CN105997584A - Camellia oleosa seed oil repairing lipstick and preparation method thereof - Google Patents
Camellia oleosa seed oil repairing lipstick and preparation method thereof Download PDFInfo
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- CN105997584A CN105997584A CN201610374352.2A CN201610374352A CN105997584A CN 105997584 A CN105997584 A CN 105997584A CN 201610374352 A CN201610374352 A CN 201610374352A CN 105997584 A CN105997584 A CN 105997584A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/671—Vitamin A; Derivatives thereof, e.g. ester of vitamin A acid, ester of retinol, retinol, retinal
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention discloses a camellia oleosa seed oil repairing lipstick and a preparation method of the camellia oleosa seed oil repairing lipstick. The camellia oleosa seed oil repairing lipstick is prepared from camellia oleosa seed oil, wax, a film-forming agent, a moisturizer, an emulsifier, an antioxidant and a preservative. The preparation method comprises the following steps: heating the camellia oleosa seed oil to 25 DEG C, and adding alkaline liquor into the heated camellia oleosa seed oil; heating to 60 DEG C, carrying out stirring till flocculent soapstock emerges, and carrying out centrifugation for removing the flocculent soapstock; heating the material to 80 DEG C, adding the wax and the film-forming agent into the material, and carrying out stirring till the transparent liquid is obtained; keeping at 80 DEG C, adding the moisturizer and the emulsifier into the transparent liquid, and carrying out stirring for homogenizing; keeping at 80 DEG C, adding the antioxidant and the preservative into the homogeneous liquid, carrying out stirring till the liquid is homogeneous, placing the mixed material into a vacuum drying oven, carrying out reduced pressure treatment for removing air bubbles, taking out the mixed material and carrying out filling, and placing the filled mixed material in a mould for forming. The camellia oleosa seed oil repairing lipstick is yellow or milk white wax paste, is stick-shaped at normal temperature, has relatively good flexibility, has the natural smell of camellia oleosa, and has relatively good applying property and relatively good ductility, an applied layer is soft and moist, and the camellia oleosa seed oil repairing lipstick is safe without irritation, and has the health care effect after being used for a long time.
Description
Technical field
The present invention relates to field of lip cosmetics, be specifically related to a kind of lip pomade and corresponding preparation method.
Background technology
Lip balm product is aimed at the special physiological structure of lip and designs.Lip is to be made up of mucosa, with other portions
Point skin is compared mutually, does not has the accessory organs such as hair follicle, sebaceous gland, sweat gland, and horny layer is relatively thin, therefore its sebum and hidropoiesis
Measure the fewest, and at any time and air contact, it is easy to because ambient humidity change and desiccation.Lip balm product materials should be nothing
Poison, prevent user from being taken in by product during diet is drunk water internal, owing to lip and oral mucosa are close, therefore it is required that
Lip balm product does not has zest and specific peculiar smell.
Oil tea (CAMELLIA OLEIFERA) seed oil, for colourless to weak yellow liquid, its composition becomes split-phase with human body skin
Seemingly, oleic acid and linoleic acid total content are up to more than 90%, mainly three sweet three esters of oleic acid, are difficult to disappear without erucic acid, behenic acid etc.
Change component, VE content, than Fructus Canarii albi innage, has the laudatory title of " east olive oil ", China as edible vegetable oil,
It derives from food industry, has suitable safety.
Furthermore camellia seed oil is good with skin affinity, there is preferable permeability, it is easy to skin absorption.Camellia seed oil can improve
Erythrocyte superoxide dismutase activity, has antioxidation, can effectively remove free radical, the oxygen of suppression cortex liposome
Change.Camellia seed oil can repair the damage in cells of superficial layer membrane structure rich in unsaturated fatty acid, improves cytoactive, just has
To immunoregulation effect, medical science has the application played in terms of its pharmacological action, external curing scalds, burn, prevent and treat chap, scabies
Skin ulcer, dermatitis, eczema etc..In terms of cosmetics, camellia seed oil can play antipyretic and itching-stopping, effect of convergence skin moistening, is excellent protecting
Skin oils and fats.
The lip pomade great majority circulated on the market are with raw material making such as Dormant oils, mineral wax, vaseline, only form closure
Oil film reaches to lock water effect, and the materials safety in petrochemical industry source causes anxiety.Along with the development of cosmetic industry, pursue real
Safely and effectively product become trend.
There are the custom of edible oil Oleum Camelliae, the tradition of the most useful camellia seed oil skin Caring, Semen Camelliae in each area of China
Serviceability and the health-care effect of oil obtain being widely recognized as of the public, and therefore developing a kind of lip pomade based on camellia seed oil is ability
The problem that solution is needed in territory badly.
Summary of the invention
For existing lip pomade great majority with Dormant oils, mineral wax, the problem of the raw material making such as vaseline, the main mesh of the present invention
Be a kind of lip pomade with camellia seed oil as raw material is provided；It is simultaneous for this lip pomade and a kind of preparation method is provided；It is achieved in
Fully develop natural resources, improve the economic interests rate of Semen Camelliae, and the lip of the green effect type of exploitation makes to apply some make up.
In order to achieve the above object, the present invention adopts the following technical scheme that:
Scheme 1: a kind of camellia seed oil maintenance lip pomade, described maintenance lip pomade includes the component of following weight portion:
In above-mentioned camellia seed oil maintenance lip pomade one preferred version, described camellia seed oil be proportion 0.9l61 (d20/20),
Refraction coefficient 1.4612 (n40), acid number 1.12mg/g, the camellia seed oil of peroxide value 3.42mmol/kg.
In above-mentioned camellia seed oil maintenance lip pomade one preferred version, described wax is castor oil hydrogenated, candelilla wax, white honeybee
Wax, babassu vegetable wax, tribehenin essence, stearyl alcohol Cera Flava acid esters, in spermol ricinoleate ester one or more
Mixture.
In above-mentioned camellia seed oil maintenance lip pomade one preferred version, described film former be polyisobutylene, glyceryl abietate,
One or more mixture in pentaerythritol abietate, organic siliconresin.
In above-mentioned camellia seed oil maintenance lip pomade one preferred version, described wetting agent is glycerol, dipropylene glycol, 1,3 fourth two
One or more mixture in alcohol.
In above-mentioned camellia seed oil maintenance lip pomade one preferred version, described emulsifying agent is tristerin, glycerol Pilus Caprae seu Ovis
One or more mixture in acid esters, PEG-20 lanoline acid esters.
In above-mentioned camellia seed oil maintenance lip pomade one preferred version, described antioxidant is tocopherol acetas, retinol palm fibre
One or more mixture in palmitic acid acid esters, retinyl acetate, retinyl propionate.
In above-mentioned camellia seed oil maintenance lip pomade one preferred version, described preservative is o-p-Cymene-5-alcohol, bisabolol
In one or both mixture.
Scheme 2: the preparation method of a kind of camellia seed oil maintenance lip pomade, described preparation method comprises the following steps:
(1) camellia seed oil is heated to 20-30 DEG C, adds alkali liquor；
(2) it is warming up to 55-65 DEG C, is stirred, treat cotton-shaped soap stock emersion, be centrifuged off；
(3) temperature of charge being risen to 70-85 DEG C, add wax and film former, stirring is to transparency liquid；
(4) keep temperature, add wetting agent and emulsifying agent, stir homogenizing；
(5) keep temperature, add antioxidant and preservative, be stirred until homogeneous, mixed material is placed in vacuum drying oven
In, carry out removed under reduced pressure bubble, take out fill, be placed in die for molding.
In one preferred version of above-mentioned preparation method, adding the alkali liquor of oil quality 0.2% in step (1), this alkali liquor is dense
Degree is 15%, adds alkali liquor in 10min.
Based on such scheme, it is possible to form maintenance lip pomade with camellia seed oil for primary raw material, this maintenance lip pomade room temperature keeps
Bar-shaped, there is preferable pliability, have the natural abnormal smells from the patient of oil tea, have preferable smear and ductility, smear layer softness is moistened；Peace
Entirely do not stimulate, made health-care effect for a long time.
Furthermore, natural resources can be fully developed in the application of this programme, improve the economic interests rate of Semen Camelliae；Realize simultaneously
Further exploitation to camellia seed oil, the lip of the green effect type of exploitation makes to apply some make up.
It addition, the actual application of this programme also has the advantages that
(1) the camellia seed oil maintenance lip pomade formed according to this programme can promote lip tissue water content, reduces epidermis gauffer
Phenomenon, plays desalination cheilogramma, and compact skin, promotes the effect of the plumpness of skin of lip.
(2) the camellia seed oil maintenance lip pomade formed according to this programme can promote subcutaneous collagen protein content so that lip
More soft, healthy, full, flexible.
(3) the camellia seed oil maintenance lip pomade formed according to this programme, safety non-toxic, gentle non-stimulated, there is natural sense, make
Good with sense, life-time service can reach health-care effect.
(3) the camellia seed oil maintenance lip pomade formed according to this programme, the natural safety of its raw material, preparation technology is rigorous, quality
Controllability is strong, it is easy to industrialized production, has novelty in production development.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and be easy to understand with effect, below knot
Close instantiation, the present invention is expanded on further.
Characteristic based on camellia seed oil, this example is constituted maintenance lip pomade with camellia seed oil for primary raw material.
Calculating by weight in this maintenance lip pomade, its raw material composition and content are as follows:
On this basis, this example additionally provides and has synergistic concrete formula:
For the camellia seed oil in this example, based on its characteristic as the primary raw material of maintenance lip pomade.This camellia seed oil is adopted
With proportion 0.9l61 (d20/20), refraction coefficient 1.4612 (n40), acid number 1.12mg/g, the oil of peroxide value 3.42mmol/kg
Oleum Camelliae.
For the wax in this example, by synergism, make maintenance lip pomade keep bar-shaped at room temperature, have the most pliable and the toughest
Property.
Accordingly, the wax in this example is specially castor oil hydrogenated, candelilla wax, cera alba, babassu vegetable wax, tribehenin
Essence, stearyl alcohol Cera Flava acid esters, one or more the mixture in spermol ricinoleate ester, it is further ensured that effect with this
Really.
For the film former in this example, by synergism, form lasting film when the maintenance lip pomade formed uses,
Prevent the moisture loss of epidermis.
Accordingly, the specially polyisobutylene of the film former in this example, glyceryl abietate, pentaerythritol abietate, have
One or more mixture in machine silicones.
For the wetting agent in this example, keep moisture when maintenance lip pomade uses, it is to avoid epidermis is dried.
Accordingly, the wetting agent in this example is specially glycerol, dipropylene glycol, one or more in 1,3 butanediol
Mixture.
For the emulsifying agent in this example, for synergism, to form emulsification system, the formation of emulsification system, to water
Divide and active matter has slowly releasing effect.
Accordingly, the emulsifying agent in this example is specially tristerin, glycerol Pilus Caprae seu Ovis acid esters, PEG-20 lanoline acid esters
In one or more mixture.
For the antioxidant in this example, for synergism, so that superoxide radical and DPPH are carried out cancellation.
Accordingly, the antioxidant in this example be specially tocopherol acetas, retinyl palmitate, retinyl acetate,
One or more mixture in retinyl propionate.
For the preservative in this example, for synergism, to prevent microbial growth from causing oils and fats corrupt and system
Rupture.
Accordingly, the preservative in this example is specially o-p-Cymene-5-alcohol, one or both the mixing in bisabolol
Thing.
For the camellia seed oil maintenance lip pomade being made up of according to corresponding proportioning said components, this example furthermore provides right
The preparation method answered.This preparation method comprises the steps:
(1) camellia seed oil being heated to 20-30 DEG C, preferably 25 DEG C, add the alkali liquor of oil quality 0.2%, concentration of lye is
Alkali liquor is added in 15%, 10min.
It is possible to well camellia seed oil be carried out refine, it is achieved deacidification and degumming, effectively prevent camellia seed oil rear
The corruption of free fatty during Xu.
(2) it is warming up to 55-65 DEG C, preferably 60 DEG C, is stirred with the speed of 80rpm, treat cotton-shaped soap stock emersion, be centrifuged and remove
Go.
(3) temperature of charge is risen to 70-85 DEG C, preferably 80 DEG C, adds wax class and film former, stir to transparency liquid,
Wherein mixing speed 100rpm, mixing time 20min.
(4) keep 80 DEG C, add wetting agent and emulsifying agent, stir homogenizing, wherein mixing speed 3000rpm, mixing time
5min。
(5) keep 80 DEG C, add antioxidant and preservative, be stirred until homogeneous, mixed material is placed in vacuum drying oven
In, carry out removed under reduced pressure bubble 20min under the conditions of 200Pa, take out fill, molding in a mold under the conditions of being placed in 4 DEG C.
By such scheme when forming camellia seed oil maintenance lip pomade, it is achieved fully develop natural resources, improve Semen Camelliae
Economic interests rate；Realizing developing further camellia seed oil, the lip of the green effect type of exploitation makes to apply some make up.
Below in conjunction with specific embodiment, the present invention is expanded on further.Should be understood that these embodiments are merely to illustrate the present invention
Rather than restriction the scope of the present invention.The experimental technique of unreceipted actual conditions in the following example, generally marks according to country
Quasi-mensuration.If there is no corresponding national standard, then according to general international standard, normal condition or built according to manufacturer
The condition of view is carried out.Unless otherwise indicated, the most all of number is weight portion, and all of percentage ratio is weight percentage.
Unless otherwise defined or described herein, all specialties used herein and scientific words and the skilled people of art technology
The same meaning that member is familiar with.The most any method similar or impartial to described content and material all can be applicable to the present invention
In method.
Embodiment 1
Camellia seed oil maintenance lip pomade formula in this example is as follows:
Camellia seed oil in the present embodiment is proportion 0.9l61 (d20/20), refraction coefficient 1.4612 (n40), acid number
1.12mg/g, the camellia seed oil of peroxide value 3.42mmol/kg；And this camellia seed oil adding proportion is 50%.
Wax and adding proportion thereof in the present embodiment are babassu vegetable wax 10%, tribehenin essence 6%, cera alba 6%, hydrogen
Change Oleum Ricini 3%, the mixture of candelilla wax 1%.
Wetting agent in the present embodiment and the mixture that adding proportion is glycerol 4%, 1,3 butanediol 4% thereof.
Film former and adding proportion thereof in the present embodiment are glyceryl abietate 5%.
Emulsifying agent and adding proportion thereof in the present embodiment are tristerin 5% and glycerol Pilus Caprae seu Ovis acid esters 5.6%
Mixture.
Antioxidant and adding proportion thereof in the present embodiment are tocopherol acetas 0.1% and retinyl palmitate
The mixture of 0.1%.
Preservative in the present embodiment and adding proportion thereof are the mixed of o-p-Cymene-5-alcohol 0.1% and bisabolol 0.1%
Compound.
Each raw material based on above-mentioned formation, the camellia seed oil maintenance lip pomade in this example prepared by following process:
(1) camellia seed oil being heated to 25 DEG C, add the alkali liquor of oil quality 0.2%, concentration of lye is 15%, in 10min
Add alkali liquor.
(2) 60 DEG C it are warming up to, mixing speed 80rpm, treat cotton-shaped soap stock emersion, be centrifuged off.
(3) temperature of charge rising to 80 DEG C, add wax class and film former, stirring is to transparency liquid, mixing speed
100rpm, mixing time 20min.
(4) keep 80 DEG C, add wetting agent and emulsifying agent, stir homogenizing, wherein mixing speed 3000rpm, mixing time
5min。
(5) keep 80 DEG C, add antioxidant and preservative, be stirred until homogeneous, mixed material is placed in vacuum drying oven
In, carry out removed under reduced pressure bubble 20min under the conditions of 200Pa, take out fill, molding in a mold under the conditions of being placed in 4 DEG C.
The camellia seed oil maintenance lip pomade prepared according to the method described above is that yellow is to the wax-like mastic of milky, room temperature retention bar
Shape, has preferable pliability, has the natural abnormal smells from the patient of oil tea, has preferable smear and ductility, and smear layer softness is moistened.
This lip pomade is carried out following laboratory observation, places 12 months ,-10 DEG C of cold storages including 50 DEG C of heat storages one month, room temperature
24h, cold storage (-10 DEG C, 24h) and heat storage (50 DEG C, 24h) 3 circulations, all without separation, floating oil, perspire, go mouldy, spoiled, variable color
Phenomenon.Camellia seed oil maintenance lip pomade keeps good quality stability in long-term storage.
Embodiment 2
Camellia seed oil maintenance lip pomade formula in this example is as follows:
In this example, the preparation method of camellia seed oil maintenance lip pomade and laboratory observation method are with embodiment 1.
Embodiment 3
Camellia seed oil maintenance lip pomade formula in this example is as follows:
In this example, the preparation method of camellia seed oil maintenance lip pomade and laboratory observation method are with embodiment 1.
Embodiment 4
Camellia seed oil maintenance lip pomade formula in this example is as follows:
In this example, the preparation method of camellia seed oil maintenance lip pomade and laboratory observation method are with embodiment 1.
Embodiment 5 safety testing
The safety fruit of the camellia seed oil maintenance lip pomade of investigation embodiments of the invention 1 gained, carries out acute oral toxicity
Experiment GB 15193.3-2014.Carry out 12 months in animal body according to camellia seed oil maintenance lip pomade prepared by above-described embodiment
Long term toxicity test, every day to rat oral gavage be administered, dosage is respectively 1g, 5g.
| Tract | Observe and the project of inspection | Performance |
| Nervous system | Irritant reaction | Normally |
| Respiratory system | Breathe character and speed | Normally |
| Cardiovascular system | Heart beating and pulse | Normally |
| Digestive system | Secretions and organ | Normally |
| Urinary system | Secretions and organ | Normally |
| Skin and by hair | Complete appearance | Normally |
| Mucosa | Appearance color | Normally |
| Blood | Routine blood test | Normally |
| Rank | Oral Administration in Rats LD50/(mg/kg) | Be equivalent to people lethal dose g/ people |
| Actual nontoxic | >5000 | >500 |
Result shows, in the range of dosage, obvious adverse reaction, camellia seed oil maintenance lip does not occur in study subject
Cream is safety when Clinical practice, and its materials are nontoxic, even if user is careless by Semen Camelliae during diet is drunk water
Oil maintenance lip pomade absorption is internal also will not produce toxic and side effects.Camellia seed oil maintenance lip pomade can contact lip and oral mucosa,
Gentle non-stimulated, safety reliably can be with life-time service.
Embodiment 6 smoothing wrinkle performance test
The effect of the camellia seed oil maintenance lip pomade desalination cheilogramma of investigation embodiments of the invention 1 gained, surveys with wrinkle of skin
30 experimenter's skin of lip are tested by test system Skin-Visiometer SV600.Method of testing is: choose at lip
Tested region, by tested skin physiological saline wiping once, the silica gel processed with firming agent after drying uniformly is coated with on tested
Smear, peel off when silica gel solidifies laggard row, obtain the replicate sample of lip surface reversed image structure, then laminating adhesive is carried out transverse section and cut
Sheet, utilizes graphical analysis determining instrument to collect the optical signal of diaphragm different parts, obtains skin by photoelectricity and digitized processing
3-D view, be then analyzed with special-purpose software, i.e. can get the test section on subjects skin and blank region
Skin texture parameter.
Experimenter is used the camellia seed oil maintenance lip pomade lip dermatoglyph degree of depth (μm) data as a control group of first 10 days, often
It is spaced test in 5 days once.Experimenter is allowed to use camellia seed oil maintenance lip pomade 10 days, deep at interval of lip dermatoglyph of test in 5 days
Degree (μm) is as tested group of data.
The above results shows, the camellia seed oil maintenance lip pomade of embodiment 1 gained, uses latter 10 days in, the dermatoglyph degree of depth (μm),
Dermatoglyph bar number, gauffer volume (μm3) index is all decreased obviously, and is significantly improved lip texture, is i.e. suppression skin collagen fall
Solving, repair collagenous fiber bundle structure, make subcutaneous fibrotic girder recover supporting role, compact skin, reduces epidermis gauffer phenomenon,
Promote hyaluronic acid synthesis between histiocyte, promote lip tissue water content, promote the plumpness of skin of lip, reach to desalinate lip
The effect of stricture of vagina.Illustrate that camellia seed oil maintenance lip pomade has good skin-protecting function and a certain anti-ageing effect, safe healthcare, permissible
Life-time service.
Embodiment 7 lip flexibility test
The improvement to skin of lip elasticity of the camellia seed oil maintenance lip pomade of investigation embodiments of the invention 1 gained, uses skin
30 experimenter's skin of lip are tested by elasticity tester Germany Courage Khazaka company MPA580.Test philosophy
It is the deformation size produced under external force based on skin, and external force removes the restorable degree of rear skin.Tested
The skin surface of examination produces (2*103)～(5*104) Pa (20～500mbar) negative pressure, specific for skin inspiration one test is visited
In head, the degree of depth that skin is sucked in test probe is recorded by a contactless optic testing system.
Experimenter is used the camellia seed oil maintenance lip pomade skin of lip elasticity increment rate data as a control group of first 10 days,
At interval of test in 2 days once.Experimenter is allowed to use camellia seed oil maintenance lip pomade 10 days, at interval of skin of lip of test in 2 days
Elastic increment rate is as tested group of data.
| Group | Lip thickness change (μm) | Elastic parameter (Ur/Uf) |
| Tested group | 287.17 | 0.95 |
| Matched group | 22.1 | 0.21 |
The above results shows, the camellia seed oil maintenance lip pomade of embodiment 1 gained, and having in using latter 10 days significantly increases lip
Portion's spring rate, is i.e. the increase in the horny layer lock outlet capacity of skin of lip, promotes subcutaneous collagen protein content, promote skin elasticity
Fiber and dermal connective tissue density increase, and improve biological characteristics and the histologic characteristics of skin so that lip is more imbued with bullet
Property.Illustrating that camellia seed oil maintenance lip pomade has good health care and the most both effectiveness, safety is nourished, can be made for a long time
With.
By above-described embodiment, it is aqueous that the camellia seed oil maintenance lip pomade formed by this programme can promote lip tissue
Amount, reduces epidermis gauffer phenomenon, plays desalination cheilogramma, and compact skin, promotes the effect of the plumpness of skin of lip；This maintenance lip
Cream can also promote subcutaneous collagen protein content so that lip is more soft, healthy, full, flexible.Furthermore this camellia seed oil is repaiied
Lip-stick safety non-toxic, gentle non-stimulated, there is natural sense, use sense good, life-time service can reach health-care effect.
It addition, this programme is with camellia seed oil as primary raw material, fully develop natural resources, improve the economic interests of Semen Camelliae
Rate, it is achieved the lip of the green effect type of exploitation makes to apply some make up.
Therefore, camellia seed oil maintenance lip pomade scheme (formula and preparation method) that the present invention provides not only efficiently solves existing
There is the problem existing for technology, also reached beyond thought excellent effect.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.The technology of the industry
Personnel, it should be appreciated that the present invention is not restricted to the described embodiments, simply illustrating this described in above-described embodiment and description
The principle of invention, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, and these become
Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and
Equivalent defines.
Claims (10)
1. a camellia seed oil maintenance lip pomade, it is characterised in that described maintenance lip pomade includes the component of following weight portion:
A kind of camellia seed oil maintenance lip pomade the most according to claim 1, it is characterised in that described camellia seed oil is proportion
0.9l61 (d20/20), refraction coefficient 1.4612 (n40), acid number 1.12mg/g, the camellia seed oil of peroxide value 3.42mmol/kg.
A kind of camellia seed oil maintenance lip pomade the most according to claim 1, it is characterised in that described wax is hydrogenated castor
Oil, candelilla wax, cera alba, babassu vegetable wax, tribehenin essence, stearyl alcohol Cera Flava acid esters, in spermol ricinoleate ester
One or more mixture.
A kind of camellia seed oil maintenance lip pomade the most according to claim 1, it is characterised in that described film former is poly-isobutyl
One or more mixture in alkene, glyceryl abietate, pentaerythritol abietate, organic siliconresin.
A kind of camellia seed oil maintenance lip pomade the most according to claim 1, it is characterised in that described wetting agent is glycerol,
Dipropylene glycol, one or more the mixture in 1,3 butanediol.
A kind of camellia seed oil maintenance lip pomade the most according to claim 1, it is characterised in that described emulsifying agent is stearic acid
One or more mixture in glyceride, glycerol Pilus Caprae seu Ovis acid esters, PEG-20 lanoline acid esters.
A kind of camellia seed oil maintenance lip pomade the most according to claim 1, it is characterised in that described antioxidant is tocopherol
One or more mixture in acetas, retinyl palmitate, retinyl acetate, retinyl propionate.
A kind of camellia seed oil maintenance lip pomade the most according to claim 1, it is characterised in that described preservative is o-umbrella flower
Hydrocarbon-5-alcohol, one or both the mixture in bisabolol.
9. the preparation method of a camellia seed oil maintenance lip pomade, it is characterised in that described preparation method comprises the following steps:
(1) camellia seed oil is heated to 20-30 DEG C, adds alkali liquor；
(2) it is warming up to 55-65 DEG C, is stirred, treat cotton-shaped soap stock emersion, be centrifuged off；
(3) temperature of charge being risen to 70-85 DEG C, add wax and film former, stirring is to transparency liquid；
(4) keep temperature, add wetting agent and emulsifying agent, stir homogenizing；
(5) keep temperature, add antioxidant and preservative, be stirred until homogeneous, mixed material be placed in vacuum drying oven, enter
Row removed under reduced pressure bubble, takes out fill, is placed in die for molding.
The preparation method of a kind of camellia seed oil maintenance lip pomade the most according to claim 9, it is characterised in that in step (1)
The alkali liquor of middle addition oil quality 0.2%, this concentration of lye is 15%, adds alkali liquor in 10min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610374352.2A CN105997584A (en) | 2016-05-27 | 2016-05-27 | Camellia oleosa seed oil repairing lipstick and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201610374352.2A CN105997584A (en) | 2016-05-27 | 2016-05-27 | Camellia oleosa seed oil repairing lipstick and preparation method thereof |
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| CN201610374352.2A Pending CN105997584A (en) | 2016-05-27 | 2016-05-27 | Camellia oleosa seed oil repairing lipstick and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107496213A (en) * | 2017-09-23 | 2017-12-22 | 马述腾 | A kind of gestational period Oleum Ovum Gallus domesticus Flavus lip gloss |
| CN108403610A (en) * | 2018-06-04 | 2018-08-17 | 内蒙古农业大学 | A kind of lip repair and preparation method thereof with cracking resistance |
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| CN102329690A (en) * | 2011-04-07 | 2012-01-25 | 贵州大龙健康油脂有限公司 | Low-temperature cold-pressing and bivariate continuous refining and processing method for oiltea camellia seed oil |
| CN103040699A (en) * | 2012-12-14 | 2013-04-17 | 吴江市德佐日用化学品有限公司 | Moisturizing antibacterial lipstick |
| CN103142451A (en) * | 2013-04-03 | 2013-06-12 | 长沙理工大学 | Lip protector containing oil-tea camellia seed oil |
| CN103655414A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Mild and refreshing lip balm |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102329690A (en) * | 2011-04-07 | 2012-01-25 | 贵州大龙健康油脂有限公司 | Low-temperature cold-pressing and bivariate continuous refining and processing method for oiltea camellia seed oil |
| CN103040699A (en) * | 2012-12-14 | 2013-04-17 | 吴江市德佐日用化学品有限公司 | Moisturizing antibacterial lipstick |
| CN103142451A (en) * | 2013-04-03 | 2013-06-12 | 长沙理工大学 | Lip protector containing oil-tea camellia seed oil |
| CN103655414A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Mild and refreshing lip balm |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107496213A (en) * | 2017-09-23 | 2017-12-22 | 马述腾 | A kind of gestational period Oleum Ovum Gallus domesticus Flavus lip gloss |
| CN108403610A (en) * | 2018-06-04 | 2018-08-17 | 内蒙古农业大学 | A kind of lip repair and preparation method thereof with cracking resistance |
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Application publication date: 20161012 |