CN105778763A - Preparation process of anion decoration plate - Google Patents
Preparation process of anion decoration plate Download PDFInfo
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- CN105778763A CN105778763A CN201610352443.6A CN201610352443A CN105778763A CN 105778763 A CN105778763 A CN 105778763A CN 201610352443 A CN201610352443 A CN 201610352443A CN 105778763 A CN105778763 A CN 105778763A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D201/00—Coating compositions based on unspecified macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
A preparation process of an anion decoration plate includes the steps of firstly brushing a calcium silicate substrate with damp-proof sealing paint in a rolling mode, spraying base coat on the sealing paint after drying the sealing paint, printing pattern paint on the base coat after drying the base coat, spraying finish-coat paint after drying the pattern paint, and covering and pressing a film after drying the finish-coat paint to obtain the anion decoration plate.By means of the preparation process, in the use process, anions with extremely strong adsorption and oxidation effects can be produced, bacteria and viruses in air can be efficiently killed, the indoor living environment where the decoration plate is used can be improved, and a certain healthcare effect is achieved for human bodies; the decoration plate is bright in color, good in covering force, resistant to scrubbing, capable of preventing mildew and bacteria and meeting the requirement of modern people for environmentally friendliness of the living environment and suitable for being used and popularized in related industries of building indoor decoration plates.
Description
Technical field
The invention belongs to environment-friendly building materials preparation field, be specially the preparation technology of a kind of anion decorative panel.
Background technology
In the various construction materials of interior decoration, containing various harmful volatile organic matters, these poisonous and hazardous Organic substances include halogenated hydrocarbon compound, arene compound, aldehydes, ketone and lipoid substance, indoor environment after finishing and air are caused very big pollution, human health is constituted potentially hazardous.
Traditional inner wall of building decorative board structure and function are more single, it is easy to produce the harmful substances such as formaldehyde, very easily human body are produced injury, it is impossible to meet modern's requirement to Green environment-friendlyhome home environment.
The charged particle that atom or atomic group are formed after losing or obtain electronics is in ion, and anion refers to the ion with one or more negative charges, also known as " anion ".Negative ions in air is divided into large, medium and small three kinds of ions according to the size of mobility.The anion of little particle diameter has good biological activity, it is easy to through human body blood brain barrier, enters human body and plays its biological effect.Based on the effect of anion, it has again the title of " air vitamin ".Countless clinical researches find, anion can improve neurasthenia, insomnia, unobstructed cardiovascular and cerebrovascular vessel, reduce blood viscosity, improve body immunity, to improving insomnia, asthma, alleviating the persistent ailment such as hypertension, diabetes and have significant curative effect, correlational study is awarded in the works such as " environment, health and the negative oxygen ion " of chief editor at Chen Jingzao " the modern physics therapeutics " edited and Tsing-Hua University's woods gold penetrating judgment detailed explaination.
Summary of the invention
Harden that structure is single and problem not environmentally to solve traditional decoration, it is an object of the invention to the preparation technology of a kind of anion decorative panel, by using the anion paint of safety and environmental protection to replace traditional finish on the basis of traditional decoration plate preparation technology, the anion that decorative panel produces when in use is made to have extremely strong absorption and Oxidation, the antibacterial in air and virus can be killed efficiently, the indoor living environment using decorative panel of the present invention can be improved simultaneously, human body is had certain health-care effect, meet modern's requirement to living environment environmental protection.
The present invention is to solve that the technical scheme that the problems referred to above are taked is:
nullA kind of preparation technology of anion decorative panel，First the seal coat that round brush is moistureproof on calcium silicates substrate，Base coat is sprayed after seal coat drying，Impressing pattern paint after base coat drying，Coating hood finish paint after pattern paint is dried，Finish carries out overlay film and suppresses the anion decorative panel namely obtained after drying，According to weight ratio，Described finish preparation process is by 60-80 part emulsion、2-6 part mill base、10-16 part coloring agent and 0.05-0.13 part preservative dispersed with stirring are uniform，Add 1-4 part thickening agent and 2-6 part anion liquid is stirred，It is eventually adding 0.08-0.7 part defoamer and carries out low speed dispersion stirring，The alkaline solution containing hydroxide ion is used to adjust pH value to 8.5-10，With the nylon net filter of 150 orders after standing 10min，Filtrate stands 2h，Obtain finish；
System ensure alkaline environment simultaneously need to the Mg that dispels in system2+, add the soluble salt solutions with hydroxide ion, adjust the pH value of system on the one hand, on the other hand hydroxide ion and Mg2+Interact reaction, form Mg (OH)2Crystallization, use nylon wire be filtered removing bigger crystallization, remain less crystallization and can strengthen viscosity and the stability of finish.
Described emulsion is sufficiently mixed prepared by industry emulsion, sodium chloride solution, starch, polyvinyl alcohol and sodium carboxymethyl cellulose according to the ratio of 40:10:4:2:1, and wherein the solvent in sodium chloride solution is hardness is the soft water of 4, and the mass fraction of solute is 3-5%；
Industry emulsion not easy-to-use pure water dilution, in water, ion containing debita spissitudo contributes to the dilution of industry emulsion, but the Mg in water2+And Ca2+Then impacting, therefore the result of use of distilled water and tap water is all bad, the soft water that the present invention selects hardness to be 4, is because the Mg in soft water2+And Ca2+Concentration is relatively low does not have the industry uneven situation that caking occurs of emulsion dilution.
According to weight ratio, described mill base is made up of 1 part of titanium dioxide, 23 parts of barium sulfate, 60 parts of distilled water and 0.08 part of polyacrylamide, and wherein the fineness of titanium dioxide and barium sulfate is 500 orders；
According to weight ratio, described anion liquid is made up of 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water, 0.06 part of former times purine natural gum, 0.05 part of disodiumedetate, 0.3 part of dodecyl sodium sulfate, and wherein the fineness of tourmaline powder and medical stone powder is 3000 orders；
Described defoamer is organic silicon emulsion, and thickening agent is sodium carboxymethyl cellulose, and preservative is Methylisothiazolinone.
According to weight ratio, described finish preparation process is by uniform to 70 parts of emulsions, 5 parts of mill bases, 15 parts of coloring agent and 0.1 part of preservative dispersed with stirring, add 3 parts of thickening agents and 5 parts of anion liquid are stirred, it is eventually adding 0.5 part of defoamer and carries out low speed dispersion stirring, to be mixed uniformly rear with the nylon net filter of 150 orders, stand 2h after filtration, obtain finish.
At 40 DEG C, carry out the high-speed stirred that rotating speed is 1200 revs/min after 60-80 part emulsion, 2-6 part mill base, 10-16 part coloring agent and 0.05-0.13 part preservative are mixed by described finish preparation process, stir 30min.
High-speed stirred can use high velocity dispersators, making mixed liquor in agitator is rolling annular flow, produces strong vortex, and mixed liquor surface particle drops to bottom eddy current in the shape of a spiral, form turbulent area at 2.5-5mm place, dispersion impeller edge, mixed liquor and particle therein are subject to intensive shear and impact；Forming upper and lower two lines outside stirring region, mixed liquor is fully circulated and is stirred.By the mixed liquor distributed components that this alr mode is stirred, in stable condition, it is not susceptible to layering after standing.
The preparation process of described anion liquid is that 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water and 0.06 part of former times purine natural gum are at room temperature carried out the stirring that rotating speed is 800 revs/min, mixing time is 10min, add 0.05 part of disodiumedetate and 0.3 part of dodecyl sodium sulfate stirs, gained mixture carries out ultrasound wave aerofluxus, obtains anion liquid.
Disodiumedetate is added in the formula of anion liquid and uses as chelating agent.There is stronger complexing power, the complexation degree needed just can be reached at the even minimum consumption of less consumption, itself also has dispersion, suspension effect, because anion liquid contains the water-fast granule such as tourmaline powder and medical stone powder, the situation of layering easily occurs when standing, therefore adds disodiumedetate and can improve the stability of the suspended state of anion liquid.
Dodecyl sodium sulfate, as a kind of anion surfactant, has stronger emulsification, uses in anion liquid, and anion liquid plays emulsifying and stable effect while not affecting anion release.
Described calcium silicates substrate is through overdetermined thickness sanding to 4cm, and round brush seal coat on sanding face, round brush thickness is 40 grams every square.
Described drying course is drying 30-50min in the environment of 50 DEG C.
The coating thickness of described base coat is 50 grams every square metre；The printing thickness of described pattern paint is 35 grams every square metre；The coating thickness of described finish is 20 grams every square metre.
Beneficial effects of the present invention:
The preparation technology of a kind of anion decorative panel of the present invention, traditional finish is replaced by employing the anion paint of safety and environmental protection on the basis of traditional decoration plate preparation technology, wherein in anion paint, industry emulsion employs the sodium chloride solution that solvent is soft water and is diluted, the calcium ion in solvent and magnesium ion are dispelled, avoid both examples with some the element generation combination reactions in anion liquid thus affecting finish to produce the effect of anion, in anion liquid, additionally with the addition of a certain proportion of medical stone powder, Maifanitum is to no toxic biological and have certain biological activity, main component is except aluminosilicate and some macroelements, possibly together with various trace elements and rare earth element, its rare earth elements interacts with tourmaline powder can significantly improve the anion growing amount of finish.
In sum, the preparation technology of a kind of anion decorative panel of the present invention, obtained decorative panel can produce the anion with extremely strong absorption and Oxidation in the process used, the antibacterial in air and virus can be killed efficiently, the indoor living environment using decorative panel of the present invention can be improved simultaneously, human body is had certain health-care effect, again because preparation process of the present invention successively coats four layers of paint, and in the end finish with the addition of Methylisothiazolinone, make anion decorative panel bright in luster, covering power is good, scrubbing resistance and mildew-resistant are fungi-proofing, meet modern's requirement to living environment environmental protection, be suitable to the relevant industries at Indoor decorative plate for building promote the use of.
Detailed description of the invention
In conjunction with specific examples below, the present invention is described in further detail, and protection scope of the present invention is not limited to following example.Implementing the process of the present invention, condition, reagent, experimental technique etc., outside the lower content mentioned specially, be the universal knowledege of this area and known general knowledge, the present invention is not particularly limited content.
nullA kind of preparation technology of anion decorative panel，First the seal coat that round brush is moistureproof on calcium silicates substrate，Base coat is sprayed after seal coat drying，Impressing pattern paint after base coat drying，Coating hood finish paint after pattern paint is dried，Finish carries out overlay film and suppresses the anion decorative panel namely obtained after drying，According to weight ratio，Described finish preparation process is by 60-80 part emulsion、2-6 part mill base、10-16 part coloring agent and 0.05-0.13 part preservative dispersed with stirring are uniform，Add 1-4 part thickening agent and 2-6 part anion liquid is stirred，It is eventually adding 0.08-0.7 part defoamer and carries out low speed dispersion stirring，The alkaline solution containing hydroxide ion is used to adjust pH value to 8.5-10，With the nylon net filter of 150 orders after standing 10min，Filtrate stands 2h，Obtain finish；
System ensure alkaline environment simultaneously need to the Mg that dispels in system2+, add the soluble salt solutions with hydroxide ion, adjust the pH value of system on the one hand, on the other hand hydroxide ion and Mg2+Interact reaction, form Mg (OH)2Crystallization, use nylon wire be filtered removing bigger crystallization, remain less crystallization and can strengthen viscosity and the stability of finish.
Described emulsion is sufficiently mixed prepared by industry emulsion, sodium chloride solution, starch, polyvinyl alcohol and sodium carboxymethyl cellulose according to the ratio of 40:10:4:2:1, and wherein the solvent in sodium chloride solution is hardness is the soft water of 4, and the mass fraction of solute is 3-5%；
Industry emulsion not easy-to-use pure water dilution, in water, ion containing debita spissitudo contributes to the dilution of industry emulsion, but the Mg in water2+And Ca2+Then impacting, therefore the result of use of distilled water and tap water is all bad, the soft water that the present invention selects hardness to be 4, is because the Mg in soft water2+And Ca2+Concentration is relatively low does not have the industry uneven situation that caking occurs of emulsion dilution.
According to weight ratio, described mill base is made up of 1 part of titanium dioxide, 23 parts of barium sulfate, 60 parts of distilled water and 0.08 part of polyacrylamide, and wherein the fineness of titanium dioxide and barium sulfate is 500 orders；
According to weight ratio, described anion liquid is made up of 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water, 0.06 part of former times purine natural gum, 0.05 part of disodiumedetate, 0.3 part of dodecyl sodium sulfate, and wherein the fineness of tourmaline powder and medical stone powder is 3000 orders；
Described defoamer is organic silicon emulsion, and thickening agent is sodium carboxymethyl cellulose, and preservative is Methylisothiazolinone.
According to weight ratio, described finish preparation process is by uniform to 70 parts of emulsions, 5 parts of mill bases, 15 parts of coloring agent and 0.1 part of preservative dispersed with stirring, add 3 parts of thickening agents and 5 parts of anion liquid are stirred, it is eventually adding 0.5 part of defoamer and carries out low speed dispersion stirring, to be mixed uniformly rear with the nylon net filter of 150 orders, stand 2h after filtration, obtain finish.
At 40 DEG C, carry out the high-speed stirred that rotating speed is 1200 revs/min after 60-80 part emulsion, 2-6 part mill base, 10-16 part coloring agent and 0.05-0.13 part preservative are mixed by described finish preparation process, stir 30min.
High-speed stirred can use high velocity dispersators, making mixed liquor in agitator is rolling annular flow, produces strong vortex, and mixed liquor surface particle drops to bottom eddy current in the shape of a spiral, form turbulent area at 2.5-5mm place, dispersion impeller edge, mixed liquor and particle therein are subject to intensive shear and impact；Forming upper and lower two lines outside stirring region, mixed liquor is fully circulated and is stirred.By the mixed liquor distributed components that this alr mode is stirred, in stable condition, it is not susceptible to layering after standing.
The preparation process of described anion liquid is that 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water and 0.06 part of former times purine natural gum are at room temperature carried out the stirring that rotating speed is 800 revs/min, mixing time is 10min, add 0.05 part of disodiumedetate and 0.3 part of dodecyl sodium sulfate stirs, gained mixture carries out ultrasound wave aerofluxus, obtains anion liquid.
Disodiumedetate is added in the formula of anion liquid and uses as chelating agent.There is stronger complexing power, the complexation degree needed just can be reached at the even minimum consumption of less consumption, itself also has dispersion, suspension effect, because anion liquid contains the water-fast granule such as tourmaline powder and medical stone powder, the situation of layering easily occurs when standing, therefore adds disodiumedetate and can improve the stability of the suspended state of anion liquid.
Dodecyl sodium sulfate, as a kind of anion surfactant, has stronger emulsification, uses in anion liquid, and anion liquid plays emulsifying and stable effect while not affecting anion release.
Described calcium silicates substrate is through overdetermined thickness sanding to 4cm, and round brush seal coat on sanding face, round brush thickness is 40 grams every square.
Described drying course is drying 30-50min in the environment of 50 DEG C.
The coating thickness of described base coat is 50 grams every square metre；The printing thickness of described pattern paint is 35 grams every square metre；The coating thickness of described finish is 20 grams every square metre.
Embodiment 1
nullA kind of preparation technology of anion decorative panel，First the seal coat that round brush is moistureproof on calcium silicates substrate，Calcium silicates substrate is through overdetermined thickness sanding to 4cm，Round brush thickness is 40 grams every square，Seal coat sprays base coat after drying 30min in the environment of 50 DEG C，The coating thickness of base coat is 50 grams every square metre，Base coat dries impressing pattern paint after 30min in the environment of 50 DEG C，The printing thickness of pattern paint is 35 grams every square metre，Coating hood finish paint after pattern paint dries 30min in the environment of 50 DEG C，The coating thickness of finish is 20 grams every square metre，Finish carries out overlay film and suppresses the anion decorative panel namely obtained after drying，According to weight ratio，Described finish preparation process is by 60 parts of emulsions、2 parts of mill bases、10 parts of coloring agent and 0.05 part of preservative dispersed with stirring are uniform，Add 1 part of thickening agent and 2 parts of anion liquid are stirred，It is eventually adding 0.08 part of defoamer and carries out low speed dispersion stirring，The alkaline solution containing hydroxide ion is used to adjust pH value to 8.5，With the nylon net filter of 150 orders after standing 10min，Filtrate stands 2h，Obtain finish；Finish preparation process carries out, after 60 parts of emulsions, 2 parts of mill bases, 10 parts of coloring agent and 0.05 part of preservative mixing, the high-speed stirred that rotating speed is 1200 revs/min at 40 DEG C, stirs 30min.
Described emulsion is sufficiently mixed prepared by industry emulsion, sodium chloride solution, starch, polyvinyl alcohol and sodium carboxymethyl cellulose according to the ratio of 40:10:4:2:1, and wherein the solvent in sodium chloride solution is hardness is the soft water of 4, and the mass fraction of solute is 3%；
According to weight ratio, described mill base is made up of 1 part of titanium dioxide, 23 parts of barium sulfate, 60 parts of distilled water and 0.08 part of polyacrylamide, and wherein the fineness of titanium dioxide and barium sulfate is 500 orders；
According to weight ratio, described anion liquid is made up of 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water, 0.06 part of former times purine natural gum, 0.05 part of disodiumedetate, 0.3 part of dodecyl sodium sulfate, and wherein the fineness of tourmaline powder and medical stone powder is 3000 orders；Preparation process is that 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water and 0.06 part of former times purine natural gum are at room temperature carried out the stirring that rotating speed is 800 revs/min, mixing time is 10min, add 0.05 part of disodiumedetate and 0.3 part of dodecyl sodium sulfate stirs, gained mixture carries out ultrasound wave aerofluxus, obtains anion liquid.
Described defoamer is organic silicon emulsion, and thickening agent is sodium carboxymethyl cellulose, and preservative is Methylisothiazolinone.
Embodiment 2
nullA kind of preparation technology of anion decorative panel，First the seal coat that round brush is moistureproof on calcium silicates substrate，Calcium silicates substrate is through overdetermined thickness sanding to 4cm，Round brush thickness is 40 grams every square，Seal coat sprays base coat after drying 35min in the environment of 50 DEG C，The coating thickness of base coat is 50 grams every square metre，Base coat dries impressing pattern paint after 35min in the environment of 50 DEG C，The printing thickness of pattern paint is 35 grams every square metre，Coating hood finish paint after pattern paint dries 35min in the environment of 50 DEG C，The coating thickness of finish is 20 grams every square metre，Finish carries out overlay film and suppresses the anion decorative panel namely obtained after drying，According to weight ratio，Described finish preparation process is by 65 parts of emulsions、3 parts of mill bases、12 parts of coloring agent and 0.08 part of preservative dispersed with stirring are uniform，Add 1.5 parts of thickening agents and 3 parts of anion liquid are stirred，It is eventually adding 0.15 part of defoamer and carries out low speed dispersion stirring，The alkaline solution containing hydroxide ion is used to adjust pH value to 9，With the nylon net filter of 150 orders after standing 10min，Filtrate stands 2h，Obtain finish；Finish preparation process carries out, after 65 parts of emulsions, 3 parts of mill bases, 12 parts of coloring agent and 0.08 part of preservative mixing, the high-speed stirred that rotating speed is 1200 revs/min at 40 DEG C, stirs 30min.
Described emulsion is sufficiently mixed prepared by industry emulsion, sodium chloride solution, starch, polyvinyl alcohol and sodium carboxymethyl cellulose according to the ratio of 40:10:4:2:1, and wherein the solvent in sodium chloride solution is hardness is the soft water of 4, and the mass fraction of solute is 3.5%；
According to weight ratio, described mill base is made up of 1 part of titanium dioxide, 23 parts of barium sulfate, 60 parts of distilled water and 0.08 part of polyacrylamide, and wherein the fineness of titanium dioxide and barium sulfate is 500 orders；
According to weight ratio, described anion liquid is made up of 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water, 0.06 part of former times purine natural gum, 0.05 part of disodiumedetate, 0.3 part of dodecyl sodium sulfate, and wherein the fineness of tourmaline powder and medical stone powder is 3000 orders；Preparation process is that 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water and 0.06 part of former times purine natural gum are at room temperature carried out the stirring that rotating speed is 800 revs/min, mixing time is 10min, add 0.05 part of disodiumedetate and 0.3 part of dodecyl sodium sulfate stirs, gained mixture carries out ultrasound wave aerofluxus, obtains anion liquid.
Described defoamer is organic silicon emulsion, and thickening agent is sodium carboxymethyl cellulose, and preservative is Methylisothiazolinone.
Embodiment 3
nullA kind of preparation technology of anion decorative panel，First the seal coat that round brush is moistureproof on calcium silicates substrate，Calcium silicates substrate is through overdetermined thickness sanding to 4cm，Round brush thickness is 40 grams every square，Seal coat sprays base coat after drying 40min in the environment of 50 DEG C，The coating thickness of base coat is 50 grams every square metre，Base coat dries impressing pattern paint after 40min in the environment of 50 DEG C，The printing thickness of pattern paint is 35 grams every square metre，Coating hood finish paint after pattern paint dries 40min in the environment of 50 DEG C，The coating thickness of finish is 20 grams every square metre，Finish carries out overlay film and suppresses the anion decorative panel namely obtained after drying，According to weight ratio，Described finish preparation process is by 70 parts of emulsions、5 parts of mill bases、15 parts of coloring agent and 0.1 part of preservative dispersed with stirring are uniform，Add 3 parts of thickening agents and 5 parts of anion liquid are stirred，It is eventually adding 0.5 part of defoamer and carries out low speed dispersion stirring，To be mixed uniformly rear with the nylon net filter of 150 orders，2h is stood after filtration，Obtain finish.Finish preparation process carries out, after 70 parts of emulsions, 5 parts of mill bases, 15 parts of coloring agent and 0.1 part of preservative mixing, the high-speed stirred that rotating speed is 1200 revs/min at 40 DEG C, stirs 30min.
Described emulsion is sufficiently mixed prepared by industry emulsion, sodium chloride solution, starch, polyvinyl alcohol and sodium carboxymethyl cellulose according to the ratio of 40:10:4:2:1, and wherein the solvent in sodium chloride solution is hardness is the soft water of 4, and the mass fraction of solute is 4%；
According to weight ratio, described mill base is made up of 1 part of titanium dioxide, 23 parts of barium sulfate, 60 parts of distilled water and 0.08 part of polyacrylamide, and wherein the fineness of titanium dioxide and barium sulfate is 500 orders；
According to weight ratio, described anion liquid is made up of 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water, 0.06 part of former times purine natural gum, 0.05 part of disodiumedetate, 0.3 part of dodecyl sodium sulfate, and wherein the fineness of tourmaline powder and medical stone powder is 3000 orders；Preparation process is that 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water and 0.06 part of former times purine natural gum are at room temperature carried out the stirring that rotating speed is 800 revs/min, mixing time is 10min, add 0.05 part of disodiumedetate and 0.3 part of dodecyl sodium sulfate stirs, gained mixture carries out ultrasound wave aerofluxus, obtains anion liquid.
Described defoamer is organic silicon emulsion, and thickening agent is sodium carboxymethyl cellulose, and preservative is Methylisothiazolinone.
Embodiment 4
nullA kind of preparation technology of anion decorative panel，First the seal coat that round brush is moistureproof on calcium silicates substrate，Calcium silicates substrate is through overdetermined thickness sanding to 4cm，Round brush thickness is 40 grams every square，Seal coat sprays base coat after drying 45min in the environment of 50 DEG C，The coating thickness of base coat is 50 grams every square metre，Base coat dries impressing pattern paint after 45min in the environment of 50 DEG C，The printing thickness of pattern paint is 35 grams every square metre，Coating hood finish paint after pattern paint dries 45min in the environment of 50 DEG C，The coating thickness of finish is 20 grams every square metre，Finish carries out overlay film and suppresses the anion decorative panel namely obtained after drying，According to weight ratio，Described finish preparation process is by 75 parts of emulsions、5 parts of mill bases、15 parts of coloring agent and 0.11 part of preservative dispersed with stirring are uniform，Add 3 parts of thickening agents and 5 parts of anion liquid are stirred，It is eventually adding 0.6 part of defoamer and carries out low speed dispersion stirring，The alkaline solution containing hydroxide ion is used to adjust pH value to 8.5-10，With the nylon net filter of 150 orders after standing 10min，Filtrate stands 2h，Obtain finish；Finish preparation process carries out, after 75 parts of emulsions, 5 parts of mill bases, 15 parts of coloring agent and 0.11 part of preservative mixing, the high-speed stirred that rotating speed is 1200 revs/min at 40 DEG C, stirs 30min.
Described emulsion is sufficiently mixed prepared by industry emulsion, sodium chloride solution, starch, polyvinyl alcohol and sodium carboxymethyl cellulose according to the ratio of 40:10:4:2:1, and wherein the solvent in sodium chloride solution is hardness is the soft water of 4, and the mass fraction of solute is 3-5%；
According to weight ratio, described mill base is made up of 1 part of titanium dioxide, 23 parts of barium sulfate, 60 parts of distilled water and 0.08 part of polyacrylamide, and wherein the fineness of titanium dioxide and barium sulfate is 500 orders；
According to weight ratio, described anion liquid is made up of 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water, 0.06 part of former times purine natural gum, 0.05 part of disodiumedetate, 0.3 part of dodecyl sodium sulfate, and wherein the fineness of tourmaline powder and medical stone powder is 3000 orders；Preparation process is that 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water and 0.06 part of former times purine natural gum are at room temperature carried out the stirring that rotating speed is 800 revs/min, mixing time is 10min, add 0.05 part of disodiumedetate and 0.3 part of dodecyl sodium sulfate stirs, gained mixture carries out ultrasound wave aerofluxus, obtains anion liquid.
Described defoamer is organic silicon emulsion, and thickening agent is sodium carboxymethyl cellulose, and preservative is Methylisothiazolinone.
Embodiment 5
nullA kind of preparation technology of anion decorative panel，First the seal coat that round brush is moistureproof on calcium silicates substrate，Calcium silicates substrate is through overdetermined thickness sanding to 4cm，Round brush thickness is 40 grams every square，Seal coat sprays base coat after drying 50min in the environment of 50 DEG C，The coating thickness of base coat is 50 grams every square metre，Base coat dries impressing pattern paint after 50min in the environment of 50 DEG C，The printing thickness of pattern paint is 35 grams every square metre，Coating hood finish paint after pattern paint dries 50min in the environment of 50 DEG C，The coating thickness of finish is 20 grams every square metre，Finish carries out overlay film and suppresses the anion decorative panel namely obtained after drying，According to weight ratio，Described finish preparation process is by 80 parts of emulsions、6 parts of mill bases、16 parts of coloring agent and 0.13 part of preservative dispersed with stirring are uniform，Add 4 parts of thickening agents and 6 parts of anion liquid are stirred，It is eventually adding 0.7 part of defoamer and carries out low speed dispersion stirring，The alkaline solution containing hydroxide ion is used to adjust pH value to 10，With the nylon net filter of 150 orders after standing 10min，Filtrate stands 2h，Obtain finish；Finish preparation process carries out, after 80 parts of emulsions, 6 parts of mill bases, 16 parts of coloring agent and 0.13 part of preservative mixing, the high-speed stirred that rotating speed is 1200 revs/min at 40 DEG C, stirs 30min.
Described emulsion is sufficiently mixed prepared by industry emulsion, sodium chloride solution, starch, polyvinyl alcohol and sodium carboxymethyl cellulose according to the ratio of 40:10:4:2:1, and wherein the solvent in sodium chloride solution is hardness is the soft water of 4, and the mass fraction of solute is 5%；
According to weight ratio, described mill base is made up of 1 part of titanium dioxide, 23 parts of barium sulfate, 60 parts of distilled water and 0.08 part of polyacrylamide, and wherein the fineness of titanium dioxide and barium sulfate is 500 orders；
According to weight ratio, described anion liquid is made up of 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water, 0.06 part of former times purine natural gum, 0.05 part of disodiumedetate, 0.3 part of dodecyl sodium sulfate, and wherein the fineness of tourmaline powder and medical stone powder is 3000 orders；Preparation process is that 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water and 0.06 part of former times purine natural gum are at room temperature carried out the stirring that rotating speed is 800 revs/min, mixing time is 10min, add 0.05 part of disodiumedetate and 0.3 part of dodecyl sodium sulfate stirs, gained mixture carries out ultrasound wave aerofluxus, obtains anion liquid.
Described defoamer is organic silicon emulsion, and thickening agent is sodium carboxymethyl cellulose, and preservative is Methylisothiazolinone.
Claims (7)
- null1. the preparation technology of an anion decorative panel，First the seal coat that round brush is moistureproof on calcium silicates substrate，Base coat is sprayed after seal coat drying，Impressing pattern paint after base coat drying，Coating hood finish paint after pattern paint is dried，Finish carries out overlay film and suppresses the anion decorative panel namely obtained after drying，It is characterized in that: according to weight ratio，Described finish preparation process is by 60-80 part emulsion、2-6 part mill base、10-16 part coloring agent and 0.05-0.13 part preservative dispersed with stirring are uniform，Add 1-4 part thickening agent and 2-6 part anion liquid is stirred，It is eventually adding 0.08-0.7 part defoamer and carries out low speed dispersion stirring，The alkaline solution containing hydroxide ion is used to adjust pH value to 8.5-10，With the nylon net filter of 150 orders after standing 10min，Filtrate stands 2h，Obtain finish；Described emulsion is sufficiently mixed prepared by industry emulsion, sodium chloride solution, starch, polyvinyl alcohol and sodium carboxymethyl cellulose according to the ratio of 40:10:4:2:1, and wherein the solvent in sodium chloride solution is hardness is the soft water of 4, and the mass fraction of solute is 3-5%；According to weight ratio, described mill base is made up of 1 part of titanium dioxide, 23 parts of barium sulfate, 60 parts of distilled water and 0.08 part of polyacrylamide, and wherein the fineness of titanium dioxide and barium sulfate is 500 orders；According to weight ratio, described anion liquid is made up of 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water, 0.06 part of former times purine natural gum, 0.05 part of disodiumedetate, 0.3 part of dodecyl sodium sulfate, and wherein the fineness of tourmaline powder and medical stone powder is 3000 orders；Described defoamer is organic silicon emulsion, and thickening agent is sodium carboxymethyl cellulose, and preservative is Methylisothiazolinone.
- 2. the preparation technology of a kind of anion decorative panel as claimed in claim 1, it is characterized in that: according to weight ratio, described finish preparation process is by uniform to 70 parts of emulsions, 5 parts of mill bases, 15 parts of coloring agent and 0.1 part of preservative dispersed with stirring, add 3 parts of thickening agents and 5 parts of anion liquid are stirred, it is eventually adding 0.5 part of defoamer and carries out low speed dispersion stirring, to be mixed uniformly rear with the nylon net filter of 150 orders, stand 2h after filtration, obtain finish.
- 3. the preparation technology of a kind of anion decorative panel as claimed in claim 1, it is characterized in that: at 40 DEG C, after 60-80 part emulsion, 2-6 part mill base, 10-16 part coloring agent and 0.05-0.13 part preservative are mixed by described finish preparation process, carry out the high-speed stirred that rotating speed is 1200 revs/min, stir 30min.
- 4. the preparation technology of a kind of anion decorative panel as claimed in claim 1, it is characterized in that: the preparation process of described anion liquid is that 20 parts of tourmaline powders, 10 parts of medical stone powders, 70 parts of distilled water and 0.06 part of former times purine natural gum are at room temperature carried out the stirring that rotating speed is 800 revs/min, mixing time is 10min, add 0.05 part of disodiumedetate and 0.3 part of dodecyl sodium sulfate stirs, gained mixture carries out ultrasound wave aerofluxus, obtains anion liquid.
- 5. the preparation technology of a kind of anion decorative panel as claimed in claim 1, it is characterised in that: described calcium silicates substrate is through overdetermined thickness sanding to 4cm, and round brush seal coat on sanding face, round brush thickness is 40 grams every square.
- 6. the preparation technology of a kind of anion decorative panel as claimed in claim 1, it is characterised in that: described drying course is drying 30-50min in the environment of 50 DEG C.
- 7. the preparation technology of a kind of anion decorative panel as claimed in claim 1, it is characterised in that: the coating thickness of described base coat is 50 grams every square metre；The printing thickness of described pattern paint is 35 grams every square metre；The coating thickness of described finish is 20 grams every square metre.
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| CN109487971A (en) * | 2018-12-29 | 2019-03-19 | 山东鲁泰建筑产业化材料有限公司 | A kind of energy health decoration plate and preparation method thereof |
| CN115521673A (en) * | 2022-09-01 | 2022-12-27 | 龙牌涂料(北京)有限公司 | Environment-friendly exterior wall texture coating not prone to blooming during spraying and preparation method thereof |
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| CN105778763B (en) | 2018-03-02 |
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