CN1060109A - High efficient sterilizing toilet soap - Google Patents

High efficient sterilizing toilet soap Download PDF

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Publication number
CN1060109A
CN1060109A CN 90107854 CN90107854A CN1060109A CN 1060109 A CN1060109 A CN 1060109A CN 90107854 CN90107854 CN 90107854 CN 90107854 A CN90107854 A CN 90107854A CN 1060109 A CN1060109 A CN 1060109A
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China
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high efficient
efficient sterilizing
toilet soap
weight
sterilizing toilet
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CN 90107854
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Chinese (zh)
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铁汉
铁毅
铁萍
铁燕
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Individual
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Individual
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Abstract

The invention provides a kind of high efficient sterilizing toilet soap, make with boiling process or half boiled process, cold method for making by Viscotrol C, Oleum Cocois, alkali lye, fractional oil of haw kernel, soft water, ethanol, pure glycerin, dyestuff, spices etc.That high efficient sterilizing toilet soap can be made into solid, liquid or powdered.It obviously is better than the various medicated soaps of today, and it the time not only has dense foam in washing, and can kill the Pseudomonas aeruginosa that hides in skin histology, intestinal bacteria, Bacillus proteus, streptococcus aureus, yeast-like fungi, streptococcus faecium etc.To various skin sick as: neurodermatitis, eczema, tickling dermatosis have special efficacy.Also can regulate metabolism, stimulate circulation.Life-time service can make skin, face reach the purpose of beauty treatment.Its production technique is simple, with low cost, easy to use.

Description

High efficient sterilizing toilet soap
The present invention relates to a kind of new soap, particularly slip the high efficient sterilizing toilet soap that wet goods makes, and make the method for this high efficient sterilizing toilet soap with Semen Crataegi.
At present, the soap of selling on the market mainly contains the function of removing dirt and decomposing the oil skinning on the skin, and the effect of its sterilization and disinfection is very poor.
In order to solve the problem that general soap exists, some medicated soaps are come out one after another, as: carbolic soap, superchlorination hydrogen soap, sulfur soap, iodoform soap, boric soap etc.But very little to killing the bacterium ability of hiding in skin histology, what have also has pungency to skin, and perhaps cost is higher.
The objective of the invention is to overcome the shortcoming that above-mentioned existing soap exists; make a kind of dirt and the cutting grease property skinning that can not only remove on the skin; and can kill the bacterium that hides in skin histology, nonirritant and any pair of effect again has the high efficient sterilizing toilet soap of provide protection to skin.
The present invention is achieved in that a certain amount of oil fusing, add alkali lye and begin to carry out saponification, add a certain amount of Semen Crataegi then successively and slip oil, soft water, alcohol, pure glycerin, dye solution (usefulness soft water molten it), spices, use boiling process, perhaps half boiled process, cold method for making promptly can be made into finished product.
Particularly, the used Semen Crataegi slide oil of the present invention is the inventor's an invention achievement.It is the nuclear by Rosaceae may Fruit of Pashi Pear, through doing a kind of fraction of slipping and obtaining, forms through evaporation concentration again, its proterties is the black thick liquid, and deeply worried smell is arranged, and PH is 2-2.5, proportion is 1.13-1.19, and is water insoluble, dissolves in organic solvents such as ether.Semen Crataegi slide oil has extremely strong killing action to Pseudomonas aeruginosa, intestinal bacteria, Bacillus proteus, streptococcus aureus, yeast-like fungi, streptococcus faecium etc.It just is being based on above characteristics as sterilant in the present invention.Its in the present invention content be 0.5-8%(weight), be preferably 1.2-5%(weight).
Being used to make the glyceride stock of the present invention's high efficient sterilizing toilet soap, can be the grease of any plant and animal.As Oleum Cocois, plam oil, Viscotrol C, soya-bean oil, tea oil, Semen Maydis oil, peanut oil, Tallow Inedible Grade, lard, bone fat oil, house oil, whale oil, fish oil, or similar grease is as lipid acid, winterized stearin, resin, bitter edible plant acids.Commercially available Viscotrol C and Oleum Cocois have been used in a preferred embodiment of the invention.
Oleum Cocois is the solid of white softness at normal temperatures, special fragrance is arranged, proportion 0.926.Because of its Chemical Composition contains bay resin, the cardamom fat of volume,, and eliminate very speed so the soap bubble foam that is become is abundant especially, very easily water-soluble, though use high alkali liquid under low temperature, also play saponification, its in the present invention content be 10-30%(weight), be preferably 20-27%(weight).
Viscotrol C is the dense oil of colourless or little green, though very sticky, be placed in the air and can not do with fixed attention, optical rotatory power is very strong, and proportion is very big, is 0.950-0.970.Can both dissolve with any ratio of straight alcohol.It is very few that its composition contains solid fatty acid, based on ricinolic acid, alkalinization in various oil for the easiest can with the high alkali liquid chemical combination of 30 ° of-36 ° of BE, though add, also react at once in low temperature.Only foam is not rich, therefore with Oleum Cocois mixing soapmaking better effects if, its in the present invention content be 3-22%(weight), be preferably 5-19%(weight).
The alkali lye that is used to make the present invention's high efficient sterilizing toilet soap can be alkali lye such as caustic lye of soda, potassium hydroxide solution, yellow soda ash liquid, or salt of wormwood liquid.Used commercially available caustic lye of soda in a preferred embodiment of the invention, or potassium hydroxide solution.
Sodium hydroxide (NaOH) is also referred to as caustic soda, is the feathery crystalline material of White-opalescent, molecular weight 40.01, fusing point is 320 °-324 ℃ centre, the boiling point height, viscosity is big, and thermal conductivity is low, it is not evaporable reason, matter is very crisp, is dissolved in the very high heat of generation in the water, and the aqueous solution is strong basicity, its content in the present invention is 10-31%(weight), be preferably 12-28%(weight).
Alcohol claims ethanol (CH again 3CH 2OH), be the most frequently used Cidex-7, in the present invention as solvent.It can promote the chemical combination speed of grease and alkali lye, can make dense alkali lye and grease chemical combination rapid, and saponification is complete.Therefore the solubleness of soap in alcohol can get clean clear solution greater than the solubleness of water, behind the vaporized alcohol, then only leaves gluey transparent soap matter.It accounts for 5-23%(weight in the present invention), be preferably 8-20%(weight).
Glycerine (glycerol), molecular formula C 3H 8O 3, be colourless magma, it is slightly sweet to distinguish the flavor of.Can not only absorb airborne moisture content, make local organization softening, increase the soft and moist property of skin, and in the present invention also as solvent.It can promote grease and the rapid chemical combination of alkali lye, makes their saponification complete, and the soap qualitative change is soft, can also increase the transparency of high efficient sterilizing toilet soap in addition.It accounts for 1-10%(weight in the present invention), be preferably 2-8.5%(weight).
Soft water is raw material indispensable among the present invention, and oil and alkali no doubt can be saponified into soap, if but there is not water as media, endure also difficult one-tenth soap though often boil for a long time.Therefore the present invention selects the soft water (in case becoming insoluble calcium soap and magnesium soap) of salt such as calcic magnesium not for use, and with the effect of the washing sterilization and disinfection that increases high efficient sterilizing toilet soap, it accounts for 2-18%(weight in the present invention), be preferably 3-14%(weight).
Spices not only can use its fragrance, makes it to bring out spiritual happiness and excitement, and has sterilizing power, and is also very remarkable on the usefulness for anticorrosion and health.It can also shelter the oily smelly of soap, makes the people play aesthetic feeling.Spices among the present invention is synthetic perfume or natural perfume, be to concoct by the spices of majority to form, and add fixer or fixative therein, to suppress the volatilization of fragrance, it accounts for 0.1%-2.5%(weight in the present invention), be preferably 0.5-1.5%(weight).
The present invention can use various dyestuffs, makes the soap of various colors as required.But must note to add the dyestuff (as Prussian blue) of the effect of giving birth to soap.It accounts for 0.01 ‰-0.1 ‰ (weight) in the present invention, is preferably 0.02 ‰-0.08 ‰ (weight).
The production technique of high efficient sterilizing toilet soap can adopt boiling process, and half boiled process or cold method for making with Oleum Cocois and Viscotrol C fusing, add alkali lye again, add Semen Crataegi slide oil, soft water, alcohol glycerine, dyestuff, spices etc. then successively.After effect is finished, inject soap frame and solidify.Stripping and slicing then, die mould promptly make finished product.
Embodiment one:
Boiling process system high efficient sterilizing toilet soap:
With 158 jin of Oleum Cocois, Viscotrol C is put into pot for 56 jin, 37 ° of-49 ℃ of fusings, add 135 jin of caustic lye of sodas (38 ° of BE), left standstill 24 hours, feeding steam then boiled 3-4 hour, stir with agitator simultaneously, the soap saponification is finished, see that the limpid heating power that is about to of mixture deducts, add Semen Crataegi this moment and slip oily 20 jin, stir.Add 30.75 jin of soft water, after stirring with agitator, left standstill again one hour.In stirring rapidly, add 110 jin of ethanol, 34 jin of pure glycerins with molten it.This moment, pot should heat, but should not exceed 55 °-70 ℃.Then soap solution is placed in the distiller, and connects a condenser, promptly have the ethanol about 65% recoverable.Be transported into cold trap deviating from the alcoholic acid soap lye, before not solidifying, add 1.5 jin of dye solutions (1/4 liang of acid green adds 1.25 jin of soft water), synthetic perfume 2 jin of (3 liang of violet roots, 3 liang of Oleum lavandula angustifolias, 5 liang of sarcodactylis oil fus, 3 liang of Oleum Cinnamomis, M-nitro benzoic acid<be fixative>6 liang), stir.Be stripping and slicing, die mould after waiting it to condense, promptly get transparent high efficient sterilizing toilet soap.
Embodiment two:
Half boiled process system high efficient sterilizing toilet soap:
With 100 jin of Viscotrol C, 150 jin of injection mixing machines of Oleum Cocois, heat is to 75 °-80 ℃.Caustic lye of soda (38 ° of BE) is added stirring for 150 jin.Feed with dry steam simultaneously, make the mixing machine temperature remain on 80 ° of-90 ℃ of centres.Stir after half an hour, add Semen Crataegi and slip oily 8 jin, under lasting the stirring, add 61.5 jin of soft water, stir 55 jin of ethanol of back adding, 20 jin of pure glycerins, the stirring 2-3 that does not stop hour, and temperature is remained between 80 °-90 ℃ always.Add dye solution (1/2 liang of acid violet dyestuff adds 2.5 jin of soft water) then, add 3 jin of spices (1.2 jin of santal oils, 0.8 jin of sarcodactylis oil fu, sunflower olein<for fixative>1 jin) at last.Leave standstill after stirring.When the material in the mixing machine becomes smooth and during the uniform soap glue of stiff, injects soap frame, must stir the fraud of avoiding taking place striped half an hour this moment, gets final product stripping and slicing, die mould after solidifying.Promptly get high efficient sterilizing toilet soap.
Embodiment three:
Cold method for making system high efficient sterilizing toilet soap:
With 260 jin of Oleum Cocois, 180 jin of Viscotrol C are put the installing steam sleeve into and are reached the pot of having agitator, and with 37 ° of-44 ℃ of fusings, (38 ° of BE) puts into 268 jin of caustic lye of sodas.The buck temperature is 21 °-26 ℃ in summer, and must heat just can add in the oil to 27 ℃ winter.Constantly stir so that oil and alkali gradually emulsification become sticky thick.A little checks it to take out sample, and is not estranged from phenomenon.When emulsification is the pulpous state of stiff, add Semen Crataegi and slip oily 50 jin, 67 jin of soft water of back adding stir, continuing to add 130 jin of alcohol, 70 jin of pure glycerins under the stirring, be stirred to mixture evenly after, feed exsiccant steam and make it temperature and be increased to 58 °-65 ℃ this moment, continue to stir 15-30 minute, it is mixed.Place half an hour, take out sample a little, whether check contains excessive free alkali etc.Till suitable fully.The brown dye solution (1 liang of brown dye adds 5 jin of soft water) that has prepared is put into, continuing under the stirring, add 4.75 jin of spices at last (with 1.5 jin of rose leaf oils, 1.75 jin of sassafras wood oils, synthetic musk<for fixative>1.5 jin synthetic spices) effect is finished back injection soap frame and is solidified, at room temperature placed 3-7 days.Cut bar, stripping and slicing, die mould then, can obtain the high high efficient sterilizing toilet soap of slickness.
If add ash charge alkali, borax or sodium phosphate etc. in the above-described embodiment, under stirring rapidly, be blown into pressurized air, when soap glue still is the semi liquid state of softness, dislocation is on the cold breakdown mill, and the surface that is distributed in cylinder will feed cold water for film like in the cylinder, then cool off and crystallization, milling at last is powdery, through sieving, can obtain the powdered high efficient sterilizing toilet soap again.
In addition,, change and be potassium hydroxide solution, can be made into the high efficient sterilizing toilet soap of liquid if the caustic lye of soda in the foregoing description.
High efficient sterilizing toilet soap of the present invention is cured attached the People's Hospital clinic trial through north, think that there is stable no Decomposition in the soap in the sterilant Semen Crataegi slide oil in the high efficient sterilizing toilet soap.It has dense foam, and quick permeation can directly contact with bacterium, can kill the Pseudomonas aeruginosa that hides in skin histology, streptococcus aureus, gas bacillus, intestinal bacteria, Bacillus proteus, streptococcus faecium etc.And to the various skin disease, as neurodermatitis, eczema, tickling dermatosis etc. are had special efficacy.
High efficient sterilizing toilet soap of the present invention obviously is better than the various medicated soaps of today, can regulate metabolism, stimulates circulation.Life-time service can make skin, face feel comfortably cool, smooth, soft and moist, reach the purpose of beauty treatment.Be applicable to family, medical institutions, kindergarten etc.And production technique is simple, and cost is low holds concurrently, easy to use.

Claims (10)

1, a kind of high efficient sterilizing toilet soap is made of sterilant, oil, alkali lye, soft water, ethanol, pure glycerin, dyestuff, spices.It is characterized in that said sterilant is a Semen Crataegi slide oil.Said oil can be the grease of any plant or animal.Or similar grease, wherein preferably Oleum Cocois and Viscotrol C.Said alkali lye can be caustic lye of soda, potassium hydroxide solution, yellow soda ash liquid, salt of wormwood liquid etc.Wherein preferably caustic lye of soda and potassium hydroxide solution.
2, according to the said high efficient sterilizing toilet soap of claim 1, it is characterized in that the added therein sufficient quantity of Semen Crataegi slide oil is a 0.5-8%(weight).
3,, it is characterized in that the added therein sufficient quantity of Oleum Cocois is a 10-30%(weight according to the said high efficient sterilizing toilet soap of claim 1), the added therein sufficient quantity of Viscotrol C is a 3-22%(weight).
4, according to the said high efficient sterilizing toilet soap of claim 1, it is characterized in that the added therein sufficient quantity of caustic lye of soda is a 10-31%(weight).
5, according to the said high efficient sterilizing toilet soap of claim 1, it is characterized in that the added therein sufficient quantity of soft water is a 2-18%(weight).
6, according to the said high efficient sterilizing toilet soap of claim 1, it is characterized in that the added therein sufficient quantity of ethanol is a 5-23%(weight).
7, according to the said high efficient sterilizing toilet soap of claim 1, it is characterized in that the added therein sufficient quantity of pure glycerin is a 1-10%(weight).
8,, it is characterized in that the added therein sufficient quantity of dyestuff is 0.01 ‰-0.1 ‰ (weight) according to the said high efficient sterilizing toilet soap of claim 1.
9, according to the said high efficient sterilizing toilet soap of claim 1, it is characterized in that the added therein sufficient quantity of spices is a 0.1%-0.25%(weight).
10, according to the said high efficient sterilizing toilet soap of claim 1, it is characterized in that can be made into solid, liquid or the powdered finished product.
CN 90107854 1990-09-25 1990-09-25 High efficient sterilizing toilet soap Pending CN1060109A (en)

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Application Number Priority Date Filing Date Title
CN 90107854 CN1060109A (en) 1990-09-25 1990-09-25 High efficient sterilizing toilet soap

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Application Number Priority Date Filing Date Title
CN 90107854 CN1060109A (en) 1990-09-25 1990-09-25 High efficient sterilizing toilet soap

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CN1060109A true CN1060109A (en) 1992-04-08

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1038768C (en) * 1994-03-28 1998-06-17 吉林市日用化学工业公司 Toilet soap special for women
CN1045991C (en) * 1994-06-10 1999-10-27 钮韵雯 Cleaning and sterilizing agent
CN1058747C (en) * 1996-06-28 2000-11-22 青岛医学院附属专科医院 Cosmetic soap for removing acne
CN1062010C (en) * 1994-06-10 2001-02-14 钮韵雯 Cleaning and sterilizing soap
CN1088103C (en) * 1997-12-30 2002-07-24 张长进 Medicinal soap containing propolis
CN1101404C (en) * 1998-07-29 2003-02-12 中德联合研究院 Anti Bacillus pyocyaneu Flugge vitelline immunoglobulin products and use thereof
CN110835587A (en) * 2019-11-20 2020-02-25 茗汲(浙江)生物科技有限公司 White tea antibacterial handmade soap and preparation method thereof
CN111979065A (en) * 2020-08-27 2020-11-24 刘克武 Wormwood soap and preparation method thereof

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1038768C (en) * 1994-03-28 1998-06-17 吉林市日用化学工业公司 Toilet soap special for women
CN1045991C (en) * 1994-06-10 1999-10-27 钮韵雯 Cleaning and sterilizing agent
CN1062010C (en) * 1994-06-10 2001-02-14 钮韵雯 Cleaning and sterilizing soap
CN1058747C (en) * 1996-06-28 2000-11-22 青岛医学院附属专科医院 Cosmetic soap for removing acne
CN1088103C (en) * 1997-12-30 2002-07-24 张长进 Medicinal soap containing propolis
CN1101404C (en) * 1998-07-29 2003-02-12 中德联合研究院 Anti Bacillus pyocyaneu Flugge vitelline immunoglobulin products and use thereof
CN110835587A (en) * 2019-11-20 2020-02-25 茗汲(浙江)生物科技有限公司 White tea antibacterial handmade soap and preparation method thereof
CN111979065A (en) * 2020-08-27 2020-11-24 刘克武 Wormwood soap and preparation method thereof

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