CN105948675A - Indoor heat-reflective heat-insulating diatom ooze and preparation method thereof - Google Patents

Indoor heat-reflective heat-insulating diatom ooze and preparation method thereof Download PDF

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Publication number
CN105948675A
CN105948675A CN201610415227.1A CN201610415227A CN105948675A CN 105948675 A CN105948675 A CN 105948675A CN 201610415227 A CN201610415227 A CN 201610415227A CN 105948675 A CN105948675 A CN 105948675A
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heat
diatom ooze
indoor heat
insulating
parts
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CN201610415227.1A
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CN105948675B (en
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张启明
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Male (shanghai) New Mstar Technology Ltd
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Male (shanghai) New Mstar Technology Ltd
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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/14—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00482—Coating or impregnation materials
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20—Resistance against chemical, physical or biological attack

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Paints Or Removers (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

The invention discloses indoor heat-reflective heat-insulating diatom ooze and a preparation method thereof. The indoor heat-reflective heat-insulating diatom ooze is prepared from, by weight, 45-55 parts of gypsum, 35-55 parts of re-dispersible rubber powder, 20-35 parts of hollow glass microspheres, 5-15 parts of pigment, 15-25 parts of talcum powder, 15-25 parts of silica, 20-30 parts of diatomite, 3-9 parts of a dispersing agent and 1-5 parts of thickening agent. According to the indoor heat-reflective heat-insulating diatom ooze and the preparation method thereof, the types and using amounts of dispersing agents and thickening agents suitable for the indoor heat-reflective heat-insulating diatom ooze are preferably selected by adopting reasonable proportion, the heat reflectivity, antimicrobial properties, waterproof properties, corrosion resistance and excellent stability are improved, and the indoor heat-reflective heat-insulating diatom ooze is high in bonding strength, safe, non-toxic, short in curing time, convenient to construct and high in efficiency.

Description

Indoor heat-reflecting heat-insulating diatom ooze and preparation method thereof
Technical field
The present invention relates to technical field of coatings, particularly relate to a kind of indoor heat-reflecting heat-insulating diatom ooze and Preparation method.
Background technology
Solar energy is the necessary requirement of human survival and life, but the life band of the mankind is also given in strong radiation Serve inconvenience.Such as sunlight in summer irradiate on a metal plate, its surface temperature up to 70-80 DEG C, as This will certainly bring inconvenience and cause material damage.In urban area, dark asphalt road and pitch room Top etc. can absorb the heat from the sun, forms so-called " heat island " effect, makes city temperature than ground, rural area District exceeds about 1-3 DEG C.
Exterior wall to be improved and roof insulation performance, major measure has: (1) improves building thermal technology property Energy；(2) improve the reflectance of outer surface, reduce the heat of incoming indoor；(3) outer surface is improved Emissivity；(4) improve the thermal capacity of roofing, reduce the mode such as heat of incoming indoor.
Under conditions of building external structure determines, there is high sunlight reflectivity and the roof of high emissivity Study hotspot with exterior wall coating becomes architectural energy saving system, has been widely used at building surface.Instead Penetrate insulating moulding coating and can play significant cooling-down effect in summer, thus reduce energy consumption of air conditioning in summer.Pass through It is the most most effective, the easiest with emissivity that brushing heat-reflecting insulating coating improves building superficial reflex ratio Mode.The generally rutile TiO in building face coat2Can strongly absorb the ultraviolet in sunlight, Reduce its destruction to coating paint film.If can be gone back by ultraviolet reflection, protected effect can be more preferable, but This realizes highly difficult for nonmetallic materials are such as coating.So we generally consider visible reflectance Maximizing than with near infrared light reflectivity, these two parts contain the solar irradiation energy of 95%.
The feature of ordinary hot reflective coating be surface color be white or light, can be used for the flat of commercial facility Aspect, low gradient roofing and exterior wall.Overhead infrared photograph clearly illustrates that ground surface temperature has the biggest difference Different.This species diversity is mainly caused by the reflection on surface and radiation characteristic.High reflection, the table of high radiation Face " the coldest ".Actually light color and dark surface is all likely to be of high radiance, and traditional height is warm The coating of reflectivity the most always white or light color.But in actual applications, light color or white are coated with There is the shortcomings such as stain resistance is poor, weatherability difference in material paint film, after using a period of time out of doors, and can be because of Coating surface is dirty, variable color causes heat reflection performance to be greatly reduced, it is often more important that light color or color white Dull, it is impossible to meet and decorate diversified requirement.
The invention provides a kind of indoor heat-reflecting heat-insulating diatom ooze, there is the heat reflection cooling effect of excellence Really.
Summary of the invention
For above-mentioned deficiency present in prior art, one of the technical problem to be solved is to carry For a kind of indoor heat-reflecting heat-insulating diatom ooze.
The two of the technical problem to be solved are to provide a kind of indoor heat-reflecting heat-insulating diatom ooze Preparation method.
The present invention seeks to be achieved through the following technical solutions:
A kind of indoor heat-reflecting heat-insulating diatom ooze, is prepared from by the raw material of following weight parts:
Gypsum Fibrosum 45-55 part, redispersible rubber powder 35-55 part, hollow glass microbead 20-35 part, pigment 5-15 part, Pulvis Talci 15-25 part, silica 1 5-25 part, kieselguhr 20-30 part, dispersant 3-9 Part, thickening agent 1-5 part.
Preferably, described thickening agent is carboxymethyl cellulose, carboxymethyl starch, hydroxypropyl methyl fiber One or more mixture in element.
It is highly preferred that described thickening agent is by carboxymethyl cellulose, carboxymethyl starch, hydroxypropyl methyl fibre Dimension element composition, described carboxymethyl cellulose, carboxymethyl starch, the mass ratio of hydroxypropyl methyl cellulose are (1-3): (1-3): (1-3).
Preferably, described dispersant be a kind of in sodium hexameta phosphate, sodium pyrophosphate, sodium trimetaphosphate or Multiple mixture.
It is highly preferred that described dispersant is made up of sodium hexameta phosphate, sodium pyrophosphate, sodium trimetaphosphate, Described sodium hexameta phosphate, sodium pyrophosphate, the mass ratio of sodium trimetaphosphate are (1-3): (1-3): (1-3).
Preferably, described redispersible rubber powder can be bought or prepare, it is also possible to reference to patent Application number: in 201110240131.3 prepared by the method for embodiment 1.
Preferably, described pigment is that the phthalein mountain valley with clumps of trees and bamboo is green, exterior wall is red, the red middle one or many of iron oxide yellow, exterior wall The mixture planted.
Present invention also offers the preparation method of above-mentioned indoor heat-reflecting heat-insulating diatom ooze: by Gypsum Fibrosum, can Redispersibility rubber powder, hollow glass microbead, pigment, Pulvis Talci, silicon dioxide, kieselguhr, dispersant, Thickening agent mix homogeneously and get final product.
Indoor heat-reflecting heat-insulating diatom ooze that the present invention provides and preparation method thereof, by rational proportioning, Preferably go out dispersant, thickening agent kind and the consumption of applicable indoor heat-reflecting heat-insulating diatom ooze, improve Heat reflectivity, antibiotic property, water proofing property, corrosion resistance and excellent in stability, adhesion strength is high, safe nothing Poison, hardening time is short, easy construction, and efficiency is high.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further, the following stated, only to the present invention Preferred embodiment, not does the restriction of other forms, any technology being familiar with this specialty to the present invention Personnel are changed to the Equivalent embodiments changed on an equal basis possibly also with the technology contents of the disclosure above.Every Without departing from the present invention program content, any letter following example done according to the technical spirit of the present invention Single amendment or equivalent variations, all fall within protection scope of the present invention.
Each raw material introduction in embodiment:
Gypsum Fibrosum, uses the GRG superfine Gypsum Fibrosum powder that Dong Tai source, Zaozhuang Gypsum Fibrosum company limited provides.
Redispersible rubber powder, with reference to number of patent application: the method for embodiment 1 in 201110240131.3 Preparation.
Silicon dioxide, No. CAS: 7631-86-9, particle diameter 20-40nm.
Pulvis Talci, No. CAS: 14807-96-6, specifically use Lingshou County Yong Chang mineral products processing factory to produce 1250 mesh Pulvis Talci.
Carboxymethyl cellulose, No. CAS: 9000-11-7, use Renqiu City Run Da Chemical Co., Ltd. to provide Carboxymethyl cellulose.
Hollow glass microbead, the grade using Xinyang Yong Kai insulation material company limited to provide is 2018, Particle diameter is the hollow glass microbead of 65-75 μm.
Carboxymethyl starch, No. CAS: 9063-38-1, Jinan Yuan Tong Chemical Co., Ltd. provides.
Hydroxypropyl methyl cellulose, No. CAS: 9004-65-3, Jinan Yuan Tong Chemical Co., Ltd. provides.
Sodium hexameta phosphate, No. CAS: 10124-56-8.
Sodium pyrophosphate, No. CAS: 13472-36-1.
Sodium trimetaphosphate, No. CAS: 7785-84-4.
Pigment employing iron oxide yellow, No. CAS: 51274-00-1, use Shanghai Yan Chen pigment company limited 600 mesh produced, model is the iron oxide yellow of 920..
Kieselguhr, No. CAS: 91053-39-3, specifically use Lingshou County Yong Chang mineral products processing factory to produce The calcined diatomite of 600 mesh.
Embodiment 1
Indoor heat-reflecting heat-insulating diatom ooze raw material (weight portion):
50 parts of Gypsum Fibrosum, redispersible rubber powder 45 parts, hollow glass microbead 25 parts, iron oxide yellow 6 Part, Pulvis Talci 20 parts, silicon dioxide 20 parts, 25 parts of kieselguhr, dispersant 6 parts, thickening agent 3 Part.
Described thickening agent is pressed quality by carboxymethyl cellulose, carboxymethyl starch, hydroxypropyl methyl cellulose Obtain than being uniformly mixed for 1:1:1.
Described dispersant is stirred for 1:1:1 in mass ratio by sodium hexameta phosphate, sodium pyrophosphate, sodium trimetaphosphate Mix mix homogeneously to obtain.
The preparation method of indoor heat-reflecting heat-insulating diatom ooze: by Gypsum Fibrosum, redispersible rubber powder, hollow Glass microballoon, pigment, Pulvis Talci, silicon dioxide, kieselguhr, dispersant, thickening agent use cantilever double Cone and screw mixer stirs 15 minutes mix homogeneously and get final product.
Embodiment 2
Substantially the same manner as Example 1, differ only in: described thickening agent is by carboxymethyl starch, hydroxypropyl Ylmethyl cellulose is uniformly mixed for 1:1 in mass ratio and obtains.Obtain the indoor heat of embodiment 2 Reflective insulation diatom ooze.
Embodiment 3
Substantially the same manner as Example 1, differ only in: described thickening agent is by carboxymethyl cellulose, hydroxyl Propyl methocel is uniformly mixed for 1:1 in mass ratio and obtains.Obtain the indoor of embodiment 3 Heat-reflecting heat-insulating diatom ooze.
Embodiment 4
Substantially the same manner as Example 1, differ only in: described thickening agent is by carboxymethyl cellulose, carboxylic Methyl starch is uniformly mixed for 1:1 in mass ratio and obtains.Obtain the indoor heat reflection of embodiment 4 Heat insulation diatom ooze.
Embodiment 5
Substantially the same manner as Example 1, differ only in: described dispersant is by sodium pyrophosphate, three inclined phosphorus Acid sodium is uniformly mixed for 1:1 in mass ratio and obtains.Obtain the indoor heat-reflecting heat-insulating of embodiment 5 Diatom ooze.
Embodiment 6
Substantially the same manner as Example 1, differ only in: described dispersant is by sodium hexameta phosphate, three inclined Sodium phosphate is uniformly mixed for 1:1 in mass ratio and obtains.Obtain the indoor heat reflection of embodiment 6 every Hot diatom ooze.
Embodiment 7
Substantially the same manner as Example 1, differ only in: described dispersant is by sodium hexameta phosphate, burnt phosphorus Acid sodium is uniformly mixed for 1:1 in mass ratio and obtains.Obtain the indoor heat-reflecting heat-insulating of embodiment 7 Diatom ooze.
Test case 1
The indoor heat-reflecting heat-insulating diatom ooze preparing embodiment 1-7, takes 1-7 respectively and is prepared into To indoor heat-reflecting heat-insulating diatom ooze 10kg and 5.5kg water be uniformly mixed i.e. to obtain and can be used for executing Work, anti-microbial property press GB/T21866-2008 antibiotic paint anti-microbial property assay method and antibacterial effect, HG/T 3980-2007 antibiotic paint measures.Concrete outcome is shown in Table 1.
Table 1: anti-microbial property test result table
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (carboxymethyl cellulose, carboxymethyl starch, hydroxyl Propyl methocel compounds) anti-microbial property is substantially better than embodiment 2-4 (carboxymethyl cellulose, carboxylic first In base starch, hydroxypropyl methyl cellulose, arbitrarily the two is compounding).
Comparing embodiment 1 and embodiment 5-7, embodiment 1 (sodium hexameta phosphate, sodium pyrophosphate, three inclined phosphorus Acid sodium compounds) anti-microbial property is substantially better than embodiment 5-7 (sodium hexameta phosphate, sodium pyrophosphate, three inclined phosphorus In acid sodium, arbitrarily the two is compounding).
Test case 2
The indoor heat-reflecting heat-insulating diatom ooze preparing embodiment 1-7 carries out heat reflection test, point Do not take indoor heat-reflecting heat-insulating diatom ooze 10kg and the 5.5kg water that 1-7 prepares to be uniformly mixed Must can be used for constructing, according to JC/T1040-2007, " outer surface of building is with indoor heat-reflecting heat-insulating silicon Algae mud " test.The reflectivity results of sunlight light heat ray is shown in Table 2.
Table 2: heat reflection performance test result table
Sample Reflectance, %
Embodiment 1 97.8
Embodiment 2 94.8
Embodiment 3 94.2
Embodiment 4 95.1
Embodiment 5 93.3
Embodiment 6 93.7
Embodiment 7 92.6
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (carboxymethyl cellulose, carboxymethyl starch, hydroxyl Propyl methocel compounds) heat reflection performance is substantially better than embodiment 2-4 (carboxymethyl cellulose, carboxylic In methyl starch, hydroxypropyl methyl cellulose, arbitrarily the two is compounding).
Comparing embodiment 1 and embodiment 5-7, embodiment 1 (sodium hexameta phosphate, sodium pyrophosphate, three inclined phosphorus Acid sodium compounds) to be substantially better than embodiment 5-7 (sodium hexameta phosphate, sodium pyrophosphate, three inclined for heat reflection performance In sodium phosphate, arbitrarily the two is compounding).

Claims (7)

1. an indoor heat-reflecting heat-insulating diatom ooze, it is characterised in that by the raw material system of following weight parts For forming: be prepared from by the raw material of following weight parts: Gypsum Fibrosum 45-55 part, redispersible rubber powder 35-55 Part, hollow glass microbead 20-35 part, pigment 5-15 part, Pulvis Talci 15-25 part, silica 1 5-25 Part, kieselguhr 20-30 part, dispersant 3-9 part, thickening agent 1-5 part.
Indoor heat-reflecting heat-insulating diatom ooze the most as claimed in claim 1, it is characterised in that: described Thickening agent is that one or more in carboxymethyl cellulose, carboxymethyl starch, hydroxypropyl methyl cellulose are mixed Compound.
Indoor heat-reflecting heat-insulating diatom ooze the most as claimed in claim 2, it is characterised in that: described Thickening agent is made up of carboxymethyl cellulose, carboxymethyl starch, hydroxypropyl methyl cellulose, described carboxymethyl Cellulose, carboxymethyl starch, the mass ratio of hydroxypropyl methyl cellulose are (1-3): (1-3): (1-3).
4. the indoor heat-reflecting heat-insulating diatom ooze as according to any one of claim 1-3, its feature exists It is one or more mixed in sodium hexameta phosphate, sodium pyrophosphate, sodium trimetaphosphate in: described dispersant Compound.
Indoor heat-reflecting heat-insulating diatom ooze the most as claimed in claim 4, it is characterised in that: described Dispersant is made up of sodium hexameta phosphate, sodium pyrophosphate, sodium trimetaphosphate, described sodium hexameta phosphate, burnt phosphorus Acid sodium, the mass ratio of sodium trimetaphosphate are (1-3): (1-3): (1-3).
6. the indoor heat-reflecting heat-insulating diatom ooze as according to any one of claim 1-3, its feature exists Be that the phthalein mountain valley with clumps of trees and bamboo is green, exterior wall is red in: described pigment, iron oxide yellow, exterior wall red in one or more mixing Thing.
7. the preparation method of the indoor heat-reflecting heat-insulating diatom ooze as described in any one of claim 1-6, It is characterized in that: by Gypsum Fibrosum, redispersible rubber powder, hollow glass microbead, pigment, Pulvis Talci, two Silicon oxide, kieselguhr, dispersant, thickening agent mix homogeneously and get final product.
CN201610415227.1A 2016-06-14 2016-06-14 Indoor heat-reflecting heat-insulating diatom ooze and preparation method thereof Expired - Fee Related CN105948675B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20090120922A (en) * 2008-05-21 2009-11-25 (주) 에스와이씨 Panel with formaldehyde adsorption, water adsorption and desorption functions and preparation thereof
CN103787614A (en) * 2014-02-11 2014-05-14 江苏麦阁吸附剂有限公司 Wall material with function of promoting negative ion release and preparation method thereof
CN104030611A (en) * 2014-05-30 2014-09-10 沈承舟 Diatom ooze environment-friendly decorating material
CN104177021A (en) * 2014-08-06 2014-12-03 南京市苏宝节能科技有限公司 Diatomite putty dry material
CN104496329A (en) * 2014-12-31 2015-04-08 上海墙特节能材料有限公司 Interior inorganic dry powder heat-insulating diatom ooze and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20090120922A (en) * 2008-05-21 2009-11-25 (주) 에스와이씨 Panel with formaldehyde adsorption, water adsorption and desorption functions and preparation thereof
CN103787614A (en) * 2014-02-11 2014-05-14 江苏麦阁吸附剂有限公司 Wall material with function of promoting negative ion release and preparation method thereof
CN104030611A (en) * 2014-05-30 2014-09-10 沈承舟 Diatom ooze environment-friendly decorating material
CN104177021A (en) * 2014-08-06 2014-12-03 南京市苏宝节能科技有限公司 Diatomite putty dry material
CN104496329A (en) * 2014-12-31 2015-04-08 上海墙特节能材料有限公司 Interior inorganic dry powder heat-insulating diatom ooze and preparation method thereof

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