CN105638682A - Bactericidal composition comprising kasugamycin and bismerthiazol - Google Patents
Bactericidal composition comprising kasugamycin and bismerthiazol Download PDFInfo
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- CN105638682A CN105638682A CN201410631833.8A CN201410631833A CN105638682A CN 105638682 A CN105638682 A CN 105638682A CN 201410631833 A CN201410631833 A CN 201410631833A CN 105638682 A CN105638682 A CN 105638682A
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Abstract
The invention relates to a bactericidal composition comprises kasugamycin and bismerthiazol. The weight ratio of kasugamycin to bismerthiazol ranges between 2 to 5 and 20 to 23. The bactericidal composition is water dispersible granules, wettable powder or emulsion in water. Compared to common bactericidal compositions, the bactericidal composition comprising kasugamycin and bismerthiazol has outstanding control efficiency to rice blast, which is proved by field trial.
Description
Technical field
The present invention relates to pesticide sterilizing composite, particularly relate to a kind of bactericidal composition containing kasugarnycin and MBAMT.
Background technology
MBAMT N.N '-methylene-bis-(2-amino-5-sulfenyl-1,3,4-thiadiazoles) is the interior suction series bactericidal agent that China independently formulates. It is mainly used to prevent and treat bacterial diseases of plants, bacterial blight of rice and bacterial stripe, citrus ulcer are had good prevention effect. Systemic fungicide. There is good treatment and prevention effect. Bacteriosis is had good preventive effect. Anti-rain drop erosion.
Kasugarnycin (Kasugamycin) is also known as kasugarnycin, kasumin, chemical name 5-amino-2-methyl-6-(2, 3, 4, 5, 6-carbonyl cyclohexyl oxo) pyrans-3-base amino-a-IMDA, belong to antibiotics antibacterial, may interfere with the esterase system of amino acid metabolism, thus affecting the synthesis of protein, suppress hyphal elongation and cause cell granulations, there is stronger systemic activity, its therapeutic effect is more notable, it it is preventing and treating vegetable, the various bacteria of the crops such as melon and fruit and the favourable agents of fungal disease, and the melon leaf color after dispenser can be made dark green and extend harvest time.
Above two medicament is owing to being used alone for a long time, it is easily caused the drug-fast generation of pathogenic bacteria, drug effect is caused to be decreased obviously, thus causing that dosage rises significantly, spray cycle time, and result of use is poor, add cost, the use of a large amount of pesticide, make pathogenic bacteria resistance more serious, also environment is affected, the drug residue of agricultural product also increases, have influence on the mankind, the health of animal etc. and normal existence, kasugarnycin and MBAMT are carried out the composite synergism using preventing and treating corps diseases can give full play to microorganism and chemical agent, reach to have complementary advantages, expanding prevention scope, reduce chemical agent dosage, reduce drug cost, while improving prevention effect, improve ecological environment, decrease chemical agent residual quantity in Oryza sativa L..
Rice blast is the Major Diseases of Oryza sativa L., and seedling morbidity is often crispaturaed withered; Also can be withered or have a strong impact on growth promoter when tillering stage, leaf spot lesion was many; The morbidity of rice strain stipes subjects to windbreak; Fringe neck and branch stalk morbidity then cause dead ears or half dead ears, lose very big. The measure controlling at present rice blast depends on spraying fungicide, but Pyricularia oryzae develops immunity to drugs to producing upper most of antibacterial for preventing and treating rice blast, be wherein no lack of Isoprothiolane, tricyclazole etc. efficiently, the medicament of lasting period length. Therefore, pesticide new variety, the screening of novel form and the development of new complex preparation or introducing are the important measures reducing fungicide resistance risk, the service life extending them and resistance management.Select simultaneously the biological pesticide of high-efficiency low-toxicity, different pesticide rational mixture mixed and develop new high-efficiency preparation preventing and treating rice blast there is great economic benefit, social benefit.
Summary of the invention
It is an object of the invention to provide a kind of bactericidal composition being effective ingredient with kasugarnycin and MBAMT, for realizing this purpose, the invention provides techniques below scheme.
A kind of bactericidal composition containing kasugarnycin and MBAMT, its effective ingredient is kasugarnycin and MBAMT, and wherein kasugarnycin and MBAMT are 2��5: 20��23 by weight.
Can use conventional methods is water dispersible granules, wettable powder or aqueous emulsion by the preparation of described bactericidal composition.
When the preparation of the described bactericidal composition containing kasugarnycin and MBAMT is for water dispersible granules, by weight, formula is as follows: kasugarnycin 2��5 parts, MBAMT 20��23 parts, auxiliary agent 1��5 part, 1��10 part of carrier, binding agent 0.5��3 part, then mends to 100 parts with Kaolin.
The described water dispersible granules containing kasugarnycin and MBAMT, wherein said auxiliary agent at least one in sodium lauryl sulphate, Polyethylene Glycol; Described carrier selected from sodium lignin sulfonate, sulfonic acid polyformaldehyde condensation substance, pull open in powder one or more; One or more in sodium carboxymethyl cellulose, ammonium sulfate, lauric acid polyoxyethylene ether of described binding agent.
The described water dispersible granules containing kasugarnycin and MBAMT, preferably formula is as follows by weight: kasugarnycin 2��5 parts, MBAMT 20��23 parts, sodium lauryl sulphate 1��2 part, Polyethylene Glycol 1��3 part, lignosulfonates 1��3 part, sulfonic acid polyformaldehyde condensation substance (NNO) 1��3 part, sodium carboxymethyl cellulose 0.5��1 part, 0.5��1 part of ammonium sulfate, polyoxyethylene lauryl ether 0.5��1 part, then mends to 100 parts with Kaolin.
As a kind of preferred forms of the described water dispersible granules containing kasugarnycin and MBAMT, formula is as follows:
Kasugarnycin 5g, MBAMT 20g, sodium lauryl sulphate 2g, Polyethylene Glycol 1g, lignosulfonates 2g, sulfonic acid polyformaldehyde condensation substance (NNO) 2g, sodium carboxymethyl cellulose 1g, ammonium sulfate 0.5g, polyoxyethylene lauryl ether 1g, mend to 100g with Kaolin.
When the preparation of the described bactericidal composition containing kasugarnycin and MBAMT is for wettable powder, by weight, including following formula: kasugarnycin 2��5 parts, MBAMT 20��23 parts, auxiliary agent 1��10 part, 1��10 part of carrier, binding agent 0��5 part, then mend to 100 parts with Linesless charcoal black earth.
The described wettable powder containing kasugarnycin and MBAMT, wherein, one or more in sodium lauryl sulphate, Polyethylene Glycol of described auxiliary agent; Described carrier selected from sodium lignin sulfonate, the poly-first condensation substance of sulfonic acid, pull open in powder one or more; One or more in sodium carboxymethyl cellulose, ammonium sulfate, lauric acid polyoxyethylene ether of described binding agent.
The described wettable powder containing kasugarnycin and MBAMT, preferably formula is as follows by weight: kasugarnycin 2��5 parts, MBAMT 20��23 parts, sodium lauryl sulphate 1��1.5 part, lignosulfonates 4��5 parts, pull open 3��5 parts of powder (BX), then mends to 100 parts with Linesless charcoal black earth.
As a kind of preferred forms of the described wettable powder containing kasugarnycin and MBAMT, formula is as follows:
Kasugarnycin 5g, MBAMT 20g, sodium lauryl sulphate 1g, sodium lignin sulfonate 4g, pull open powder (BX) 4g, supply 100g with Linesless charcoal black earth.
When the preparation of the described bactericidal composition containing kasugarnycin and MBAMT is for aqueous emulsion, by weight, including following formula: kasugarnycin 2��5 parts, MBAMT 20��23 parts, solvent 10��30 parts, emulsifying agent 1��5 part, antifreeze 2��10 parts, thickening agent 0.1��2 part, defoamer 0.5��1 part.
The described aqueous emulsion containing kasugarnycin and MBAMT, wherein, described solvent at least one in N-Methyl pyrrolidone, phenethyl fluosite polyoxyethyl ether; Described emulsifying agent at least one in alkyl benzene calcium sulfonate, lauric acid polyoxyethylene ether; Described antifreeze at least one in sodium xylene sulfonate, Polyethylene Glycol; Described thickening agent at least one in xanthan gum, aluminium-magnesium silicate; Described defoamer at least one in organosilicon oils chemical substance.
The preferably described aqueous emulsion containing kasugarnycin and MBAMT, formula is as follows by weight: kasugarnycin 2��5 parts, MBAMT 20��23 parts, N-Methyl pyrrolidone 5��6 parts, phenethyl phenol mela mine-formaldehyde resin polyoxyethyl ether 5��7 parts, alkyl benzene calcium sulfonate 1��3 part, Polyethylene Glycol 2��5 parts, xanthan gum 0.1��1 part, aluminium-magnesium silicate 0.5��1 part, and polydimethylsiloxane 0.5��1 part, then use use water are mended to 100 parts.
As a kind of preferred forms of the aqueous emulsion containing kasugarnycin and MBAMT, formula is as follows:
Kasugarnycin 5g, MBAMT 20g, N-Methyl pyrrolidone 5g, phenethyl phenol mela mine-formaldehyde resin polyoxyethyl ether 5g, alkyl benzene calcium sulfonate 3g, Polyethylene Glycol 2g, xanthan gum 0.1g, aluminium-magnesium silicate 0.5g, polydimethylsiloxane 0.5g, mend to 100g with water.
Search pertinent literature, according to conventional field efficacy and index, the content proportioning of selected pesticides, owing to kasugarnycin mainly prevents and treats rice blast, therefore test in land for growing field crops, the prevention effect of statistics rice blast. Experiment place: the rural area that Jilin Province's Yanji is divided into. Experimental period: 2012��2014. The bactericidal composition of the present invention is proved by field test, compared with conventional sterilization compositions, rice blast has significant prevention effect.
Detailed description of the invention
Following example are used for illustrating the present invention, but are not limited to the scope of the present invention.
Embodiment 1 water dispersible granules
The present invention is containing the water dispersible granules of 25% kasugarnycin MBAMT effective ingredient, and formula is as follows:
Kasugarnycin 5g, MBAMT 20g, sodium lauryl sulphate 2g, Polyethylene Glycol 1g, lignosulfonates 2g, sulfonic acid polyformaldehyde condensation substance (NNO) 2g, sodium carboxymethyl cellulose 1g, ammonium sulfate 0.5g, polyoxyethylene lauryl ether 1g, mend to 100g with Kaolin.
By effective ingredient kasugarnycin and MBAMT, auxiliary agent sodium lauryl sulphate and Polyethylene Glycol, carrier sulfonic acid polyformaldehyde condensation substance with pull open powder mixing, after stirring, it is grinding to obtain female powder. Mother's powder is mixed homogeneously with binding agent sodium carboxymethyl cellulose and polyoxyethylene lauryl ether, then pelletize, dries, sieve, namely prepare 25% kasugarnycin MBAMT water dispersible granules.
Embodiment 2
The present embodiment differs only in embodiment 1, and formula is as follows:
Kasugarnycin 2g, MBAMT 23g, sodium lauryl sulphate 1g, Polyethylene Glycol 2g, lignosulfonates 1g, sulfonic acid polyformaldehyde condensation substance (NNO) 1g, sodium carboxymethyl cellulose 0.5g, ammonium sulfate 1g, polyoxyethylene lauryl ether 0.5g, Kaolin is mended to 100g, prepares 25% kasugarnycin MBAMT water dispersible granules.
Embodiment 3
The present embodiment differs only in embodiment 1, and formula is as follows:
Kasugarnycin 4g, MBAMT 22g, sodium lauryl sulphate 1.5g, Polyethylene Glycol 3g, lignosulfonates 3g, sulfonic acid polyformaldehyde condensation substance (NNO) 3g, sodium carboxymethyl cellulose 0.8g, ammonium sulfate 0.7g, polyoxyethylene lauryl ether 0.6g, then mend to 100g with Kaolin.
Embodiment 4
The present embodiment differs only in embodiment 1, and formula is as follows:
Kasugarnycin 3g, MBAMT 21g, Polyethylene Glycol 1g, pulling open powder 1g, lauric acid polyoxyethylene ether 0.5g, then Kaolin is mended to 100g.
Embodiment 5
The present embodiment differs only in embodiment 1, and formula is as follows:
Kasugarnycin 4g, MBAMT 23g, Polyethylene Glycol 5g, sulfonic acid polyformaldehyde condensation substance (NNO) 3g, pulling open powder 7g, ammonium sulfate 3g, then Kaolin is mended to 100g.
Embodiment 6 wettable powder
The present invention is containing the wettable powder of 25% kasugarnycin MBAMT effective ingredient, and formula is as follows:
Kasugarnycin 5g, MBAMT 20g, sodium lauryl sulphate 1g, sodium lignin sulfonate 4g, pull open powder (BX) 4g, supply 100g with Linesless charcoal black earth.
By effective ingredient kasugarnycin and MBAMT, auxiliary agent sodium lauryl sulphate and carrier sodium lignin sulfonate, pull open powder mixing, after comminution by gas stream, mix and blend 30 minutes in cone-type mixer, can be prepared by 25% kasugarnycin MBAMT wettable powder.
Embodiment 7
The present embodiment differs only in embodiment 6, and formula is as follows:
Kasugarnycin 2g, MBAMT 23g, sodium lauryl sulphate 1.5g, sodium lignin sulfonate 5g, pull open powder (BX) 3g, supply 100g with white carbon.
Embodiment 8
The present embodiment differs only in embodiment 6, and formula is as follows:
Kasugarnycin 3g, MBAMT 21g, sodium lauryl sulphate 1.2g, sodium lignin sulfonate 4.5g, pull open powder (BX) 5g, supply 100g with white carbon.
Embodiment 9
The present embodiment differs only in embodiment 6, and formula is as follows:
Kasugarnycin 4g, MBAMT 22g, Polyethylene Glycol 4g, pull open powder 6g, the poly-first condensation substance 5g of sulfonic acid, pull open powder 5g, lauric acid polyoxyethylene ether 5g, then mend to 100g with Linesless charcoal black earth.
Embodiment 10
The present embodiment differs only in embodiment 6, and formula is as follows:
Kasugarnycin 4g, MBAMT 22g, Polyethylene Glycol 4g, sodium lignin sulfonate 1g, sulfonic acid gather first condensation substance 1g, sodium carboxymethyl cellulose 1g, ammonium sulfate 1g, lauric acid polyoxyethylene ether 1g, then mend to 100g with Linesless charcoal black earth.
Embodiment 11 aqueous emulsion
The present invention is containing the aqueous emulsion of 25% kasugarnycin MBAMT effective ingredient, and formula is as follows:
Kasugarnycin 5g, MBAMT 20g, N-Methyl pyrrolidone 5g, phenethyl phenol mela mine-formaldehyde resin polyoxyethyl ether 5g, alkyl benzene calcium sulfonate 3g, Polyethylene Glycol 2g, xanthan gum 0.1g, aluminium-magnesium silicate 0.5g, polydimethylsiloxane 0.5g, mend to 100g with water.
Effective ingredient kasugarnycin and MBAMT, solvent N-methyl pyrilidone, phenethyl fluosite polyoxyethyl ether, emulsifying agent alkyl benzene calcium sulfonate are added together, are dissolved into homogeneous oil phase; Water, antifreeze sodium xylene sulfonate, thickening agent xanthan gum, aluminium-magnesium silicate, defoamer polydimethylsiloxane are mixed, becomes homogeneous aqueous phase. Under high velocity agitation, aqueous phase is added oil phase, can be prepared by 25% kasugarnycin MBAMT aqueous emulsion.
Embodiment 12
The present embodiment differs only in embodiment 11, and formula is as follows:
Kasugarnycin 2g, MBAMT 23g, N-Methyl pyrrolidone 6g, phenethyl phenol mela mine-formaldehyde resin polyoxyethyl ether 6g, alkyl benzene calcium sulfonate 1g, Polyethylene Glycol 5g, xanthan gum 1g, aluminium-magnesium silicate 1g, polydimethylsiloxane 1g, mend to 100g with water.
Embodiment 13
The present embodiment differs only in embodiment 11, and formula is as follows:
Kasugarnycin 4g, MBAMT 22g, N-Methyl pyrrolidone 5.5g, phenethyl phenol mela mine-formaldehyde resin polyoxyethyl ether 7g, alkyl benzene calcium sulfonate 2g, Polyethylene Glycol 10g, xanthan gum 0.15g, aluminium-magnesium silicate 1.0g, polydimethylsiloxane 0.6g, then mend to 100g with water.
Embodiment 14
The present embodiment differs only in embodiment 11, and formula is as follows:
Kasugarnycin 3g, MBAMT 21g, N-Methyl pyrrolidone 16g, phenethyl phenol mela mine-formaldehyde resin polyoxyethyl ether 14g, alkyl benzene calcium sulfonate 1g, sodium xylene sulfonate 2g, Polyethylene Glycol 4g, xanthan gum 0.1g, polydimethylsiloxane 0.8g.
Contrast experiment 1 measures the drug effect to rice blast of the bactericidal composition containing different activities composition
Wherein, reference substance 1 is water dispersible granules, and it is compared with embodiment 1, and differing only in its active component be content is 25% MBAMT.
Reference substance 2 is wettable powder, and it is compared with embodiment 6, and differing only in its active component is 25% kasugarnycin.
Reference substance 3 is aqueous emulsion, and it is compared with embodiment 11, and differing only in its active component is 25% carbendazim.
Reference substance 4 is 20% kasugarnycin cyazofamid water dispersible granules, its component prescription quality content is: kasugarnycin 1%, cyazofamid 19%, sodium lignin sulfonate 6%, PO-EO block polyether 4%, sodium lauryl sulphate 3%, ammonium sulfate 5%, precipitated calcium carbonate surplus.
Reference substance 5 is 70% Flutriafol kasugarnycin wettable powder, its component prescription quality content is: Flutriafol 62%, kasugarnycin 8%, polycarboxylate 5%, sodium lauryl sulphate 3%, white carbon 8%, Kaolin supply 100% mixing through comminution by gas stream, prepares 70% Flutriafol kasugarnycin wettable powder.
Reference substance 6 is wettable powder, and its component prescription quality content is: Zhongshengmycin 6%, MBAMT 11%, copper acetate 18%, sodium lauryl sulphate 3%, Flutriafol 62%.
Reference substance 7 is water dispersible granules, and it differs only in embodiment 1: active ingredient is kasugarnycin 12g, MBAMT 13g.
Experimental technique: divide into field, one piece of rural area on August 20th, 2012 at Jilin Province's Yanji and the Oryza sativa L. suffering from rice blast is sprayed, every mu is sprayed 28g, and after sprinkling, prevention effect is in Table 1:
Table 1
| 10 days preventive effects (%) after medicine | 20 days preventive effects (%) after medicine | |
| Embodiment 1 | 85.7 | 89.9 |
| Embodiment 5 | 83.5 | 87.6 |
| Embodiment 6 | 84.9 | 90.1 |
| Embodiment 10 | 83.8 | 88.5 |
| Embodiment 11 | 85.2 | 89.6 |
| Embodiment 14 | 84.3 | 86.8 |
| Reference substance 1 | 76.1 | 78.2 |
| Reference substance 2 | 75.2 | 79.1 |
| Reference substance 3 | 73.5 | 77.4 |
| Reference substance 4 | 80.6 | 82.9 |
| Reference substance 5 | 79.8 | 81.7 |
| Reference substance 6 | 73.2 | 76.1 |
| Reference substance 7 | 70.5 | 75.5 |
As shown in Table 1, rice blast preventive effect is better than the reference substance medicament containing other activity parts by the bactericidal composition that the present invention contains kasugarnycin and MBAMT; And bactericidal composition of the present invention containing kasugarnycin 2��5%, MBAMT 20��23% is the most notable to rice blast prevention effect, and the bactericidal effect of relatively low consumption is good, is better than the bactericidal effect of the high bactericidal composition of content, can reduce drug cost.
The bactericidal composition of the present invention is shown by field test results: rice blast has significant prevention effect. It is compared with conventional sterilization compositions, has the advantage that 1 has obvious potentiation with single dose phase comparison rice blast, is remarkably improved prevention effect; 2, reduce dosage, reduce the residual of environmental pollution and agricultural product; 3, the rice blast Drug resistance to single bactericidal composition can be delayed; 4, having prophylactic treatment effect, the lasting period is long, compared with single medicament, it is possible to decrease cost.
Although, above use generality explanation, detailed description of the invention and test, the present invention is described in detail, but on basis of the present invention, it is possible to it is made some modifications or improvements, and this will be apparent to those skilled in the art. Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, belong to the scope of protection of present invention.
Claims (10)
1. the bactericidal composition containing kasugarnycin and MBAMT, it is characterised in that: its effective ingredient is kasugarnycin and MBAMT, and wherein kasugarnycin and MBAMT are 2��5: 20��23 by weight.
2. bactericidal composition according to claim 1, the preparation of described bactericidal composition is water dispersible granules, it is characterized in that: by weight, formula is as follows: kasugarnycin 2��5 parts, MBAMT 20��23 parts, auxiliary agent 1��5 part, 1��10 part of carrier, binding agent 0.5��3 part, then mends to 100 parts with Kaolin.
3. bactericidal composition according to claim 2, it is characterised in that: described auxiliary agent at least one in sodium lauryl sulphate, Polyethylene Glycol; Described carrier selected from sodium lignin sulfonate, sulfonic acid polyformaldehyde condensation substance, pull open in powder one or more; One or more in sodium carboxymethyl cellulose, ammonium sulfate, lauric acid polyoxyethylene ether of described binding agent.
4. bactericidal composition according to claim 3, it is characterized in that: by weight, formula is as follows: kasugarnycin 2��5 parts, MBAMT 20��23 parts, sodium lauryl sulphate 1��2 part, Polyethylene Glycol 1��3 part, lignosulfonates 1��3 part, sulfonic acid polyformaldehyde condensation substance (NNO) 1��3 part, sodium carboxymethyl cellulose 0.5��1 part, 0.5��1 part of ammonium sulfate, polyoxyethylene lauryl ether 0.5��1 part, then mends to 100 parts with Kaolin.
5. bactericidal composition according to claim 1, the preparation of described bactericidal composition is wettable powder, it is characterized in that: by weight, formula is as follows: kasugarnycin 2��5 parts, MBAMT 20��23 parts, auxiliary agent 1��10 part, 1��10 part of carrier, binding agent 0��5 part, then mends to 100 parts with Linesless charcoal black earth.
6. bactericidal composition according to claim 5, it is characterised in that: one or more in sodium lauryl sulphate, Polyethylene Glycol of described auxiliary agent; Described carrier selected from sodium lignin sulfonate, the poly-first condensation substance of sulfonic acid, pull open in powder one or more; One or more in sodium carboxymethyl cellulose, ammonium sulfate, lauric acid polyoxyethylene ether of described binding agent.
7. bactericidal composition according to claim 6, it is characterized in that: formula is as follows: kasugarnycin 2��5 parts, MBAMT 20��23 parts, sodium lauryl sulphate 1��1.5 part, lignosulfonates 4��5 parts, pull open 3��5 parts of powder (BX), then mend to 100 parts with Linesless charcoal black earth.
8. bactericidal composition according to claim 1, the preparation of described bactericidal composition is aqueous emulsion, it is characterized in that: by weight, including following formula: kasugarnycin 2��5 parts, MBAMT 20��23 parts, solvent 10��30 parts, emulsifying agent 1��5 part, antifreeze 2��10 parts, thickening agent 0.1��2 part, defoamer 0.5��1 part.
9. bactericidal composition according to claim 8, it is characterised in that: described solvent at least one in N-Methyl pyrrolidone, phenethyl fluosite polyoxyethyl ether; Described emulsifying agent at least one in alkyl benzene calcium sulfonate, lauric acid polyoxyethylene ether;Described antifreeze at least one in sodium xylene sulfonate, Polyethylene Glycol; Described thickening agent at least one in xanthan gum, aluminium-magnesium silicate; Described defoamer at least one in organosilicon oils chemical substance.
10. bactericidal composition according to claim 9, it is characterized in that: by weight, formula is as follows: kasugarnycin 2��5 parts, MBAMT 20��23 parts, N-Methyl pyrrolidone 5��6 parts, phenethyl phenol mela mine-formaldehyde resin polyoxyethyl ether 5��7 parts, alkyl benzene calcium sulfonate 1��3 part, Polyethylene Glycol 2��5 parts, xanthan gum 0.1��1 part, aluminium-magnesium silicate 0.5��1 part, polydimethylsiloxane 0.5��1 part, then mends to 100 parts with water.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101176449A (en) * | 2007-10-26 | 2008-05-14 | 张少武 | Agricultural chemical composition made mainly of leaf dried azoles and use thereof |
| WO2012172061A1 (en) * | 2011-06-17 | 2012-12-20 | Basf Se | Compositions comprising fungicidal substituted dithiines and further actives |
| CN102986487A (en) * | 2012-12-07 | 2013-03-27 | 山东禾宜生物科技有限公司 | Method for preventing and treating watermelon blotch |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101176449A (en) * | 2007-10-26 | 2008-05-14 | 张少武 | Agricultural chemical composition made mainly of leaf dried azoles and use thereof |
| WO2012172061A1 (en) * | 2011-06-17 | 2012-12-20 | Basf Se | Compositions comprising fungicidal substituted dithiines and further actives |
| CN102986487A (en) * | 2012-12-07 | 2013-03-27 | 山东禾宜生物科技有限公司 | Method for preventing and treating watermelon blotch |
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