CN105908538A - Process for printing and dyeing wool fabric - Google Patents
Process for printing and dyeing wool fabric Download PDFInfo
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- CN105908538A CN105908538A CN201610332829.0A CN201610332829A CN105908538A CN 105908538 A CN105908538 A CN 105908538A CN 201610332829 A CN201610332829 A CN 201610332829A CN 105908538 A CN105908538 A CN 105908538A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
- D06P3/148—Wool using reactive dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
- D06P1/48—Derivatives of carbohydrates
- D06P1/50—Derivatives of cellulose
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
- D06P1/613—Polyethers without nitrogen
- D06P1/6131—Addition products of hydroxyl groups-containing compounds with oxiranes
- D06P1/6135—Addition products of hydroxyl groups-containing compounds with oxiranes from aromatic alcohols or from phenols, naphthols
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
- D06P1/613—Polyethers without nitrogen
- D06P1/6138—Polymerisation products of glycols, e.g. Carbowax, Pluronics
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/623—Aliphatic, aralophatic or cycloaliphatic
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/625—Aromatic
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- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/649—Compounds containing carbonamide, thiocarbonamide or guanyl groups
- D06P1/6495—Compounds containing carbonamide -RCON= (R=H or hydrocarbons)
- D06P1/6496—Condensation products from carboxylic acids and hydroxyalkyl amine (Kritchewski bases)
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
- D06P1/67358—Halides or oxyhalides
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- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
- D06P1/67375—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341 with sulfur-containing anions
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- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/96—Dyeing characterised by a short bath ratio
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- Textile Engineering (AREA)
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Abstract
The invention provides a process for printing and dyeing a wool fabric. The process comprises the following steps of: a preparation procedure, washing, an ionic liquid pretreatment process, a printing and dyeing process, an aging process, an after treatment process, and obtaining of the finished product. The process for printing and dyeing a wool fabric provided by the present invention effectively increases the dye-uptake of the wool fabric by means of the pretreatment using the ionic liquid to the wool fabric; secondly, a reactive dye is used in the printing and dyeing process herein, and an acid-releasing agent is added to effectively regulate the pH value in the dyeing process such that the dye is uniformly attached on the fabric. The process for printing and dyeing the wool fabric provided by the present invention is safe and non-toxic, and further is capable of improving the color fastness, reducing the dyeing bath ratio and reducing the dosages of the dye and printing and dyeing auxiliaries. Furthermore, the process is simple, obvious in beneficial effects, and suitable for popularization and use.
Description
Technical field
The present invention relates to wool fabric colouring art, further relate to a kind of wool fabric dyeing.
Background technology
Along with growth and the raising of quality of life of the size of population, single cotton textiles, pure wool, silk, change
Fine product can not meet people should the various functions such as the most warming, smooth attractive in appearance be wanted fabric
Ask.Bafta has excellent feel and a taking, and wool fabric has fine and soft, moisture absorption, the spy such as warming
Point, merges both advantages, just creates this novel garment material of wool fabric.
Wool fabric is generally divided into two kinds: (1) shuttle-woven fabric, also referred to as woven fabric are mutual to warp thread and weft yarn
The fabric that vertical weave in is formed.There are plain weave, twill, three kinds of satin weave in its elementary organization.Different
Shuttle-woven fabric be also to constitute by these three elementary organization and by its protean tissue.(2) knitting
Fabric, constitutes coil with knitting needle by yarn or long filament, then coil is mutually gone here and there set and form, due to knitting
The loop construction feature of thing, in unit length, yarn storage amount is more, the most mostly has good elasticity.
Wool fabric has advantages such as warming, hair matter softness, good springiness, thermal insulation are strong, but wool
Due to the design feature of its natural scale cladding, in dyeing process, through friction, rub and easily lead
The problems such as cause fiber loss, makes wool fiber displacement produce felting, upper aberration, accordingly, it would be desirable to a kind of
New technical scheme solves the problems referred to above.
For solving the problems referred to above, disclose a kind of employing ionic liquid at Chinese patent 201310232949.X
The cashmere low-temperature dyeing method of pretreatment, the ionic liquid that cashmere uses volumetric concentration be 5%～10%
After pretreatment, the dyestuff using volumetric concentration to be 5%～10%, the glauber salt of 6g/L, adjust pH value
To 4～5, water-bath, at 80 DEG C, add cryogenic booster dyeing.Described pre-process in temperature 80 DEG C,
Bath raio 1:50, water-bath 10～20min.In described staining procedure, the bath raio of water-bath is 1:50, time
Between 60～80min.Described cryogenic booster is cryogenic booster JL-D or cryogenic booster ZJ-W.Described
The volumetric concentration of cryogenic booster is 0.5%～2%.After low temperature dyeing of the present invention, strength is than normal woolenless cloth
Dyeing exceeds 10.5%, can greatly improve yarn spinnability, reduces the damage that fiber is caused by dyeing.
Although this patent improves the strength after cashmere dyeing, but there is bath raio greatly in it, produces waste water many,
The problems such as upper colourity is low.
Summary of the invention
It is an object of the invention to overcome the deficiencies in the prior art, it is provided that a kind of wool fabric dyeing,
The wool fabric dyeing of the present invention, reduces the damage that fiber is caused by dyeing, on wool fabric
Colourity is high, and dyeing bath raio is little.
For reaching above-mentioned purpose, the technical solution used in the present invention is: a kind of wool fabric dyeing and printing process,
It is characterized in that: include step:
(1) preparatory process: prepare the wool fabric of band dyeing；
(2) pre-treating technology: wool fabric is made chlorination dephosphorization, brightening agent is bleached, wash, reduce drift
Wash, wash, drying and processing；
(3) ion liquor treating process: ionic liquid pretreatment volumetric concentration is 5%～10%；
(4) dyeing and printing process: the wool fabric processed through ionic liquid is dyeed, by NaOH
2-4g/L, sodium carbonate 8-16g/L, aldehyde-free colour stabilizer L 3-5g/L, levelling agent TF-210 3-5g/L,
Reactive dye 0.5-1.5g/L is sequentially placed in water, at normal temperatures after fuel dissolution, is soaked by wool fabric
Adding printing and dyeing assistant and acid-releasing agent after entering in dye liquor, wool fabric is contaminated 30 minutes in dye liquor,
Being warming up to 50 DEG C, add softening agent, be incubated 30-40min, regulation pH value is 7.5, is warming up to 75 DEG C,
It is incubated 30 minutes；
(5) steaming technique: carry out steaming process by the wool fabric printed and dyed, steaming temperature is
95-105 DEG C, the time of steaming is 30-40min；
(6) aftertreatment technology: use the warm water of 25-35 DEG C to be rinsed steaming complete wool fabric,
Washing time is 5-15min；
(6) drying and shaping: drying temperature and be 110-120 DEG C, the time is 10-20min；
(7) finished product: the fabric after dyeing packages, and is transported to subsequent processing.
Preferably, in described step (2) pre-treating technology, the concentration of brightening agent is 2.5%-4%.
Preferably, the ionic liquid of described step (3) is Hydrophobic Ionic liquid.
Preferably, the reactive dye of described step (4) include that major ingredient and dispensing, described major ingredient include 4～6
The polyoxyethylene alkylphenol of part, alkarylsulphonic acid of 5～8 parts, the succinate of 2～4 parts, dispensing
Including the enuatrol of 2～3,2～5 parts of sodium sulfites, 3～4 parts of sodium citrates, the oxalic acid of 2～5 parts
Sodium, the sodium chloride of 1～4 part.
Preferably, the printing and dyeing assistant of described step (4) includes cocounut oil diglycollic amide, sodium sulfite, gathers
Ethylene glycol laurate, dioctyl sodium sulfosuccinate, sodium carboxymethylcellulose, borax, barium chloride
Composition, the mass fraction of the most each composition is: cocounut oil diglycollic amide 13-15 part, sodium sulfite
3-6 part, polyethylene glycol laurate 8-16 part, dioctyl sodium sulfosuccinate 20-25 part, carboxylic
Sodium carboxymethylcellulose pyce 5-8 part, barium chloride 2-3 part.
Preferably, the acid-releasing agent of described step (4) is ammonium acetate or ammonium sulfate.
Preferably, printing and dyeing bath raio 1:10-20 in described step (4).
The beneficial effects of the present invention is: the present invention provide wool fabric printing and dyeing safety non-toxic, carry
High color fastness, dye bath ratio can be reduced, reduce reactive dye consumption and the consumption of printing and dyeing assistant, subtract
The generation of few dyeing waste water.
Detailed description of the invention
Below by specific embodiment, the present invention is described further, but embodiment is not limiting as this
The protection domain of invention.
Table 1 is the chemical group of the reactive dye of wool fabric dyeing and printing process described in the embodiment of the present invention
Divide list；Table 2 is for stating the printing and dyeing assistant chemistry of wool fabric dyeing and printing process described in the embodiment of the present invention
Component list.
Table 1
Table 2
Embodiment 1
(1) preparatory process: prepare the wool fabric of band dyeing；
(2) pre-treating technology: wool fabric is made chlorination dephosphorization, concentration is 2.5% brightening agent bleaching, washes
Wash, reduce rinsing, washing, drying and processing；
(3) ion liquor treating process: Hydrophobic Ionic liquid pretreatment volumetric concentration is 5%；
(4) dyeing and printing process: the wool fabric processed through ionic liquid is dyeed, by NaOH
2g/L, sodium carbonate 8g/L, aldehyde-free colour stabilizer L 3g/L, levelling agent TF-210 3g/L, reactive dye
0.5g/L is sequentially placed in water, at normal temperatures after fuel dissolution, after being immersed in dye liquor by wool fabric again
Adding printing and dyeing assistant and acid-releasing agent ammonium acetate, wool fabric is contaminated 30 minutes in dye liquor, and bath raio is
1:10, is warming up to 50 DEG C, adds softening agent, is incubated 30min, and regulation pH value is 7.5, is warming up to
75 DEG C, it is incubated 30 minutes；
(5) steaming technique: carry out steaming process by the wool fabric printed and dyed, steaming temperature is 95 DEG C,
The time of steaming is 30min；
(6) aftertreatment technology: use the warm water of 25 DEG C to be rinsed steaming complete wool fabric, punching
The time of washing is 5min；
(6) drying and shaping: drying temperature is 110 DEG C, and the time is 10min；
(7) finished product: the fabric after dyeing packages, and is transported to subsequent processing.
Embodiment 2
(1) preparatory process: prepare the wool fabric of band dyeing；
(2) pre-treating technology: wool fabric is made chlorination dephosphorization, concentration be 3% brightening agent bleaching, washing,
Reduction rinsing, washing, drying and processing；
(3) ion liquor treating process: Hydrophobic Ionic liquid pretreatment volumetric concentration is 8%；
(4) dyeing and printing process: the wool fabric processed through ionic liquid is dyeed, by NaOH
3g/L, sodium carbonate 10g/L, aldehyde-free colour stabilizer L 4g/L, levelling agent TF-210 4g/L, activity dye
Material 1g/L is sequentially placed in water, at normal temperatures after fuel dissolution, after being immersed in dye liquor by wool fabric
Adding printing and dyeing assistant and ammonium sulfate acid-releasing agent, wool fabric is contaminated 30 minutes in dye liquor, bath raio
Being warming up to 50 DEG C for 1:15, add softening agent, be incubated 35min, regulation pH value is 7.5, heats up
To 75 DEG C, it is incubated 30 minutes；
(5) steaming technique: carry out steaming process by the wool fabric printed and dyed, steaming temperature is 100 DEG C,
The time of steaming is 35min；
(6) aftertreatment technology: use the warm water of 30 DEG C to be rinsed steaming complete wool fabric, punching
The time of washing is 15min；
(6) drying and shaping: drying temperature is 115 DEG C, and the time is 15min；
(7) finished product: the fabric after dyeing packages, and is transported to subsequent processing.
Embodiment 3
(1) preparatory process: prepare the wool fabric of band dyeing；
(2) pre-treating technology: wool fabric is made chlorination dephosphorization, concentration be 4% brightening agent bleaching, washing,
Reduction rinsing, washing, drying and processing；
(3) ion liquor treating process: Hydrophobic Ionic liquid pretreatment volumetric concentration is 10%；
(4) dyeing and printing process: the wool fabric processed through ionic liquid is dyeed, by NaOH
4g/L, sodium carbonate 16g/L, aldehyde-free colour stabilizer L 5g/L, levelling agent TF-210 5g/L, activity dye
Material 1.5g/L is sequentially placed in water, at normal temperatures after fuel dissolution, after being immersed in dye liquor by wool fabric
Adding printing and dyeing assistant and ammonium sulfate acid-releasing agent, wool fabric is contaminated 30 minutes in dye liquor, bath raio
Being warming up to 50 DEG C for 1:20, add softening agent, be incubated 40min, regulation pH value is 7.5, heats up
To 75 DEG C, it is incubated 30 minutes；
(5) steaming technique: carry out steaming process by the wool fabric printed and dyed, steaming temperature is
95-105 DEG C, the time of steaming is 40min；
(6) aftertreatment technology: use the warm water of 35 DEG C to be rinsed steaming complete wool fabric, punching
The time of washing is 15min；
(6) drying and shaping: drying temperature is 120 DEG C, and the time is 20min；
(7) finished product: the fabric after dyeing packages, and is transported to subsequent processing.
Embodiment 4
(1) preparatory process: prepare the wool fabric of band dyeing；
(2) pre-treating technology: wool fabric is made chlorination dephosphorization, concentration be 4% brightening agent bleaching, washing,
Reduction rinsing, washing, drying and processing；
(3) ion liquor treating process: Hydrophobic Ionic liquid pretreatment volumetric concentration is 10%；
(4) dyeing and printing process: the wool fabric processed through ionic liquid is dyeed, by NaOH
3g/L, sodium carbonate 15g/L, aldehyde-free colour stabilizer L 5g/L, levelling agent TF-210 5g/L, activity dye
Material 1.0g/L is sequentially placed in water, at normal temperatures after fuel dissolution, after being immersed in dye liquor by wool fabric
Adding printing and dyeing assistant and ammonium acetate acid-releasing agent, wool fabric is contaminated 30 minutes in dye liquor, bath raio
For 1:10, being warming up to 50 DEG C, add softening agent, be incubated 35min, regulation pH value is 7.5, heats up
To 75 DEG C, it is incubated 30 minutes；
(5) steaming technique: carry out steaming process by the wool fabric printed and dyed, steaming temperature is 105 DEG C,
The time of steaming is 35min；
(6) aftertreatment technology: use the warm water of 30 DEG C to be rinsed steaming complete wool fabric, punching
The time of washing is 10min；
(6) drying and shaping: drying temperature is 120 DEG C, and the time is 20min；
(7) finished product: the fabric after dyeing packages, and is transported to subsequent processing.
Embodiment 5
(1) preparatory process: prepare the wool fabric of band dyeing；
(2) pre-treating technology: wool fabric is made chlorination dephosphorization, concentration be 4% brightening agent bleaching, washing,
Reduction rinsing, washing, drying and processing；
(3) ion liquor treating process: Hydrophobic Ionic liquid pretreatment volumetric concentration is 10%；
(4) dyeing and printing process: the wool fabric processed through ionic liquid is dyeed, by NaOH
4g/L, sodium carbonate 16g/L, aldehyde-free colour stabilizer L 5g/L, levelling agent TF-210 5g/L, activity dye
Material 1.5g/L is sequentially placed in water, at normal temperatures after fuel dissolution, after being immersed in dye liquor by wool fabric
Adding printing and dyeing assistant and ammonium acetate acid-releasing agent, wool fabric is contaminated 30 minutes in dye liquor, bath raio
For 1:20, being warming up to 50 DEG C, add softening agent, be incubated 40min, regulation pH value is 7.5, heats up
To 75 DEG C, it is incubated 30 minutes；
(5) steaming technique: carry out steaming process by the wool fabric printed and dyed, steaming temperature is 105 DEG C,
The time of steaming is 40min；
(6) aftertreatment technology: use the warm water of 35 DEG C to be rinsed steaming complete wool fabric, punching
The time of washing is 15min；
(6) drying and shaping: drying temperature is 120 DEG C, and the time is 10-20min；
(7) finished product: the fabric after dyeing packages, and is transported to subsequent processing.
The dyed cloth of embodiment 1-embodiment 5 all meets " GB/T 3921-2008 textile look jail
Degree test fastness to soaping " examination criteria.
It should be noted that above example is only in order to illustrate technical scheme and unrestricted.
Although being described in detail the present invention with reference to preferred embodiment, those of ordinary skill in the art should
Work as understanding, the technical scheme of invention can be modified or equivalent, without deviating from the present invention
The scope of technical scheme, it all should be contained in scope of the presently claimed invention.
Claims (7)
1. a wool fabric dyeing and printing process, it is characterised in that: include step:
(1) preparatory process: prepare the wool fabric of band dyeing；
(2) pre-treating technology: wool fabric is made chlorination dephosphorization, brightening agent is bleached, wash, reduce rinsing, washing, drying and processing；
(3) ion liquor treating process: pretreated ion liquid volume concentrations is
5%~10%；
(4) dyeing and printing process: the wool fabric processed through ionic liquid is dyeed, by NaOH 2-4g/L, sodium carbonate 8-16g/L, aldehyde-free colour stabilizer L 3-5g/L, levelling agent TF-210 3-5g/L, reactive dye 0.5-1.5g/L is sequentially placed in water, at normal temperatures after fuel dissolution, adding printing and dyeing assistant and acid-releasing agent after being immersed in dye liquor by wool fabric, wool fabric is contaminated 30 minutes in dye liquor, it is warming up to 50 DEG C, adding softening agent, be incubated 30-40min, regulation pH value is 7.5, it is warming up to 75 DEG C, is incubated 30 minutes；
(5) steaming technique: carry out steaming process by the wool fabric printed and dyed, steam temperature and be 95-105 DEG C, the time of steaming is 30-40min；
(6) aftertreatment technology: using the warm water of 25-35 DEG C to be rinsed steaming complete wool fabric, washing time is 5-15min；
(6) drying and shaping: drying temperature and be 110-120 DEG C, the time is 10-20min；
(7) finished product: the fabric after dyeing packages, and is transported to subsequent processing.
A kind of wool fabric dyeing and printing process the most according to claim 1, it is characterised in that: in described step (2) pre-treating technology, the concentration of brightening agent is 2.5%-4%.
A kind of wool fabric dyeing and printing process the most according to claim 1, it is characterised in that: the pretreated ion liquid of described step (3) is Hydrophobic Ionic liquid.
A kind of wool fabric dyeing and printing process the most according to claim 1, it is characterized in that: the reactive dye of described step (4) include major ingredient and dispensing, described major ingredient includes the polyoxyethylene alkylphenol of 4～6 parts, alkarylsulphonic acid of 5～8 parts, the succinate of 2～4 parts, dispensing includes the enuatrol of 2～3,2～5 parts of sodium sulfites, 3～4 parts of sodium citrates, the sodium oxalate of 2～5 parts, the sodium chloride of 1～4 part.
A kind of wool fabric dyeing and printing process the most according to claim 1, it is characterized in that: the printing and dyeing assistant of described step (4) includes that cocounut oil diglycollic amide, sodium sulfite, polyethylene glycol laurate, dioctyl sodium sulfosuccinate, sodium carboxymethylcellulose, borax, barium chloride form, the mass fraction of the most each composition is
: cocounut oil diglycollic amide 13-15 part, sodium sulfite 3-6 part, polyethylene glycol laurate 8-16 part, dioctyl sodium sulfosuccinate 20-25 part, sodium carboxymethylcellulose 5-8 part, barium chloride 2-3 part.
A kind of wool fabric dyeing and printing process the most according to claim 1, it is characterised in that: the acid-releasing agent of described step (4) is ammonium acetate or ammonium sulfate.
A kind of wool fabric dyeing and printing process the most according to claim 1, it is characterised in that: printing and dyeing bath raio 1:10-20 in described step (4).
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107503184A (en) * | 2017-09-26 | 2017-12-22 | 句容市后白镇迎瑞印花厂 | A kind of printing and dyeing assistant and preparation method thereof |
| CN109295761A (en) * | 2018-10-29 | 2019-02-01 | 长沙浩然医疗科技有限公司 | A kind of cloth dyeing and printing process |
| CN110565400A (en) * | 2019-07-30 | 2019-12-13 | 嘉兴市南秀丝语丝绸有限公司 | anti-pilling wool scarf |
| CN113564775A (en) * | 2021-07-05 | 2021-10-29 | 杭州圣玛特毛绒有限公司 | Improved blended straight woolen cloth and processing technology thereof |
Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58163791A (en) * | 1982-03-24 | 1983-09-28 | 住友化学工業株式会社 | Washing of reactive dye printed fabric |
| WO2009024766A2 (en) * | 2007-08-17 | 2009-02-26 | The Queen's University Of Belfast | Dyeing process in ionic liquid solvents |
| CN102277754A (en) * | 2011-06-28 | 2011-12-14 | 湖南工程学院 | Method of wool surface modification and low temperature dyeing |
| CN103194919A (en) * | 2013-04-24 | 2013-07-10 | 太仓市其盛化纤厂 | Printing method beneficial to improving color saturation of wool fabric |
| CN103255644A (en) * | 2013-06-13 | 2013-08-21 | 太仓协大申泰羊毛衫有限公司 | Low temperature dyeing method of wool fibers |
| CN103266501A (en) * | 2013-06-13 | 2013-08-28 | 太仓协大申泰羊毛衫有限公司 | Low-temperature cashmere dyeing method adopting ionic liquid for pretreatment |
| CN103451966A (en) * | 2012-06-05 | 2013-12-18 | 太仓协大申泰羊毛衫有限公司 | Dyeing process of Modal cloth |
| CN103451926A (en) * | 2012-06-05 | 2013-12-18 | 太仓协大申泰羊毛衫有限公司 | Moth-proofing finishing technique of woollen sweater |
| CN105088827A (en) * | 2015-08-14 | 2015-11-25 | 湖州市云巢染料化工厂 | Reactive dye |
| CN105178062A (en) * | 2015-10-15 | 2015-12-23 | 互太(番禺)纺织印染有限公司 | Dyeing process for acidic fluorescent dye |
| CN105463883A (en) * | 2015-12-15 | 2016-04-06 | 桐乡市濮院羊毛衫职业技术学校 | Printing and dyeing auxiliary |
| CN105544242A (en) * | 2015-12-30 | 2016-05-04 | 江阴市长泾花园毛纺织有限公司 | Low-temperature dyeing technology for wool fabric |
-
2016
- 2016-05-19 CN CN201610332829.0A patent/CN105908538B/en active Active
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58163791A (en) * | 1982-03-24 | 1983-09-28 | 住友化学工業株式会社 | Washing of reactive dye printed fabric |
| WO2009024766A2 (en) * | 2007-08-17 | 2009-02-26 | The Queen's University Of Belfast | Dyeing process in ionic liquid solvents |
| CN102277754A (en) * | 2011-06-28 | 2011-12-14 | 湖南工程学院 | Method of wool surface modification and low temperature dyeing |
| CN103451966A (en) * | 2012-06-05 | 2013-12-18 | 太仓协大申泰羊毛衫有限公司 | Dyeing process of Modal cloth |
| CN103451926A (en) * | 2012-06-05 | 2013-12-18 | 太仓协大申泰羊毛衫有限公司 | Moth-proofing finishing technique of woollen sweater |
| CN103194919A (en) * | 2013-04-24 | 2013-07-10 | 太仓市其盛化纤厂 | Printing method beneficial to improving color saturation of wool fabric |
| CN103255644A (en) * | 2013-06-13 | 2013-08-21 | 太仓协大申泰羊毛衫有限公司 | Low temperature dyeing method of wool fibers |
| CN103266501A (en) * | 2013-06-13 | 2013-08-28 | 太仓协大申泰羊毛衫有限公司 | Low-temperature cashmere dyeing method adopting ionic liquid for pretreatment |
| CN105088827A (en) * | 2015-08-14 | 2015-11-25 | 湖州市云巢染料化工厂 | Reactive dye |
| CN105178062A (en) * | 2015-10-15 | 2015-12-23 | 互太(番禺)纺织印染有限公司 | Dyeing process for acidic fluorescent dye |
| CN105463883A (en) * | 2015-12-15 | 2016-04-06 | 桐乡市濮院羊毛衫职业技术学校 | Printing and dyeing auxiliary |
| CN105544242A (en) * | 2015-12-30 | 2016-05-04 | 江阴市长泾花园毛纺织有限公司 | Low-temperature dyeing technology for wool fabric |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107503184A (en) * | 2017-09-26 | 2017-12-22 | 句容市后白镇迎瑞印花厂 | A kind of printing and dyeing assistant and preparation method thereof |
| CN109295761A (en) * | 2018-10-29 | 2019-02-01 | 长沙浩然医疗科技有限公司 | A kind of cloth dyeing and printing process |
| CN109295761B (en) * | 2018-10-29 | 2020-11-24 | 佛山市南海泰源印染有限公司 | Cloth printing and dyeing process |
| CN110565400A (en) * | 2019-07-30 | 2019-12-13 | 嘉兴市南秀丝语丝绸有限公司 | anti-pilling wool scarf |
| CN113564775A (en) * | 2021-07-05 | 2021-10-29 | 杭州圣玛特毛绒有限公司 | Improved blended straight woolen cloth and processing technology thereof |
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|---|---|
| CN105908538B (en) | 2018-10-19 |
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