CN106106518A - A kind of compositions preventing and treating orange caterpillar and preparation method thereof - Google Patents
A kind of compositions preventing and treating orange caterpillar and preparation method thereof Download PDFInfo
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- CN106106518A CN106106518A CN201610462809.5A CN201610462809A CN106106518A CN 106106518 A CN106106518 A CN 106106518A CN 201610462809 A CN201610462809 A CN 201610462809A CN 106106518 A CN106106518 A CN 106106518A
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- parts
- fumaric acid
- zinc sulfate
- synergist
- imperialine
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/06—Unsaturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/24—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms
- A01N43/26—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings
- A01N43/28—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings with two hetero atoms in positions 1,3
- A01N43/30—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with two or more hetero atoms five-membered rings with two hetero atoms in positions 1,3 with two oxygen atoms in positions 1,3, condensed with a carbocyclic ring
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of compositions preventing and treating orange caterpillar and preparation method thereof, including the raw material of following weight portion: volution bacterium amine, 15～25 parts；Imperialine, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Totally 7～9 parts of synergist fumaric acid and zinc sulfate, the weight ratio of fumaric acid and zinc sulfate is 6～8:1.The compositions that the present invention provides can prevent and treat orange caterpillar, the pesticide of preventing and treating orange caterpillar can be developed into, prevention effect is relevant with the weight ratio of synergist fumaric acid and zinc sulfate in raw material, and when the weight ratio of fumaric acid and zinc sulfate is 6～8:1, prevention effect is best.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating orange caterpillar and preparation method thereof.
Background technology
Volution bacterium amine is sterol biosynthesis inhibitor, the main synthesis suppressing C-14 demethylation enzyme.Controlling object is little
Wheat powdery mildew and various rust, barley leaf blotch and stripe disease.The foliage fungicide of interior absorption, the most effective to powdery mildew.Make
With speed is fast and the lasting period is long, has protection therapeutical effect concurrently, both can be used alone, again can be with other fungicide compoundings to expand
Fungicidal spectrum.
Imperialine is the common alkaloid component in Liliaceae Fritillaria Linn, for its active ingredient, has treatment lung
The effects such as the few expectorant of hot cough caused by dryness, dry cough.
Have not yet to see volution bacterium amine and work in coordination with the report preventing and treating orange caterpillar with imperialine.
Summary of the invention
It is an object of the invention to provide a kind of preventing and treating orange caterpillar containing volution bacterium amine and imperialine compositions and
Its application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating orange caterpillar, including the raw material of following weight portion: volution bacterium amine, 15～25 parts；Western shellfish
Female alkali, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Totally 7～9 parts of synergist fumaric acid and zinc sulfate, rich horse
The weight ratio of acid and zinc sulfate is 6～8:1.
Further, the compositions of described preventing and treating orange caterpillar includes the raw material of following weight portion: volution bacterium amine, 20
Part；Imperialine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Totally 8 parts of synergist fumaric acid and zinc sulfate, fumaric acid and zinc sulfate
Weight ratio be 7:1.
Further, the compositions of described preventing and treating orange caterpillar includes the raw material of following weight portion: volution bacterium amine, 15
Part；Imperialine, 10 parts；Ethanol, 120 parts；Water, 440 parts；Totally 7 parts of synergist fumaric acid and zinc sulfate, fumaric acid and zinc sulfate
Weight ratio be 6:1.
Further, the compositions of described preventing and treating orange caterpillar includes the raw material of following weight portion: volution bacterium amine, 25
Part；Imperialine, 20 parts；Ethanol, 140 parts；Water, 480 parts；Totally 9 parts of synergist fumaric acid and zinc sulfate, fumaric acid and zinc sulfate
Weight ratio be 8:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, by volution bacterium amine, imperialine and synergist fumaric acid ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat orange caterpillar, can develop into the pesticide of preventing and treating orange caterpillar.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model
Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right
Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating orange caterpillar
Parts by weight of raw materials compares:
Volution bacterium amine, 20 parts；Imperialine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist fumaric acid and zinc sulfate
Totally 8 parts, the weight ratio of fumaric acid and zinc sulfate is 7:1.
Preparation method:
Step S1, by volution bacterium amine, imperialine and synergist fumaric acid ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating orange caterpillar
Parts by weight of raw materials compares:
Volution bacterium amine, 15 parts；Imperialine, 10 parts；Ethanol, 120 parts；Water, 440 parts；Synergist fumaric acid and zinc sulfate
Totally 7 parts, the weight ratio of fumaric acid and zinc sulfate is 6:1.
Preparation method:
Step S1, by volution bacterium amine, imperialine and synergist fumaric acid ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating orange caterpillar
Parts by weight of raw materials compares:
Volution bacterium amine, 25 parts；Imperialine, 20 parts；Ethanol, 140 parts；Water, 480 parts；Synergist fumaric acid and zinc sulfate
Totally 9 parts, the weight ratio of fumaric acid and zinc sulfate is 8:1.
Preparation method:
Step S1, by volution bacterium amine, imperialine and synergist fumaric acid ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating orange caterpillar
Parts by weight of raw materials compares:
Volution bacterium amine, 20 parts；Imperialine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist fumaric acid and zinc sulfate
Totally 8 parts, the weight ratio of fumaric acid and zinc sulfate is 6:1.
Preparation method:
Step S1, by volution bacterium amine, imperialine and synergist fumaric acid ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating orange caterpillar
Parts by weight of raw materials compares:
Volution bacterium amine, 20 parts；Imperialine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist fumaric acid and zinc sulfate
Totally 8 parts, the weight ratio of fumaric acid and zinc sulfate is 8:1.
Preparation method:
Step S1, by volution bacterium amine, imperialine and synergist fumaric acid ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, fumaric acid and zinc sulfate is 5:1
Parts by weight of raw materials compares:
Volution bacterium amine, 20 parts；Imperialine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist fumaric acid and zinc sulfate
Totally 8 parts, the weight ratio of fumaric acid and zinc sulfate is 5:1.
Preparation method:
Step S1, by volution bacterium amine, imperialine and synergist fumaric acid ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, fumaric acid and zinc sulfate is 9:1
Parts by weight of raw materials compares:
Volution bacterium amine, 20 parts；Imperialine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist fumaric acid and zinc sulfate
Totally 8 parts, the weight ratio of fumaric acid and zinc sulfate is 9:1.
Preparation method:
Step S1, by volution bacterium amine, imperialine and synergist fumaric acid ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
The compositions of the testing example 1～7 preparation preventing and treating effective percentage (%) to orange caterpillar respectively.
During use, present composition water carries out 40 times of dilutions, and fountain height is 30 liters/mu.
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 100 |
| Embodiment 4 | 98 |
| Embodiment 5 | 98 |
| Embodiment 6 | 65 |
| Embodiment 7 | 68 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat orange caterpillar, can develop into preventing and treating Citrus aphid
The pesticide of worm, prevention effect is relevant with the weight ratio of synergist fumaric acid and zinc sulfate in raw material, fumaric acid and zinc sulfate
Weight ratio when being 6～8:1, prevention effect is best.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this
Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent,
Essence and protection domain without deviating from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating orange caterpillar, it is characterised in that include the raw material of following weight portion: volution bacterium amine, 15～
25 parts；Imperialine, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Synergist fumaric acid and zinc sulfate totally 7
～9 parts, the weight ratio of fumaric acid and zinc sulfate is 6～8:1.
The compositions of preventing and treating orange caterpillar the most according to claim 1, it is characterised in that include the former of following weight portion
Material: volution bacterium amine, 20 parts；Imperialine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Totally 8 parts of synergist fumaric acid and zinc sulfate,
The weight ratio of fumaric acid and zinc sulfate is 7:1.
The compositions of preventing and treating orange caterpillar the most according to claim 1, it is characterised in that include the former of following weight portion
Material: volution bacterium amine, 15 parts；Imperialine, 10 parts；Ethanol, 120 parts；Water, 440 parts；Totally 7 parts of synergist fumaric acid and zinc sulfate,
The weight ratio of fumaric acid and zinc sulfate is 6:1.
The compositions of preventing and treating orange caterpillar the most according to claim 1, it is characterised in that include the former of following weight portion
Material: volution bacterium amine, 25 parts；Imperialine, 20 parts；Ethanol, 140 parts；Water, 480 parts；Totally 9 parts of synergist fumaric acid and zinc sulfate,
The weight ratio of fumaric acid and zinc sulfate is 8:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, by volution bacterium amine, imperialine and synergist fumaric acid ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610462809.5A CN106106518A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating orange caterpillar and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610462809.5A CN106106518A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating orange caterpillar and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106106518A true CN106106518A (en) | 2016-11-16 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610462809.5A Pending CN106106518A (en) | 2016-06-22 | 2016-06-22 | A kind of compositions preventing and treating orange caterpillar and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102308801A (en) * | 2011-04-28 | 2012-01-11 | 陕西韦尔奇作物保护有限公司 | Germicide composition containing spiroxamine and antibiotics compound |
| CN103875671A (en) * | 2014-04-15 | 2014-06-25 | 海南正业中农高科股份有限公司 | Bactericidal composition |
| CN104145973A (en) * | 2011-04-26 | 2014-11-19 | 陕西韦尔奇作物保护有限公司 | Sterilization composition containing spiroxamine and methoxy acrylate |
| CN104285953A (en) * | 2014-10-15 | 2015-01-21 | 济南凯因生物科技有限公司 | Bactericidal composition for preventing and treating wheat powdery mildew |
-
2016
- 2016-06-22 CN CN201610462809.5A patent/CN106106518A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104145973A (en) * | 2011-04-26 | 2014-11-19 | 陕西韦尔奇作物保护有限公司 | Sterilization composition containing spiroxamine and methoxy acrylate |
| CN102308801A (en) * | 2011-04-28 | 2012-01-11 | 陕西韦尔奇作物保护有限公司 | Germicide composition containing spiroxamine and antibiotics compound |
| CN103875671A (en) * | 2014-04-15 | 2014-06-25 | 海南正业中农高科股份有限公司 | Bactericidal composition |
| CN104285953A (en) * | 2014-10-15 | 2015-01-21 | 济南凯因生物科技有限公司 | Bactericidal composition for preventing and treating wheat powdery mildew |
Non-Patent Citations (1)
| Title |
|---|
| 刘长令: "《世界农药大全 杀菌剂卷》", 31 January 2006 * |
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Application publication date: 20161116 |