CN105802774A - Antibacterial facial soap and preparation method thereof - Google Patents

Antibacterial facial soap and preparation method thereof Download PDF

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Publication number
CN105802774A
CN105802774A CN201610212028.0A CN201610212028A CN105802774A CN 105802774 A CN105802774 A CN 105802774A CN 201610212028 A CN201610212028 A CN 201610212028A CN 105802774 A CN105802774 A CN 105802774A
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China
Prior art keywords
parts
oil
soap
antibacterial
face cleaning
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610212028.0A
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Chinese (zh)
Inventor
沈莲
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Tianling Chinese Traditional Medicine Slice Co Ltd
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Suzhou Tianling Chinese Traditional Medicine Slice Co Ltd
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Priority to CN201610212028.0A priority Critical patent/CN105802774A/en
Publication of CN105802774A publication Critical patent/CN105802774A/en
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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C11D10/042Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/12Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses antibacterial facial soap and a preparation method thereof. The antibacterial facial soap is prepared from olive oil, coconut oil, palm oil, castor oil, wheat germ oil, avocado oil, sodium hydroxide, propolis, sodium carboxymethyl cellulose, glycerol, camptothecin, menthol, polyethylene glycol, sodium chloride, deionized water, a surfactant and an emulsifier. The preparation method comprises steps as follows: firstly, a soap base is prepared from fatty acid and sodium hydroxide, then the soap base and other components are heated, stirred and mixed, and the antibacterial facial soap is obtained through mold casting, air drying and demolding. The propolis is added to the facial soap and contains various inorganic salts, vitamins, organic acids, fructose, glucose, reductase and the like, can moisten and maintain beauty, has an antibacterial action and can solve problems of dry skin, itching and the like; the plant extract camptothecin is also added to the facial soap, has a good antibacterial effect and further improves the antibacterial performance of the facial soap. Besides, the preparation method is simple and mass production is facilitated.

Description

A kind of antibacterial face cleaning soap and preparation method thereof
Technical field
The present invention relates to cosmetics of everyday use technical field, be specifically related to a kind of antibacterial face cleaning soap and preparation method thereof.
Background technology
Face cleaning soap, also known as beauty soap, clean skin soap, nourishing soap, is the beauty and skin care class fancy soap with moisturizing, control oil, anti-acne, Bearberry Extract, and present face cleaning soap has become the star of face cleaning family, and face cleaning soap has many iron vermicellis.Return natural, use face cleaning soap in the middle of the atmosphere of organic component, gentle demand, break away from and wash face soap to dry and astringent tight, the image that soap is highly seasoned of people in the past, sweep across beauty treatment circle once again.Present composition is more exquisite, has the exclusive face cleaning soap for different skin quality, different skin problem and different curative effect.
Along with the generally raising hierarchy of consumption in addition of people's living standard is superior, people are constantly risen for the quality requirements of daily chemical product.This high request is not only embodied in commodity in process of production superior, constantly perfect on production link, and scientific and reasonable in production and sales process, it is also embodied in from source and the high request people of the essential attribute of product are constantly increased for the demand desire of natural prodcuts.And propolis, then show one's talent in this cry as a kind of high-quality natural prodcuts.
Propolis (Propolis) is apis mellifera collection colloidal state thing in plant surface and twig, and in special body of gland and other nest, material carries out comprehensive process mixing and a kind of sticky colloid substance with distinctive odor of making in its oral cavity.Propolis is many jelly, for solid matter;Color is brown-green to brownish red not etc., and this is determined by its inherent composition.Owing to being chronically at moist stuffy state in Nidus Vespae, and comparatively warm, this just provides natural hotbed for growing of microorganism, but due to the existence of propolis, but makes microbial growth obtain obvious suppression.In fact, the application for propolis is ancient, and people it can be used as excellent medical material to be applied, and obtains the experience of preciousness.In the modern times; the continuous Efficient Operation of the universal and high-tech industry owing to producing; increasing chemical products are flooded with the every aspect of people's daily life; " the chemistry crisis " thus caused makes people produce greatly to query for day-to-day chemical product safety, causes that these natural prodcuts of propolis occur in the visual field of people.And few people are applied to propolis in the manufacture of face cleaning soap at present.
Summary of the invention
For the deficiencies in the prior art, the present invention provides a kind of antibacterial face cleaning soap and preparation method thereof, and the face cleaning soap of preparation has good antibacterial effect.
The technical solution used in the present invention is as follows:
A kind of antibacterial face cleaning soap, the following components including with parts by weight: 25~35 parts of olive oil, Oleum Cocois 25~35 parts, Petiolus Trachycarpi oil 10~20 parts, Oleum Ricini 15~20 parts, Semen Tritici aestivi germ oil 15~20 parts, Avocado Oil 15~20 parts, sodium hydroxide 40~50 parts, propolis 10~15 parts, sodium carboxymethyl cellulose 5~10 parts, glycerol 20~30 parts, camptothecine 0.5~3 part, menthol 2~5 parts, Polyethylene Glycol 3~8 parts, 2~10 parts of sodium chloride, deionized water 50~80 parts, 3~10 parts of surfactant, emulsifying agent 8~15 parts.
Preferably, described antibacterial face cleaning soap, the following components including with parts by weight: 30 parts of olive oil, Oleum Cocois 30 parts, Petiolus Trachycarpi oil 15 parts, Oleum Ricini 16 parts, Semen Tritici aestivi germ oil 18 parts, Avocado Oil 18 parts, sodium hydroxide 45 parts, propolis 12 parts, sodium carboxymethyl cellulose 6 parts, glycerol 25 parts, camptothecine 2 parts, menthol 3 parts, Polyethylene Glycol 5 parts, 5 parts of sodium chloride, deionized water 75 parts, 6 parts of surfactant, emulsifying agent 12 parts.
Preferably, described surfactant is dodecyl sodium sulfate.
Preferably, described emulsifying agent is Tween-80 or TritonX-100.
The preparation method of described antibacterial face cleaning soap, comprises the following steps:
(1) each component is weighed by weight, standby;
(2) sodium hydroxide is dissolved in deionized water, obtain sodium hydroxide solution, add in water bath containers after olive oil, Oleum Cocois, Petiolus Trachycarpi oil, Oleum Ricini, Semen Tritici aestivi germ oil, Avocado Oil mixing, water proof heating under 50 DEG C~60 DEG C conditions, stirring mixing 3h~5h, adds sodium hydroxide solution, is stirred continuously, until stirring to stir motionless, make soap base standby;
(3) soap base step (2) prepared and propolis, sodium carboxymethyl cellulose, glycerol, camptothecine, menthol, Polyethylene Glycol, sodium chloride, surfactant, emulsifying agent join in rustless steel container, under 60 DEG C~80 DEG C conditions, stirring 2h~3h, obtain soap lye, discharging moulding, cooling molding, the air-dry demoulding can obtain antibacterial face cleaning soap.
Beneficial effect: add propolis in the face cleaning soap of the present invention, containing plurality of inorganic salt, vitamin, organic acid and fructose, glucose, reductase etc., gentle skin care in propolis, and has antibacterial action, it is possible to alleviate the problems such as xerosis cutis pruritus;Face cleaning soap also added plant extract camptothecine, there is good antibacterial effect equally, further increase the anti-microbial property of face cleaning soap.And preparation method of the present invention is simple, is beneficial to large-scale production.
Detailed description of the invention
Below by specific embodiment, the present invention is further described in detail, but is not limited to this.
Embodiment 1
A kind of antibacterial face cleaning soap, the following components including with parts by weight: 35 parts of olive oil, Oleum Cocois 35 parts, Petiolus Trachycarpi oil 20 parts, Oleum Ricini 20 parts, Semen Tritici aestivi germ oil 20 parts, Avocado Oil 20 parts, sodium hydroxide 50 parts, propolis 15 parts, sodium carboxymethyl cellulose 10 parts, glycerol 30 parts, camptothecine 3 parts, menthol 5 parts, Polyethylene Glycol 8 parts, 10 parts of sodium chloride, deionized water 80 parts, dodecyl sodium sulfate 10 parts, Tween-8015 part.
The preparation method of described antibacterial face cleaning soap, comprises the following steps:
(1) each component is weighed by weight, standby;
(2) sodium hydroxide is dissolved in deionized water, obtain sodium hydroxide solution, add in water bath containers after olive oil, Oleum Cocois, Petiolus Trachycarpi oil, Oleum Ricini, Semen Tritici aestivi germ oil, Avocado Oil mixing, water proof heating under 50 DEG C of conditions, stirring mixing 3h, adds sodium hydroxide solution, is stirred continuously, until stirring to stir motionless, make soap base standby;
(3) soap base step (2) prepared and propolis, sodium carboxymethyl cellulose, glycerol, camptothecine, menthol, Polyethylene Glycol, sodium chloride, dodecyl sodium sulfate, Tween-80 join in rustless steel container, under 60 DEG C of conditions, stirring 2h, obtain soap lye, discharging moulding, cooling molding, the air-dry demoulding can obtain antibacterial face cleaning soap.
Embodiment 2
A kind of antibacterial face cleaning soap, the following components including with parts by weight: 25 parts of olive oil, Oleum Cocois 25 parts, Petiolus Trachycarpi oil 10 parts, Oleum Ricini 15 parts, Semen Tritici aestivi germ oil 15 parts, Avocado Oil 150 parts, sodium hydroxide 40 parts, propolis 10 parts, sodium carboxymethyl cellulose 5 parts, glycerol 20 parts, camptothecine 0.5 part, menthol 2 parts, Polyethylene Glycol 3 parts, 2 parts of sodium chloride, deionized water 50 parts, dodecyl sodium sulfate 3 parts, TritonX-1008 parts.
The preparation method of described antibacterial face cleaning soap, comprises the following steps:
(1) each component is weighed by weight, standby;
(2) sodium hydroxide is dissolved in deionized water, obtain sodium hydroxide solution, add in water bath containers after olive oil, Oleum Cocois, Petiolus Trachycarpi oil, Oleum Ricini, Semen Tritici aestivi germ oil, Avocado Oil mixing, water proof heating under 60 DEG C of conditions, stirring mixing 5h, adds sodium hydroxide solution, is stirred continuously, until stirring to stir motionless, make soap base standby;
(3) soap base step (2) prepared and propolis, sodium carboxymethyl cellulose, glycerol, camptothecine, menthol, Polyethylene Glycol, sodium chloride, dodecyl sodium sulfate, TritonX-100 join in rustless steel container, under 80 DEG C of conditions, stirring 3h, obtain soap lye, discharging moulding, cooling molding, the air-dry demoulding can obtain antibacterial face cleaning soap.
Embodiment 3
A kind of antibacterial face cleaning soap, the following components including with parts by weight: 32 parts of olive oil, Oleum Cocois 32 parts, Petiolus Trachycarpi oil 18 parts, Oleum Ricini 18 parts, Semen Tritici aestivi germ oil 16 parts, Avocado Oil 16 parts, sodium hydroxide 48 parts, propolis 13 parts, sodium carboxymethyl cellulose 7.5 parts, glycerol 28 parts, camptothecine 1 part, menthol 4.5 parts, Polyethylene Glycol 4 parts, 3 parts of sodium chloride, deionized water 60 parts, dodecyl sodium sulfate 5 parts, Tween-8010 part.
The preparation method of described antibacterial face cleaning soap, comprises the following steps:
(1) each component is weighed by weight, standby;
(2) sodium hydroxide is dissolved in deionized water, obtain sodium hydroxide solution, add in water bath containers after olive oil, Oleum Cocois, Petiolus Trachycarpi oil, Oleum Ricini, Semen Tritici aestivi germ oil, Avocado Oil mixing, water proof heating under 55 DEG C of conditions, stirring mixing 3.5h, adds sodium hydroxide solution, is stirred continuously, until stirring to stir motionless, make soap base standby;
(3) soap base step (2) prepared and propolis, sodium carboxymethyl cellulose, glycerol, camptothecine, menthol, Polyethylene Glycol, sodium chloride, dodecyl sodium sulfate, Tween-80 join in rustless steel container, under 70 DEG C of conditions, stirring 2.5h, obtain soap lye, discharging moulding, cooling molding, the air-dry demoulding can obtain antibacterial face cleaning soap.
Embodiment 4
A kind of antibacterial face cleaning soap, the following components including with parts by weight: 30 parts of olive oil, Oleum Cocois 30 parts, Petiolus Trachycarpi oil 15 parts, Oleum Ricini 16 parts, Semen Tritici aestivi germ oil 18 parts, Avocado Oil 18 parts, sodium hydroxide 45 parts, propolis 12 parts, sodium carboxymethyl cellulose 6 parts, glycerol 25 parts, camptothecine 2 parts, menthol 3 parts, Polyethylene Glycol 5 parts, 5 parts of sodium chloride, deionized water 75 parts, 6 parts of surfactant, TritonX-10012 parts.
The preparation method of described antibacterial face cleaning soap, comprises the following steps:
(1) each component is weighed by weight, standby;
(2) sodium hydroxide is dissolved in deionized water, obtain sodium hydroxide solution, add in water bath containers after olive oil, Oleum Cocois, Petiolus Trachycarpi oil, Oleum Ricini, Semen Tritici aestivi germ oil, Avocado Oil mixing, water proof heating under 60 DEG C of conditions, stirring mixing 4h, adds sodium hydroxide solution, is stirred continuously, until stirring to stir motionless, make soap base standby;
(3) soap base step (2) prepared and propolis, sodium carboxymethyl cellulose, glycerol, camptothecine, menthol, Polyethylene Glycol, sodium chloride, dodecyl sodium sulfate, TritonX-100 join in rustless steel container, under 75 DEG C of conditions, stirring 2.5h, obtain soap lye, discharging moulding, cooling molding, the air-dry demoulding can obtain antibacterial face cleaning soap.
The antibacterial face cleaning soap that above-described embodiment is prepared carries out bacteria clearance test: uses sterilizing sampler to sample in experimenter's buccal many places, and cultivates.Then experimenter's buccal is carried out determining area, wiping of fixing time, wiping liquid is variable concentrations antimicrobial factors soap lye.After operation terminates, cleaning in region in experimenter's buccal and be sampled, and sample is carried out microorganism culturing, calculate its microbe colony sum, bacteria clearance after finally calculating before washing one's face and washing one's face, wherein bacteria clearance computational methods are:
Result is as shown in the table:

Claims (5)

1. an antibacterial face cleaning soap, it is characterised in that include the following components with parts by weight: 25~35 parts of olive oil, Oleum Cocois 25~35 parts, Petiolus Trachycarpi oil 10~20 parts, Oleum Ricini 15~20 parts, Semen Tritici aestivi germ oil 15~20 parts, Avocado Oil 15~20 parts, sodium hydroxide 40~50 parts, propolis 10~15 parts, sodium carboxymethyl cellulose 5~10 parts, glycerol 20~30 parts, camptothecine 0.5~3 part, menthol 2~5 parts, Polyethylene Glycol 3~8 parts, 2~10 parts of sodium chloride, deionized water 50~80 parts, 3~10 parts of surfactant, emulsifying agent 8~15 parts.
2. antibacterial face cleaning soap according to claim 1, it is characterised in that include the following components with parts by weight: 30 parts of olive oil, Oleum Cocois 30 parts, Petiolus Trachycarpi oil 15 parts, Oleum Ricini 16 parts, Semen Tritici aestivi germ oil 18 parts, Avocado Oil 18 parts, sodium hydroxide 45 parts, propolis 12 parts, sodium carboxymethyl cellulose 6 parts, glycerol 25 parts, camptothecine 2 parts, menthol 3 parts, Polyethylene Glycol 5 parts, 5 parts of sodium chloride, deionized water 75 parts, 6 parts of surfactant, emulsifying agent 12 parts.
3. antibacterial face cleaning soap according to claim 1, it is characterised in that described surfactant is dodecyl sodium sulfate.
4. antibacterial face cleaning soap according to claim 1, it is characterised in that described emulsifying agent is Tween-80 or TritonX-100.
5. the preparation method of the antibacterial face cleaning soap described in Claims 1-4 any one, it is characterised in that comprise the following steps:
(1) each component is weighed by weight, standby;
(2) sodium hydroxide is dissolved in deionized water, obtain sodium hydroxide solution, add in water bath containers after olive oil, Oleum Cocois, Petiolus Trachycarpi oil, Oleum Ricini, Semen Tritici aestivi germ oil, Avocado Oil mixing, water proof heating under 50 DEG C~60 DEG C conditions, stirring mixing 3h~5h, adds sodium hydroxide solution, is stirred continuously, until stirring to stir motionless, make soap base standby;
(3) soap base step (2) prepared and propolis, sodium carboxymethyl cellulose, glycerol, camptothecine, menthol, Polyethylene Glycol, sodium chloride, surfactant, emulsifying agent join in rustless steel container, under 60 DEG C~80 DEG C conditions, stirring 2h~3h, obtain soap lye, discharging moulding, cooling molding, the air-dry demoulding can obtain antibacterial face cleaning soap.
CN201610212028.0A 2016-04-07 2016-04-07 Antibacterial facial soap and preparation method thereof Pending CN105802774A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106675892A (en) * 2016-12-26 2017-05-17 江西宜信堂医疗科技有限公司 Moisturizing toilet soap and preparation method thereof
CN106675895A (en) * 2016-12-28 2017-05-17 安徽紫檀科技有限公司 Low-irritation perfumed soap and preparation method thereof
CN108004060A (en) * 2017-12-15 2018-05-08 浙江海洋大学 A kind of intestines Enteromorpha skin care soap and preparation method thereof
CN108998306A (en) * 2018-06-27 2018-12-14 跨越生物科技(滁州)有限公司 A kind of cleaning function is good and the perfumed soap preparation method that can effectively sterilize
TWI695063B (en) * 2019-06-06 2020-06-01 林聖凱 Cured product of human cleaning agent and method for preparing the same

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1263146A (en) * 2000-03-14 2000-08-16 乞永艳 Mosquito-expelling bactericidal propolis medicated soap
CN102670820A (en) * 2012-05-29 2012-09-19 浙江农林大学 Camptothecin-containing external bacteriostatic medicine and preparation method and application thereof
JP2013155369A (en) * 2012-01-05 2013-08-15 Nippon Eisei Center:Kk Shirasu soap (volcanic ash soap)
CN103756817A (en) * 2014-01-26 2014-04-30 夏程 Preparation method for manually ground soap
CN104928079A (en) * 2014-03-17 2015-09-23 高洋 Propolis perfumed soap
CN105062727A (en) * 2015-08-20 2015-11-18 北京农科亿健蜂产品研究院 Health-care perfumed soap and producing method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1263146A (en) * 2000-03-14 2000-08-16 乞永艳 Mosquito-expelling bactericidal propolis medicated soap
JP2013155369A (en) * 2012-01-05 2013-08-15 Nippon Eisei Center:Kk Shirasu soap (volcanic ash soap)
CN102670820A (en) * 2012-05-29 2012-09-19 浙江农林大学 Camptothecin-containing external bacteriostatic medicine and preparation method and application thereof
CN103756817A (en) * 2014-01-26 2014-04-30 夏程 Preparation method for manually ground soap
CN104928079A (en) * 2014-03-17 2015-09-23 高洋 Propolis perfumed soap
CN105062727A (en) * 2015-08-20 2015-11-18 北京农科亿健蜂产品研究院 Health-care perfumed soap and producing method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106675892A (en) * 2016-12-26 2017-05-17 江西宜信堂医疗科技有限公司 Moisturizing toilet soap and preparation method thereof
CN106675895A (en) * 2016-12-28 2017-05-17 安徽紫檀科技有限公司 Low-irritation perfumed soap and preparation method thereof
CN108004060A (en) * 2017-12-15 2018-05-08 浙江海洋大学 A kind of intestines Enteromorpha skin care soap and preparation method thereof
CN108998306A (en) * 2018-06-27 2018-12-14 跨越生物科技(滁州)有限公司 A kind of cleaning function is good and the perfumed soap preparation method that can effectively sterilize
TWI695063B (en) * 2019-06-06 2020-06-01 林聖凱 Cured product of human cleaning agent and method for preparing the same

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Application publication date: 20160727