CN105754021B - 一种均粒磁性聚合物微球制备方法 - Google Patents
一种均粒磁性聚合物微球制备方法 Download PDFInfo
- Publication number
- CN105754021B CN105754021B CN201610329610.5A CN201610329610A CN105754021B CN 105754021 B CN105754021 B CN 105754021B CN 201610329610 A CN201610329610 A CN 201610329610A CN 105754021 B CN105754021 B CN 105754021B
- Authority
- CN
- China
- Prior art keywords
- suspension
- iron oleate
- initiator
- monomer
- polymer microsphere
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F112/00—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
- C08F112/02—Monomers containing only one unsaturated aliphatic radical
- C08F112/04—Monomers containing only one unsaturated aliphatic radical containing one ring
- C08F112/06—Hydrocarbons
- C08F112/08—Styrene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/44—Polymerisation in the presence of compounding ingredients, e.g. plasticisers, dyestuffs, fillers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F212/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
- C08F212/02—Monomers containing only one unsaturated aliphatic radical
- C08F212/04—Monomers containing only one unsaturated aliphatic radical containing one ring
- C08F212/06—Hydrocarbons
- C08F212/08—Styrene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F212/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
- C08F212/34—Monomers containing two or more unsaturated aliphatic radicals
- C08F212/36—Divinylbenzene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2265—Oxides; Hydroxides of metals of iron
- C08K2003/2275—Ferroso-ferric oxide (Fe3O4)
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/01—Magnetic additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polymerisation Methods In General (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610329610.5A CN105754021B (zh) | 2016-05-18 | 2016-05-18 | 一种均粒磁性聚合物微球制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610329610.5A CN105754021B (zh) | 2016-05-18 | 2016-05-18 | 一种均粒磁性聚合物微球制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105754021A CN105754021A (zh) | 2016-07-13 |
CN105754021B true CN105754021B (zh) | 2018-04-03 |
Family
ID=56323093
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610329610.5A Active CN105754021B (zh) | 2016-05-18 | 2016-05-18 | 一种均粒磁性聚合物微球制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN105754021B (zh) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108607479A (zh) * | 2018-05-14 | 2018-10-02 | 苏州知益微球科技有限公司 | 一种均一磺酸基修饰的均粒磁性微球的制备方法 |
CN108559028B (zh) * | 2018-05-14 | 2020-08-11 | 苏州知益微球科技有限公司 | 一种粒径可控的羧基磁性微球的制备方法 |
CN108641028A (zh) * | 2018-05-14 | 2018-10-12 | 苏州知益微球科技有限公司 | 一种粒径可控的磁性二氧化硅微球制备方法 |
CN108554325A (zh) * | 2018-05-14 | 2018-09-21 | 苏州知益微球科技有限公司 | 一种均粒磁性二氧化硅微球制备方法 |
CN108745220A (zh) * | 2018-05-14 | 2018-11-06 | 苏州知益微球科技有限公司 | 一种均粒环氧基磁性微球的制备方法 |
CN108704587A (zh) * | 2018-05-14 | 2018-10-26 | 苏州知益微球科技有限公司 | 一种单分散氨基修饰的磁性微球的制备方法 |
CN108948557A (zh) * | 2018-07-09 | 2018-12-07 | 苏州知益微球科技有限公司 | 一种荧光磁性微球的制备方法 |
CN109206557A (zh) * | 2018-07-19 | 2019-01-15 | 苏州知益微球科技有限公司 | 一种黑色高分子磁性微球的制备方法 |
CN110294816B (zh) * | 2019-06-06 | 2021-07-16 | 东莞东阳光科研发有限公司 | 磁性纳米聚苯乙烯羧基微球及其制备方法 |
CN110511309A (zh) * | 2019-09-06 | 2019-11-29 | 无锡迈科为生物科技有限公司 | 一种磁性高分子微球的制备方法 |
CN112023841A (zh) * | 2020-07-24 | 2020-12-04 | 无锡迈科为生物科技有限公司 | 一种高载量核酸提取用均一磁性微球的制备方法 |
CN111892033A (zh) * | 2020-07-24 | 2020-11-06 | 无锡迈科为生物科技有限公司 | 一种羟基磷灰石微球的制备方法 |
CN114073940B (zh) * | 2020-08-20 | 2023-05-12 | 清华大学 | 一种核壳颗粒及其制备方法 |
CN114247393B (zh) * | 2021-12-22 | 2023-09-05 | 苏州知益微球科技有限公司 | 一种磁性聚合物微球及其制备方法和应用 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS59221302A (ja) * | 1983-05-31 | 1984-12-12 | Japan Synthetic Rubber Co Ltd | 磁性重合体粒子の製造方法 |
EP1316599B1 (en) * | 2000-08-21 | 2014-03-26 | National Institute of Advanced Industrial Science and Technology | Magnetic particles and process for producing the same |
-
2016
- 2016-05-18 CN CN201610329610.5A patent/CN105754021B/zh active Active
Non-Patent Citations (3)
Title |
---|
Fe3O4磁性纳米粒子表面修饰研究进展;熊雷等;《材料导报》;20080531;第22卷(第5期);第31-35页 * |
Preparation of Magnetic Polystyrene Microspheres with a Narrow Size Distribution;Chengli Yang et al;《American Institute of Chemical Engineers》;20050731;第51卷(第7期);第2011-2015页 * |
Preparation of Monodisperse Magnetic Polymer Microspheres by Swelling and Thermolysis Technique;Chengli Yang et al;《Langmuir》;20091112;第26卷(第7期);第5179-5183页 * |
Also Published As
Publication number | Publication date |
---|---|
CN105754021A (zh) | 2016-07-13 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN105754021B (zh) | 一种均粒磁性聚合物微球制备方法 | |
CN104250350A (zh) | 一种具有通孔结构的聚合物多孔材料的制备方法 | |
CN104151764B (zh) | 一种聚合物刷修饰的磁性复合微球及其制备方法与应用 | |
CN110522734A (zh) | 一种以聚多巴胺为模板的复合纳米微球的制备方法 | |
CA2926883C (en) | Improved process for producing magnetic monodisperse polymer particles | |
CN101085874A (zh) | 亲水性聚合物磁性微球及其制备方法和用途 | |
Ji et al. | Preparation of hollow magnetic molecularly imprinted polymer and its application in silybin recognition and controlled release | |
Abatari et al. | Superporous pellicular κ-Carrageenan–Nickel composite beads; morphological, physical and hydrodynamics evaluation for expanded bed adsorption application | |
Wang et al. | Facile fabrication of snowman-like magnetic molecularly imprinted polymer microspheres for bisphenol A via one-step Pickering emulsion polymerization | |
Asadi et al. | Synthesis, recognition and evaluation of molecularly imprinted polymer nanoparticle using miniemulsion polymerization for controlled release and analysis of risperidone in human plasma samples | |
CN104072656B (zh) | 一种制备四氧化三铁-高分子磁性复合微球的方法 | |
CN108892144B (zh) | 一种功能化多孔粒径单分散二氧化硅球形材料的制备方法 | |
Puncha-Arnon et al. | Effects of crosslinking temperature and time on microstructure and stability of cassava starch microspheres | |
CN102580642B (zh) | 一种制备高磁含量壳聚糖纳米球的方法 | |
CN104151471B (zh) | 纳米银/聚苯乙烯空心复合微球及其制备方法 | |
CN104403030A (zh) | 一种悬浮聚合法制备聚苯乙烯包覆四氧化三铁磁性复合颗粒的方法 | |
CN104448355A (zh) | 一种聚苯乙烯/贵金属复合粒子的制备方法 | |
Liu et al. | Preparation of monodisperse biodegradable magnetic microspheres using a T-shaped microchannel reactor | |
CN104177642B (zh) | 一种扩张床吸附基质及其制备方法 | |
Li et al. | Synthesis of sub-100 nm PMMA nanoparticles initiated by ammonium persulfate/ascorbic acid in acetone-water mixture | |
CN108948557A (zh) | 一种荧光磁性微球的制备方法 | |
CN114558471B (zh) | 一种松油醇改性氧化石墨烯纳米颗粒在皮克林乳液中的应用 | |
Wang et al. | Modeling controlled release from hollow porous nanospheres | |
Mirzataheria et al. | Emulsion polymerization and encapsulation of micro and nanoparticles within polymer droplets | |
CN104603160A (zh) | 混合的盐悬浮聚合法以及由其制备的树脂和催化剂 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20200602 Address after: 214174 room 50311, No. 1699, Huishan Avenue, Huishan Economic Development Zone, Wuxi City, Jiangsu Province Patentee after: Wuxi maikewei Biotechnology Co.,Ltd. Address before: 215200, Changan Road, Wujiang Economic Development Zone, Jiangsu, Suzhou province (Science and Technology Pioneer Park) Patentee before: SUZHOU KNOWLEDGE & BENEFIT SPHERE TECH. Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20220415 Address after: 215200 east side of Chang'an Road, Wujiang Economic and Technological Development Zone, Suzhou City, Jiangsu Province Patentee after: SUZHOU KNOWLEDGE & BENEFIT SPHERE TECH. Co.,Ltd. Address before: Room 50311, No. 1699, Huishan Avenue, Huishan Economic Development Zone, Wuxi, Jiangsu 214174 Patentee before: Wuxi maikewei Biotechnology Co.,Ltd. |