CN106038352A - Environment-friendly super-concentrated hand washing slices/granules and manufacturing method thereof - Google Patents
Environment-friendly super-concentrated hand washing slices/granules and manufacturing method thereof Download PDFInfo
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- CN106038352A CN106038352A CN201610379567.3A CN201610379567A CN106038352A CN 106038352 A CN106038352 A CN 106038352A CN 201610379567 A CN201610379567 A CN 201610379567A CN 106038352 A CN106038352 A CN 106038352A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/022—Powders; Compacted Powders
- A61K8/0225—Granulated powders
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/37—Esters of carboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/66—Enzymes
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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Abstract
The invention discloses environment-friendly super-concentrated hand washing slices/granules and a manufacturing method thereof. The slices/granules are prepared from 15-60% of anion active agent, 10-30% of non-ionic active agent, 1-15% of ampholytic active agent, 1-6% of small molecular peptide complex enzyme, 2-6% of thickening agent, 1-3% of fatting agent, skin moisturizer, skin moisturizing agent and pH regulator, 0.1-1% of antibacterial agent, preservative, slip reducing agent and essence, and the balance water. The slices/granules have the advantages that small molecular peptide powder is added to the complex enzyme, and therefore the excitation effect of the complex enzyme on various active substances is enhanced, and the decontamination capacity of the active substances is greatly improved; meanwhile, through the scientific process of drying and then enzyme spraying and autonomous-developed hand washing slice/granule production devices, it is effectively ensured that active components of enzyme can not be damaged.
Description
Technical field
The present invention relates to articles for washing technical field, the environmental protection ultra concentration especially relating to a kind of dirt-removing power strong is washed one's hands
Sheet/granule and preparation method thereof.
Background technology
Handwashing liquid is requisite daily cleaning articles for use during people live, and is widely used in family, hotel, dining room, meeting
The places such as shop, require height to ability of cleaning greasy dirt and environmental-protecting performance.At present, handwashing liquid is all liquid condition, not only carries the most square
Just, easy water clock when using, and make the high expensive of packed and transported, it is often more important that usage amount is difficulty with being precisely controlled.
Not enough in order to solve prior art, inventor have developed a kind of environmental protection ultra concentration and washes one's hands sheet/granule, and carries
Go out a kind of method making this sheet/granule of washing one's hands, produced equipment by independent development, make washing one's hands in sheet/granule after drying
The content of active matter and effective decontamination composition is the highest can reach more than 90%, and detergency meets and exceeds conventional on the market washing
The decontamination standard of hands liquid, compensate for gaps in market.
Summary of the invention
The present invention provides environmental protection ultra concentration to wash one's hands sheet/granule, to solve that handwashing liquid of the prior art is the most portable, easily to drip
The problems such as leakage, packed and transported cost is high, usage amount is the most accurate.
Technical problem solved by the invention realizes by the following technical solutions:
A kind of environmental protection ultra concentration is washed one's hands sheet/granule, it is characterised in that this sheet/granule of washing one's hands includes following mass percent
Component:
Accounting is the anion active agent of 15-60%, and described anion active agent is laureth sulfosuccinate
Disodium (be called for short CAS), Brij 35 sodium sulfate (being called for short AES), MES (being called for short MES),
Fatty acid methyl ester ethoxylate sulfonate (being called for short FMES), alpha-olefin sodium sulfonate (being called for short AOS), 16 SASs
In (being called for short SAS), lauroyl sodium isethionate (being called for short Yi Jiebang A), N-lauroyl sodium hydrogen alpha-aminoglutarate, potash soap, soda soap one
Plant or multiple mixture；
Accounting is the tween of 10-30%, and described tween is alkyl polyglucoside (APG for short), Cortex cocois radicis
One or both mixture in fatty acid oil single ethanol amide (being called for short CMEA)；
Accounting is the amphoteric surfactant of 1-15%, and described amphoteric surfactant is that cocoamidopropyl dimethyl is sweet
One or more in dish alkali, glycol distearate, coco imidoazolinium, decyl dimethyl hydroxypropyl sulfobetaines
Mixture；
Accounting is the small-molecular peptides compound enzyme of 1-6%；
Accounting is the fatting agent of 1-3%, described fatting agent be monoglyceride, glyceryl cocoate, isopropyl myristate,
One or more mixing in glycerol cocoyl macrogol ester, octyl group hydroxy stearic acid ester, polyquaternary ammonium salt-7, glycerol, pantothenylol
Thing；
Accounting is the skin moistening wetting agent of 1-3%, described skin moistening wetting agent be liquid paraffin, glycerol, ethylene glycol, sorbitol,
One or more mixture in propylene glycol and alkyl polyglucoside；
Accounting is the skin moisturizing agent of 1-3%, and described skin moisturizing agent is sorbitol, propylene glycol, Aloe, Mel, Radix Ginseng
One or more mixture in liquid, Margarita liquid, pollen, milk, silicone oil, glycerol, aminoacid；
Accounting is the pH value regulator of 1-3%, and described pH value regulator is citric acid；
Accounting is the thickening agent of 2-6%, described thickening agent be xanthan gum, sodium alginate, carrageenan, hydroxymethyl cellulose,
One or more mixture in sodium chloride, polyvinyl alcohol；
Accounting is the antibacterial of 0.1-1%, and described antibacterial is triclocarban, triclosan, hydroxyl phenylate, xylene chloride
One or more mixture in phenol；
Accounting is the preservative of 0.1-0.5%, and described preservative is Kazon, sodium benzoate, phenoxyethanol, lactoperoxidase
One or more mixture in enzyme；
Accounting be 0.1-1% subtract lubrication prescription, described in subtract lubrication prescription be C18-20 sec alkanol polyethers-9；
Accounting is the essence of 0.1-1%；
The deionized water of surplus.
Wherein, described small-molecular peptides compound enzyme is that small-molecular peptides powder is carried out according to the mixing ratio of 1:4 1:19 with compound enzyme
The complex of mixing, wherein, described compound enzyme is by two in amylase, protease, lipase, cellulase, mannase
Kind or two or more mix.
Described compound enzyme is that amylase, lipase, three kinds of enzymes of protease carry out mixed three according to the mixing ratio of 3:3:4
Unification compound enzyme；
Or, described compound enzyme is amylase, lipase, four kinds of enzymes of mannonase protease mixing according to 2:3:1:4
Composition and division in a proportion carries out mixed four-in-one compound enzyme；
Or, described compound enzyme be cellulase, amylase, lipase, five kinds of enzymes of mannonase protease according to 3:2:
The mixing ratio of 1:1:3 carries out mixed five in one compound enzyme.
The invention allows for a kind of environmental protection ultra concentration to wash one's hands the manufacture method of sheet/granule, it is characterised in that this making side
Method comprises the following steps:
Step S001, take above-mentioned anion active agent, tween and amphoteric surfactant in proportion and put into
Preparation container in, be stirred continuously, then take in proportion fatting agent, skin moistening wetting agent, skin moisturizing agent, pH value regulator, thickening
Agent, antibacterial, preservative, subtract lubrication prescription, essence and appropriate amount of deionized water and put into described preparation container equally, constantly stir evenly
And make each component be sufficiently mixed, obtain wash one's hands sheet/granule of liquid environment-friendly ultra concentration and make raw material；
Step S002, sheet/granule of liquid environment-friendly ultra concentration obtained in above-mentioned steps S001 being washed one's hands make raw material and put
In the pelletizer with mummification function, carry out moisture evaporation under the condition of high temperature more than 80 degrees Celsius, and prepare aqueous
The amount ultra concentration type less than 6% is washed one's hands sheet；
Step S003, take described small-molecular peptides compound enzyme, and it is carried out dilute with water according to the thinner ratio being not less than 1:0.5
Add after releasing in a kind of flusher；
Step S004, by small-molecular peptides compound enzyme described in the liquid state in flusher described in above-mentioned steps S003, spray
It is sprinkled upon in above-mentioned steps S002 obtained ultra concentration type to wash one's hands on sheet surface, and dries.
Further, the invention allows for a kind of environmental protection ultra concentration and wash one's hands the manufacture method of granule, this manufacture method
Preamble work is as consistent in the wash one's hands manufacture method of sheet of above-mentioned environmental protection ultra concentration, and follow-up work is: will be through above-mentioned steps S004
Chip solid ultra concentration type after process sheet of washing one's hands puts into comminutor, and producing particle diameter, to be not less than the graininess of 0.1cm super dense
Miniature is washed one's hands granule.
The invention have the advantages that: by adding small-molecular peptides powder in compound enzyme, and then strengthen compound enzyme pair
The excitation of each active matter, thus the dirt-removing power of active matter is substantially improved.Meanwhile, the science work of enzyme is sprayed after utilizing first mummification
Skill and sheet of the washing one's hands/particle manufacture equipment of independent research, effectively ensure that the active component of enzyme will not be destroyed.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below knot
Conjunction is embodied as illustrating, and the present invention is expanded on further.
Embodiment 1
A kind of environmental protection ultra concentration is washed one's hands sheet/granule, and this environmental protection ultra concentration sheet/granule of washing one's hands is prepared by following method；
Step S001, with 100 grams for the full part of constituent, take anion active agent dodecyl alcohol polyoxyethylene in proportion
Ether sodium sulfate (being called for short AES) 55 grams, tween alkyl polyglucoside (APG for short) 12 grams, amphoteric surfactant cocos nucifera oil acyl
Amine propyl-dimethyl glycine betaine 15 grams, puts into preparation container and is stirred continuously；
Take fatting agent glycerol cocoyl macrogol ester 2 grams, skin moistening wetting agent sorbitol 1 gram, skin moisturizing the most in proportion
Agent Mel 1.5 grams, pH value regulator citric acid 2 grams, 0.5 gram of thickening agent sodium chloride, antibacterial triclocarban 1 gram, preservative card
Pine 0.3 gram, subtract lubrication prescription (C18-20 sec alkanol polyethers-9) 0.2 gram, 0.5 gram of essence and appropriate amount of deionized water, put into equally
In described preparation container, constantly stir evenly and make each component be sufficiently mixed, obtaining wash one's hands sheet/granule of liquid environment-friendly ultra concentration and make former
Material；
Step S002, sheet/granule of liquid environment-friendly ultra concentration obtained in above-mentioned steps S001 being washed one's hands make raw material and put
In the pelletizer of band mummification function, carry out moisture evaporation by the high temperature of more than 80 degree, super dense by calculating liquid environment-friendly
Contracting is washed one's hands the thickness of sheet and enter the area in desiccation apparatus, carrys out Based Intelligent Control evaporation time, and then realizes surpassing liquid environment-friendly
Concentrate the moisture evaporation washing one's hands in sheet, and obtain the water content solid, shaped environmental protection ultra concentration type less than 6% and wash one's hands sheet；
Step S003, take described small-molecular peptides compound enzyme 5 grams in proportion, and by its with water according to being not less than the dilute of 1:0.5
Releasing ratio and add in a kind of flusher after being diluted, wherein, described small-molecular peptides compound enzyme is with compound by small-molecular peptides powder
Enzyme carries out the complex mixed according to the mixing ratio of 1:12, and compound enzyme described among these is amylase, lipase, protease three
Plant enzyme and carry out mixed three-in-one compound enzyme according to the mixing ratio of 3:3:4；
Step S004, will in flusher described in above-mentioned steps S003 dilution after described small-molecular peptides compound enzyme, spray
It is sprinkled upon in above-mentioned steps S002 obtained solid, shaped environmental protection ultra concentration type to wash one's hands on sheet surface, and dries.
Further, the present embodiment also proposed a kind of environmental protection ultra concentration and washes one's hands the manufacture method of granule, this manufacture method
Preamble work as the wash one's hands manufacture method of sheet of above-mentioned environmental protection ultra concentration consistent, follow-up work is: will be through above-mentioned steps
Chip solid environmental protection ultra concentration type sheet of washing one's hands after S004 processes puts into comminutor, produce particle diameter be not less than 0.1cm
Granular environmental protection ultra concentration type is washed one's hands granule.
In sum, environmental protection ultra concentration type out made by the present embodiment is washed one's hands sheet/granule, its constituent and percentage
Ratio is as described below:
Above-mentioned environmental protection ultra concentration type out made by the present embodiment is washed one's hands sheet/granule, is had compared with existing product
Unique distinction be: the three-in-one compound enzyme of small-molecular peptides utilizing mixing ratio to be 1:12, come anion active agent dodecyl
Polyoxyethylenated alcohol sodium sulfate, tween alkyl polyglucoside and amphoteric surfactant cocoamidopropyl dimethyl
The active ingredient of glycine betaine carries out exciting of maximum capacity, and then promotes the solubilization dirt-removing power of above-mentioned activating agent at double.Especially
Be the protease in three-in-one compound enzyme under the facilitation of small-molecular peptides, can be by anion active agent dodecyl alcohol polyoxy
The deoiling of vinyl Ether sodium sulfate, detergent power performs to ultimate attainment.
Meanwhile, by adding pH value regulator citric acid in integral formula so that overall pH value is closer to human body skin
Acidic physique, alkalogenic burn feeling will not be produced；Also by fatting agent glycerol cocoyl macrogol ester, skin moistening wetting agent mountain
Pears alcohol and the interpolation of skin moisturizing agent Mel, be possible not only to effectively to protect the hands of user will not occur defat, dry and cracked,
The discomforts such as puckery wrinkle, and may also operate as good moistening and effect of maintenance hand skin；Add also by integral formula
Plus-minus lubrication prescription C18-20 sec alkanol polyethers-9 so that user rinses more quick, does not has soapy feeling, more saves preciousness
Water resource.
The present embodiment, also by first high temperature mummification, sprays the innovative technology of enzyme the most again, is effectively protected above-mentioned little molecule
The activity of the three-in-one compound enzyme of peptide will not be destroyed by high temperature, and then ensure that the effectiveness of overall efficacy.
Embodiment 2
A kind of environmental protection ultra concentration is washed one's hands sheet/granule, and this environmental protection ultra concentration sheet/granule of washing one's hands is made by following method；
Step S001, with 100 grams for the full part of constituent, take anion active agent laureth sulfosuccinic in proportion
Acid esters disodium (being called for short CAS) 26 grams, 16 grams of fatty acid methyl ester ethoxylate sulfonate (being called for short FMES) also make both mix
Compound, thus form gross mass be 42 grams, mixing ratio be the mixed type anion active agent of 13:8；
The most negated ionic surfactant alkyl polyglucoside (APG for short) 15 grams, coconut oil fatty acid monoethanolamide (letter
Claim CMEA) 12 grams and make both carry out mixture, thus form gross mass be 27 grams, mixing ratio be the mixed type nonionic of 5:4
Activating agent；
Take amphoteric surfactant glycol distearate 10 grams the most in proportion, with above-mentioned mixed type anion active agent
And mixed type tween puts into preparation container being stirred continuously together；
Take fatting agent isopropyl myristate and 2 grams of the mixture of octyl group hydroxy stearic acid ester, skin moistening moisturizing the most in proportion
Agent propylene glycol 1.5 grams, skin moisturizing agent Aloe 1.5 grams, pH value regulator citric acid 2 grams, thickening agent xanthan gum 0.5 gram, antibacterial
Agent triclosan 1 gram, preservative sodium benzoate 0.3 gram, subtract lubrication prescription (C18-20 sec alkanol polyethers-9) 0.2 gram, 0.5 gram of essence,
And deionized water 30 grams, put into described preparation container equally, constantly stir evenly and make each component be sufficiently mixed, obtaining liquid ring
Protect wash one's hands sheet/granule of ultra concentration and make raw material；
Step S002, sheet/granule of liquid environment-friendly ultra concentration obtained in above-mentioned steps S001 being washed one's hands make raw material and put
In the pelletizer of band mummification function, carry out moisture evaporation by the high temperature of more than 80 degree, super dense by calculating liquid environment-friendly
Contracting is washed one's hands the thickness of sheet and enter the area in desiccation apparatus, carrys out Based Intelligent Control evaporation time, and then realizes surpassing liquid environment-friendly
Concentrate the moisture evaporation washing one's hands in sheet, and obtain the water content solid, shaped environmental protection ultra concentration type less than 6% and wash one's hands sheet；
Step S003, take described small-molecular peptides compound enzyme 5 grams, and it is entered according to the thinner ratio being not less than 1:0.5 with water
Add after row dilution in a kind of flusher, wherein, described small-molecular peptides compound enzyme be by small-molecular peptides powder and compound enzyme according to
The mixing ratio of 1:10 carries out the complex mixed, and compound enzyme described among these is amylase, lipase, mannonase egg
White four kinds of enzymes of enzyme carry out mixed four-in-one compound enzyme according to the mixing ratio of 2:3:1:4；
Step S004, will in flusher described in above-mentioned steps S003 dilution after described small-molecular peptides compound enzyme, spray
It is sprinkled upon in above-mentioned steps S002 obtained solid, shaped environmental protection ultra concentration type to wash one's hands on sheet surface, and dries.
Further, the present embodiment also proposed a kind of environmental protection ultra concentration and washes one's hands the manufacture method of granule, this manufacture method
Preamble work as the wash one's hands manufacture method of sheet of above-mentioned environmental protection ultra concentration consistent, follow-up work is: will be through above-mentioned steps
Chip solid environmental protection ultra concentration type sheet of washing one's hands after S004 processes puts into comminutor, produce particle diameter be not less than 0.1cm
Granular environmental protection ultra concentration type is washed one's hands granule.
In sum, environmental protection ultra concentration type out made by the present embodiment is washed one's hands sheet/granule, its constituent and percentage
Ratio is as described below:
Above-mentioned environmental protection ultra concentration type out made by the present embodiment is washed one's hands sheet/granule, is had compared with existing product
Unique distinction be: utilize the small-molecular peptides four-in-one compound enzyme that mixing ratio is 1:10, come to anion active agent lauryl alcohol gather
Ether sulfosuccinates disodium and the mixture of fatty acid methyl ester ethoxylate sulfonate, tween alkyl polyglucoside with
The mixture of coconut oil fatty acid monoethanolamide and the active ingredient of amphoteric surfactant glycol distearate enter
Exciting of row maximum capacity, and then promote the solubilization dirt-removing power of above-mentioned activating agent at double.Especially in four-in-one compound enzyme
The detergent power of anion active agent, under the facilitation of small-molecular peptides, can be performed to ultimate attainment by protease.
Meanwhile, by adding pH value regulator citric acid in integral formula so that overall pH value is closer to human body skin
Acidic physique, alkalogenic burn feeling will not be produced；Also by fatting agent isopropyl myristate and octyl group hydroxy stearic acid ester
Mixture, skin moistening wetting agent propylene glycol and the interpolation of skin moisturizing agent Aloe, be possible not only to effectively protect user
Hands will not occur the discomfort such as defat, dry and cracked, puckery wrinkle, and may also operate as good moistening and effect of maintenance hand skin；
Lubrication prescription C18-20 sec alkanol polyethers-9 is subtracted so that user rinses more quick, does not has also by adding in integral formula
Soapy feeling, more saves the water resource of preciousness.
The present embodiment, also by first high temperature mummification, sprays the innovative technology of enzyme the most again, is effectively protected above-mentioned little molecule
The activity of peptide four-in-one compound enzyme will not be destroyed by high temperature, and then ensure that the effectiveness of overall efficacy.
Embodiment 3
A kind of environmental protection ultra concentration is washed one's hands sheet/granule, and this environmental protection ultra concentration sheet/granule of washing one's hands is made by following method；
Step S001, with 100 grams for the full part of constituent, take anion active agent alpha-olefin sodium sulfonate in proportion and (be called for short
AOS) 26 grams, 16 SASs (be called for short SAS) 18 grams, N-lauroyl sodium hydrogen alpha-aminoglutarate 16 grams make three mix
Thing, thus form gross mass be 60 grams, mixing ratio be the mixed type anion active agent of 13:9:8；
The most negated ionic surfactant coconut oil fatty acid monoethanolamide (being called for short CMEA) 8 grams, amphoteric surface live
Property agent decyl dimethyl hydroxypropyl sulfobetaines 13 grams, puts into preparation container together with above-mentioned mixed type anion active agent
In and be stirred continuously；
Take the most in proportion fatting agent pantothenylol 2 grams, skin moistening wetting agent liquid paraffin 1.5 grams, skin moisturizing agent Margarita liquid 1 gram,
PH value regulator citric acid 2 grams, thickening agent carrageenan 0.5 gram, 1 gram of antibacterial xylene chloride phenol, preservative lactoperoxidase
Enzyme 0.3 gram, subtract lubrication prescription (C18-20 sec alkanol polyethers-9) 0.2 gram, 0.5 gram of essence and deionized water 30 grams, put into equally
In described preparation container, constantly stir evenly and make each component be sufficiently mixed, obtaining wash one's hands sheet/granule of liquid environment-friendly ultra concentration and make former
Material；
Step S002, sheet/granule of liquid environment-friendly ultra concentration obtained in above-mentioned steps S001 being washed one's hands make raw material and put
In the pelletizer of band mummification function, carry out moisture evaporation by the high temperature of more than 80 degree, super dense by calculating liquid environment-friendly
Contracting is washed one's hands the thickness of sheet and enter the area in desiccation apparatus, carrys out Based Intelligent Control evaporation time, and then realizes surpassing liquid environment-friendly
Concentrate the moisture evaporation washing one's hands in sheet, and obtain the water content solid, shaped environmental protection ultra concentration type less than 6% and wash one's hands sheet；
Step S003, take described small-molecular peptides compound enzyme 5 grams, and it is entered according to the thinner ratio being not less than 1:0.5 with water
Add after row dilution in a kind of flusher, wherein, described small-molecular peptides compound enzyme be by small-molecular peptides powder and compound enzyme according to
The mixing ratio of 1:4 carries out the complex mixed, and the most described compound enzyme is cellulase, amylase, lipase, mannan
Enzyme, five kinds of enzymes of protease carry out mixed five in one compound enzyme according to the mixing ratio of 3:2:1:1:3；
Step S004, will in flusher described in above-mentioned steps S003 dilution after described small-molecular peptides compound enzyme, spray
It is sprinkled upon in above-mentioned steps S002 obtained solid, shaped environmental protection ultra concentration type to wash one's hands on sheet surface, and dries.
Further, the present embodiment also proposed a kind of environmental protection ultra concentration and washes one's hands the manufacture method of granule, this manufacture method
Preamble work as the wash one's hands manufacture method of sheet of above-mentioned environmental protection ultra concentration consistent, follow-up work is: will be through above-mentioned steps
Chip solid environmental protection ultra concentration type sheet of washing one's hands after S004 processes puts into comminutor, produce particle diameter be not less than 0.1cm
Granular environmental protection ultra concentration type is washed one's hands granule.
In sum, environmental protection ultra concentration type out made by the present embodiment is washed one's hands sheet/granule, its constituent and percentage
Ratio is as described below:
Above-mentioned environmental protection ultra concentration type out made by the present embodiment is washed one's hands sheet/granule, is had compared with existing product
Unique distinction be: utilize the small-molecular peptides five in one compound enzyme that mixing ratio is 1:4, come anion active agent alpha-olefin sulfonic acid
Sodium, 16 SASs, the mixture of N-lauroyl sodium hydrogen alpha-aminoglutarate three, tween coco-nut oil fatty acid list
The mixture of glycollic amide and the active ingredient of amphoteric surfactant decyl dimethyl hydroxypropyl sulfobetaines are carried out
Exciting of maximum capacity, and then promote the solubilization dirt-removing power of above-mentioned activating agent at double.The especially egg in five in one compound enzyme
The detergent power of anion active agent, under the facilitation of small-molecular peptides, can be performed to ultimate attainment by white enzyme.
Meanwhile, by adding pH value regulator citric acid in integral formula so that overall pH value is closer to human body skin
Acidic physique, alkalogenic burn feeling will not be produced；Also by fatting agent pantothenylol, skin moistening wetting agent liquid paraffin and skin
The interpolation of moisturizing agent Margarita liquid, is possible not only to effectively protect the hands of user that the discomfort such as defat, dry and cracked, puckery wrinkle will not occur,
And may also operate as good moistening and effect of maintenance hand skin；Lubrication prescription C18-is subtracted also by adding in integral formula
20 sec alkanol polyethers-9 so that user rinses more quick, does not has soapy feeling, more saves the water resource of preciousness.
The present embodiment, again by first high temperature mummification, sprays the innovative technology of enzyme the most again, is effectively protected above-mentioned little point
The activity of sub-peptide five in one compound enzyme will not be destroyed by high temperature, and then ensure that the effectiveness of overall efficacy.
Detersive efficiency contrast experiment
Take made by above-mentioned 3 kinds of embodiments environmental protection ultra concentration out to wash one's hands sheet/granule, with washing of current commercial type
Hands liquid carries out contrast test, respectively from removing fatty oil, vegetable oil, machine oil, and the detersive efficiency of several dirt such as pigment, dirt,
And whether there is burn feeling, soapy feeling etc. and carry out comparative evaluation when using, result such as following table.
Above-mentioned experiment finds, the sheet/granule of washing one's hands of the environmental protection ultra concentration made by 3 kinds of embodiments provided by the present invention is each
Item detersive efficiency is above the most existing washing one's hands.
The ultimate principle of the present invention and principal character and advantages of the present invention have more than been shown and described.The technology of the industry
Personnel, it should be appreciated that the present invention is not restricted to the described embodiments, simply illustrating this described in above-described embodiment and description
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these become
Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and
Equivalent defines.
Claims (8)
1. environmental protection ultra concentration is washed one's hands sheet/granule, it is characterised in that this sheet/granule of washing one's hands includes the component of following mass percent:
Accounting is the anion active agent of 10-60%, described anion active agent be laureth sulfosuccinate disodium,
Brij 35 sodium sulfate, MES, fatty acid methyl ester ethoxylate sulfonate, alpha-olefin
The one of sodium sulfonate, 16 SASs, lauroyl sodium isethionate, N-lauroyl sodium hydrogen alpha-aminoglutarate, potash soap, soda soap etc.
Plant or multiple mixture；
Accounting is the tween of 10-30%, and described tween is alkyl polyglucoside, coco-nut oil fatty acid monoethanol
One or both mixture of amide etc.；
Accounting is the amphoteric surfactant of 1-15%, and described amphoteric surfactant is cocoamidopropyl dimethyl Radix Betae
One or more of alkali, glycol distearate, coco imidoazolinium, decyl dimethyl hydroxypropyl sulfobetaines etc. are mixed
Compound；
Accounting is the small-molecular peptides compound enzyme of 1-6%；
Accounting is the fatting agent of 1-3%, and described fatting agent is monoglyceride, glyceryl cocoate, isopropyl myristate, glycerol
One or more mixture in cocoyl macrogol ester, octyl group hydroxy stearic acid ester, polyquaternary ammonium salt-7, glycerol, pantothenylol；
Accounting is the skin moistening wetting agent of 1-3%, described skin moistening wetting agent be liquid paraffin, glycerol, ethylene glycol, sorbitol, the third two
One or more mixture in alcohol and alkyl polyglucoside；
Accounting is the skin moisturizing agent of 1-3%, and described skin moisturizing agent is sorbitol, propylene glycol, Aloe, Mel, ginseng liquid, treasure
One or more mixture of pearl liquid, pollen, milk, silicone oil, glycerol, aminoacid etc.；
Accounting is the pH value regulator of 1-3%, and described pH value regulator is citric acid；
Accounting is the thickening agent of 2-6%, and described thickening agent is xanthan gum, sodium alginate, carrageenan, hydroxymethyl cellulose, chlorination
One or more mixture in sodium, polyvinyl alcohol；
Accounting is the antibacterial of 0.1-1%, and described antibacterial is in triclocarban, triclosan, hydroxyl phenylate, xylene chloride phenol
One or more mixture；
Accounting is the preservative of 0.1-0.5%, and described preservative is in Kazon, sodium benzoate, phenoxyethanol, lactoperoxidase
One or more mixture；
Accounting be 0.1-0.5% subtract lubrication prescription；
Accounting is the essence of 0.1-1%；
The deionized water of surplus.
Environmental protection ultra concentration the most according to claim 1 is washed one's hands sheet/granule, it is characterised in that this environmental protection ultra concentration wash one's hands sheet/
Constituent and mass percent after granule drying are as described below:
。
Environmental protection ultra concentration the most according to claim 1 is washed one's hands sheet/granule, it is characterised in that this environmental protection ultra concentration is washed one's hands sheet
Constituent and mass percent after drying/granule are as described below:
。
Environmental protection ultra concentration the most according to claim 1 is washed one's hands sheet/granule, it is characterised in that this environmental protection ultra concentration wash one's hands sheet/
Constituent and mass percent after granule drying are as described below:
。
5. wash one's hands sheet/granule according to the environmental protection ultra concentration described in claim 1-4 any one claim, it is characterised in that
Described small-molecular peptides compound enzyme is the complex that small-molecular peptides powder carries out according to the mixing ratio of 1:4 1:19 with compound enzyme mixing,
Wherein, described compound enzyme is mixed by two or more in amylase, protease, lipase, cellulase, mannase
Conjunction forms.
Environmental protection ultra concentration the most according to claim 5 is washed one's hands sheet/granule, it is characterised in that described compound enzyme be amylase,
Lipase, three kinds of enzymes of protease carry out mixed three-in-one compound enzyme according to the mixing ratio of 3:3:4；
Or, described compound enzyme is that amylase, lipase, four kinds of enzymes of mannonase protease are according to the mixing ratio of 2:3:1:4
Carry out mixed four-in-one compound enzyme；
Or, described compound enzyme be cellulase, amylase, lipase, five kinds of enzymes of mannonase protease according to 3:2:1:1:
The mixing ratio of 3 carries out mixed five in one compound enzyme.
7. environmental protection ultra concentration is washed one's hands the manufacture method of sheet/granule, it is characterised in that this manufacture method comprises the following steps:
Step S001, in proportion take anion active agent described in the claims 14 any one, tween,
And amphoteric surfactant put into preparation container, be stirred continuously, then take the claims 14 any one in proportion
Described fatting agent, skin moistening wetting agent, skin moisturizing agent, pH value regulator, thickening agent, antibacterial, preservative, subtract lubrication prescription, perfume (or spice)
Essence and appropriate amount of deionized water put into described preparation container equally, constantly stir evenly and make each component be sufficiently mixed, obtaining liquid
Wash one's hands sheet/granule of environmental protection ultra concentration makes raw material；
Step S002, sheet/granule of liquid environment-friendly ultra concentration obtained in above-mentioned steps S001 being washed one's hands make raw material and are placed in band
In having the pelletizer of mummification function, carry out moisture evaporation under the condition of high temperature more than 80 degrees Celsius, and prepared water content is not
Ultra concentration type more than 6% is washed one's hands sheet；
Step S003, take described small-molecular peptides compound enzyme, and after itself and water are diluted according to the thinner ratio being not less than 1:0.5
Add in flusher；
Step S004, by small-molecular peptides compound enzyme described in the liquid state in flusher described in above-mentioned steps S003, be sprayed at
Ultra concentration type obtained in above-mentioned steps S002 is washed one's hands on sheet surface, and dries.
Environmental protection ultra concentration the most according to claim 7 is washed one's hands the manufacture method of sheet/granule, it is characterised in that will be through institute
State the chip solid ultra concentration type sheet of washing one's hands after step S004 processes and put into comminutor, produce particle diameter and be not less than 0.1cm's
Graininess ultra concentration type is washed one's hands granule.
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| CN201610379567.3A CN106038352A (en) | 2016-06-01 | 2016-06-01 | Environment-friendly super-concentrated hand washing slices/granules and manufacturing method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110200846A (en) * | 2019-07-11 | 2019-09-06 | 武汉轻工大学 | A kind of oil-control moisturizing mildy wash and preparation method thereof |
| CN110924175A (en) * | 2019-12-13 | 2020-03-27 | 广州立白企业集团有限公司 | Fabric care tablet |
| CN113603976A (en) * | 2021-08-17 | 2021-11-05 | 广州北极光生物科技有限公司 | Preparation method of macromolecular rheological slip reducer |
| GB2601632A (en) * | 2020-11-30 | 2022-06-08 | Henkel Ag & Co Kgaa | Process for the preparation of a ready-to-use, cosmetic, flowable detergent |
| US20220323339A1 (en) * | 2021-04-01 | 2022-10-13 | baresop Pty Ltd | Cleanser |
-
2016
- 2016-06-01 CN CN201610379567.3A patent/CN106038352A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110200846A (en) * | 2019-07-11 | 2019-09-06 | 武汉轻工大学 | A kind of oil-control moisturizing mildy wash and preparation method thereof |
| CN110924175A (en) * | 2019-12-13 | 2020-03-27 | 广州立白企业集团有限公司 | Fabric care tablet |
| GB2601632A (en) * | 2020-11-30 | 2022-06-08 | Henkel Ag & Co Kgaa | Process for the preparation of a ready-to-use, cosmetic, flowable detergent |
| US20220323339A1 (en) * | 2021-04-01 | 2022-10-13 | baresop Pty Ltd | Cleanser |
| CN113603976A (en) * | 2021-08-17 | 2021-11-05 | 广州北极光生物科技有限公司 | Preparation method of macromolecular rheological slip reducer |
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Application publication date: 20161026 |