CN1056057A - The preparation method of " Linglan " concentrated liquid - Google Patents
The preparation method of " Linglan " concentrated liquid Download PDFInfo
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- CN1056057A CN1056057A CN 91103550 CN91103550A CN1056057A CN 1056057 A CN1056057 A CN 1056057A CN 91103550 CN91103550 CN 91103550 CN 91103550 A CN91103550 A CN 91103550A CN 1056057 A CN1056057 A CN 1056057A
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Abstract
The preparation method of " Linglan " concentrated liquid is a raw material with the edible fungi Ganoderma of plant Herb Gynostemmae Pentaphylli, passes through effective component extracting ginsenoside, Herb Gynostemmae Pentaphylli total glycosides and organic germanium, ganoderan respectively, again with extracting solution respectively through edulcoration purification, mix after concentrating.Can be used as the stock solution of making health-care beverage series or be pressed into tablet etc.Raw material of the present invention is extensive, and technology is simple, need not special installation, product purity height, cost be low, contain the main effective ingredient of abundant Radix Ginseng, two kinds of raw materials produce collaborative health-care effects, have blood fat reducing, blood circulation promoting is unimpeded, resisting fatigue and health care old and feeble, anti-cancer and cancer-preventing.
Description
The present invention relates to be mainly used in the preparation method of the stock solution of preparing non-alcoholic beverage, particularly a kind of is the preparation method of the " Linglan " concentrated liquid of raw material with wild resource Herb Gynostemmae Pentaphylli and edible fungi Ganoderma.
Herb Gynostemmae Pentaphylli is the Cucurbitaceae herbaceos perennial, and record such as China Ming Dynasty herbal for Relief of Famines can be edible.The contained Saponin of Herb Gynostemmae Pentaphylli kind more than 80, basic chemical structure is a dammarane type, can be considered the isomer of protopanoxadiol, triol, wherein gypenoside 3,4,8,12 respectively with ginsenoside R
B1, R
B3, R
d, F
2Structure is identical.Total saponin content of gynostemma pentaphyllum is four times of Radix Ginseng.Have effects such as blood fat reducing, resisting fatigue, defying age, growth promotion, anti-cancer and cancer-preventing.Ganoderma is the long traditional tonic medicine of a kind of applicating history, also is a kind of edible fungi that generally uses.The most precious composition of recent studies proof Ganoderma is an organic germanium.Organic germanium also is the main effective ingredient of Radix Ginseng, and Ganoderma contains organic germanium and is higher than Radix Ginseng 3-6 doubly.Organic germanium can make blood circulation unimpeded, increases erythrocyte band ability to take oxygen, and can enhance metabolism, can slow down aging.
It is various in style that health beverage was gone on the market in recent years, respectively execute extraordinary splendor, but be that base stock is made with Radix Ginseng, royal jelly, pollen mostly, often take improper or overdose can cause toxic and side effects that easily causing property drought is ripe to take the health-care agent of ginseng product as the child though have certain function of health care.And the above-mentioned raw materials resource-constrained, processed complex costs an arm and a leg, and can not satisfy the demand that people prevented and cured diseases, do not have disease and health fully.Though China and foreign countries have gynostemma health-care drink at present, it is single that health care still seems, do not reach the traditional Chinese medical science and require whole purpose to human body adjustment treatment.
The objective of the invention is to fully develop the wild resource Herb Gynostemmae Pentaphylli and the Ganoderma of China's abundant, it is remarkable to prepare a kind of effect, have no side effect, cheap, preparation technology simply is mainly used in the preparation health-care beverage series or is pressed into the preparation method of the " Linglan " concentrated liquid of tablet, and everybody slogan of enjoying health care was made contributions for realize that World Health Organization (WHO) proposes 2000.
The objective of the invention is to reach by following measure:
A kind of preparation method of " Linglan " concentrated liquid, adopting dry material proportion is that 1.0: 0.4～1.5 wild plant Herb Gynostemmae Pentaphylli and edible fungi Ganoderma are raw material, respectively through extracting effective ingredient organic germanium, the ganoderan in effective ingredient ginsenoside, Herb Gynostemmae Pentaphylli total glycosides and the Ganoderma in the Herb Gynostemmae Pentaphylli, again with extracting solution respectively through edulcoration purification, be condensed into to be mixed with after the underflow and form.
Herb Gynostemmae Pentaphylli underflow and Ganoderma underflow that above-mentioned preparation method is prepared are mixed, and add the flavouring agent of certain proportioning, can be made into health-care beverage series such as oral liquid, general beverage, electuary by the conventional production process of beverage, also can be pressed into tablet etc.
Purpose of the present invention can also reach by following measure:
The preparation method of Herb Gynostemmae Pentaphylli underflow can adopt Herb Gynostemmae Pentaphylli raw material cleaning remove impurity, pulverizing back water logging bubble are extracted effective ingredient ginsenoside and Herb Gynostemmae Pentaphylli total glycosides, remove by filter cellulose and other solid content rear filtrate employing ion exchange resin edulcoration purification, inject the impurity of the lixiviating solution filtrate in the ion exchange resin column earlier with water wash, then use alcoholic solution eluting ginsenoside and Herb Gynostemmae Pentaphylli total glycosides, the eluate heating that at last it is contained eluted effective ingredient ginsenoside and Herb Gynostemmae Pentaphylli total glycosides is concentrated into no ethanol flavor and makes underflow.It is to remove impurity such as dust that raw material cleans purpose with clear water, in order to avoid influence filter operation.The resin that the edulcoration purification resin column is adopted is a macroporous resin.Inject the impurity of the lixiviating solution filtrate in the resin column earlier with clear water drip washing, reuse alcoholic solution eluting effective ingredient can reduce the ethanol consumption like this, and effective component yield can improve about 15%.The eluate heating that at last it is contained eluted effective ingredient is concentrated into no ethanol flavor.
When lixiviate ginsenoside and Herb Gynostemmae Pentaphylli total glycosides, take first normal-temperature water to soak to extract to be no less than 3 hours reheat flooding effective ingredient 2-3 time to the 80-120 ℃ of temperature, lixiviate 1-2 hour at every turn.
During with lixiviating solution filtrate effective ingredient ginsenoside in the alcoholic solution eluting injection resin column and Herb Gynostemmae Pentaphylli total glycosides, should be the edible ethanol of 10-30% with concentration earlier, the back be the edible ethanol eluting of 90-95% with concentration.
The preparation method of Herb Gynostemmae Pentaphylli underflow of the present invention also can adopt soaks Herb Gynostemmae Pentaphylli raw material cleaning remove impurity, the first normal-temperature water in pulverizing back effective component extracting and is no less than 3 hours, reheat lixiviate 2-3 time to the 80-120 ℃ of temperature, each 1-2 hour, lixiviating solution is filtered, the filtrate heating is concentrated into the 1/4-1/10 of original volume, add ethanol again, ethanol content is to precipitate (it is heavy promptly to spill) under the condition of 60-80% in lixiviating solution, so that protein, cellulose etc. form the bulky grain precipitation.Filtering once more filtrate is distilled and is reclaimed ethanol to there not being the ethanol flavor.
The preparation method of Ganoderma underflow of the present invention, can take after Ganoderma raw material cleaning remove impurity, the section, elder generation's normal-temperature water soaks the effective component extracting organic germanium and ganoderan is no less than 3 hours, again in being heated under 60-80 ℃ the temperature conditions lixiviating effective components 3-5 hour, and preferably lixiviate several times.Lixiviating solution is filtered the 1/4-1/10 that rear filtrate heating is concentrated into original volume, add ethanol again, ethanol content is to precipitate (wine is heavy) under the condition of 60-80% in lixiviating solution, filters once more, and filtrate is distilled and reclaimed ethanol to there being the ethanol flavor.
Preparation method of the present invention is simple, need not special installation, and is with short production cycle, the product purity height; Institute's water and edible ethanol safety non-toxic, product do not contain the residual amount of methanol, make human body avoid methanol and poison; The " Linglan " concentrated liquid that this preparation method obtained had both contained the abundant main effective ingredient ginsenoside of Radix Ginseng of Herb Gynostemmae Pentaphylli and the gypenoside of similar constituent of ginseng, contain the ganoderan in the Ganoderma and the main effective ingredient organic germanium of Radix Ginseng again, and has the main health care of similar Radix Ginseng respectively, they are united two into one, remedy each other, produce collaborative health-care effect, its effect significantly is better than total effect that two kinds of raw materials separately use, and makes it not to be that Radix Ginseng but surpasses Radix Ginseng.The total saponin content of gynostemma pentaphyllum of its " Linglan " concentrated liquid is 30-50% after measured, and organic germanium content is 0.5-1%, but also contains 18 seed amino acids, vitamin, trace element.Thereby the health-care beverage series of preparing with " Linglan " concentrated liquid has stronger plurality of health care functions, energy blood fat reducing, resisting fatigue, defying age, growth promotion, anti-cancer and cancer-preventing etc.Herb Gynostemmae Pentaphylli and Ganoderma all belong to wild plant, and resource is extremely abundant, thereby with low cost, and the present invention has opened up wide prospect for the utilization of wild resource.
Accompanying drawing is a process flow diagram of the present invention.
Describe the present invention in detail below in conjunction with embodiment.
Embodiment one.
Get Herb Gynostemmae Pentaphylli Radix Glycyrrhizae 100Kg, with impurity such as flushing with clean water dust, be cut into the long section of 1cm with the marking knife machine, soaked 10 hours, and added water 800Kg again, with being steam heated to 120 ℃ of effective component extracting ginsenosides and Herb Gynostemmae Pentaphylli total glycosides 2 hours, filter, the gained filtering residue adds water 500Kg again and extracted 1 hour with being steam heated to same temperature, and room temperature all stirs when heat soaking extracts with adding, and refilters.Filter method is taked to filter with multilamellar gauze (or medical Cotton Gossypii) in filter, and the ion exchange resin column that filtrate injection is equipped with macroporous resin carries out edulcoration purification.Injecting the impurity of the lixiviating solution filtrate in the ion exchange resin column earlier with water wash, is edible ethanol eluting effective ingredient ginsenoside and the Herb Gynostemmae Pentaphylli total glycosides of 10-30% then with concentration, is 90-95% edible ethanol eluting with concentration at last.Eluent heating concentrate and recovered alcohol to alcohol-free distinguish the flavor of the Herb Gynostemmae Pentaphylli underflow.
Other gets Ganoderma siccative 140Kg, removes impurity with flushing with clean water, and 80 ℃ of hot water lixiviates of reuse 3 hours, multilamellar filtered through gauze were soaked 8 hours in section in water at normal temperature.Same 80 ℃ of lixiviates for the second time 2 hours are filtered.Merging filtrate, filtrate Steam Heating in concentrator is concentrated into 1/10 of original volume, adds edible ethanol, and edible alcohol content is to staticly settle 48 hours under 75% the cryogenic conditions in lixiviating solution, supernatant liquid filtering, filtrate carry out recovery of alcohol distillation to alcohol-free distinguish the flavor of the Ganoderma underflow.
Above-mentioned Herb Gynostemmae Pentaphylli underflow and Ganoderma underflow are mixed, promptly get " Linglan " concentrated liquid.
Embodiment two.
Get Herb Gynostemmae Pentaphylli siccative 100Kg, Ganoderma siccative 50Kg, preparation method is same as embodiment one substantially, when dissimilarity is to prepare the Herb Gynostemmae Pentaphylli underflow, temperature when adding the heat soaking effective component extracting is 84 ℃, spent ion exchange resin edulcoration purification not after the lixiviate, and lixiviating solution is filtered, filtrate is heated to and is concentrated into 1/4 of original volume under 100 ℃ of conditions, add ethanol again, ethanol content is to precipitate under 60% the condition in lixiviating solution, filters once more, and filtrate is distilled and reclaimed ethanol to there being the ethanol flavor.
Soak down in 65 ℃ of heating conditions Ganoderma raw material section back, and lixiviating solution filters rear filtrate and is concentrated into 1/4 of original volume, adds ethanol ethanol content in lixiviating solution again and be under 60% the condition to precipitate.
Claims (6)
1, a kind of preparation method of " Linglan " concentrated liquid, it is characterized in that adopting dry material proportion is that 10: 0.4～1.5 wild plant Herb Gynostemmae Pentaphylli and edible fungi Ganoderma are raw material, respectively through extracting effective ingredient organic germanium, the ganoderan in effective ingredient ginsenoside, Herb Gynostemmae Pentaphylli total glycosides and the Ganoderma in the Herb Gynostemmae Pentaphylli, again extracting solution is passed through edulcoration purification respectively, be condensed into to be mixed with after the underflow and form.
2, preparation method according to claim 1, the preparation method that it is characterized in that the Herb Gynostemmae Pentaphylli underflow is that the water logging bubble extracted effective ingredient ginsenoside and Herb Gynostemmae Pentaphylli total glycosides after the Herb Gynostemmae Pentaphylli raw material was cleaned remove impurity, pulverizing, filter rear filtrate and adopt the ion exchange resin edulcoration purification, earlier with the lixiviating solution filtrate in the water wash injection ion exchange resin column, the back is concentrated into no ethanol flavor with the above-mentioned effective ingredient of alcoholic solution eluting, the eluate heating that at last it is contained eluted effective ingredient.
3, preparation method according to claim 2, it is characterized in that the flooding ginsenoside, during Herb Gynostemmae Pentaphylli total glycosides, take first normal-temperature water to soak and be no less than 3 hours, reheat water logging bubble effective component extracting 2-3 time to the 80-120 ℃ of temperature, lixiviate 1-2 hour at every turn.
4, according to claim 2 or 3 described preparation methoies, when it is characterized in that, be the edible ethanol of 10-30% with concentration earlier with the effective ingredient in the lixiviating solution filtrate in the alcoholic solution eluting resin column, the back is the edible ethanol eluting of 90-95% with concentration.
5, preparation method according to claim 1, the preparation method that it is characterized in that the Herb Gynostemmae Pentaphylli underflow also can adopt to be cleaned the Herb Gynostemmae Pentaphylli raw material remove impurity, pulverizes the first normal-temperature water in back and soak effective component extracting and be no less than 3 hours, reheat lixiviate 2-3 time to the 80-120 ℃ of temperature, each lixiviate 1-2 hour, lixiviating solution is filtered, the filtrate heating is concentrated into the 1/4-1/10 of original volume, add ethanol again, ethanol content is to precipitate under the condition of 60-80% in lixiviating solution, filter once more, filtrate is distilled and is reclaimed ethanol to there not being the ethanol flavor.
6, preparation method according to claim 1, the preparation method that it is characterized in that the Ganoderma underflow is that the Ganoderma raw material is cleaned remove impurity, after the section, elder generation's normal-temperature water soaks the effective component extracting organic germanium and ganoderan is no less than 3 hours, again in being heated under 60-80 ℃ the temperature conditions lixiviating effective components 3-5 hour, and preferably lixiviate several times, lixiviating solution is filtered the 1/4-1/10 that post-heating is concentrated into original volume, add ethanol again, ethanol content is to precipitate under the condition of 60-80% in lixiviating solution, filter once more, filtrate is distilled and is reclaimed ethanol to there not being the ethanol flavor.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 91103550 CN1056057A (en) | 1991-05-26 | 1991-05-26 | The preparation method of " Linglan " concentrated liquid |
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| CN 91103550 CN1056057A (en) | 1991-05-26 | 1991-05-26 | The preparation method of " Linglan " concentrated liquid |
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| CN1056057A true CN1056057A (en) | 1991-11-13 |
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| CN 91103550 Pending CN1056057A (en) | 1991-05-26 | 1991-05-26 | The preparation method of " Linglan " concentrated liquid |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102613648A (en) * | 2012-03-26 | 2012-08-01 | 张可池 | Preparation method of original ecological bamboo germanium nutrient solution |
| CN101455371B (en) * | 2008-11-27 | 2012-10-03 | 成都润馨堂药业有限公司 | Health-care product containing buckwheat flavone and preparation method thereof |
| CN104172408A (en) * | 2014-07-29 | 2014-12-03 | 北京上尚品生物科技有限公司 | Truffle health oral solution and production process of truffle health oral solution |
| CN104489846A (en) * | 2014-12-02 | 2015-04-08 | 东莞市荷花食品有限公司 | Solid gynostemma pentaphylla beverage and preparation method thereof |
| CN106214633A (en) * | 2016-08-31 | 2016-12-14 | 中国热带农业科学院农产品加工研究所 | A kind of preparation method of ecosystem Ganoderma oral liquid |
| CN108618150A (en) * | 2018-06-12 | 2018-10-09 | 三明市园艺学会 | A kind of liver-protecting fat-dropping Capsules of health productions and its manufacture craft |
| CN114767798A (en) * | 2022-04-14 | 2022-07-22 | 李逢波 | Liver-protecting fat-reducing oral liquid and preparation method thereof |
| CN115192651A (en) * | 2022-05-12 | 2022-10-18 | 海南医学院 | Li medicine composition and Li medicine preparation for hyperlipidemia and preparation method and application thereof |
-
1991
- 1991-05-26 CN CN 91103550 patent/CN1056057A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101455371B (en) * | 2008-11-27 | 2012-10-03 | 成都润馨堂药业有限公司 | Health-care product containing buckwheat flavone and preparation method thereof |
| CN102613648A (en) * | 2012-03-26 | 2012-08-01 | 张可池 | Preparation method of original ecological bamboo germanium nutrient solution |
| CN104172408A (en) * | 2014-07-29 | 2014-12-03 | 北京上尚品生物科技有限公司 | Truffle health oral solution and production process of truffle health oral solution |
| CN104489846A (en) * | 2014-12-02 | 2015-04-08 | 东莞市荷花食品有限公司 | Solid gynostemma pentaphylla beverage and preparation method thereof |
| CN106214633A (en) * | 2016-08-31 | 2016-12-14 | 中国热带农业科学院农产品加工研究所 | A kind of preparation method of ecosystem Ganoderma oral liquid |
| CN108618150A (en) * | 2018-06-12 | 2018-10-09 | 三明市园艺学会 | A kind of liver-protecting fat-dropping Capsules of health productions and its manufacture craft |
| CN114767798A (en) * | 2022-04-14 | 2022-07-22 | 李逢波 | Liver-protecting fat-reducing oral liquid and preparation method thereof |
| CN115192651A (en) * | 2022-05-12 | 2022-10-18 | 海南医学院 | Li medicine composition and Li medicine preparation for hyperlipidemia and preparation method and application thereof |
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