CN106147429B - A kind of heat-reflecting heat-insulating diatom ooze - Google Patents
A kind of heat-reflecting heat-insulating diatom ooze Download PDFInfo
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- CN106147429B CN106147429B CN201610506953.4A CN201610506953A CN106147429B CN 106147429 B CN106147429 B CN 106147429B CN 201610506953 A CN201610506953 A CN 201610506953A CN 106147429 B CN106147429 B CN 106147429B
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- diatom ooze
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D131/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid, or of a haloformic acid; Coating compositions based on derivatives of such polymers
- C09D131/02—Homopolymers or copolymers of esters of monocarboxylic acids
- C09D131/04—Homopolymers or copolymers of vinyl acetate
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
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- Inorganic Chemistry (AREA)
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Abstract
The invention discloses a kind of heat-reflecting heat-insulating diatom ooze, it is prepared by the raw material of following weight parts：42 48 parts of redispersible rubber powder, 22 32 parts of hollow glass microbead, 6 12 parts of pigment, 15 25 parts of titanium dioxide, 20 30 parts of calcium carbonate, 15 25 parts of alumina silicate, 22 28 parts of diatomite, 10 20 parts of heat-insulated synergist, 0.5 5 parts of antifreezing agent.Heat-reflecting heat-insulating diatom ooze provided by the invention, can effectively prevent the heat of the sun from being accumulated in body surface and heat up, and can carry out heat heat loss through radiation cooling automatically, and antibiotic property, high abrasion resistance are easy for construction, efficient.
Description
Technical field
The present invention relates to technical field of coatings, more particularly to a kind of heat-reflecting heat-insulating diatom ooze.
Background technology
Current building energy consumption accounts for the 30% of whole society's energy consumption, wherein main is due to the use of air-conditioning.Hot summer,
Sunlight is absorbed by roofing and is transferred within doors, indoor temperature is lifted, according to statistics, when roofing receives sunshine by direct projection to roofing
Between it is most long, and the heat that roofing absorbs accounts for house always absorbs heat 46%, therefore researches and develops insulating mold coating for construction tool
There are great economic benefit, environmental benefit and social benefit.
By reflective insulation coating brush on building surface, it becomes possible to reduce that building Xia Redong is cold and hot summer and warm winter region,
Low emissivity heat transfer structure is formed, improves building structure heat insulation, so as to reach the mesh for reducing air conditioner refrigerating energy consumption, saving the energy
's.Its mechanism of heat insulation is high mainly due to heat reflectivity, effectively reduces radiant heat transfer and convection current heat transfer.But use at present every
Hot coating is such as easy to aging over time and easy to wear by solar radiation also there are many shortcomings, can thus to apply
Expect that heat insulation variation, the service life of film shorten.
The present invention provides a kind of heat-reflecting heat-insulating diatom ooze, has excellent heat reflection cooling-down effect.
The content of the invention
For above-mentioned deficiency existing in the prior art, technology to be solved by this invention ask be to provide a kind of heat reflection every
Hot diatom ooze.
The present invention seeks to what is be achieved through the following technical solutions：
A kind of heat-reflecting heat-insulating diatom ooze, is prepared by the raw material of following weight parts：
42-48 parts of redispersible rubber powder, 22-32 parts of hollow glass microbead, 6-12 parts of pigment, 15-25 parts of titanium dioxide,
20-30 parts of calcium carbonate, 15-25 parts of alumina silicate, 22-28 parts of diatomite, synergist 10-20 parts heat-insulated, 0.5-5 parts of antifreezing agent.
Preferably, the heat-insulated synergist is made of zirconium dioxide, silica, diboron trioxide, the titanium dioxide
Zirconium, silica, the mass ratio of diboron trioxide are (1-3)：(1-3)：(1-3).
Preferably, the antifreezing agent is made of 1,3-PD, isopropanol, ethylene glycol, the 1,3-PD, isopropyl
Alcohol, the mass ratio of ethylene glycol are (1-3)：(1-3)：(1-3).
Preferably, the redispersible rubber powder can be bought or be prepared, can also be with reference to number of patent application：
201110240131.3 prepared by the method for middle embodiment 1.
Preferably, the pigment is the mixture that the phthalein mountain valley with clumps of trees and bamboo is green, exterior wall is red, one or more in chrome oxide green.
Present invention also offers the preparation method of above-mentioned heat-reflecting heat-insulating diatom ooze：By redispersible rubber powder, hollow glass
Glass microballon, pigment, calcium carbonate, alumina silicate, titanium dioxide, diatomite, heat-insulated synergist, antifreezing agent are uniformly mixed to obtain the final product.
Heat-reflecting heat-insulating diatom ooze provided by the invention, can effectively prevent the heat of the sun from being accumulated in body surface and rise
Temperature, and heat heat loss through radiation cooling can be carried out automatically, antibiotic property, high abrasion resistance are easy for construction, efficient.
Embodiment
Each raw material introduction in embodiment：
Redispersible rubber powder, with reference to number of patent application：201110240131.3 prepared by the method for middle embodiment 1.
Alumina silicate, No. CAS：12141-46-7, the technical grade provided using Changzhou Yu En new materials Science and Technology Ltd.
Alumina silicate, granularity are 2500 mesh.
Titanium dioxide, No. CAS：13463-67-7, using Du Pont, the rutile titanium dioxide of model R-960.
Calcium carbonate, No. CAS：471-34-1, the light calcium powder provided using Hebei Yan Xu mineral products Co., Ltd, granularity
1200 mesh.
Hollow glass microbead, uses the grade that Xinyang Yong Kai thermal insulation materials Co., Ltd provides as 2018, particle diameter 65-
75 μm of hollow glass microbead.
Zirconium dioxide, No. CAS：1314-23-4, particle diameter：30-40nm.
Silica, No. CAS：7631-86-9, particle diameter：30-40nm.
Diboron trioxide, No. CAS：1303-86-2, particle diameter：30-40nm.
1,3-PD, No. CAS：504-63-2.
Isopropanol, No. CAS：67-63-0.
Ethylene glycol, No. CAS：107-21-1.
Pigment uses chrome oxide green, No. CAS：1308-38-9, the model produced using Shanghai Yan Chen pigment Co., Ltd
The nanoscale chrome green of T22.
Diatomite, No. CAS：91053-39-3, specific 600 purposes using the production of Lingshou County Yong Chang mineral products processings factory are forged
Burn diatomite.
Embodiment 1
Heat-reflecting heat-insulating diatom ooze raw material (parts by weight)：
45 parts of redispersible rubber powder, 30 parts of hollow glass microbead, 6 parts of chrome oxide green, 20 parts of titanium dioxide, calcium carbonate 25
Part, 20 parts of alumina silicate, 25 parts of diatomite, 15 parts of heat-insulated synergist, 1.5 parts of antifreezing agent.
It is 1 in mass ratio that the heat-insulated synergist is made of zirconium dioxide, silica, diboron trioxide:1:1 stirring
It is uniformly mixed and obtains.
The antifreezing agent is 1 in mass ratio by 1,3- propane diols, isopropanol, ethylene glycol:1:1 is uniformly mixed
Arrive.
The preparation method of heat-reflecting heat-insulating diatom ooze：By redispersible rubber powder, hollow glass microbead, chrome oxide green, two
Titanium oxide, calcium carbonate, alumina silicate, diatomite, antifreezing agent, heat-insulated synergist stir 15 points using cantilever double-spiral conical mixer
Clock is uniformly mixed the heat-reflecting heat-insulating diatom ooze up to embodiment 1.
Embodiment 2
It is substantially the same manner as Example 1, differ only in：The heat-insulated synergist presses matter by zirconium dioxide, silica
Amount is than being 1:1 is uniformly mixed to obtain.Obtain the heat-reflecting heat-insulating diatom ooze of embodiment 2.
Embodiment 3
It is substantially the same manner as Example 1, differ only in：The heat-insulated synergist is pressed by zirconium dioxide, diboron trioxide
Mass ratio is 1:1 is uniformly mixed to obtain.Obtain the heat-reflecting heat-insulating diatom ooze of embodiment 3.
Embodiment 4
It is substantially the same manner as Example 1, differ only in：The heat-insulated synergist is pressed by silica, diboron trioxide
Mass ratio is 1:1 is uniformly mixed to obtain.Obtain the heat-reflecting heat-insulating diatom ooze of embodiment 4.
Embodiment 5
It is substantially the same manner as Example 1, differ only in：The antifreezing agent is by 1,3- propane diols, isopropanol, in mass ratio
For 1:1 is uniformly mixed to obtain.Obtain the heat-reflecting heat-insulating diatom ooze of embodiment 5.
Embodiment 6
It is substantially the same manner as Example 1, differ only in：The antifreezing agent by 1,3- propane diols, ethylene glycol in mass ratio
For 1:1 is uniformly mixed to obtain.Obtain the heat-reflecting heat-insulating diatom ooze of embodiment 6.
Embodiment 7
It is substantially the same manner as Example 1, differ only in：The antifreezing agent is 1 in mass ratio by isopropanol, ethylene glycol:1
It is uniformly mixed to obtain.Obtain the heat-reflecting heat-insulating diatom ooze of embodiment 7.
Test case 1
The heat-reflecting heat-insulating diatom ooze that embodiment 1-7 is prepared, the heat-reflecting heat-insulating silicon for taking 1-7 to be prepared respectively
Algal gel 10kg and 5.5kg water is uniformly mixed up to can be used for constructing, and anti-microbial property presses GB/T21866-2008 antibiotic paints
Anti-microbial property assay method and antibacterial effect, HG/T 3980-2007 antibiotic paints measure.Concrete outcome is shown in Table 1.
Table 1：Anti-microbial property test result table
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (zirconium dioxide, silica, diboron trioxide compounding) antibacterial
Performance is substantially better than embodiment 2-4 (the two any compounding in zirconium dioxide, silica, diboron trioxide).
Comparing embodiment 1 and embodiment 5-7, embodiment 1 (1,3-PD, isopropanol, ethylene glycol compounding) anti-microbial property
It is substantially better than embodiment 5-7 (the two any compounding in 1,3- propane diols, isopropanol, ethylene glycol).
Test case 2
The heat-reflecting heat-insulating diatom ooze that embodiment 1-7 is prepared carries out thermal reflection test, takes 1-7 to be prepared respectively
Heat-reflecting heat-insulating diatom ooze 10kg and 5.5kg water be uniformly mixed up to can be used for construct, according to JC/T1040-2007
《Outer surface of building heat-reflecting heat-insulating diatom ooze》Tested.2 are shown in Table to the reflectivity results of sunlight photo-thermal ray.
Table 2：Heat reflection performance test result table
| Sample | Reflectivity, % |
| Embodiment 1 | 98.1 |
| Embodiment 2 | 94.1 |
| Embodiment 3 | 93.4 |
| Embodiment 4 | 94.3 |
| Embodiment 5 | 95.4 |
| Embodiment 6 | 94.8 |
| Embodiment 7 | 94.1 |
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (zirconium dioxide, silica, diboron trioxide compounding) heat are anti-
Penetrate performance and be substantially better than embodiment 2-4 (the two any compounding in zirconium dioxide, silica, diboron trioxide).
Comparing embodiment 1 and embodiment 5-7, embodiment 1 (1,3-PD, isopropanol, ethylene glycol compounding) heat reflectivity
Embodiment 5-7 (the two any compounding in 1,3- propane diols, isopropanol, ethylene glycol) can be substantially better than.
Claims (2)
1. a kind of heat-reflecting heat-insulating diatom ooze, it is characterised in that be prepared by the raw material of following weight parts：Redispersible glue
42-48 parts of powder, 22-32 parts of hollow glass microbead, 6-12 parts of pigment, 15-25 parts of titanium dioxide, 20-30 parts of calcium carbonate, alumina silicate
15-25 parts, 22-28 parts of diatomite, synergist 10-20 parts heat-insulated, 0.5-5 parts of antifreezing agent
The antifreezing agent is made of 1,3-PD, isopropanol, ethylene glycol, the 1,3-PD, isopropanol, ethylene glycol
Mass ratio is (1-3)：(1-3)：(1-3)
The heat-insulated synergist is made of zirconium dioxide, silica, diboron trioxide, the zirconium dioxide, silica,
The mass ratio of diboron trioxide is (1-3)：(1-3)：(1-3).
2. heat-reflecting heat-insulating diatom ooze as claimed in claim 1, it is characterised in that：The pigment for the phthalein mountain valley with clumps of trees and bamboo is green, exterior wall is red,
One or more mixture in chrome oxide green.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610506953.4A CN106147429B (en) | 2016-06-30 | 2016-06-30 | A kind of heat-reflecting heat-insulating diatom ooze |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610506953.4A CN106147429B (en) | 2016-06-30 | 2016-06-30 | A kind of heat-reflecting heat-insulating diatom ooze |
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| Publication Number | Publication Date |
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| CN106147429A CN106147429A (en) | 2016-11-23 |
| CN106147429B true CN106147429B (en) | 2018-05-11 |
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| CN201610506953.4A Expired - Fee Related CN106147429B (en) | 2016-06-30 | 2016-06-30 | A kind of heat-reflecting heat-insulating diatom ooze |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107459300A (en) * | 2017-08-15 | 2017-12-12 | 安徽琦家科技股份有限公司 | A kind of Multifunctional diatom ooze |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101209915A (en) * | 2006-12-26 | 2008-07-02 | 涂国义 | Building inside and outside wall thermal insulation putty |
| WO2009125478A1 (en) * | 2008-04-09 | 2009-10-15 | Ｓｃｉ－Ｐａｉｎｔ Ｊａｐａｎ株式会社 | Thermal insulation coating material |
| CN101648794A (en) * | 2009-09-21 | 2010-02-17 | 吕海涛 | Dry-type heat-insulating waterproof coating |
| CN104496329A (en) * | 2014-12-31 | 2015-04-08 | 上海墙特节能材料有限公司 | Interior inorganic dry powder heat-insulating diatom ooze and preparation method thereof |
-
2016
- 2016-06-30 CN CN201610506953.4A patent/CN106147429B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101209915A (en) * | 2006-12-26 | 2008-07-02 | 涂国义 | Building inside and outside wall thermal insulation putty |
| WO2009125478A1 (en) * | 2008-04-09 | 2009-10-15 | Ｓｃｉ－Ｐａｉｎｔ Ｊａｐａｎ株式会社 | Thermal insulation coating material |
| CN101648794A (en) * | 2009-09-21 | 2010-02-17 | 吕海涛 | Dry-type heat-insulating waterproof coating |
| CN104496329A (en) * | 2014-12-31 | 2015-04-08 | 上海墙特节能材料有限公司 | Interior inorganic dry powder heat-insulating diatom ooze and preparation method thereof |
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Inventor after: Liu Hengda Inventor before: Wang Feifen |
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Effective date of registration: 20180117 Address after: 571924 Hainan Province Old City Development Zone Industrial Avenue Macun Port Road Macun port A, B Applicant after: Hainan Heng Xiang Jia Energy Saving Technology Co., Ltd. Address before: Hongkou District Tianbao road 200092 Shanghai 248 Lane 3, Room 302 Applicant before: Wang Feifen |
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