CN106007811B - A kind of preparation method of microcrystalline diamond ceramic tile - Google Patents
A kind of preparation method of microcrystalline diamond ceramic tile Download PDFInfo
- Publication number
- CN106007811B CN106007811B CN201610358021.XA CN201610358021A CN106007811B CN 106007811 B CN106007811 B CN 106007811B CN 201610358021 A CN201610358021 A CN 201610358021A CN 106007811 B CN106007811 B CN 106007811B
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- Prior art keywords
- ceramic tile
- charity
- preparation
- microcrystalline diamond
- base
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- 239000000919 ceramic Substances 0.000 title claims abstract description 28
- 229910003460 diamond Inorganic materials 0.000 title claims abstract description 19
- 239000010432 diamond Substances 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000011449 brick Substances 0.000 claims abstract description 47
- 238000010304 firing Methods 0.000 claims abstract description 12
- 238000005498 polishing Methods 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 238000009966 trimming Methods 0.000 claims abstract description 7
- 238000007688 edging Methods 0.000 claims abstract description 6
- 238000007639 printing Methods 0.000 claims abstract description 6
- 239000010410 layer Substances 0.000 abstract description 15
- 238000005516 engineering process Methods 0.000 abstract description 4
- 230000003373 anti-fouling effect Effects 0.000 abstract description 3
- 239000011248 coating agent Substances 0.000 abstract description 3
- 238000000576 coating method Methods 0.000 abstract description 3
- 239000002344 surface layer Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 238000005034 decoration Methods 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 239000004575 stone Substances 0.000 description 3
- 239000000428 dust Substances 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- KZHJGOXRZJKJNY-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Si]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O.O=[Al]O[Al]=O KZHJGOXRZJKJNY-UHFFFAOYSA-N 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000003475 lamination Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000013081 microcrystal Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052863 mullite Inorganic materials 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28B3/00—Producing shaped articles from the material by using presses; Presses specially adapted therefor
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Finishing Walls (AREA)
- Devices For Post-Treatments, Processing, Supply, Discharge, And Other Processes (AREA)
Abstract
The present invention relates to building dress ceramic technology fields to include the following steps in particular to a kind of preparation method of microcrystalline diamond ceramic tile：1）It will be used for the mixing of base brick adobe raw material and be pressed into base brick adobe；2）The charity overglaze in base brick adobe surface；3）Colored printing pattern is oozed in ink-jet on overglaze；4）Clear frit is enclosed in one layer of Buddha's warrior attendant glaze of the surface profile charity, then in surrounding charity one；5）Into klining system；6）After firing after polishing, trimming, edging finished product.Microcrystalline diamond ceramic tile surface layer microcrystalline coating prepared by the present invention is relatively thin, wearability is good, antifouling strong.
Description
Technical field
The present invention relates to building dress ceramic technology fields, in particular to a kind of preparation side of microcrystalline diamond ceramic tile
Method.
Background technology
Ceramics are applied to building trade more and more, and ceramic brick product is widely used in communal facility, building trade
And in family.With the raising of modern architecture ceramic building material finishing requirements, the building with characteristics such as lithotome fashion, noble qualities
Ceramic microcrystalline Buddha's warrior attendant stone ceramic tile is increasingly used widely.
Although traditional crystallite stone ceramic tile has sparkling and crystal-clear soft and moist, the brilliant decorative effect of plate face, surface glaze layer glass
Xiang Duo, Mohs' hardness is relatively low, is easy to scratch.
Although another traditional crystallite stone ceramic tile solves pattern diversification, color is more bright-coloured, svelteness, but production technology
Upper glassy layer is thicker to be also easy to produce stomata, and antifouling property is poor and production cost is higher.
Invention content
The object of the present invention is to provide a kind of preparation methods of microcrystalline diamond ceramic tile, to solve the microcrystalline diamond prepared
The problem of thicker, not wear-resisting, the antifouling difference of ceramic tile surface layer microcrystalline coating.
To achieve the purpose of the present invention, the technical solution used for：
A kind of preparation method of microcrystalline diamond ceramic tile, includes the following steps：
1）It will be used for the mixing of base brick adobe raw material and be pressed into base brick adobe；
2）The charity overglaze in base brick adobe surface；
3）Colored printing pattern is oozed in ink-jet on overglaze；
4）Clear frit is enclosed in one layer of Buddha's warrior attendant glaze of the surface profile charity, then in surrounding charity one；
5）Into klining system；
6）After firing after polishing, trimming, edging finished product.
Preferably, the step 1）Middle compacting is that the press using tonnage more than 1000 tons is suppressed.
Preferably, the step 1）Surrounding has regular groove at base brick adobe marginal surface obtained.
Preferably, in the groove side group brick adobe surface edge at flat.
Preferably, the groove distance base brick adobe edge 5-30mm, the recess width is 0.5 3cm, depth 0.2
−3mm。
Preferably, the step 4）Charity Buddha's warrior attendant glaze and clear frit also can be used the compacting of 2200 tons of press fill it is flat.
Preferably, the step 5）It once fires in kiln and is completed by two stages, first stage firing temperature is
1150-1180 DEG C, 1200-1350 DEG C of second stage.
Advantageous effect of the present invention：
One, flower is oozed using ink-jet, realizes pattern diversification, texture is more rich, and color development is more bright-coloured, and tone is distincter.
Two, full wafer brick texture is more perfect, and the effect used is more preferable, and the diamond dust that surface charity contains 350-1000 mesh is transparent
Glaze forms Buddha's warrior attendant glaze, Buddha's warrior attendant glazed thickness is less than 1mm, and the transparent glazed thickness of edge reduces the glass in brick face in 1-3mm
Glass phase improves the Mohs' hardness and abrasion resistance of product added with diamond dust, and in adobe surrounding flaky process, charity is transparent again
Glaze has saved raw material in this way, while making that its surface has the brick face texture of microlite and side is apparent thicker microcrystalline coating,
Improve sparkling and crystal-clear penetrating texture effect of the mullite crystalline phase of product surface without influencing brick face.
Three, the present invention uses great tonnage press using adobe compacting, closeer tight after so that adobe is suppressed, while also being adopted to glaze layer
It is compressed and is tamped with press, then be equipped with temperature firing of the later stage using different gradients, final products bubble-free generates, and surface only needs one
The small rut of secondary polishing, generation is few, therefore it also has very good soil resistance, and gloss is all kept for a long time after use
Degree, cleaning are convenient.
Four, groove is surrounded by when adobe is suppressed, trimming is convenient, while using same transparent engobe, surface layer and four
The glaze layer contact position in week is not in lamination, reaches and is perfectly combined.
Five, the ceramic tile prepared using the present invention has saved materials in the case where original process performance parameters do not reduce,
Reduce cost.
Description of the drawings
Fig. 1 is the vertical view of base brick adobe.
Fig. 2 is the sectional view of base brick adobe.
Specific implementation mode
As shown in Figure 1, 2, adobe is pressed by the brick adobe of structure base shown in Fig. 21 using press, which is provided with groove 2,
Clear frit is filled in groove 2, the base brick adobe surface of 2 inside of groove is equipped with cover coat 3, printed layer 4 and Buddha's warrior attendant glaze layer 5 successively,
Adobe surface edge uses flat on the inside of groove, and later stage cutting rear side viewing can form the process of a gradual change, promote aesthetic feeling.
It designs groove 1 and fills clear frit in it, post-production is cut in 1 vertical direction of groove, and such upper layer shows as micro-
Crystal layer, lower layer show as ceramic tile bottom base layer.
Embodiment 1
A kind of preparation method of microcrystalline diamond ceramic tile, includes the following steps：
1）It will be used for the mixing of base brick adobe raw material, tonnage is used to be pressed into base brick adobe, base brick brick for 1000 tons of press
Base surface edge surrounding has a regular groove, and side group brick adobe surface edge is at flat, groove distance base brick adobe side in groove
Edge 5mm, recess width 0.5cm, depth 0.2mm；
2）The charity overglaze in base brick adobe surface, plays decoration and bottom buffer action；
3）Colored printing pattern is oozed in ink-jet on overglaze；
4）Clear frit is enclosed in one layer of Buddha's warrior attendant glaze of the surface profile charity, then in surrounding charity one, 2200 are used after charity
Ton press fills Buddha's warrior attendant glaze and clear frit compacting flat；
5）Into klining system, once to fire in kiln and completed by two stages, first stage firing temperature is 1150 DEG C, the
1200 DEG C of two-stage；
6）After firing after polishing, trimming, edging finished product.
Embodiment 2
A kind of preparation method of microcrystalline diamond ceramic tile, includes the following steps：
1）It will be used for the mixing of base brick adobe raw material, tonnage is used to be pressed into base brick adobe, base brick brick for 8000 tons of press
Base surface edge surrounding has a regular groove, and side group brick adobe surface edge is at flat, groove distance base brick adobe table in groove
Face edge 15mm, recess width 1.5cm, depth 0.9mm；
2）The charity overglaze in base brick adobe surface, plays decoration and bottom buffer action；
3）Colored printing pattern is oozed in ink-jet on overglaze；
4）Clear frit is enclosed in one layer of Buddha's warrior attendant glaze of the surface profile charity, then in surrounding charity one, 2200 are used after charity
Ton press fills Buddha's warrior attendant glaze and clear frit compacting flat；
5）Into klining system, once to fire in kiln and completed by two stages, first stage firing temperature is 1165 DEG C, the
1290 DEG C of two-stage；
6）After firing after polishing, trimming, edging finished product.
Embodiment 3
A kind of preparation method of microcrystalline diamond ceramic tile, includes the following steps：
1）It will be used for the mixing of base brick adobe raw material, tonnage is used to be pressed into base brick adobe, base brick brick for 9000 tons of press
Base surface edge surrounding has a regular groove, and side group brick adobe surface edge is at flat, groove distance base brick adobe table in groove
Face edge 30mm, recess width 3cm, depth 3mm；
2）The charity overglaze in base brick adobe surface, plays decoration and bottom buffer action；
3）Colored printing pattern is oozed in ink-jet on overglaze；
4）Clear frit is enclosed in one layer of Buddha's warrior attendant glaze of the surface profile charity, then in surrounding charity one, 2200 are used after charity
Ton press fills Buddha's warrior attendant glaze and clear frit compacting flat；
5）Into klining system, once to fire in kiln and completed by two stages, first stage firing temperature is 1180 DEG C, the
1350 DEG C of two-stage；
6）After firing after polishing, trimming, edging finished product.
It should be understood that the application of the present invention is not limited to the above for those of ordinary skills can
With improvement or transformation based on the above description, all these modifications and variations should all belong to the guarantor of appended claims of the present invention
Protect range.
Claims (6)
1. a kind of preparation method of microcrystalline diamond ceramic tile, it is characterised in that：Include the following steps：
1）It will be used for the mixing of base brick adobe raw material and be pressed into base brick adobe；
2）The charity overglaze in base brick adobe surface；
3）Colored printing pattern is oozed in ink-jet on overglaze；
4）Clear frit is enclosed in one layer of Buddha's warrior attendant glaze of the surface profile charity, then in surrounding charity one；
5）Into klining system；
6）After firing after polishing, trimming, edging finished product；
The step 1）There is regular groove at base brick adobe marginal surface obtained.
2. the preparation method of microcrystalline diamond ceramic tile according to claim 1, it is characterised in that：The step 1）Middle compacting is
Press using tonnage more than 1000 tons or more is suppressed.
3. the preparation method of microcrystalline diamond ceramic tile according to claim 1, it is characterised in that：Side group brick brick in the groove
At flat at base marginal surface.
4. the preparation method of microcrystalline diamond ceramic tile according to claim 1, it is characterised in that：The groove distance base brick brick
Base edge 5-30mm, the recess width is 0.5 3cm, depth is 0.2 3mm.
5. the preparation method of microcrystalline diamond ceramic tile according to claim 1, it is characterised in that：The step 4）Charity Buddha's warrior attendant
Glaze and clear frit are filled flat using 2200 tons of press compactings.
6. the preparation method of microcrystalline diamond ceramic tile according to claim 1, it is characterised in that：The step 5）One in kiln
Secondary fire is completed by two stages, and first stage firing temperature is 1150-1180 DEG C, 1200-1350 DEG C of second stage.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610358021.XA CN106007811B (en) | 2016-05-26 | 2016-05-26 | A kind of preparation method of microcrystalline diamond ceramic tile |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610358021.XA CN106007811B (en) | 2016-05-26 | 2016-05-26 | A kind of preparation method of microcrystalline diamond ceramic tile |
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| Publication Number | Publication Date |
|---|---|
| CN106007811A CN106007811A (en) | 2016-10-12 |
| CN106007811B true CN106007811B (en) | 2018-10-23 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610358021.XA Expired - Fee Related CN106007811B (en) | 2016-05-26 | 2016-05-26 | A kind of preparation method of microcrystalline diamond ceramic tile |
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| Country | Link |
|---|---|
| CN (1) | CN106007811B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111848224A (en) * | 2020-07-22 | 2020-10-30 | 佛山欧神诺陶瓷有限公司 | Ceramic tile with metal flickering effect and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102329135A (en) * | 2011-09-30 | 2012-01-25 | 广东东鹏陶瓷股份有限公司 | Production method capable of firing polished crystal tile in one step |
| CN104311162A (en) * | 2014-10-11 | 2015-01-28 | 德清诺贝尔陶瓷有限公司 | Bump texture glazed tile and preparation method thereof |
| CN105272375A (en) * | 2015-10-29 | 2016-01-27 | 佛山市中成硅酸盐科技有限公司 | Wear resistant and high-hardness diamond glaze, preparation method and application |
-
2016
- 2016-05-26 CN CN201610358021.XA patent/CN106007811B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102329135A (en) * | 2011-09-30 | 2012-01-25 | 广东东鹏陶瓷股份有限公司 | Production method capable of firing polished crystal tile in one step |
| CN104311162A (en) * | 2014-10-11 | 2015-01-28 | 德清诺贝尔陶瓷有限公司 | Bump texture glazed tile and preparation method thereof |
| CN105272375A (en) * | 2015-10-29 | 2016-01-27 | 佛山市中成硅酸盐科技有限公司 | Wear resistant and high-hardness diamond glaze, preparation method and application |
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| Publication number | Publication date |
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| CN106007811A (en) | 2016-10-12 |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method of microcrystalline diamond ceramic brick Effective date of registration: 20181205 Granted publication date: 20181023 Pledgee: Jiajiang County Branch of Agricultural Bank of China Ltd. Pledgor: SICHUAN XINWANXING PORCELAIN CO.,LTD. Registration number: 2018510000132 |
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Date of cancellation: 20220630 Granted publication date: 20181023 Pledgee: Jiajiang County Branch of Agricultural Bank of China Ltd. Pledgor: SICHUAN XINWANXING PORCELAIN CO.,LTD. Registration number: 2018510000132 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method of microcrystalline diamond ceramic tile Effective date of registration: 20220708 Granted publication date: 20181023 Pledgee: Jiajiang County Branch of Agricultural Bank of China Ltd. Pledgor: SICHUAN XINWANXING PORCELAIN CO.,LTD. Registration number: Y2022980010172 |
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Granted publication date: 20181023 |