CN106093215A - 一种测量水中溶解性有机卤含量的方法及*** - Google Patents
一种测量水中溶解性有机卤含量的方法及*** Download PDFInfo
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- CN106093215A CN106093215A CN201610362531.4A CN201610362531A CN106093215A CN 106093215 A CN106093215 A CN 106093215A CN 201610362531 A CN201610362531 A CN 201610362531A CN 106093215 A CN106093215 A CN 106093215A
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- dissolubility
- groove
- organic halogen
- room groove
- measured
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Links
- 229910052736 halogen Inorganic materials 0.000 title claims abstract description 163
- 150000002367 halogens Chemical class 0.000 title claims abstract description 149
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 116
- 238000000034 method Methods 0.000 title claims abstract description 83
- 229910001502 inorganic halide Inorganic materials 0.000 claims abstract description 70
- 238000004458 analytical method Methods 0.000 claims abstract description 24
- 230000001699 photocatalysis Effects 0.000 claims abstract description 24
- 238000007146 photocatalysis Methods 0.000 claims abstract description 18
- 238000005516 engineering process Methods 0.000 claims abstract description 14
- 239000012528 membrane Substances 0.000 claims description 36
- 239000008151 electrolyte solution Substances 0.000 claims description 22
- 238000005259 measurement Methods 0.000 claims description 21
- 239000003014 ion exchange membrane Substances 0.000 claims description 15
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 claims description 15
- 229910052753 mercury Inorganic materials 0.000 claims description 14
- 238000000926 separation method Methods 0.000 claims description 14
- 230000005684 electric field Effects 0.000 claims description 11
- 238000002347 injection Methods 0.000 claims description 10
- 239000007924 injection Substances 0.000 claims description 10
- 239000000243 solution Substances 0.000 claims description 9
- 229910000497 Amalgam Inorganic materials 0.000 claims description 5
- 229910052724 xenon Inorganic materials 0.000 claims description 5
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 claims description 5
- 230000003197 catalytic effect Effects 0.000 claims description 4
- 238000001223 reverse osmosis Methods 0.000 claims description 4
- 230000001678 irradiating effect Effects 0.000 claims description 3
- 230000002829 reductive effect Effects 0.000 claims description 3
- 238000012360 testing method Methods 0.000 abstract description 32
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 26
- 238000002485 combustion reaction Methods 0.000 abstract description 24
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract description 9
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract description 9
- 229910052794 bromium Inorganic materials 0.000 abstract description 9
- 239000003054 catalyst Substances 0.000 abstract description 9
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract description 8
- 229910052801 chlorine Inorganic materials 0.000 abstract description 8
- 239000000460 chlorine Substances 0.000 abstract description 8
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 7
- 229910052740 iodine Inorganic materials 0.000 abstract description 7
- 239000011630 iodine Substances 0.000 abstract description 7
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 abstract description 6
- 229910052731 fluorine Inorganic materials 0.000 abstract description 6
- 239000011737 fluorine Substances 0.000 abstract description 6
- 239000003610 charcoal Substances 0.000 abstract description 5
- 238000001179 sorption measurement Methods 0.000 abstract description 4
- 150000002500 ions Chemical class 0.000 description 32
- 210000004379 membrane Anatomy 0.000 description 23
- 238000006243 chemical reaction Methods 0.000 description 18
- -1 halogen ion Chemical class 0.000 description 17
- 230000007613 environmental effect Effects 0.000 description 14
- 230000008859 change Effects 0.000 description 13
- 238000010586 diagram Methods 0.000 description 10
- 238000012956 testing procedure Methods 0.000 description 8
- 238000001816 cooling Methods 0.000 description 7
- 238000005342 ion exchange Methods 0.000 description 6
- 230000004044 response Effects 0.000 description 5
- DTQVDTLACAAQTR-UHFFFAOYSA-N Trifluoroacetic acid Chemical compound OC(=O)C(F)(F)F DTQVDTLACAAQTR-UHFFFAOYSA-N 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 238000010828 elution Methods 0.000 description 4
- 238000007654 immersion Methods 0.000 description 4
- XMBWDFGMSWQBCA-UHFFFAOYSA-M iodide Chemical compound [I-] XMBWDFGMSWQBCA-UHFFFAOYSA-M 0.000 description 4
- 229940006461 iodide ion Drugs 0.000 description 4
- 238000004255 ion exchange chromatography Methods 0.000 description 4
- 238000011017 operating method Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 3
- 238000005553 drilling Methods 0.000 description 3
- 235000020188 drinking water Nutrition 0.000 description 3
- 239000003651 drinking water Substances 0.000 description 3
- 239000009512 hedan Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 238000001556 precipitation Methods 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000013375 chromatographic separation Methods 0.000 description 2
- 238000004587 chromatography analysis Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 230000009977 dual effect Effects 0.000 description 2
- 238000001471 micro-filtration Methods 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 description 1
- 229910021608 Silver(I) fluoride Inorganic materials 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229940006460 bromide ion Drugs 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000005341 cation exchange Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000005695 dehalogenation reaction Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910001410 inorganic ion Inorganic materials 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Substances [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- REYHXKZHIMGNSE-UHFFFAOYSA-M silver monofluoride Chemical compound [F-].[Ag+] REYHXKZHIMGNSE-UHFFFAOYSA-M 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 235000017557 sodium bicarbonate Nutrition 0.000 description 1
- 239000007785 strong electrolyte Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 238000000825 ultraviolet detection Methods 0.000 description 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/96—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation using ion-exchange
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/34—Purifying; Cleaning
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/40—Concentrating samples
- G01N1/4005—Concentrating samples by transferring a selected component through a membrane
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/14—Preparation by elimination of some components
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/18—Water
- G01N33/1826—Organic contamination in water
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/40—Concentrating samples
- G01N1/4005—Concentrating samples by transferring a selected component through a membrane
- G01N2001/4011—Concentrating samples by transferring a selected component through a membrane being a ion-exchange membrane
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/40—Concentrating samples
- G01N2001/4038—Concentrating samples electric methods, e.g. electromigration, electrophoresis, ionisation
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N2030/022—Column chromatography characterised by the kind of separation mechanism
- G01N2030/027—Liquid chromatography
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N2030/067—Preparation by reaction, e.g. derivatising the sample
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N30/14—Preparation by elimination of some components
- G01N2030/146—Preparation by elimination of some components using membranes
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Immunology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Physics & Mathematics (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Biomedical Technology (AREA)
- Molecular Biology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Water Treatment By Electricity Or Magnetism (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
Description
Claims (10)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610362531.4A CN106093215B (zh) | 2016-05-26 | 2016-05-26 | 一种测量水中溶解性有机卤含量的方法及*** |
PCT/CN2017/000244 WO2017202029A1 (zh) | 2016-05-26 | 2017-03-21 | 一种测量水中溶解性有机卤含量的方法及*** |
US16/199,325 US20190094191A1 (en) | 2016-05-26 | 2018-11-26 | Method and system for measuring content of dissolved organic halogens in water |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610362531.4A CN106093215B (zh) | 2016-05-26 | 2016-05-26 | 一种测量水中溶解性有机卤含量的方法及*** |
Publications (2)
Publication Number | Publication Date |
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CN106093215A true CN106093215A (zh) | 2016-11-09 |
CN106093215B CN106093215B (zh) | 2019-09-06 |
Family
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CN201610362531.4A Expired - Fee Related CN106093215B (zh) | 2016-05-26 | 2016-05-26 | 一种测量水中溶解性有机卤含量的方法及*** |
Country Status (3)
Country | Link |
---|---|
US (1) | US20190094191A1 (zh) |
CN (1) | CN106093215B (zh) |
WO (1) | WO2017202029A1 (zh) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107096572A (zh) * | 2017-04-24 | 2017-08-29 | 太原师范学院 | 一种制备双极膜表面粉末态光催化剂的方法 |
WO2017202029A1 (zh) * | 2016-05-26 | 2017-11-30 | 哈尔滨工业大学深圳研究生院 | 一种测量水中溶解性有机卤含量的方法及*** |
CN107721041A (zh) * | 2017-06-01 | 2018-02-23 | 哈尔滨工业大学深圳研究生院 | 一种测量水中总卤代有机物的预处理方法 |
CN110044762A (zh) * | 2019-04-26 | 2019-07-23 | 华中科技大学 | 一种催化还原脱溴测定总有机溴含量的方法 |
CN111196661A (zh) * | 2020-02-14 | 2020-05-26 | 淄博格瑞水处理工程有限公司 | 一种含有机碘高盐废水资源化零排放装置 |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6573620B2 (ja) | 2014-02-10 | 2019-09-11 | フレッド ハッチンソン キャンサー リサーチ センター | 心臓発作及び虚血損傷のハロゲン治療 |
CN112557142B (zh) * | 2020-12-24 | 2024-05-31 | 广州博诺通技术股份有限公司 | 样品前处理方法、卤素含量的检测方法及应用 |
Citations (2)
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CN103969411A (zh) * | 2014-04-09 | 2014-08-06 | 陈白杨 | 一种基于电渗析预处理方式直接测量水体中溶解性有机氮浓度的方法 |
CN203965218U (zh) * | 2014-04-09 | 2014-11-26 | 哈尔滨工业大学深圳研究生院 | 一种电渗析预处理装置 |
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JP4800288B2 (ja) * | 2007-11-08 | 2011-10-26 | ハウス食品株式会社 | 光触媒を用いた食品等の有機化合物を含む試料中のイプロジオン及び/又はイプロジオン代謝物の分析方法 |
CN101571530A (zh) * | 2009-03-27 | 2009-11-04 | 浙江树人大学 | 离子色谱柱后衍生紫外检测含硫阴离子化合物 |
CN101708883B (zh) * | 2009-12-18 | 2011-08-03 | 哈尔滨工业大学 | 一种光促脱卤复合药剂/光联用去除水中卤代有机物的方法 |
CN103983685B (zh) * | 2014-05-30 | 2016-04-27 | 中国地质科学院水文地质环境地质研究所 | 一种氯代除草剂中氯同位素的低温转化与测定方法 |
CN204874184U (zh) * | 2015-06-10 | 2015-12-16 | 河海大学 | 光催化膜蒸馏印染废水处理回用*** |
CN105152444B (zh) * | 2015-09-23 | 2017-09-15 | 山东默锐环境产业股份有限公司 | 一种hbcd生产废水深度处理与废水中溴的回收综合处理工艺 |
CN105467041A (zh) * | 2016-01-28 | 2016-04-06 | 吴江华衍水务有限公司 | 一种改进的水中总有机溴的测定方法 |
CN106093215B (zh) * | 2016-05-26 | 2019-09-06 | 深圳合核环境科技有限公司 | 一种测量水中溶解性有机卤含量的方法及*** |
-
2016
- 2016-05-26 CN CN201610362531.4A patent/CN106093215B/zh not_active Expired - Fee Related
-
2017
- 2017-03-21 WO PCT/CN2017/000244 patent/WO2017202029A1/zh active Application Filing
-
2018
- 2018-11-26 US US16/199,325 patent/US20190094191A1/en not_active Abandoned
Patent Citations (2)
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CN103969411A (zh) * | 2014-04-09 | 2014-08-06 | 陈白杨 | 一种基于电渗析预处理方式直接测量水体中溶解性有机氮浓度的方法 |
CN203965218U (zh) * | 2014-04-09 | 2014-11-26 | 哈尔滨工业大学深圳研究生院 | 一种电渗析预处理装置 |
Non-Patent Citations (4)
Title |
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BAIYANG CHEN等: "Critical Application of Pretreatment Methods for Reliable Dissolved Organic Nitrogen Analysis", 《CRITICAL REVIEWS IN ENVIRONMENTAL SCIENCE AND TECHNOLOGY》 * |
MARTIN REINHARD等: "Molecular Weight Distribution of Dissolved Organic Carbon and Dissolved Organic Halogen in Advanced Treated Wastewaters", 《ENVIRON. SCI. TECHNOL》 * |
张红专等: "预臭氧化去除水中有机卤代物的效果", 《上海师范大学学报(自然科学版)》 * |
陈焕军: "离子色谱-紫外消解测定有机卤素", 《第十二届全国离子色谱学术报告会论文集》 * |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2017202029A1 (zh) * | 2016-05-26 | 2017-11-30 | 哈尔滨工业大学深圳研究生院 | 一种测量水中溶解性有机卤含量的方法及*** |
CN107096572A (zh) * | 2017-04-24 | 2017-08-29 | 太原师范学院 | 一种制备双极膜表面粉末态光催化剂的方法 |
CN107721041A (zh) * | 2017-06-01 | 2018-02-23 | 哈尔滨工业大学深圳研究生院 | 一种测量水中总卤代有机物的预处理方法 |
WO2018218960A1 (zh) * | 2017-06-01 | 2018-12-06 | 哈尔滨工业大学深圳研究生院 | 一种测量水中总卤代有机物的预处理方法 |
CN110044762A (zh) * | 2019-04-26 | 2019-07-23 | 华中科技大学 | 一种催化还原脱溴测定总有机溴含量的方法 |
CN111196661A (zh) * | 2020-02-14 | 2020-05-26 | 淄博格瑞水处理工程有限公司 | 一种含有机碘高盐废水资源化零排放装置 |
CN111196661B (zh) * | 2020-02-14 | 2023-05-02 | 山东博苑医药化学股份有限公司 | 一种含有机碘高盐废水资源化零排放装置 |
Also Published As
Publication number | Publication date |
---|---|
WO2017202029A1 (zh) | 2017-11-30 |
CN106093215B (zh) | 2019-09-06 |
US20190094191A1 (en) | 2019-03-28 |
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