CN106106473A - A kind of compositions preventing and treating Caulis et Folium Brassicae capitatae diamondback moth and preparation method thereof - Google Patents

A kind of compositions preventing and treating Caulis et Folium Brassicae capitatae diamondback moth and preparation method thereof Download PDF

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Publication number
CN106106473A
CN106106473A CN201610450152.0A CN201610450152A CN106106473A CN 106106473 A CN106106473 A CN 106106473A CN 201610450152 A CN201610450152 A CN 201610450152A CN 106106473 A CN106106473 A CN 106106473A
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parts
mercaptoethanol
zinc sulfate
diamondback moth
folium brassicae
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CN201610450152.0A
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殷佩琼
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
    • A01N31/02—Acyclic compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • A01N37/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof containing the group, wherein Cn means a carbon skeleton not containing a ring; Thio analogues thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16—Heavy metals; Compounds thereof

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The invention discloses a kind of compositions preventing and treating Caulis et Folium Brassicae capitatae diamondback moth and preparation method thereof, including the raw material of following weight portion: zoxamide, 15～25 parts；Sophoridine, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Totally 7～9 parts of synergist mercaptoethanol and zinc sulfate, the weight ratio of mercaptoethanol and zinc sulfate is 6～8:1.The compositions that the present invention provides can prevent and treat Caulis et Folium Brassicae capitatae diamondback moth, the pesticide of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth can be developed into, prevention effect is relevant with the weight ratio of synergist mercaptoethanol and zinc sulfate in raw material, and when the weight ratio of mercaptoethanol and zinc sulfate is 6～8:1, prevention effect is best.

Description

A kind of compositions preventing and treating Caulis et Folium Brassicae capitatae diamondback moth and preparation method thereof
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating Caulis et Folium Brassicae capitatae diamondback moth and preparation method thereof.
Background technology
The mechanism of action of zoxamide is unique in Oomycete antibacterial, and it is by the knot of tubulin β-subunit Close and rupturing of microtubule cytoskeleton suppresses sclerotium to divide.Zoxamide do not affect travelling spore in travelling, sporangiocyst formed or Sprout.Along with caryocinetic first circulation of bacterium, the elongation of germ tube is suppressed, thus stops disease mattress to penetrate host plant.
Have not yet to see zoxamide and work in coordination with the report preventing and treating Caulis et Folium Brassicae capitatae diamondback moth with sophoridine.
Summary of the invention
It is an object of the invention to provide a kind of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth containing zoxamide and sophoridine compositions and Its application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating Caulis et Folium Brassicae capitatae diamondback moth, including the raw material of following weight portion: zoxamide, 15～25 parts；Chinese scholartree Determine alkali, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Totally 7～9 parts of synergist mercaptoethanol and zinc sulfate, mercapto The weight ratio of base ethanol and zinc sulfate is 6～8:1.
Further, the compositions of described preventing and treating Caulis et Folium Brassicae capitatae diamondback moth includes the raw material of following weight portion: zoxamide, 20 Part；Sophoridine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Totally 8 parts of synergist mercaptoethanol and zinc sulfate, mercaptoethanol and sulphuric acid The weight ratio of zinc is 7:1.
Further, the compositions of described preventing and treating Caulis et Folium Brassicae capitatae diamondback moth includes the raw material of following weight portion: zoxamide, 15 Part；Sophoridine, 10 parts；Ethanol, 120 parts；Water, 440 parts；Totally 7 parts of synergist mercaptoethanol and zinc sulfate, mercaptoethanol and sulphuric acid The weight ratio of zinc is 6:1.
Further, the compositions of described preventing and treating Caulis et Folium Brassicae capitatae diamondback moth includes the raw material of following weight portion: zoxamide, 25 Part；Sophoridine, 20 parts；Ethanol, 140 parts；Water, 480 parts；Totally 9 parts of synergist mercaptoethanol and zinc sulfate, mercaptoethanol and sulphuric acid The weight ratio of zinc is 8:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, by zoxamide, sophoridine and synergist mercaptoethanol ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat Caulis et Folium Brassicae capitatae diamondback moth, can develop into the pesticide of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth
Parts by weight of raw materials compares:
Zoxamide, 20 parts；Sophoridine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist mercaptoethanol and zinc sulfate Totally 8 parts, the weight ratio of mercaptoethanol and zinc sulfate is 7:1.
Preparation method:
Step S1, by zoxamide, sophoridine and synergist mercaptoethanol ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth
Parts by weight of raw materials compares:
Zoxamide, 15 parts；Sophoridine, 10 parts；Ethanol, 120 parts；Water, 440 parts；Synergist mercaptoethanol and zinc sulfate Totally 7 parts, the weight ratio of mercaptoethanol and zinc sulfate is 6:1.
Preparation method:
Step S1, by zoxamide, sophoridine and synergist mercaptoethanol ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth
Parts by weight of raw materials compares:
Zoxamide, 25 parts；Sophoridine, 20 parts；Ethanol, 140 parts；Water, 480 parts；Synergist mercaptoethanol and zinc sulfate Totally 9 parts, the weight ratio of mercaptoethanol and zinc sulfate is 8:1.
Preparation method:
Step S1, by zoxamide, sophoridine and synergist mercaptoethanol ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth
Parts by weight of raw materials compares:
Zoxamide, 20 parts；Sophoridine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist mercaptoethanol and zinc sulfate Totally 8 parts, the weight ratio of mercaptoethanol and zinc sulfate is 6:1.
Preparation method:
Step S1, by zoxamide, sophoridine and synergist mercaptoethanol ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth
Parts by weight of raw materials compares:
Zoxamide, 20 parts；Sophoridine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist mercaptoethanol and zinc sulfate Totally 8 parts, the weight ratio of mercaptoethanol and zinc sulfate is 8:1.
Preparation method:
Step S1, by zoxamide, sophoridine and synergist mercaptoethanol ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, mercaptoethanol and zinc sulfate is 5:1
Parts by weight of raw materials compares:
Zoxamide, 20 parts；Sophoridine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist mercaptoethanol and zinc sulfate Totally 8 parts, the weight ratio of mercaptoethanol and zinc sulfate is 5:1.
Preparation method:
Step S1, by zoxamide, sophoridine and synergist mercaptoethanol ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, mercaptoethanol and zinc sulfate is 9:1
Parts by weight of raw materials compares:
Zoxamide, 20 parts；Sophoridine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist mercaptoethanol and zinc sulfate Totally 8 parts, the weight ratio of mercaptoethanol and zinc sulfate is 9:1.
Preparation method:
Step S1, by zoxamide, sophoridine and synergist mercaptoethanol ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
The compositions of the testing example 1～7 preparation preventing and treating effective percentage (%) to Caulis et Folium Brassicae capitatae diamondback moth respectively.
During use, present composition water carries out 40 times of dilutions, and fountain height is 25 liters/mu.
Result such as following table.
Preventing and treating effective percentage (%)
Embodiment 1 100
Embodiment 4 98
Embodiment 5 99
Embodiment 6 72
Embodiment 7 74
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat Caulis et Folium Brassicae capitatae diamondback moth, can develop into preventing and treating Caulis et Folium Brassicae capitatae The pesticide of diamondback moth, prevention effect is relevant with the weight ratio of synergist mercaptoethanol and zinc sulfate in raw material, mercaptoethanol When being 6～8:1 with the weight ratio of zinc sulfate, prevention effect is best.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent, Essence and protection domain without deviating from technical solution of the present invention.

Claims (5)

1. the compositions preventing and treating Caulis et Folium Brassicae capitatae diamondback moth, it is characterised in that include the raw material of following weight portion: zoxamide, 15 ～25 parts；Sophoridine, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Synergist mercaptoethanol and zinc sulfate are altogether 7～9 parts, the weight ratio of mercaptoethanol and zinc sulfate is 6～8:1.
The compositions of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth the most according to claim 1, it is characterised in that include the former of following weight portion Material: zoxamide, 20 parts；Sophoridine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Totally 8 parts of synergist mercaptoethanol and zinc sulfate, The weight ratio of mercaptoethanol and zinc sulfate is 7:1.
The compositions of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth the most according to claim 1, it is characterised in that include the former of following weight portion Material: zoxamide, 15 parts；Sophoridine, 10 parts；Ethanol, 120 parts；Water, 440 parts；Totally 7 parts of synergist mercaptoethanol and zinc sulfate, The weight ratio of mercaptoethanol and zinc sulfate is 6:1.
The compositions of preventing and treating Caulis et Folium Brassicae capitatae diamondback moth the most according to claim 1, it is characterised in that include the former of following weight portion Material: zoxamide, 25 parts；Sophoridine, 20 parts；Ethanol, 140 parts；Water, 480 parts；Totally 9 parts of synergist mercaptoethanol and zinc sulfate, The weight ratio of mercaptoethanol and zinc sulfate is 8:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, by zoxamide, sophoridine and synergist mercaptoethanol ethanol and water dissolution；
Step S2, by zinc sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
CN201610450152.0A 2016-06-19 2016-06-19 A kind of compositions preventing and treating Caulis et Folium Brassicae capitatae diamondback moth and preparation method thereof Pending CN106106473A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108040700A (en) * 2017-12-19 2018-05-18 潘卫剑 A kind of method for preventing wild cabbage diamondback moth

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101617657A (en) * 2009-08-12 2010-01-06 深圳诺普信农化股份有限公司 Pesticide composition
CN102860312A (en) * 2012-09-28 2013-01-09 江苏省绿盾植保农药实验有限公司 Insecticide containing sophoridine and azadirachtin
CN102860313A (en) * 2012-09-28 2013-01-09 江苏省绿盾植保农药实验有限公司 Insecticide containing sophoridine and nicotine
CN103392707A (en) * 2013-08-21 2013-11-20 陕西康禾立丰生物科技药业有限公司 Pesticide for controlling plant fungal diseases and preparation method thereof
CN105265452A (en) * 2014-07-09 2016-01-27 马宗刚 Application of sophoridine as plant growth promoter

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101617657A (en) * 2009-08-12 2010-01-06 深圳诺普信农化股份有限公司 Pesticide composition
CN102860312A (en) * 2012-09-28 2013-01-09 江苏省绿盾植保农药实验有限公司 Insecticide containing sophoridine and azadirachtin
CN102860313A (en) * 2012-09-28 2013-01-09 江苏省绿盾植保农药实验有限公司 Insecticide containing sophoridine and nicotine
CN103392707A (en) * 2013-08-21 2013-11-20 陕西康禾立丰生物科技药业有限公司 Pesticide for controlling plant fungal diseases and preparation method thereof
CN105265452A (en) * 2014-07-09 2016-01-27 马宗刚 Application of sophoridine as plant growth promoter

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108040700A (en) * 2017-12-19 2018-05-18 潘卫剑 A kind of method for preventing wild cabbage diamondback moth

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Application publication date: 20161116