CN105660924A - Lung moistening and phlegm eliminating healthcare tea and preparation method thereof - Google Patents

Lung moistening and phlegm eliminating healthcare tea and preparation method thereof Download PDF

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Publication number
CN105660924A
CN105660924A CN201610035327.1A CN201610035327A CN105660924A CN 105660924 A CN105660924 A CN 105660924A CN 201610035327 A CN201610035327 A CN 201610035327A CN 105660924 A CN105660924 A CN 105660924A
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China
Prior art keywords
lung moistening
extraction
extract powder
rhizoma polygonati
tea
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CN201610035327.1A
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Chinese (zh)
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黄毅
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Shanghai Taohong Chemical Technology Co Ltd
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Shanghai Taohong Chemical Technology Co Ltd
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Priority to CN201610035327.1A priority Critical patent/CN105660924A/en
Publication of CN105660924A publication Critical patent/CN105660924A/en
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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00—Tea; Tea substitutes; Preparations thereof
    • A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00—Tea; Tea substitutes; Preparations thereof
    • A23F3/16—Tea extraction; Tea extracts; Treating tea extract; Making instant tea
    • A23F3/30—Further treatment of dried tea extract; Preparations produced thereby, e.g. instant tea

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses lung moistening and phlegm eliminating healthcare tea and a preparation method thereof.The preparation method of the lung moistening and phlegm eliminating healthcare tea includes steps: (1) respectively grinding white tea, ampelopsis grossedentata or Rhizoma Polygonati, respectively performing supercritical CO2 fluid extraction, adding an entrainer in the extraction process to obtain white tea extract liquor, ampelopsis grossedentata extract liquor or Rhizoma Polygonati extract liquor, and performing reduced pressure distillation and freeze drying to obtain white tea extract powder, ampelopsis- grossedentata extract powder or Rhizoma Polygonati extract powder; (2) well mixing, by weight, 8-12 parts of the white tea extract powder, 38-42 parts of the ampelopsis- grossedentata extract powder and 48-52 parts of Rhizoma Polygonati extract powder.The lung moistening and phlegm eliminating healthcare tea and the preparation method thereof have the advantages that due to addition of the entrainer in the extraction process, extraction yield is increased, extract products are low in solvent content, and the production process is low in environment pollution; in addition, the lung moistening and phlegm eliminating healthcare tea which contains important natural effective active ingredients is rich in nutrient, excellent in efficacies of lung moistening and phlegm eliminating and quick in action.

Description

Lung moistening is eliminated the phlegm health tea and preparation method thereof
Technical field
The present invention relates to a kind of tea, particularly relate to a kind of lung moistening and eliminate the phlegm health tea and preparation method thereof.
Background technology
Ramulus et Folium Mussaendae Pubescentis only through completing, is not kneaded after referring to a kind of harvesting, then through the tea shone or slow fire is processed after drying. Ramulus et Folium Mussaendae Pubescentis pekoe appears. Tree adopts a bud two, SANYE person, and its manufactured goods claim white peony. Ramulus et Folium Mussaendae Pubescentis be the special product major production areas of Fujian and Anji County, Zhejiang Province in Fuding, have stable political situation, Songxi, the ground such as Jianyang. Basic technology processed at the beginning of Ramulus et Folium Mussaendae Pubescentis be wither, bakee or dry in the shade, pick pick, the operation such as multiple fire. Wither be formed quality of white tea critical process. Ramulus et Folium Mussaendae Pubescentis has that profile bud milli is complete or form flower freely drape over one's shoulders all over the body the fragrant clear fresh soup color of milli milli clear in light time of aobvious green flavour sweet quality characteristic.
Ampelopsis grossedentata, it is commonly called as mountain Folium hydrangeae strigosae, manna tea, white hair monkey, MAOYANMEI, white tea cake etc., formal name used at school is Ampelopsis grossedentata, is the wild wooden defoliation liana of one of Vitaceae Ampelopsis, is distributed mainly on the ground such as China Hunan, Hubei, Yunnan, Guizhou, Guangdong, Guangxi, Fujian.
Ramulus et Folium Mussaendae Pubescentis and Ampelopsis grossedentata have abundant nutritive value, have the effect treating multiple disease, have no side effect, and all-ages, long-term drink can strengthen resistance of human body, disease-relieving and physique enhancing, life lengthening comprehensively.
Rhizoma Polygonati, formal name used at school: Polygonatumsibiricum, have another name called: polygonatum sibiricum Redoute, yellow chicken dish, shaft of a writing brush dish, claw ginseng, Rhizoma Polygonati Cirrhifolii, JIZHUASHEN. For HUANGJING ZANYU CAPSULE, rhizome horizontal walk, cylindric, tuberosity expands. Impeller is raw, stockless. Medicinal plants, has spleen reinforcing, the effect of the lung moistening and production of body fluid promoting.
Ramulus et Folium Mussaendae Pubescentis or Ampelopsis grossedentata extrat, main preparation methods has:
(1) organic solvent extraction
Organic solvent extraction, this method is simple, easy. It is mainly based upon in material various compositions different solubility in organic solvent, select to need not the little solvent of dissolved element dissolubility, carry out extracting the method separated.
(2) microwave?assisted extraction
Microwave extracting is with microwave heated samples in hermetic container, by a kind of method that material composition to be prepared is extracted by organic solvent from sample matrices. The method can complete the extraction of several samples component at short notice, and solvent load is few.
(3) ultrasonic assistant extraction method
It is a kind of emerging application technology that ultrasonic assistant extracts, and has obtained extensive use in recent years in some Separation of Natural Products. Its ultimate principle is the special roles such as the dissolution utilizing hyperacoustic cavitation to accelerate effective ingredients in plant, hyperacoustic pulverizing, stirring, can break plant cell wall, make solvent penetrate into as early as possible in plant cell, and dissolution is effective ingredient wherein. At present, ultrasonic assistant extractive technique is widely used to the extraction of Chemical Constituents of Chinese Traditional And Folk Medicine.
(4) supercritical fluid extraction
Supercritical liquid extraction technique is a kind of new separation technology that 20 century 70s grow up, be use higher than critical temperature, critical pressure fluid as the extraction process of solvent. It is a kind of quickly, selectivity is high and automation mechanized operation degree is higher sample preparation methods. Material is not only had high solvability by the fluid being in Near The Critical Point, and the dissolubility of material changes with the pressure of system or the change of temperature, pressure or temperature thereby through regulation system just can be conveniently carried out optionally extract and separate material.
Supercritical carbon dioxide fluid has the dual property of gas and liquid, the mobile performance of existing gas, there is again the solubility property of liquid, therefore can effectively liposoluble substance be extracted from mixture, there is the advantages such as dissolving power is strong, mass transfer rate fast, clean environment firendly, it is widely used in separation and the purification of natural product, is also the emerging lixiviate of food industry and isolation technics.
The invention provides a kind of lung moistening to eliminate the phlegm health tea, health care that lung moistening is eliminated the phlegm is significant.
Summary of the invention
For the deficiencies in the prior art, one of the technical problem to be solved is to provide a kind of lung moistening and eliminates the phlegm the preparation method of health tea.
The two of the technical problem to be solved are to provide a kind of lung moistening and eliminate the phlegm health tea.
For achieving the above object, the adopted technical solution is that:
A kind of lung moistening is eliminated the phlegm the preparation method of health tea, comprises the following steps:
(1) Ramulus et Folium Mussaendae Pubescentis or Ampelopsis grossedentata or Rhizoma Polygonati are pulverized, carry out supercritical CO respectively2Fluid extraction, adds entrainer in extraction process, obtain Ramulus et Folium Mussaendae Pubescentis extract or Ampelopsis grossedentata extract or Rhizoma Polygonati extracting solution, decompression distillation, lyophilization, obtains Ramulus et Folium Mussaendae Pubescentis and extracts powder or Ampelopsis grossedentata extraction powder or Rhizoma Polygonati extract powder;
(2) by Ramulus et Folium Mussaendae Pubescentis extract powder 8-12 part, Ampelopsis grossedentata extract powder 38-42 part and Rhizoma Polygonati extract powder 48-52 part mix homogeneously.
Preferably, in described step (1), entrainer is made up of ethanol, 1-propanol, 1,3-PD, described ethanol, 1-propanol, 1,3-PD mass ratio be (1-3): (1-3): (1-3).
Preferably, supercritical CO in described step (1)2Fluid extraction pressure 25-35Mpa, extraction temperature is 40-60 DEG C, and extraction time is 2-4h, CO2Flow be 10-20kg/h, the flow of entrainer is 0.5-1.5kg/h.
Present invention also offers a kind of lung moistening to eliminate the phlegm health tea, adopt said method to be prepared from.
Concrete, in the present invention:
1,3-PD, No. CAS: 504-63-2.
Ethanol, No. CAS: 64-17-5.
1-propanol, No. CAS: 71-23-8.
Lung moistening of the present invention is eliminated the phlegm health tea and preparation method thereof, supercritical extraction process adds entrainer, provide extraction yield, extracted products solvent is low, production technology is low in the pollution of the environment, lung moistening health tea of eliminating the phlegm is nutritious, containing important natural effective active composition, there is good Soboring-up liver-protecting effect, instant effect.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further, the following stated, it is only to presently preferred embodiments of the present invention, the present invention not does the restriction of other forms, and any those skilled in the art are changed to the equal Equivalent embodiments changed possibly also with the technology contents of the disclosure above. Every without departing from the present invention program content, any simple modification following example done according to the technical spirit of the present invention or equivalent variations, all fall within protection scope of the present invention.
Ramulus et Folium Mussaendae Pubescentis adopts Fujian one to moisten 3 years Chen Shou eyebrows in the old Ramulus et Folium Mussaendae Pubescentis in Fuding that Tea Industry company limited produces.
Longevity, mee tea effect was such as Cornu rhinocerotis, had refreshing and detoxicating, the special effect of improving eyesight pathogenic fire reducing, can control " big fire disease ", was the good medicine of bringing down a fever of children's's hyperpyrexia in Vietnam.
The longevity eyebrow golden mean of the Confucian school, cold not hot, antioxidation, help discharge toxin and the effect such as enhance metabolism, be a kind of well health tea.
Shou Mei has the effect brought down a fever, drive away summer heat, for good drink in summer. Make us spiritual happiness, relaxed and joyful, and rich in the aminoacid of needed by human body, tea polyphenols, mineral, multivitamin and zinc, selenium and other trace elements in tea, there is the effects such as promoting the production of body fluid to quench thirst, liver heat removing and eyesight improving, refreshment, be it is nowadays accepted that the green health beverage of the safest nutrition again.
Ampelopsis grossedentata adopts Fujian one to moisten Sanming, Fujian Province the Hakkas Ramulus et Folium Mussaendae Pubescentis that Tea Industry company limited produces.
Rhizoma Polygonati adopts the wild Rhizoma Polygonati sheet of auspicious happy woods Chinese dominoes China that Qingyang Chanyue Food Industry & Trade Co., Ltd. produces.
Embodiment 1
Lung moistening is eliminated the phlegm the preparation method of health tea, comprises the following steps:
(1) prepared by Ramulus et Folium Mussaendae Pubescentis extract powder: white tea powder is broken to 40 orders, takes Ramulus et Folium Mussaendae Pubescentis powder 3kg and carries out supercritical CO2Fluid extraction, adds entrainer, wherein CO in extraction process2Flow be 15kg/h, the flow of entrainer is 0.9kg/h, extracting pressure 30Mpa, extraction temperature is 50 DEG C, and extraction time is 3h, obtains Ramulus et Folium Mussaendae Pubescentis extract, then Ramulus et Folium Mussaendae Pubescentis extract is reduced pressure when vacuum 0.05Mpa distillation, be lyophilized into powder through-30 DEG C, obtain Ramulus et Folium Mussaendae Pubescentis and extract powder;
Prepared by Ampelopsis grossedentata extract powder: Ampelopsis grossedentata is crushed to 40 orders, takes Ampelopsis grossedentata powder 3kg and carries out supercritical CO2Fluid extraction, adds entrainer, wherein CO in extraction process2Flow be 15kg/h, the flow of entrainer is 0.9kg/h, extracting pressure 30Mpa, extraction temperature is 50 DEG C, and extraction time is 3h, obtains Ampelopsis grossedentata extract, then Ampelopsis grossedentata extract is reduced pressure when vacuum 0.05Mpa distillation, be lyophilized into powder through-30 DEG C, obtain Ampelopsis grossedentata and extract powder;
Prepared by Rhizoma Polygonati extract powder: Rhizoma Polygonati is crushed to 40 orders, takes Solomonseal Rhizome 3kg and carries out supercritical CO2Fluid extraction, adds entrainer, wherein CO in extraction process2Flow be 15kg/h, the flow of entrainer is 0.9kg/h, extracting pressure 30Mpa, extraction temperature is 50 DEG C, and extraction time is 3h, obtains Rhizoma Polygonati extract, then Rhizoma Polygonati extract is reduced pressure when vacuum 0.05Mpa distillation, be lyophilized into powder through-30 DEG C, obtain Rhizoma Polygonati and extract powder;
(2) by Ramulus et Folium Mussaendae Pubescentis extract powder 10 weight portion, Ampelopsis grossedentata extract powder 40 weight portion, Rhizoma Polygonati extract powder 50 weight portion mix homogeneously, obtain the lung moistening of embodiment 1 and eliminate the phlegm health tea.
In described step (1), entrainer is made up of ethanol, 1-propanol, 1,3-PD, wherein the flow of ethanol to be the flow of 0.3kg/h, 1-propanol be 0.3kg/h, 1,3-PD flow be 0.3kg/h.
Embodiment 2
Substantially the same manner as Example 1, differ only in: in described step (1), entrainer is made up of ethanol, 1-propanol, wherein the flow of ethanol is the flow of 0.45kg/h, 1-propanol is 0.45kg/h. Can be prepared by the lung moistening of embodiment 2 to eliminate the phlegm health tea.
Embodiment 3
Substantially the same manner as Example 1, differ only in: in described step (1), entrainer is made up of ethanol, 1,3-PD, wherein the flow of ethanol be 0.45kg/h, 1,3-PD flow be 0.45kg/h. Can be prepared by the lung moistening of embodiment 3 to eliminate the phlegm health tea.
Embodiment 4
Substantially the same manner as Example 1, differ only in: in described step (1), entrainer is made up of 1-propanol, 1,3-PD, wherein the flow of 1-propanol be 0.45kg/h, 1,3-PD flow be 0.45kg/h. Can be prepared by the lung moistening of embodiment 4 to eliminate the phlegm health tea.
Comparative example 1
Substantially the same manner as Example 1, differ only in: step is added without entrainer in (1), only with CO2Extract. Can be prepared by the lung moistening of comparative example 1 to eliminate the phlegm health tea.
Test case 1
Embodiment 1-6 and comparative example 1 are carried out lung moistening expectorant effect test.
Every group objects: 50 clinical observation cases, Symptoms is: heating, cough, expectoration, companion's chest pain or dyspnea, wherein male 25, women 25 (age 20-60 year).
Test object point in morning every day 9,6 pm respectively takes 3g lung moistening and eliminates the phlegm health tea, brews with boiled water and drinks, continuous one month, tests.
Criterion of therapeutical effect:
(1) recovery from illness: symptom, sign are wholly absent;
(2) effective: symptom substantially alleviates, and sign is clearly better;
(3) invalid: before and after treatment, non-evident sympton improves, or increases the weight of.
Concrete test data are in Table 1.
Table 1: therapeutic effect test result table
Recovery from illness Effectively Invalid
Embodiment 1 35 14 1
Embodiment 2 31 16 3
Embodiment 3 33 15 2
Embodiment 4 32 15 3
Comparative example 1 31 14 5
It is demonstrated experimentally that the lung moistening of the present invention is eliminated the phlegm, health tea can be effectively improved cough, expectoration symptom. Comparing embodiment 1 and embodiment 2-4, embodiment 1 (ethanol, 1-propanol, 1,3-PD are composite) therapeutic effect is substantially better than embodiment 2-4 (in ethanol, 1-propanol, 1,3-PD, arbitrarily the two is composite).
Test case 2
To step (1) in embodiment 1-4 and comparative example 1 prepare Ramulus et Folium Mussaendae Pubescentis extract powder, Ampelopsis grossedentata extract powder, Rhizoma Polygonati extract powder, with reference to GB " tea polyphenols mensurations " mesotartaric acid ferrous iron method mensuration. With reference to GB " tea caffeine mensuration " medium ultraviolet spectrophotometry. Anthrone-sulfuricacid method measures tea polysaccharide. Phend-sulphuric acid measures polygonatum polysaccharide content. Concrete outcome is in Table 2-4.
Table 2: Ramulus et Folium Mussaendae Pubescentis extract powder main component extraction ratio unit: %
Tea polyphenols Caffeine Tea polysaccharide
Embodiment 1 21.96 4.04 1.66
Embodiment 2 20.29 3.31 1.33
Embodiment 3 20.31 3.28 1.30
Embodiment 4 20.32 3.29 1.31
Comparative example 1 18.24 2.97 1.05
Table 3: Ampelopsis grossedentata extract powder main component extraction ratio unit: %
Table 4: polygonatum polysaccharide leaching rate unit: %
Polygonatum polysaccharide
Embodiment 1 17.3
Embodiment 2 15.0
Embodiment 3 15.5
Embodiment 4 15.2
Comparative example 1 13.9
Comparing embodiment 1 and embodiment 2-4, embodiment 1 (ethanol, 1-propanol, 1,3-PD are composite) main component extraction ratio is apparently higher than embodiment 2-4 (in ethanol, 1-propanol, 1,3-PD, arbitrarily the two is composite).

Claims (4)

1. a lung moistening is eliminated the phlegm the preparation method of health tea, it is characterised in that comprise the following steps:
(1) Ramulus et Folium Mussaendae Pubescentis or Ampelopsis grossedentata or Rhizoma Polygonati are pulverized, carry out supercritical CO respectively2Fluid extraction, adds entrainer in extraction process, obtain Ramulus et Folium Mussaendae Pubescentis extract or Ampelopsis grossedentata extract or Rhizoma Polygonati extracting solution, decompression distillation, lyophilization, obtains Ramulus et Folium Mussaendae Pubescentis and extracts powder or Ampelopsis grossedentata extraction powder or Rhizoma Polygonati extract powder;
(2) by Ramulus et Folium Mussaendae Pubescentis extract powder 8-12 part, Ampelopsis grossedentata extract powder 38-42 part and Rhizoma Polygonati extract powder 48-52 part mix homogeneously.
2. lung moistening as claimed in claim 1 is eliminated the phlegm the preparation method of health tea, it is characterized in that, in described step (1) entrainer by ethanol, 1-propanol, 1, ammediol forms, described ethanol, 1-propanol, 1,3-PD mass ratio be (1-3): (1-3): (1-3).
3. lung moistening as claimed in claim 1 or 2 is eliminated the phlegm the preparation method of health tea, it is characterised in that supercritical CO in described step (1)2Fluid extraction pressure 25-35Mpa, extraction temperature is 40-60 DEG C, and extraction time is 2-4h, CO2Flow be 10-20kg/h, the flow of entrainer is 0.5-1.5kg/h.
4. a lung moistening is eliminated the phlegm health tea, it is characterised in that adopt method according to any one of claim 1-3 to be prepared from.
CN201610035327.1A 2016-01-19 2016-01-19 Lung moistening and phlegm eliminating healthcare tea and preparation method thereof Withdrawn CN105660924A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108686060A (en) * 2018-07-26 2018-10-23 广西中绿医药科技有限公司 A kind of lymph cancer healing liquid and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108686060A (en) * 2018-07-26 2018-10-23 广西中绿医药科技有限公司 A kind of lymph cancer healing liquid and preparation method thereof

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Application publication date: 20160615