrins in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in aqueous phase；East bouquet type composition is added drop-wise in the modified dextrins dispersion liquid of gained, continues stirring, make essence be uniformly dispersed, obtain the east floral type slow release essence of Longaacting fragrance-aretaining；Being added to by second ethanol in the east floral type slow release essence of Longaacting fragrance-aretaining, continue to stir, add antioxidant, stirring and dissolving, through being aged, be filtrated to get the east floral type perfume of Longaacting fragrance-aretaining.The east floral type perfume fragrance of the Longaacting fragrance-aretaining that the present invention obtains is fine and smooth, and lasting is lasting.
Description
Technical field
The invention belongs to household chemicals field, relate to a kind of perfume, specifically a kind of Longaacting fragrance-aretaining east floral type perfume
And preparation method thereof.
Background technology
Along with improving constantly of the development in epoch, the progress of science, human material and culture life, as the perfume (or spice) of cosmetics
Water is quickly developed.Perfume can be divided mainly into three kinds of different forms, i.e. alcohol liquid, emulsion and pulpous state liquid, generally speaking
Perfume is formulated by spice and solvent institute, and solvent used is mainly ethanol, according to essence fragrance used by perfume not
With, perfume is also classified into multiple odor type.Perfume fragrance is strong, and Main Function is to be sprayed on the hem, handkerchief and hair decorations, gives out happy people
Fragrance, for make up necessary.
The aroma quality of essence is the principal element of perfume quality, and the design of perfume essence odor type and type selecting are perfume
Crucial.Traditional perfume is the mixture of essence and ethanol, and essence is by having volatile multiple spice in note ratio group
The mixture become, volatile during directly use, fragrance remaining time is short, therefore, the design of perfume fragrance odor type and having
The development of the essence of Longaacting fragrance-aretaining has very important significance.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of Longaacting fragrance-aretaining east floral type perfume and
Its preparation method, described this Longaacting fragrance-aretaining east floral type perfume and preparation method thereof to solve perfume of the prior art
The technical problem that fragrance remaining time is short.
The invention provides a kind of Longaacting fragrance-aretaining east floral type perfume, count by weight percentage, the composition of its raw material
And content is as follows:
East bouquet type composition 10%-30%；
Modified dextrins 5%-20%；
Deionized water 10%-30%；
Antioxidant 0.1%-1%；
Surplus is the first ethanol；
Described east bouquet type composition, count by weight percentage, its composition and content are as follows:
Australene 0.01%-0.03%；
Nopinene 0.02%-0.05%；
Sabinene 0.02%-0.1%；
Myrcene 0.1%-0.3%；
Limonene 0.1%-1%；
Terpinene 0.1%-0.3%；
Folic alcohol 0.01%-0.1%；
Dihydromyrcenol 0.4%-1.4%；
Leaf Acetate 0.001%-0.01%；
Linalyl acetate 1%-3%；
Carbitol 0.005%-0.06%；
Caryophyllene 0.005%-0.01%；
Strange China ketone 0.01%-0.1%；
Linalool 1%-5%；
Patchoulene 0.01%-0.1%；
Tetrahydrogeraniol 0.01%-0.05%；
Terpineol 0.1%-0.5%；
Phenethyl acetate 0.02%-0.2%；
Guaiene 0.05%-0.15%；
Geranyl acetate 0.1%-0.5%；
Citronellol 0.1%-0.6%；
Lilestralis 1%-6%；
First position damascone 0.01%-0.04%；
Second position dihydroionone 1%-4%；
Geraniol 0.1%-0.6%；
Trans-to Herba Menthae-2-alkene 0.1%-1.5%；
Third ionoionone 0.2%-1.2%；
Second position isomethyl ionone 0.01%-0.06%；
Butanoic acid dimethylbenzyl base ester 0.1%-0.6%；
Phenethanol 0.1%-0.4%；
Hydroxycitronellal 0.1%-1%；
Cyclamen aldehyde 0.05%-0.5%；
Isopropyl myristate 1%-4%；
Anisic aldehyde 0.1%-0.6%；
Ambrotone 1%-4%；
Isoamyl salicylate 0.1%-0.6%；
Phenethyl isobutyrate,phenylethyl isobutyrate 0.1%-0.6%；
Third selinene 0.01%-0.05%；
Ambrox 0.1%-1%；
Santalol 0.01%-0.1%；
Patchouli alcohol 0.1%-0.6%；
Hydroxycitronellol 0.01%-0.12%；
Vertofix coeur 0.4%-1.4%；
Dibutyl sebacate 0.1%-1%；
Pentadacanolide 1%-5%；
Muscone 0.1%-0.6%；
MDJ 10%-25%；
Eugenol 0.1%-0.4%；
First position hexyl cinnamic aldehyde 0.2%-1.2%；
Galaxolid 2%-8%；
Certain herbaceous plants with big flowers seed Moschus 0.5%-1.5%；
Helional 0.3%-1.3%；
Triethyl citrate 0.3%-0.8%；
LYRAL 0.1%-0.7%；
Ethyl vanillin 0.05%-0.2%；
Vanillin 0.1%-0.4%；
OctMet 1%-3%；
Astrotone 15%-30%；
Salicylic acid benzyl ester 0.01%-0.06%；
Surplus is the second ethanol.
Further, described modified dextrins is a kind of derivant of starch, is a kind of commercially available prod, can be as wall
Material, is coated with essence, makes essence slowly discharge, and increases the lasting of essence.
Present invention also offers the preparation method of a kind of Longaacting fragrance-aretaining east floral type perfume stated, comprise the steps:
1) each reacting substance is weighed according to mass percent；
2) step of a preparation east bouquet type composition, by australene, nopinene, sabinene, myrcene, limonene, terpinene,
Folic alcohol, dihydromyrcenol, Leaf Acetate, linalyl acetate, carbitol, caryophyllene, strange magnificent ketone, linalool, Herba Pogostemonis
Alkene, tetrahydrogeraniol, terpineol, phenethyl acetate, guaiene, geranyl acetate, citronellol, lilestralis, Jia Wei Tujue
Ketone, second position dihydroionone, geraniol, trans-to Herba Menthae-2-alkene, third ionoionone, second position isomethyl ionone,
Butanoic acid dimethylbenzyl base ester, phenethanol, hydroxycitronellal, cyclamen aldehyde, isopropyl myristate, anisic aldehyde, ambrotone,
Isoamyl salicylate, phenethyl isobutyrate,phenylethyl isobutyrate, third selinene, ambrox, santalol, patchouli alcohol, hydroxycitronellol, first
Base cedrone, dibutyl sebacate, pentadacanolide, muscone, MDJ, eugenol, first position hexyl cinnamic aldehyde,
Galaxolid, certain herbaceous plants with big flowers seed Moschus, helional, triethyl citrate, LYRAL, ethyl vanillin, vanillin, to methoxyl group
Cinnamic acid monooctyl ester, astrotone, salicylic acid benzyl ester, the second ethanol uniformly mix and i.e. obtain east bouquet type composition；
3) add modified dextrins in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in aqueous phase
In, obtain modified dextrins dispersion liquid；
4) east bouquet type composition is added drop-wise in the modified dextrins dispersion liquid of step 3) gained, continues stirring, make essence disperse
Uniformly, and make modified dextrins form the cladding to essence molecule, obtain the east floral type slow release essence of Longaacting fragrance-aretaining；
5), in the east floral type slow release essence of the Longaacting fragrance-aretaining that the second ethanol is added to step 4) gained, continue to stir,
Adding antioxidant, stirring and dissolving, through being aged, be filtrated to get the east floral type perfume of Longaacting fragrance-aretaining.
Present invention also offers a kind of east bouquet type composition, count by weight percentage, its composition and content are as follows:
Australene 0.01%-0.03%；
Nopinene 0.02%-0.05%；
Sabinene 0.02%-0.1%；
Myrcene 0.1%-0.3%；
Limonene 0.1%-1%；
Terpinene 0.1%-0.3%；
Folic alcohol 0.01%-0.1%；
Dihydromyrcenol 0.4%-1.4%；
Leaf Acetate 0.001%-0.01%；
Linalyl acetate 1%-3%；
Carbitol 0.005%-0.06%；
Caryophyllene 0.005%-0.01%；
Strange China ketone 0.01%-0.1%；
Linalool 1%-5%；
Patchoulene 0.01%-0.1%；
Tetrahydrogeraniol 0.01%-0.05%；
Terpineol 0.1%-0.5%；
Phenethyl acetate 0.02%-0.2%；
Guaiene 0.05%-0.15%；
Geranyl acetate 0.1%-0.5%；
Citronellol 0.1%-0.6%；
Lilestralis 1%-6%；
First position damascone 0.01%-0.04%；
Second position dihydroionone 1%-4%；
Geraniol 0.1%-0.6%；
Trans-to Herba Menthae-2-alkene 0.1%-1.5%；
Third ionoionone 0.2%-1.2%；
Second position isomethyl ionone 0.01%-0.06%；
Butanoic acid dimethylbenzyl base ester 0.1%-0.6%；
Phenethanol 0.1%-0.4%；
Hydroxycitronellal 0.1%-1%；
Cyclamen aldehyde 0.05%-0.5%；
Isopropyl myristate 1%-4%；
Anisic aldehyde 0.1%-0.6%；
Ambrotone 1%-4%；
Isoamyl salicylate 0.1%-0.6%；
Phenethyl isobutyrate,phenylethyl isobutyrate 0.1%-0.6%；
Third selinene 0.01%-0.05%；
Ambrox 0.1%-1%；
Santalol 0.01%-0.1%；
Patchouli alcohol 0.1%-0.6%；
Hydroxycitronellol 0.01%-0.12%；
Vertofix coeur 0.4%-1.4%；
Dibutyl sebacate 0.1%-1%；
Pentadacanolide 1%-5%；
Muscone 0.1%-0.6%；
MDJ 10%-25%；
Eugenol 0.1%-0.4%；
First position hexyl cinnamic aldehyde 0.2%-1.2%；
Galaxolid 2%-8%；
Certain herbaceous plants with big flowers seed Moschus 0.5%-1.5%；
Helional 0.3%-1.3%；
Triethyl citrate 0.3%-0.8%；
LYRAL 0.1%-0.7%；
Ethyl vanillin 0.05%-0.2%；
Vanillin 0.1%-0.4%；
OctMet 1%-3%；
Astrotone 15%-30%；
Salicylic acid benzyl ester 0.01%-0.06%；
Surplus is the second ethanol.
The east fragrance of a flower is the odor type that people like, according to odor characteristic and the note of spice, chooses suitable raw material, allotment
Go out soft aroma and, fine and smooth, there is the east bouquet type composition of the fragrance of a flower rhythm of east feature；Then using modified dextrins is wall material,
The east bouquet type composition obtained is coated with, thus improves the lasting of essence；Add a certain proportion of deionized water, second
Alcohol and antioxidant (butylated hydroxytoluene), obtain the east floral type perfume of Longaacting fragrance-aretaining.
The present invention compares with prior art, and its technological progress is significant.A kind of east of the New-type long-acting lasting of the present invention
Side's floral type perfume, it is provided that a kind of exquisiteness, soft east fragrance of a flower odor type, and lasting is lasting.
Detailed description of the invention
Below by embodiment, the present invention is further described, but does not affect protection scope of the present invention.
Embodiment 1
A kind of Longaacting fragrance-aretaining east floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and content
As follows:
East bouquet type composition 10%(10g)
Modified dextrins 5% (5g)
Deionized water 10% (10g)
Antioxidant 0.1% (0.1g)
Ethanol 74.9% (74.9g)；
Above-mentioned a kind of Longaacting fragrance-aretaining east floral type perfume is prepared via a method which, this preparation process comprises the steps:
(1) add modified dextrins, in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in water
Xiang Zhong, obtains modified dextrins dispersion liquid；
(2), by east bouquet type composition it is added drop-wise in the modified dextrins dispersion liquid of step (1) gained, continues stirring, make essence divide
Dissipate uniformly, and make modified dextrins form the cladding to essence molecule, obtain the east floral type slow release essence of Longaacting fragrance-aretaining.
(3), in the east floral type slow release essence of the Longaacting fragrance-aretaining, by ethanol being added to step (2) gained, stirring is continued all
Even, add antioxidant, stirring and dissolving, through being aged, be filtrated to get the east floral type perfume of Longaacting fragrance-aretaining.This perfume has
The odor characteristic of the east fragrance of a flower, the clear rhythm of the fragrance of a flower lays particular stress on, and aroma strength is the most weak.This perfume is general with prepared by uncoated essence
Logical perfume carries out sensory evaluation by Wen Xiangzhi, and this perfume still can feel obvious fragrance after 10 days, and common perfume is several after 2 days
Just it is not felt by fragrance.
Above-mentioned east bouquet type composition, it is characterised in that described east bouquet type composition count by weight percentage,
Its composition and content are as follows:
Australene 0.01% (0.01g)
Nopinene 0.05% (0.05g)
Sabinene 0.02% (0.02g)
Myrcene 0.3% (0.3g)
Limonene 0.1% (0.1g)
Terpinene 0.3% (0.3g)
Folic alcohol 0.01% (0.01g)
Dihydromyrcenol 1.4% (1.4g)
Leaf Acetate 0.001% (0.001g)
Linalyl acetate 3% (3g)
Carbitol 0.005% (0.005g)
Caryophyllene 0.01% (0.01g)
Strange China's ketone 0.01% (0.01g)
Linalool 5% (5g)
Patchoulene 0.01% (0.01g)
Tetrahydrogeraniol 0.05% (0.05g)
Terpineol 0.1% (0.1g)
Phenethyl acetate 0.2% (0.2g)
Guaiene 0.05% (0.05g)
Geranyl acetate 0.5% (0.5g)
Citronellol 0.1% (0.1g)
Lilestralis 6% (6g)
First position damascone 0.01% (0.01g)
Second position dihydroionone 4% (4g)
Geraniol 0.1% (0.1g)
Trans-to Herba Menthae-2-alkene 1.5% (1.5g)
Third ionoionone 0.2% (0.2g)
Second position isomethyl ionone 0.06% (0.06g)
Butanoic acid dimethylbenzyl base ester 0.1% (0.1g)
Phenethanol 0.4% (0.4g)
Hydroxycitronellal 0.1% (0.1g)
Cyclamen aldehyde 0.5% (0.5g)
Isopropyl myristate 1% (1g)
Anisic aldehyde 0.6% (0.6g)
Ambrotone 1% (1g)
Isoamyl salicylate 0.6% (0.6g)
Phenethyl isobutyrate,phenylethyl isobutyrate 0.1% (0.1g)
Third selinene 0.05% (0.05g)
Ambrox 0.1% (0.1g)
Santalol 0.1% (0.1g)
Patchouli alcohol 0.1% (0.1g)
Hydroxycitronellol 0.12% (0.12g)
Vertofix coeur 0.4% (0.4g)
Dibutyl sebacate 1% (1g)
Pentadacanolide 5% (5g)
Muscone 0.1% (0.1g)
MDJ 25% (25g)
Eugenol 0.1% (0.1g)
First position hexyl cinnamic aldehyde 1.2% (1.2g)
Galaxolid 2% (2g)
Certain herbaceous plants with big flowers seed Moschus 1.5% (1.5g)
Helional 0.3% (0.3g)
Triethyl citrate 0.8% (0.8g)
LYRAL 0.1% (0.1g)
Ethyl vanillin 0.2% (0.2g)
Vanillin 0.1% (0.1g)
OctMet 3% (3g)
Astrotone 15% (15g)
Salicylic acid benzyl ester 0.06% (0.06g)
Ethanol 16.174% (16.174g)；
Above-mentioned east bouquet type composition is prepared by method to be prepared, and its preparation process specifically includes following steps:
By australene, nopinene, sabinene, myrcene, limonene, terpinene, folic alcohol, dihydromyrcenol, Leaf Acetate,
Linalyl acetate, carbitol, caryophyllene, strange China ketone, linalool, patchoulene, tetrahydrogeraniol, terpineol, phenethyl acetate,
Guaiene, geranyl acetate, citronellol, lilestralis, first position damascone, second position dihydroionone, geraniol, trans-right
Herba Menthae-2-alkene, third ionoionone, second position isomethyl ionone, butanoic acid dimethylbenzyl base ester, phenethanol, hydroxyl Herba Cymbopogonis Citrari
Aldehyde, cyclamen aldehyde, isopropyl myristate, anisic aldehyde, ambrotone, isoamyl salicylate, phenethyl isobutyrate,phenylethyl isobutyrate, third celery
Alkene, ambrox, santalol, patchouli alcohol, hydroxycitronellol, vertofix coeur, dibutyl sebacate, pentadacanolide,
Muscone, MDJ, eugenol, first position hexyl cinnamic aldehyde, galaxolid, certain herbaceous plants with big flowers seed Moschus, helional, Fructus Citri Limoniae
Triethylenetetraminehexaacetic acid ester, LYRAL, ethyl vanillin, vanillin, OctMet, astrotone, salicylic acid benzyl ester, ethanol are equal
Even mixing i.e. obtains east bouquet type composition.The essence fragrance obtained is fine and smooth, and the clear rhythm of the fragrance of a flower is laid particular stress on, and has the feature of the east fragrance of a flower
Fragrance.
Embodiment 2
A kind of Longaacting fragrance-aretaining east floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and content
As follows:
East bouquet type composition 30% (30g)
Modified dextrins 12% (12g)
Deionized water 15% (15g)
Antioxidant 1% (1g)
Ethanol 39% (39g)；
Above-mentioned a kind of Longaacting fragrance-aretaining east floral type perfume is prepared via a method which, this preparation process comprises the steps:
(1) add modified dextrins, in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in water
Xiang Zhong, obtains modified dextrins dispersion liquid；
(2), by east bouquet type composition it is added drop-wise in the modified dextrins dispersion liquid of step (1) gained, continues stirring, make essence divide
Dissipate uniformly, and make modified dextrins form the cladding to essence molecule, obtain the east floral type slow release essence of Longaacting fragrance-aretaining.
(3), in the east floral type slow release essence of the Longaacting fragrance-aretaining, by ethanol being added to step (2) gained, stirring is continued all
Even, add antioxidant, stirring and dissolving, through being aged, be filtrated to get the east floral type perfume of Longaacting fragrance-aretaining.This perfume has
The odor characteristic of the east fragrance of a flower, animal note lays particular stress on, and aroma strength is the strongest.This perfume is general with prepared by uncoated essence
Logical perfume carries out sensory evaluation by Wen Xiangzhi, and this perfume still can feel obvious fragrance after 15 days, and common perfume is several after 2 days
Just it is not felt by fragrance.
Above-mentioned east bouquet type composition, it is characterised in that described east bouquet type composition count by weight percentage,
Its composition and content are as follows:
Australene 0.03% (0.03g)
Nopinene 0.02% (0.02g)
Sabinene 0.1% (0.1g)
Myrcene 0.1% (0.1g)
Limonene 1% (1g)
Terpinene 0.1% (0.1g)
Folic alcohol 0.1% (0.1g)
Dihydromyrcenol 0.4% (0.4g)
Leaf Acetate 0.01% (0.01g)
Linalyl acetate 1% (1g)
Carbitol 0.06% (0.06g)
Caryophyllene 0.005% (0.005g)
Strange China's ketone 0.1% (0.1g)
Linalool 1% (1g)
Patchoulene 0.1% (0.1g)
Tetrahydrogeraniol 0.01% (0.01g)
Terpineol 0.5% (0.5g)
Phenethyl acetate 0.02% (0.02g)
Guaiene 0.15% (0.15g)
Geranyl acetate 0.1% (0.1g)
Citronellol 0.6% (0.6g)
Lilestralis 1% (1g)
First position damascone 0.04% (0.04g)
Second position dihydroionone 1% (1g)
Geraniol 0.6% (0.6g)
Trans-to Herba Menthae-2-alkene 0.1% (0.1g)
Third ionoionone 1.2% (1.2g)
Second position isomethyl ionone 0.01% (0.01g)
Butanoic acid dimethylbenzyl base ester 0.6% (0.6g)
Phenethanol 0.1% (0.1g)
Hydroxycitronellal 1% (1g)
Cyclamen aldehyde 0.05% (0.05g)
Isopropyl myristate 4% (4g)
Anisic aldehyde 0.1% (0.1g)
Ambrotone 4% (4g)
Isoamyl salicylate 0.1% (0.1g)
Phenethyl isobutyrate,phenylethyl isobutyrate 0.6% (0.6g)
Third selinene 0.01% (0.01g)
Ambrox 1% (1g)
Santalol 0.01% (0.01g)
Patchouli alcohol 0.6% (0.6g)
Hydroxycitronellol 0.01% (0.01g)
Vertofix coeur 1.4% (1.4g)
Dibutyl sebacate 0.1% (0.1g)
Pentadacanolide 1% (1g)
Muscone 0.6% (0.6g)
MDJ 10% (10g)
Eugenol 0.4% (0.4g)
First position hexyl cinnamic aldehyde 0.2% (0.2g)
Galaxolid 8% (8g)
Certain herbaceous plants with big flowers seed Moschus 0.5% (0.5g)
Helional 1.3% (1.3g)
Triethyl citrate 0.3% (0.3g)
LYRAL 0.7% (0.7g)
Ethyl vanillin 0.05% (0.05g)
Vanillin 0.4% (0.4g)
OctMet 1% (1g)
Astrotone 30% (30g)
Salicylic acid benzyl ester 0.01% (0.01g)
Ethanol 22.405% (22.405g)；
Above-mentioned east bouquet type composition is prepared by method to be prepared, and its preparation process specifically includes following steps:
By australene, nopinene, sabinene, myrcene, limonene, terpinene, folic alcohol, dihydromyrcenol, Leaf Acetate,
Linalyl acetate, carbitol, caryophyllene, strange China ketone, linalool, patchoulene, tetrahydrogeraniol, terpineol, phenethyl acetate,
Guaiene, geranyl acetate, citronellol, lilestralis, first position damascone, second position dihydroionone, geraniol, trans-right
Herba Menthae-2-alkene, third ionoionone, second position isomethyl ionone, butanoic acid dimethylbenzyl base ester, phenethanol, hydroxyl Herba Cymbopogonis Citrari
Aldehyde, cyclamen aldehyde, isopropyl myristate, anisic aldehyde, ambrotone, isoamyl salicylate, phenethyl isobutyrate,phenylethyl isobutyrate, third celery
Alkene, ambrox, santalol, patchouli alcohol, hydroxycitronellol, vertofix coeur, dibutyl sebacate, pentadacanolide,
Muscone, MDJ, eugenol, first position hexyl cinnamic aldehyde, galaxolid, certain herbaceous plants with big flowers seed Moschus, helional, Fructus Citri Limoniae
Triethylenetetraminehexaacetic acid ester, LYRAL, ethyl vanillin, vanillin, OctMet, astrotone, salicylic acid benzyl ester, ethanol are equal
Even mixing i.e. obtains east bouquet type composition.The essence fragrance obtained is fine and smooth, and animal note is laid particular stress on, and has the feature of the east fragrance of a flower
Fragrance.
Embodiment 3
A kind of Longaacting fragrance-aretaining east floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and content
As follows:
East bouquet type composition 15% (15g)
Modified dextrins 20% (20g)
Deionized water 30% (30g)
Antioxidant 0.5% (0.5g)
Ethanol 34.5% (34.5g)；
Above-mentioned a kind of Longaacting fragrance-aretaining east floral type perfume is prepared via a method which, this preparation process comprises the steps:
(1) add modified dextrins, in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in water
Xiang Zhong, obtains modified dextrins dispersion liquid；
(2), by east bouquet type composition it is added drop-wise in the modified dextrins dispersion liquid of step (1) gained, continues stirring, make essence divide
Dissipate uniformly, and make modified dextrins form the cladding to essence molecule, obtain the east floral type slow release essence of Longaacting fragrance-aretaining.
(3), in the east floral type slow release essence of the Longaacting fragrance-aretaining, by ethanol being added to step (2) gained, stirring is continued all
Even, add antioxidant, stirring and dissolving, through being aged, be filtrated to get the east floral type perfume of Longaacting fragrance-aretaining.This perfume fragrance
Moderate strength, fragrance is coordinated, is had the feature note of the east fragrance of a flower.That this perfume and uncoated essence are prepared is common fragrant
Water carries out sensory evaluation by Wen Xiangzhi, and this perfume still can feel obvious fragrance after 15 days, and common perfume after 2 days the most just
It is not felt by fragrance.
Above-mentioned east bouquet type composition, it is characterised in that described east bouquet type composition count by weight percentage,
Its composition and content are as follows:
Australene 0.02% (0.02g)
Nopinene 0.03% (0.03g)
Sabinene 0.06% (0.06g)
Myrcene 0.2% (0.2g)
Limonene 0.5% (1g)
Terpinene 0.1%-0.3% (0.5g)
Folic alcohol 0.05% (0.05g)
Dihydromyrcenol 0.9% (0.9g)
Leaf Acetate 0.005% (0.005g)
Linalyl acetate 2% (2g)
Carbitol 0.03% (0.03g)
Caryophyllene 0.007% (0.007g)
Strange China's ketone 0.05% (0.05g)
Linalool 3% (3g)
Patchoulene 0.05% (0.05g)
Tetrahydrogeraniol 0.03% (0.03g)
Terpineol 0.3% (0.3g)
Phenethyl acetate 0.1% (0.1g)
Guaiene 0.1% (0.1g)
Geranyl acetate 0.3% (0.3g)
Citronellol 0.3% (0.3g)
Lilestralis 3% (3g)
First position damascone 0.02% (0.02g)
Second position dihydroionone 2% (2g)
Geraniol 0.3% (0.3g)
Trans-to Herba Menthae-2-alkene 0.9% (0.9g)
Third ionoionone 0.8% (0.8g)
Second position isomethyl ionone 0.03% (0.03g)
Butanoic acid dimethylbenzyl base ester 0.4% (0.4g)
Phenethanol 0.2% (0.2g)
Hydroxycitronellal 0.6% (0.6g)
Cyclamen aldehyde 0.2% (0.2g)
Isopropyl myristate 2% (2g)
Anisic aldehyde 0.3% (0.3g)
Ambrotone 2% (2g)
Isoamyl salicylate 0.3% (0.3g)
Phenethyl isobutyrate,phenylethyl isobutyrate 0.4% (0.4g)
Third selinene 0.03% (0.03g)
Ambrox 0.5% (0.5g)
Santalol 0.05% (0.05g)
Patchouli alcohol 0.3% (0.3g)
Hydroxycitronellol 0.07% (0.07g)
Vertofix coeur 0.8% (0.8g)
Dibutyl sebacate 0.5% (0.5g)
Pentadacanolide 3% (3g)
Muscone 0.4% (0.4g)
MDJ 20% (20g)
Eugenol 0.2% (0.2g)
First position hexyl cinnamic aldehyde 0.6% (0.6g)
Galaxolid 5% (5g)
Certain herbaceous plants with big flowers seed Moschus 1% (1g)
Helional 0.9% (0.9g)
Triethyl citrate 0.5% (0.5g)
LYRAL 0.4% (0.4g)
Ethyl vanillin 0.1% (0.1g)
Vanillin 0.2% (0.2g)
OctMet 2% (2g)
Astrotone 20% (20g)
Salicylic acid benzyl ester 0.03% (0.03g)
Ethanol 20.938% (20.938g)；
Above-mentioned east bouquet type composition is prepared by method to be prepared, and its preparation process specifically includes following steps:
By australene, nopinene, sabinene, myrcene, limonene, terpinene, folic alcohol, dihydromyrcenol, Leaf Acetate,
Linalyl acetate, carbitol, caryophyllene, strange China ketone, linalool, patchoulene, tetrahydrogeraniol, terpineol, phenethyl acetate,
Guaiene, geranyl acetate, citronellol, lilestralis, first position damascone, second position dihydroionone, geraniol, trans-right
Herba Menthae-2-alkene, third ionoionone, second position isomethyl ionone, butanoic acid dimethylbenzyl base ester, phenethanol, hydroxyl Herba Cymbopogonis Citrari
Aldehyde, cyclamen aldehyde, isopropyl myristate, anisic aldehyde, ambrotone, isoamyl salicylate, phenethyl isobutyrate,phenylethyl isobutyrate, third celery
Alkene, ambrox, santalol, patchouli alcohol, hydroxycitronellol, vertofix coeur, dibutyl sebacate, pentadacanolide,
Muscone, MDJ, eugenol, first position hexyl cinnamic aldehyde, galaxolid, certain herbaceous plants with big flowers seed Moschus, helional, Fructus Citri Limoniae
Triethylenetetraminehexaacetic acid ester, LYRAL, ethyl vanillin, vanillin, OctMet, astrotone, salicylic acid benzyl ester, ethanol are equal
Even mixing i.e. obtains east bouquet type composition.The essence fragrance obtained is coordinated, and has the characteristic perfume of the east fragrance of a flower.
Above said content is only the basic explanation under present inventive concept, and according to appointing that technical scheme is done
What equivalent transformation, belongs to the scope of protection of the invention.
Claims (3)
1. a Longaacting fragrance-aretaining east floral type perfume, it is characterised in that count by weight percentage, the composition of its raw material and containing
Measure as follows:
East bouquet type composition 10%-30%；
Modified dextrins 5%-20%；
Deionized water 10%-30%；
Antioxidant 0.1%-1%；
Surplus is the first ethanol；
Described east bouquet type composition, count by weight percentage, its composition and content are as follows:
Australene 0.01%-0.03%；
Nopinene 0.02%-0.05%；
Sabinene 0.02%-0.1%；
Myrcene 0.1%-0.3%；
Limonene 0.1%-1%；
Terpinene 0.1%-0.3%；
Folic alcohol 0.01%-0.1%；
Dihydromyrcenol 0.4%-1.4%；
Leaf Acetate 0.001%-0.01%；
Linalyl acetate 1%-3%；
Carbitol 0.005%-0.06%；
Caryophyllene 0.005%-0.01%；
Strange China ketone 0.01%-0.1%；
Linalool 1%-5%；
Patchoulene 0.01%-0.1%；
Tetrahydrogeraniol 0.01%-0.05%；
Terpineol 0.1%-0.5%；
Phenethyl acetate 0.02%-0.2%；
Guaiene 0.05%-0.15%；
Geranyl acetate 0.1%-0.5%；
Citronellol 0.1%-0.6%；
Lilestralis 1%-6%；
First position damascone 0.01%-0.04%；
Second position dihydroionone 1%-4%；
Geraniol 0.1%-0.6%；
Trans-to Herba Menthae-2-alkene 0.1%-1.5%；
Third ionoionone 0.2%-1.2%；
Second position isomethyl ionone 0.01%-0.06%；
Butanoic acid dimethylbenzyl base ester 0.1%-0.6%；
Phenethanol 0.1%-0.4%；
Hydroxycitronellal 0.1%-1%；
Cyclamen aldehyde 0.05%-0.5%；
Isopropyl myristate 1%-4%；
Anisic aldehyde 0.1%-0.6%；
Ambrotone 1%-4%；
Isoamyl salicylate 0.1%-0.6%；
Phenethyl isobutyrate,phenylethyl isobutyrate 0.1%-0.6%；
Third selinene 0.01%-0.05%；
Ambrox 0.1%-1%；
Santalol 0.01%-0.1%；
Patchouli alcohol 0.1%-0.6%；
Hydroxycitronellol 0.01%-0.12%；
Vertofix coeur 0.4%-1.4%；
Dibutyl sebacate 0.1%-1%；
Pentadacanolide 1%-5%；
Muscone 0.1%-0.6%；
MDJ 10%-25%；
Eugenol 0.1%-0.4%；
First position hexyl cinnamic aldehyde 0.2%-1.2%；
Galaxolid 2%-8%；
Certain herbaceous plants with big flowers seed Moschus 0.5%-1.5%；
Helional 0.3%-1.3%；
Triethyl citrate 0.3%-0.8%；
LYRAL 0.1%-0.7%；
Ethyl vanillin 0.05%-0.2%；
Vanillin 0.1%-0.4%；
OctMet 1%-3%；
Astrotone 15%-30%；
Salicylic acid benzyl ester 0.01%-0.06%；
Surplus is the second ethanol.
2. the preparation method of a kind of Longaacting fragrance-aretaining east floral type perfume described in claim 1, comprises the steps:
1) each reacting substance is weighed according to mass percent；
2) step of a preparation east bouquet type composition, by australene, nopinene, sabinene, myrcene, limonene, terpinene,
Folic alcohol, dihydromyrcenol, Leaf Acetate, linalyl acetate, carbitol, caryophyllene, strange magnificent ketone, linalool, Herba Pogostemonis
Alkene, tetrahydrogeraniol, terpineol, phenethyl acetate, guaiene, geranyl acetate, citronellol, lilestralis, Jia Wei Tujue
Ketone, second position dihydroionone, geraniol, trans-to Herba Menthae-2-alkene, third ionoionone, second position isomethyl ionone,
Butanoic acid dimethylbenzyl base ester, phenethanol, hydroxycitronellal, cyclamen aldehyde, isopropyl myristate, anisic aldehyde, ambrotone,
Isoamyl salicylate, phenethyl isobutyrate,phenylethyl isobutyrate, third selinene, ambrox, santalol, patchouli alcohol, hydroxycitronellol, first
Base cedrone, dibutyl sebacate, pentadacanolide, muscone, MDJ, eugenol, first position hexyl cinnamic aldehyde,
Galaxolid, certain herbaceous plants with big flowers seed Moschus, helional, triethyl citrate, LYRAL, ethyl vanillin, vanillin, to methoxyl group
Cinnamic acid monooctyl ester, astrotone, salicylic acid benzyl ester, the second ethanol uniformly mix and i.e. obtain east bouquet type composition；
3) add modified dextrins in a reservoir, add deionized water, open stirring, make modified dextrins be uniformly dispersed in aqueous phase
In, obtain modified dextrins dispersion liquid；
4) east bouquet type composition is added drop-wise in the modified dextrins dispersion liquid of step 3) gained, continues stirring, make essence disperse
Uniformly, and make modified dextrins form the cladding to essence molecule, obtain the east floral type slow release essence of Longaacting fragrance-aretaining；
5), in the east floral type slow release essence of the Longaacting fragrance-aretaining that the second ethanol is added to step 4) gained, continue to stir,
Adding antioxidant, stirring and dissolving, through being aged, be filtrated to get the east floral type perfume of Longaacting fragrance-aretaining.
3. an east bouquet type composition, it is characterised in that count by weight percentage, its composition and content are as follows:
Australene 0.01%-0.03%；
Nopinene 0.02%-0.05%；
Sabinene 0.02%-0.1%；
Myrcene 0.1%-0.3%；
Limonene 0.1%-1%；
Terpinene 0.1%-0.3%；
Folic alcohol 0.01%-0.1%；
Dihydromyrcenol 0.4%-1.4%；
Leaf Acetate 0.001%-0.01%；
Linalyl acetate 1%-3%；
Carbitol 0.005%-0.06%；
Caryophyllene 0.005%-0.01%；
Strange China ketone 0.01%-0.1%；
Linalool 1%-5%；
Patchoulene 0.01%-0.1%；
Tetrahydrogeraniol 0.01%-0.05%；
Terpineol 0.1%-0.5%；
Phenethyl acetate 0.02%-0.2%；
Guaiene 0.05%-0.15%；
Geranyl acetate 0.1%-0.5%；
Citronellol 0.1%-0.6%；
Lilestralis 1%-6%；
First position damascone 0.01%-0.04%；
Second position dihydroionone 1%-4%；
Geraniol 0.1%-0.6%；
Trans-to Herba Menthae-2-alkene 0.1%-1.5%；
Third ionoionone 0.2%-1.2%；
Second position isomethyl ionone 0.01%-0.06%；
Butanoic acid dimethylbenzyl base ester 0.1%-0.6%；
Phenethanol 0.1%-0.4%；
Hydroxycitronellal 0.1%-1%；
Cyclamen aldehyde 0.05%-0.5%；
Isopropyl myristate 1%-4%；
Anisic aldehyde 0.1%-0.6%；
Ambrotone 1%-4%；
Isoamyl salicylate 0.1%-0.6%；
Phenethyl isobutyrate,phenylethyl isobutyrate 0.1%-0.6%；
Third selinene 0.01%-0.05%；
Ambrox 0.1%-1%；
Santalol 0.01%-0.1%；
Patchouli alcohol 0.1%-0.6%；
Hydroxycitronellol 0.01%-0.12%；
Vertofix coeur 0.4%-1.4%；
Dibutyl sebacate 0.1%-1%；
Pentadacanolide 1%-5%；
Muscone 0.1%-0.6%；
MDJ 10%-25%；
Eugenol 0.1%-0.4%；
First position hexyl cinnamic aldehyde 0.2%-1.2%；
Galaxolid 2%-8%；
Certain herbaceous plants with big flowers seed Moschus 0.5%-1.5%；
Helional 0.3%-1.3%；
Triethyl citrate 0.3%-0.8%；
LYRAL 0.1%-0.7%；
Ethyl vanillin 0.05%-0.2%；
Vanillin 0.1%-0.4%；
OctMet 1%-3%；
Astrotone 15%-30%；
Salicylic acid benzyl ester 0.01%-0.06%；
Surplus is the second ethanol.
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| CN107736375A (en) * | 2017-09-30 | 2018-02-27 | 蚌埠科卫消毒药剂有限公司 | A kind of thimerosal of floral type 84 and preparation method thereof |
| CN108866258A (en) * | 2018-06-20 | 2018-11-23 | 上海应用技术大学 | A kind of osmanthus flower fragrant leather fat and its preparation method and application |
| CN110251425A (en) * | 2019-06-19 | 2019-09-20 | 广州市珍馨香精香料有限公司 | A kind of natural essential oil fragrance perfume and preparation method thereof |
| CN111575114A (en) * | 2020-05-29 | 2020-08-25 | 广东香龙香料有限公司 | Lasting fragrance type essence and preparation method thereof |
| CN111669971A (en) * | 2018-03-20 | 2020-09-15 | 弗门尼舍有限公司 | Antimicrobial compositions |
| CN112760167A (en) * | 2020-12-15 | 2021-05-07 | 广州芬豪香精有限公司 | Oriental flower fragrance essence and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107736375A (en) * | 2017-09-30 | 2018-02-27 | 蚌埠科卫消毒药剂有限公司 | A kind of thimerosal of floral type 84 and preparation method thereof |
| CN111669971A (en) * | 2018-03-20 | 2020-09-15 | 弗门尼舍有限公司 | Antimicrobial compositions |
| CN111669971B (en) * | 2018-03-20 | 2022-03-04 | 弗门尼舍有限公司 | Antimicrobial compositions |
| CN108866258A (en) * | 2018-06-20 | 2018-11-23 | 上海应用技术大学 | A kind of osmanthus flower fragrant leather fat and its preparation method and application |
| CN108866258B (en) * | 2018-06-20 | 2021-03-05 | 上海应用技术大学 | Osmanthus-fragrance leather fatting agent and preparation method and application thereof |
| CN110251425A (en) * | 2019-06-19 | 2019-09-20 | 广州市珍馨香精香料有限公司 | A kind of natural essential oil fragrance perfume and preparation method thereof |
| CN111575114A (en) * | 2020-05-29 | 2020-08-25 | 广东香龙香料有限公司 | Lasting fragrance type essence and preparation method thereof |
| CN112760167A (en) * | 2020-12-15 | 2021-05-07 | 广州芬豪香精有限公司 | Oriental flower fragrance essence and preparation method thereof |
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