CN105780506B - A kind of insulation noise-proofing foaming paulin room material and preparation method thereof - Google Patents

A kind of insulation noise-proofing foaming paulin room material and preparation method thereof Download PDF

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Publication number
CN105780506B
CN105780506B CN201610189233.XA CN201610189233A CN105780506B CN 105780506 B CN105780506 B CN 105780506B CN 201610189233 A CN201610189233 A CN 201610189233A CN 105780506 B CN105780506 B CN 105780506B
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masking liquid
glue
polyester fiber
layer
screen cloth
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CN105780506A (en
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林生雄
黄万能
滕碧龙
谢志海
吴孙旺
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Ideal Environmental Protection Material Technology (shanghai) Co Ltd
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Ideal Environmental Protection Material Technology (shanghai) Co Ltd
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    • D06N3/00Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0002Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate
    • D06N3/0015Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the substrate using fibres of specified chemical or physical nature, e.g. natural silk
    • D06N3/0036Polyester fibres
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    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/152Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen having a hydroxy group bound to a carbon atom of a six-membered aromatic ring
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    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/35Heterocyclic compounds
    • D06M13/355Heterocyclic compounds having six-membered heterocyclic rings
    • D06M13/358Triazines
    • D06M13/364Cyanuric acid; Isocyanuric acid; Derivatives thereof
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    • D06N3/0043Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by their foraminous structure; Characteristics of the foamed layer or of cellular layers
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    • D06N3/00Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/007Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by mechanical or physical treatments
    • D06N3/0077Embossing; Pressing of the surface; Tumbling and crumbling; Cracking; Cooling; Heating, e.g. mirror finish
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    • D06N3/0086Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the application technique
    • D06N3/0088Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the application technique by directly applying the resin
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    • D06N3/00Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/04Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06N3/047Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds with fluoropolymers
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    • D06N3/00Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/04Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06N3/06Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds with polyvinylchloride or its copolymerisation products
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    • D06N3/00Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/04Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06N3/06Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds with polyvinylchloride or its copolymerisation products
    • D06N3/08Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds with polyvinylchloride or its copolymerisation products with a finishing layer consisting of polyacrylates, polyamides or polyurethanes or polyester
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    • D06N3/00Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/18Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with two layers of different macromolecular materials
    • D06N3/183Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with two layers of different macromolecular materials the layers are one next to the other
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    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16Synthetic fibres, other than mineral fibres
    • D06M2101/30Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32Polyesters
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    • D06N2209/00Properties of the materials
    • D06N2209/02Properties of the materials having acoustical properties
    • D06N2209/025Insulating, sound absorber
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Abstract

The invention discloses a kind of noiseproof foaming paulin room materials of insulation, including polyester fiber scrim layer, glue-line, foaming layer and process layer, the glue-line is respectively coated by glue-line masking liquid in the surface of polyester fiber scrim layer and bottom surface, drying, plasticizing, cooling aftershaping;The foaming layer is by glue-line of the foaming layer masking liquid coated in polyester fiber screen cloth layer surface, drying, plasticizing cool down aftershaping;The process layer is by glue-line of the process layer masking liquid coated in polyester fiber scrim layer bottom surface, paulin room insulation noise-proofing expanded material is made in drying, plasticizing, cooling aftershaping.Expanded material thermal conductivity factor produced by the present invention is low, density is small, flexibility is high, stability is good, has good heat preservation, heat-insulated, noiseproof effect, and processing is simple, is easy to build and recycle, and is suitable for the use of outdoor awning room.

Description

A kind of insulation noise-proofing foaming paulin room material and preparation method thereof
Technical field
The present invention relates to a kind of paulin room material more particularly to a kind of the keeping the temperature of technique, heat-insulated, noise-proofing foaming are scraped using applying Paulin room material and preparation method thereof.
Background technology
Paulin room is a kind of new outdoor activities temporary building, and flexible due to dismounting, accumulating is light, is referred to as " stream Dynamic house property ", it is widely used in the display and demonstration meeting of specialty, fair, celebration party, outdoor wedding, sports, festival celebration The occasions such as activity, transit depot, workshop, temporary construction, exhibitions paulin room, construction paulin room, emergency rescue.Paulin room is by movable framework It is formed with tarpaulin, frame generally has aluminium alloy and steel is critical piece, dismounts very sensitive facility, and storage facility has volume Small, easily characteristics, the tarpaulin such as transport is the highly important component in paulin room, and the security in paulin room is closed in its quality portion of directly affecting, together When also to activity security it is intimately related, therefore select high quality tarpaulin it is particularly significant.In severe cold area, especially anti-snow The disaster relief, the cold-resistant heat-insulating property of tarpaulin are most important.
But existing paulin room material property is single, as Chinese patent CN104494257A discloses a kind of paulin room heat preservation hair Foam material and preparation method thereof;And as Chinese patent CN104494264A discloses a kind of paulin room with cold-resistant heat-insulation foam material And preparation method thereof, existing paulin room expanded material cannot in heat preservation, heat-insulated, noise-proofing, cold-proof, ultraviolet radiation preventing etc. Effective balance, has seriously affected the development and application of paulin room material.
After the 1970s, production and the application under construction of external most attention thermal insulation material are made every effort to significantly The consumption of the energy is reduced, so as to reduce environmental pollution and greenhouse effects.Current country External building Peng Fangshichang also has this respect Demand, it is desirable that paulin room material has the characteristics such as thermal conductivity factor is low, density is small, flexibility is high, fire-proof and water-proof.Thermal insulation material can be received Collect waste heat, in due course steady release, graded is small, effectively reduces waste, room temperature can become, Winter protection can play it is flat Weighing apparatus acts on, and reaches heat preservation, heat-insulated, noiseproof effect, and common paulin room material is not achieved these technologies and requires at present.Therefore, such as What provides a kind of heat preservation, heat-insulated, noiseproof paulin room material to meet people's demand, certainly will become the development of current textile material Trend.
The content of the invention
The present invention to solve the above problem of the prior art, provide a kind of insulation noise-proofing foaming paulin room material and Its preparation method.The paulin room material has the characteristics such as thermal conductivity factor is low, density is small, flexibility is high, fire-proof and water-proof, achieves good Keep the temperature, be heat-insulated, noiseproof effect.
To achieve the above object, the present invention uses following technical scheme:
The first aspect of the present invention provides a kind of paulin room insulation noise-proofing expanded material, including polyester fiber net Layer of cloth, glue-line, foaming layer and process layer, the glue-line are respectively coated by glue-line masking liquid in the surface of polyester fiber scrim layer and bottom Face, drying, plasticizing, cooling aftershaping;The foaming layer is coated in the glue-line of polyester fiber screen cloth layer surface by foaming layer masking liquid On, drying, plasticizing, cooling aftershaping;The process layer is coated in the glue-line of polyester fiber scrim layer bottom surface by process layer masking liquid On, drying, plasticizing, cooling aftershaping;Wherein,
The glue-line masking liquid includes the component of following parts by weight:
Preferably, the glue-line masking liquid includes the component of following parts by weight:
The foaming layer masking liquid includes the component of following parts by weight:
Preferably, the foaming layer masking liquid includes the component of following parts by weight:
Preferably, the foaming layer masking liquid further includes 2 parts of tetradecyl trimethyl ammonium chloride.
The process layer masking liquid includes the component of following parts by weight:
5-10 parts of 2-5 parts of butanone (MEK) of Kynoar or polymethyl methacrylate.
Preferably, the process layer masking liquid includes the component of following parts by weight:
7 parts of 3 parts of butanone (MEK) of Kynoar or polymethyl methacrylate.
Further, the antioxidant presses quality proportioning 1 for antioxidant 1010 and antioxidant 164:The compound ligand of 0.5-1.2 System.
Further, the blowing agent stabilizer facilitates bubble stabilizer for K-Zn.
Further, the specific surface area of the aerosil is 90-150m2/g。
Further, the ultra-violet stabilizer presses quality proportioning 1 for UV531 and UV944:The compounding of 0.8-1.5 mixing System.
Further, PVC blending resins are F-260 in the glue-line, and the PVC paste resin in the process layer is PSM-31, the PVC paste resin in the foaming layer are P-450.
The second aspect of the invention provides a kind of preparation method of paulin room insulation noise-proofing expanded material, bag Include following steps:
1) glue-line masking liquid is prepared:Each raw material is weighed by glue-line masking liquid each component weight ratio, is then put into mixer, It is stirred 20-30 minutes, obtains glue-line masking liquid, viscosity is 10000-15000 centipoises;
2) foaming layer masking liquid is prepared:Raw material is weighed by foaming layer each component weight ratio, then puts into mixer, stirs Mixing 15-30 minutes is mixed, obtains foaming layer masking liquid, viscosity is 20000-30000 centipoises;Wherein AC foaming agents using preceding need through Grinding, fineness are less than 20 μm.
3) process layer masking liquid is prepared:Raw material is weighed by process layer masking liquid each component weight ratio, is stirred 10-20 points Clock, obtains finishing coat masking liquid, and viscosity is 100-200 centipoises;
4) prefoam:Polyester fiber screen cloth is preheated into 15-20s under 110-150 DEG C of the pre- hot-rolling of screen cloth, and carries out screen cloth Skew of weft adjusts, afterwards into vertical coaters, the upper coating glue-line masking liquid through scraper on polyester fiber screen cloth surface and bottom surface, on Paste amount is 80-100g/m2, being sent into drying and preplasticizing, oven temperature in vertical drying oven is:First gradient is 140 DEG C, the second ladder It spends for 150 DEG C of 165 DEG C of 3rd gradients, drying fusion time is 20-40s;A horizontal coating machine and horizontal two are sequentially entered afterwards Coating machine coats polyester fiber screen cloth surface, and paste amount is 110-130g/m on horizontal coater glue-line masking liquid2, Paste amount 280-320g/m on horizontal two coaters foaming layer masking liquid2, then it is respectively fed to 160-170 DEG C of a horizontal baking oven With drying in 130-150 DEG C of horizontal two baking oven and plasticizing, level-one polyester fiber screen cloth is obtained;
5) foaming:Level-one polyester fiber screen cloth is resend on coating machine, to polyester fiber screen cloth surface into Row coating coats coating glue-line masking liquid horizontal one, and upper paste amount is 100-120g/m2, a horizontal baking oven is sent at 120-150 DEG C At a temperature of dry;Then coated horizontal two and foaming layer masking liquid is coated to polyester fiber screen cloth surface, upper paste amount is 500-650g/ m2, horizontal two oven temperature is:First gradient is 150-170 DEG C, the second gradient is 190-195,3rd gradient 195-200 DEG C, 4th gradient be 205-210 DEG C, drying foamed time be 3-4min, obtain two level polyester fiber screen cloth;
6) cool down:The two level polyester fiber screen cloth come out from horizontal two baking oven is cooled down via chilled water roller;
7) coating processing layer:Two level polyester fiber screen cloth after cooling is sent between surface treatment and is surface-treated, is made Coating surface layer masking liquid is carried out with the mode that roller wheel is mounted, the coating processing layer on the bottom surface glue-line of two level polyester fiber screen cloth Upper paste amount is 40-60g/m2, subsequently into surface treatment oven for drying processing, temperature is 120-150 DEG C, dries 40-50s, cold But, the room heat-insulated heat-insulated noise-proofing expanded material of paulin is obtained.
Further, the paulin room is 3-6mm with the thickness of insulation noise-proofing expanded material.
Further, the upper paste amount of the polyester fiber folder screen cloth surface and bottom surface upper glue layer masking liquid is 180-220g/m2; The upper paste amount of the foaming layer masking liquid is 600-900g/m2;The upper paste amount of the process layer masking liquid is 40-60g/m2
Further, the polyester fiber screen cloth is antibacterial processed before glue-line is coated, the specific work of the antimicrobial treatment Skill step is:Sodium trichloro-isocyanurate and 2-hydroxy-4-n-octoxybenzophenone are taken, is configured to 3-5wt%'s with water respectively The 2-hydroxy-4-n-octoxybenzophenone solution of sodium dichloro cyanurate solution and 2-3wt%, then by weight 1:1.2- 1.5 are uniformly mixed, and obtain dressing liquid, then polyester fiber screen cloth are put into dressing liquid, two leaching two bundles, pick-up 70%-85%, Antibacterial polyester fibre screen cloth is made in drying, sizing.
The present invention compared with prior art, is had the following technical effect that using above-mentioned technical proposal:
The glue-line of paulin room of the present invention material is Corvic, process layer is Kynoar or polymethylacrylic acid Methyl esters layer;Using above formula and structure, foaming paulin room obtained material can be very good to reach thermal conductivity factor is low, density is small, The characteristics such as flexibility height, fire-proof and water-proof, radiation protection, antistatic;Thermal insulation material collects waste heat simultaneously, steadily releases in due course Put, graded is small, effectively reduces waste, and room temperature can become, Winter protection can play balanced action, reach heat preservation, it is heat-insulated, Noiseproof effect.In addition, the foaming paulin room stability of material is good, processing is simple, is easy to build and recycle, it is very suitable for family Outer paulin room uses.
Specific embodiment
The present invention is described in more detail below by specific embodiment, for a better understanding of the present invention, But following embodiments are not intended to limit the scope of the invention.
The present invention paulin room insulation noise-proofing expanded material, a strata ester fiber scrim layer, two layers of glue-line, one layer Foaming layer, layer of surface process layer.The layer of polyester fiber is located at centre, and two layers of glue-line is respectively coated in layer of polyester fiber Upper and lower surface, foaming layer are coated on surface layer glue, and surface-treated layer is coated on the glue-line of bottom.Wherein, glue-line is polychlorostyrene Vinyl, surface-treated layer are Kynoar or polymethyl methacrylate layers;It is special poly- using foaming in foaming layer Vinyl chloride paste resin (E-PVC), while addition gas forming amount is maximum in the layer formula that foams, best performance is got over, widely used AC Foaming agent in order to reduce blowing temperature, also adds a certain amount of K-Zn activators in formula.Coated, painting is scraped, dried, moulding The shaping of the operating procedures postcoolings such as change, is made paulin room insulation noise-proofing expanded material.
The preparation of 1 paulin room insulation noise-proofing expanded material of embodiment
1) glue-line masking liquid is prepared:Each raw material is weighed by glue-line masking liquid each component weight ratio, is then put into mixer, It is stirred 20-30 minutes, obtains glue-line masking liquid, viscosity is 10000-15000 centipoises;
Glue-line masking liquid includes the component of following parts by weight:
2) foaming layer masking liquid is prepared:Raw material is weighed by foaming layer each component weight ratio, then puts into mixer, stirs Mixing 15-30 minutes is mixed, obtains foaming layer masking liquid, viscosity is 20000-30000 centipoises;Wherein AC foaming agents using preceding need through Grinding, fineness are less than 20 μm.
The foaming layer masking liquid includes the component of following parts by weight:
3) process layer masking liquid is prepared:Raw material is weighed by process layer masking liquid each component weight ratio, is stirred 10-20 points Clock, obtains finishing coat masking liquid, and viscosity is 100-200 centipoises;
10 parts of 4 parts of butanone (MEK) of Kynoar.
4) prefoam:Polyester fiber screen cloth is preheated into 15-20s under 110-150 DEG C of the pre- hot-rolling of screen cloth, and carries out screen cloth Skew of weft adjusts, afterwards into vertical coaters, the upper coating glue-line masking liquid through scraper on polyester fiber screen cloth surface and bottom surface, on Paste amount is 80-100g/m2, being sent into drying and preplasticizing, oven temperature in vertical drying oven is:First gradient is 140 DEG C, the second ladder It spends for 150 DEG C of 165 DEG C of 3rd gradients, drying fusion time is 20-40s;A horizontal coating machine and horizontal two are sequentially entered afterwards Coating machine coats polyester fiber screen cloth surface, and paste amount is 110-130g/m on horizontal coater glue-line masking liquid2, Paste amount 280-320g/m on horizontal two coaters foaming layer masking liquid2, then it is respectively fed to 160-170 DEG C of a horizontal baking oven With drying in 130-150 DEG C of horizontal two baking oven and plasticizing, level-one polyester fiber screen cloth is obtained;
5) foaming:Level-one polyester fiber screen cloth is resend on coating machine, to polyester fiber screen cloth surface into Row coating coats coating glue-line masking liquid horizontal one, and upper paste amount is 100-120g/m2, a horizontal baking oven is sent at 120-150 DEG C At a temperature of dry;Then coated horizontal two and foaming layer masking liquid is coated to polyester fiber screen cloth surface, upper paste amount is 500-650g/ m2, horizontal two oven temperature is:First gradient is 150-170 DEG C, the second gradient is 190-195,3rd gradient 195-200 DEG C, 4th gradient be 205-210 DEG C, drying foamed time be 3-4min, obtain two level polyester fiber screen cloth;
6) cool down:The two level polyester fiber screen cloth come out from horizontal two baking oven is cooled down via chilled water roller;
7) coating processing layer:Two level polyester fiber screen cloth after cooling is sent between surface treatment and is surface-treated, is made Coating surface layer masking liquid is carried out with the mode that roller wheel is mounted, the coating processing layer on the bottom surface glue-line of two level polyester fiber screen cloth Upper paste amount is 40-60g/m2, subsequently into surface treatment oven for drying processing, temperature is 120-150 DEG C, dries 40-50s, cold But, the room heat-insulated heat-insulated noise-proofing expanded material of paulin is obtained.
The preparation of 2 paulin room insulation noise-proofing expanded material of embodiment
1) glue-line masking liquid is prepared:Each raw material is weighed by glue-line masking liquid each component weight ratio, is then put into mixer, It is stirred 20-30 minutes, obtains glue-line masking liquid, viscosity is 10000-15000 centipoises;
Glue-line masking liquid includes the component of following parts by weight:
2) foaming layer masking liquid is prepared:Raw material is weighed by foaming layer each component weight ratio, then puts into mixer, stirs Mixing 15-30 minutes is mixed, obtains foaming layer masking liquid, viscosity is 20000-30000 centipoises;Wherein AC foaming agents using preceding need through Grinding, fineness are less than 20 μm.
3) process layer masking liquid is prepared:Raw material is weighed by process layer masking liquid each component weight ratio, is stirred 10-20 points Clock, obtains finishing coat masking liquid, and viscosity is 100-200 centipoises;
6 parts of 5 parts of butanone (MEK) of polymethyl methacrylate.
4) prefoam:Polyester fiber screen cloth is preheated into 15-20s under 110-150 DEG C of the pre- hot-rolling of screen cloth, and carries out screen cloth Skew of weft adjusts, afterwards into vertical coaters, the upper coating glue-line masking liquid through scraper on polyester fiber screen cloth surface and bottom surface, on Paste amount is 80-100g/m2, being sent into drying and preplasticizing, oven temperature in vertical drying oven is:First gradient is 140 DEG C, the second ladder It spends for 150 DEG C of 165 DEG C of 3rd gradients, drying fusion time is 20-40s;A horizontal coating machine and horizontal two are sequentially entered afterwards Coating machine coats polyester fiber screen cloth surface, and paste amount is 110-130g/m on horizontal coater glue-line masking liquid2, Paste amount 280-320g/m on horizontal two coaters foaming layer masking liquid2, then it is respectively fed to 160-170 DEG C of a horizontal baking oven With drying in 130-150 DEG C of horizontal two baking oven and plasticizing, level-one polyester fiber screen cloth is obtained;
5) foaming:Level-one polyester fiber screen cloth is resend on coating machine, to polyester fiber screen cloth surface into Row coating coats coating glue-line masking liquid horizontal one, and upper paste amount is 100-120g/m2, a horizontal baking oven is sent at 120-150 DEG C At a temperature of dry;Then coated horizontal two and foaming layer masking liquid is coated to polyester fiber screen cloth surface, upper paste amount is 500-650g/ m2, horizontal two oven temperature is:First gradient is 150-170 DEG C, the second gradient is 190-195,3rd gradient 195-200 DEG C, 4th gradient be 205-210 DEG C, drying foamed time be 3-4min, obtain two level polyester fiber screen cloth;
6) cool down:The two level polyester fiber screen cloth come out from horizontal two baking oven is cooled down via chilled water roller;
7) coating processing layer:Two level polyester fiber screen cloth after cooling is sent between surface treatment and is surface-treated, is made Coating surface layer masking liquid is carried out with the mode that roller wheel is mounted, the coating processing layer on the bottom surface glue-line of two level polyester fiber screen cloth Upper paste amount is 40-60g/m2, subsequently into surface treatment oven for drying processing, temperature is 120-150 DEG C, dries 40-50s, cold But, the room heat-insulated heat-insulated noise-proofing expanded material of paulin is obtained.
The preparation of 3 paulin room insulation noise-proofing expanded material of embodiment
1) glue-line masking liquid is prepared:Each raw material is weighed by glue-line masking liquid each component weight ratio, is then put into mixer, It is stirred 20-30 minutes, obtains glue-line masking liquid, viscosity is 10000-15000 centipoises;
Glue-line masking liquid includes the component of following parts by weight:
2) foaming layer masking liquid is prepared:Raw material is weighed by foaming layer each component weight ratio, then puts into mixer, stirs Mixing 15-30 minutes is mixed, obtains foaming layer masking liquid, viscosity is 20000-30000 centipoises;Wherein AC foaming agents using preceding need through Grinding, fineness are less than 20 μm.
3) process layer masking liquid is prepared:Raw material is weighed by process layer masking liquid each component weight ratio, is stirred 10-20 points Clock, obtains finishing coat masking liquid, and viscosity is 100-200 centipoises;
7 parts of 3 parts of butanone (MEK) of Kynoar.
4) prefoam:Polyester fiber screen cloth is preheated into 15-20s under 110-150 DEG C of the pre- hot-rolling of screen cloth, and carries out screen cloth Skew of weft adjusts, afterwards into vertical coaters, the upper coating glue-line masking liquid through scraper on polyester fiber screen cloth surface and bottom surface, on Paste amount is 80-100g/m2, being sent into drying and preplasticizing, oven temperature in vertical drying oven is:First gradient is 140 DEG C, the second ladder It spends for 150 DEG C of 165 DEG C of 3rd gradients, drying fusion time is 20-40s;A horizontal coating machine and horizontal two are sequentially entered afterwards Coating machine coats polyester fiber screen cloth surface, and paste amount is 110-130g/m on horizontal coater glue-line masking liquid2, Paste amount 280-320g/m on horizontal two coaters foaming layer masking liquid2, then it is respectively fed to 160-170 DEG C of a horizontal baking oven With drying in 130-150 DEG C of horizontal two baking oven and plasticizing, level-one polyester fiber screen cloth is obtained;
5) foaming:Level-one polyester fiber screen cloth is resend on coating machine, to polyester fiber screen cloth surface into Row coating coats coating glue-line masking liquid horizontal one, and upper paste amount is 100-120g/m2, a horizontal baking oven is sent at 120-150 DEG C At a temperature of dry;Then coated horizontal two and foaming layer masking liquid is coated to polyester fiber screen cloth surface, upper paste amount is 500-650g/ m2, horizontal two oven temperature is:First gradient is 150-170 DEG C, the second gradient is 190-195,3rd gradient 195-200 DEG C, 4th gradient be 205-210 DEG C, drying foamed time be 3-4min, obtain two level polyester fiber screen cloth;
6) cool down:The two level polyester fiber screen cloth come out from horizontal two baking oven is cooled down via chilled water roller;
7) coating processing layer:Two level polyester fiber screen cloth after cooling is sent between surface treatment and is surface-treated, is made Coating surface layer masking liquid is carried out with the mode that roller wheel is mounted, the coating processing layer on the bottom surface glue-line of two level polyester fiber screen cloth Upper paste amount is 40-60g/m2, subsequently into surface treatment oven for drying processing, temperature is 120-150 DEG C, dries 40-50s, cold But, the room heat-insulated heat-insulated noise-proofing expanded material of paulin is obtained.
Paulin room produced by the present invention insulation noise-proofing expanded material uses the special paste that foams in surface blister layer Resin (E-PVC), while addition gas forming amount is maximum in the layer formula that foams, best performance is got over, widely used AC foaming agents.For Reduction blowing temperature, also adds a certain amount of K-Zn activators in formula.Using the paulin room material that foams made from the above method Material can be very good to reach the characteristics such as thermal conductivity factor is low, density is small, flexibility is high, fire-proof and water-proof, while thermal insulation material collects Waste heat, steady release in due course, graded is small, effectively reduces waste, and room temperature can become, Winter protection can play balance Effect reaches heat preservation, heat-insulated, noiseproof effect.
Specific embodiments of the present invention are described in detail above, but it is intended only as example, it is of the invention and unlimited It is formed on particular embodiments described above.To those skilled in the art, it is any to the equivalent modifications that carry out of the present invention and It substitutes also all among scope of the invention.Therefore, the impartial conversion made without departing from the spirit and scope of the invention and Modification, all should be contained within the scope of the invention.

Claims (4)

1. a kind of paulin room insulation noise-proofing expanded material, which is characterized in that including polyester fiber scrim layer, glue-line, hair Alveolar layer and process layer, the glue-line are respectively coated by glue-line masking liquid in the surface of polyester fiber scrim layer and bottom surface, drying, modeling Change, cooling aftershaping;The foaming layer is by glue-line of the foaming layer masking liquid coated in polyester fiber screen cloth layer surface, drying is moulded Change, cooling aftershaping;The process layer is by glue-line of the process layer masking liquid coated in polyester fiber scrim layer bottom surface, drying is moulded Change, cooling aftershaping;Wherein,
The glue-line masking liquid includes the component of following parts by weight:
The foaming layer masking liquid includes the component of following parts by weight:
The process layer masking liquid includes the component of following parts by weight:
5-10 parts of 2-5 parts of butanone (MEK) of Kynoar or polymethyl methacrylate;
The specific surface area of the aerosil is 90-150m2/g;
The antioxidant presses quality proportioning 1 for antioxidant 1010 and antioxidant 164:The compound system of 0.5-1.2;
The blowing agent stabilizer facilitates bubble stabilizer for K-Zn;
The ultra-violet stabilizer presses quality proportioning 1 for UV531 and UV944:The compound system of 0.8-1.5 mixing.
2. paulin room according to claim 1 insulation noise-proofing expanded material, which is characterized in that in the glue-line PVC blending resins are F-260, and the PVC paste resin in the foaming layer is P-450.
3. such as claim 1-2 any one of them paulin rooms preparation method of insulation noise-proofing expanded material, feature It is, comprises the following steps:
1) glue-line masking liquid is prepared:Each raw material is weighed by glue-line masking liquid each component weight ratio, is then put into mixer, stirring Mixing 20-30 minutes, obtains glue-line masking liquid, and viscosity is 10000-15000 centipoises;
2) foaming layer masking liquid is prepared:Raw material is weighed by foaming layer each component weight ratio, is then put into mixer, stirring is mixed It closes 15-30 minutes, obtains foaming layer masking liquid, viscosity is 20000-30000 centipoises;Wherein AC foaming agents need to be through grinding before Mill, fineness are less than 20 μm;
3) process layer masking liquid is prepared:Raw material is weighed by process layer masking liquid each component weight ratio, is stirred 10-20 minutes, Finishing coat masking liquid is obtained, viscosity is 100-200 centipoises;
4) prefoam:Polyester fiber screen cloth is preheated into 15-20s under 110-150 DEG C of the pre- hot-rolling of screen cloth, and carries out screen cloth skew of weft Adjustment, afterwards into vertical coaters, the upper coating glue-line masking liquid through scraper on polyester fiber screen cloth surface and bottom surface, upper paste amount For 80-100g/m2, being sent into drying and preplasticizing, oven temperature in vertical drying oven is:First gradient is 140 DEG C, the second gradient is 150 DEG C, 165 DEG C of 3rd gradient, drying fusion time are 20-40s;A horizontal coating machine and horizontal two coating are sequentially entered afterwards Machine coats polyester fiber screen cloth surface, and paste amount is 110-130g/m on horizontal coater glue-line masking liquid2, it is horizontal Paste amount 280-320g/m on two coater foaming layer masking liquids2, be then respectively fed to 160-170 DEG C a horizontal baking oven and It dries and is plasticized in 130-150 DEG C of horizontal two baking oven, obtain level-one polyester fiber screen cloth;
5) foaming:Level-one polyester fiber screen cloth on coating machine is resend, polyester fiber screen cloth surface is applied It covers, coats coating glue-line masking liquid horizontal one, upper paste amount is 100-120g/m2, a horizontal baking oven is sent into 120-150 DEG C of temperature Lower drying;Then coated horizontal two and foaming layer masking liquid is coated to polyester fiber screen cloth surface, upper paste amount is 500-650g/m2, Horizontal two oven temperature is:First gradient is 150-170 DEG C, the second gradient is 190-195,3rd gradient is 195-200 DEG C, Four gradients are 205-210 DEG C, and drying foamed time is 3-4min, obtains two level polyester fiber screen cloth;
6) cool down:The two level polyester fiber screen cloth come out from horizontal two baking oven is cooled down via chilled water roller;
7) coating processing layer:Two level polyester fiber screen cloth after cooling is sent between surface treatment and is surface-treated, uses roller The mode of cylinder wheel mounting carries out coating surface layer masking liquid, the upper paste of coating processing layer on the bottom surface glue-line of two level polyester fiber screen cloth It measures as 40-60g/m2, subsequently into surface treatment oven for drying processing, temperature is 120-150 DEG C, dries 40-50s, and cooling obtains To the room heat-insulated heat-insulated noise-proofing expanded material of paulin.
4. preparation method according to claim 3, which is characterized in that paulin room insulation noise-proofing expanded material Thickness be 3-6mm.
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