CN105585898B - A kind of UV coating dumb light ink and preparation method thereof - Google Patents
A kind of UV coating dumb light ink and preparation method thereof Download PDFInfo
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- CN105585898B CN105585898B CN201510967678.1A CN201510967678A CN105585898B CN 105585898 B CN105585898 B CN 105585898B CN 201510967678 A CN201510967678 A CN 201510967678A CN 105585898 B CN105585898 B CN 105585898B
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- dumb light
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/101—Inks specially adapted for printing processes involving curing by wave energy or particle radiation, e.g. with UV-curing following the printing
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Paints Or Removers (AREA)
Abstract
A kind of UV coating dumb light ink, it by mass percentage include: UV oligomer: 50-80%, UV monomer: 10-35%, photoinitiator: 3-9%, flatting silica: 10-45%, defoaming agent: 0.2-2% and levelling agent: 0.2-2%, the invention uses special formula and processing technology, so that the ink has many advantages, such as Environmental Safety, low cost manufacturing；Using special preparation process and formula, not only the very good solution uniform proportion of coating, also substantially increases the remaining flow of air；And the ink is after ultraviolet light solidifies, coating is anti-scratch, ethanol-tolerant, can play good protective action to institute's seal coat；The ink solidification production efficiency is higher, and dumb light decorative effect is good, can be widely used for the protective coating field of electronic product components.
Description
Technical field
The invention patent relates to a kind of ink component and its technical field of configuration method, especially a kind of UV is coated with dumb light
Ink and preparation method thereof.
Background technique
With social progress and people material and culture is horizontal steps up, and the use of electronic product is in the daily of people
Increasingly popularized in life, and then pushed the related manufacturing industry of electronic product, electronic product mainly include computer,
Communication and consumption electronic product etc. increasingly develop towards the direction of functional diversities, performance fining and decoration personalization；
In each component surface of electronic product, it is often necessary to printed coating is carried out, decoration or other function are played,
And in an assembling process, each component surface mostly uses the detergent of the equal solvent containing ethyl alcohol to be dusted processing, if not taking anti-
Shield measure, the dedustings detergent such as direct alcohol exposure have frequently resulted in the coating softening of decoration or other function effect, have become
Matter, so that effect should be had by losing it.
Summary of the invention
It is an object of the present invention to provide a kind of UV coating dumb light ink and preparation method thereof, pass through special formula and life
Production. art, so that the ink has many advantages, such as Environmental Safety, low cost manufacturing, and the UV coating dumb light ink warp
After ultraviolet light solidification, coating is anti-scratch, ethanol-tolerant, and good protective action, while the ink solidification can be played to institute's seal coat
High production efficiency, dumb light decorative effect is good, can be widely used for the protective coating field of electronic product components；
In order to solve the above technical problem, the present invention provides a kind of UV coating dumb light ink and preparation method thereof, in which:
A kind of UV coating dumb light ink, a kind of UV coating dumb light ink according to the present invention, component includes: UV oligomeric
Object, UV monomer, photoinitiator, flatting silica, defoaming agent and levelling agent；
As the preferred embodiment that one group of experimental data obtains, a kind of UV coating dumb light ink is by mass percentage
Include: UV oligomer: 50-80%, UV monomer: 10-35%, photoinitiator: 3-9%, flatting silica: 10-45%, defoaming agent:
0.2-2%, levelling agent: 0.2-2%；
As the optimum embodiment that one group of experimental data obtains, a kind of UV coating dumb light ink is by mass percentage
Include: UV oligomer: 55%, UV monomer: 20%, photoinitiator: 7%, flatting silica: 15%, defoaming agent: 2%, levelling agent:
1%；Using the formula of this mass ratio, the ink produced can be made to have the energy conservation and environmental protection scheme of best cost performance
Simultaneously, moreover it is possible to greatly improve the production efficiency of the later period ink solidification, and optimal dumb light decorative effect can be generated；
Illustrate as an example, the monomer be Sartomer CD420, CD551, SR285, SR339, SR395, SR340,
SR238, SR506 or Changxing chemical monomer EM210, EM211, EM212, EM218, EM2191, EM90, EM75, EM70,
EM2202, EM221, EM222, EM223, EM225, EM265, EM235, EM2380, EM231, or German Kening Co., Ltd 4006,
4061, one of 4017,4149,4127 or combination；
Illustrate as an example, the UV oligomer be Sartomer CN1963, CN2101, CN111, CN115,
CN119, CN120, CN121, CN2251, CN2253, CN1045M, or German Corning 3016-20R, 4703,5010,5432,
6019,6623/6893-20R or Changxing chemistry 621A80,6210G, 6215-100,623A80,6148J75,6175-2,
6196,6197,6353, one of 6314C, 6350,6063,6068,8000A or combination；
Illustrate as an example, the photoinitiator be Ciba Specialty Chemicals D-1173,184,754,369,829,
907,2022 or Tianjin Jiu company 1101,1103,1104,1108,1055,1020,1024 or Tianjin English power IHT-
One of PI 151, IHT-PI 1173, IHT-PI 910, IHT-PI MBF, 1000 IHT-PI, IHT-PI 500 or group
It closes；
Illustrate as an example, the flatting silica, which is that Suzhou is comprehensive, grinds KMR-3TA, KMR-3EA, KMR-180A or the U.S.
Step figure Tospearl 240, DSA-6, Tospearl 2000B or the HY-690 of U.S. MSE (Mai Si) company, W. R. Grace & Co
CP4-8991, SY7000, C803, C906, day Bender mountain FM14, Degussa ACEMA TT300, TT600, TS100, OK412,
OK607, OK500, one of OK520 or combination；
Illustrate as an example, the defoaming agent be DOW CORNING DC-51, DC-7, DC-8621, Ant ifoam-A,
Or BYK-066, BYK-67N, BYK-67, BYK-066N or Digao (Tego) 930, Foamax N, 902 or the day of Bi Ke chemistry
Ben Maitu TSA750S or Guangzhou ten thousand are at one of defoaming agent BYC-6800 or combination；
Illustrate as an example, the levelling agent be DOW CORNING DC-3, DC-57 or Digao (Tego) 432,410,
450, one of Glide B1484,440 or Guangzhou Zhuo energy trade RM2020 or combination；
A kind of preparation method of UV coating dumb light ink, includes the following steps:
Step 1: the UV oligomer and UV monomer are put into container, turn on agitator is stirred；
Illustrate as an example, the mixing time of the step 1 is 15 minutes, and the stirring rate of the blender is
500 revs/min；
Illustrate as an example, the stirring condition is 35 DEG C Celsius, and pressure is normal pressure；
Being sufficiently mixed for the UV oligomer and UV monomer is conducive to using relatively higher temperature；
Step 2: being slowly added to photoinitiator, flatting silica and levelling agent in completed step 1 process, and opens and stir
Device is mixed to be mixed；
Illustrate as an example, the mixing time of the step 2 is 10 minutes, and the stirring rate of the blender is
500 revs/min；
Illustrate as an example, the stirring condition of the step 2 is room temperature, normal pressure；
Step 3: being slowly added to defoaming agent, and turn on agitator after step 2 end of operation；
Illustrate as an example, the rate of the blender of the step 3 is 60 revs/min, and mixing time is 20 minutes；
Stirring condition is room temperature, normal pressure；
Using slightly longer mixing time and lower stirring rate, defoaming agent can be made to play optimal defoaming effect,
The air defective material in coating is reduced, surfacing when installation when being conducive to packaging is stored and constructed；
After the ink construction of the invention, special installation can be used after ultraviolet light, solidification is formed, after the solidification
Coating have many new effects such as anti-scratch, ethanol-tolerant, good protective action, while the ink can be also played to institute's covering
Solidify high production efficiency, dumb light decorative effect is good, can be widely used for the protective coating field of electronic product components.
Beneficial effects of the present invention:
1, the invention uses special formula and processing technology, so that the ink has Environmental Safety, low cost manufacturing etc.
Plurality of advantages；
2, using special preparation process and formula, not only the very good solution uniform proportion of coating, also mentions significantly
The high remaining flow of air；
3 and the ink after ultraviolet light solidifies, coating is anti-scratch, ethanol-tolerant, can play good protection to institute's seal coat
Effect；
4, the ink solidification production efficiency is higher, and dumb light decorative effect is good, can be widely used for the painting of electronic product components
Fill protection field；
Detailed description of the invention
Fig. 1 is a kind of flow diagram of the preparation method of UV coating dumb light ink of the present invention
Specific embodiment
With reference to the accompanying drawing to a preferred embodiment of the present invention will be described in detail；
Shown in referring to Fig.1, a kind of UV coating dumb light ink and preparation method thereof, in which:
A kind of UV coating dumb light ink, a kind of UV coating dumb light ink according to the present invention, component includes: UV oligomeric
Object, UV monomer, photoinitiator, flatting silica, defoaming agent and levelling agent；
As the preferred embodiment that one group of experimental data obtains, a kind of UV coating dumb light ink is by mass percentage
Include: UV oligomer: 50-80%, UV monomer: 10-35%, photoinitiator: 3-9%, flatting silica: 10-45%, defoaming agent:
0.2-2%, levelling agent: 0.2-2%；
As the optimum embodiment that one group of experimental data obtains, a kind of UV coating dumb light ink is by mass percentage
Include: UV oligomer: 55%, UV monomer: 20%, photoinitiator: 7%, flatting silica: 15%, defoaming agent: 2%, levelling agent:
1%；Using the formula of this mass ratio, the ink produced can be made to have the energy conservation and environmental protection scheme of best cost performance
Simultaneously, moreover it is possible to greatly improve the production efficiency of the later period ink solidification, and optimal dumb light decorative effect can be generated；
Illustrate as an example, the monomer be Sartomer CD420, CD551, SR285, SR339, SR395, SR340,
SR238, SR506 or Changxing chemical monomer EM210, EM211, EM212, EM218, EM2191, EM90, EM75, EM70,
EM2202, EM221, EM222, EM223, EM225, EM265, EM235, EM2380, EM231, or German Kening Co., Ltd 4006,
4061, one of 4017,4149,4127 or combination；
Illustrate as an example, the UV oligomer be Sartomer CN1963, CN2101, CN111, CN115,
CN119, CN120, CN121, CN2251, CN2253, CN1045M, or German Corning 3016-20R, 4703,5010,5432,
6019,6623/6893-20R or Changxing chemistry 621A80,6210G, 6215-100,623A80,6148J75,6175-2,
6196,6197,6353, one of 6314C, 6350,6063,6068,8000A or combination；
Illustrate as an example, the photoinitiator be Ciba Specialty Chemicals D-1173,184,754,369,829,
907,2022 or Tianjin Jiu company 1101,1103,1104,1108,1055,1020,1024 or Tianjin English power IHT-
One of PI 151, IHT-PI1173, IHT-PI 910, IHT-PI MBF, 1000 IHT-PI, IHT-PI 500 or group
It closes；
Illustrate as an example, the flatting silica, which is that Suzhou is comprehensive, grinds KMR-3TA, KMR-3EA, KMR-180A or the U.S.
Step figure Tospearl 240, DSA-6, Tospearl 2000B or the HY-690 of U.S. MSE (Mai Si) company, W. R. Grace & Co
CP4-8991, SY7000, C803, C906, day Bender mountain FM14, Degussa ACEMA TT300, TT600, TS100, OK412,
OK607, OK500, one of OK520 or combination；
Illustrate as an example, the defoaming agent be DOW CORNING DC-51, DC-7, DC-8621, Antifoam-A, or
BYK-066, BYK-67N, BYK-67, BYK-066N or Digao (Tego) 930, Foamax N, 902 of Bi Ke chemistry, or Japan
Figure TSA750S or Guangzhou ten thousand are stepped into one of defoaming agent BYC-6800 or combination；
Illustrate as an example, the levelling agent be DOW CORNING DC-3, DC-57 or Digao (Tego) 432,410,
450, one of Glide B1484,440 or Guangzhou Zhuo energy trade RM2020 or combination；
A kind of preparation method of UV coating dumb light ink, includes the following steps:
Step 1: the UV oligomer and UV monomer are put into container, turn on agitator is stirred；
Illustrate as an example, the mixing time of the step 1 is 15 minutes, and the stirring rate of the blender is
500 revs/min；
Illustrate as an example, the stirring condition is 35 DEG C Celsius, and pressure is normal pressure；
Being sufficiently mixed for the UV oligomer and UV monomer is conducive to using relatively higher temperature；
Step 2: being slowly added to photoinitiator, flatting silica and levelling agent in completed step 1 process, and opens and stir
Device is mixed to be mixed；
Illustrate as an example, the mixing time of the step 2 is 10 minutes, and the stirring rate of the blender is
500 revs/min；
Illustrate as an example, the stirring condition of the step 2 is room temperature, normal pressure；
Step 3: being slowly added to defoaming agent, and turn on agitator after step 2 end of operation；
Illustrate as an example, the rate of the blender of the step 3 is 60 revs/min, and mixing time is 20 minutes；
Stirring condition is room temperature, normal pressure；
Using slightly longer mixing time and lower stirring rate, defoaming agent can be made to play optimal defoaming effect, subtracted
Air defective material in few coating, surfacing when installation when being conducive to packaging is stored and constructed；
After the ink construction of the invention, special installation can be used after ultraviolet light, solidification is formed, after the solidification
Coating have many new effects such as anti-scratch, ethanol-tolerant, good protective action, while the ink can be also played to institute's covering
Solidify high production efficiency, dumb light decorative effect is good, can be widely used for the protective coating field of electronic product components；
The invention uses special formula and processing technology, so as to have Environmental Safety, low cost manufacturing etc. all for the ink
More advantages；Using special preparation process and formula, not only the very good solution uniform proportion of coating, is also substantially increased
The remaining flow of air；And the ink is after ultraviolet light solidifies, coating is anti-scratch, ethanol-tolerant, can play well to institute's seal coat
Protective action；The ink solidification production efficiency is higher, and dumb light decorative effect is good, can be widely used for the painting of electronic product components
Fill protection field；
A kind of preferred embodiment of the preparation method of UV coating dumb light ink, includes the following steps:
Step 1: the UV monomer of described 55% UV oligomer and 20% is put into container, turn on agitator is stirred
It mixes；
Illustrate as an example, the mixing time of the step 1 is 15 minutes, and the stirring rate of the blender is
500 revs/min；
Illustrate as an example, the stirring condition is 35 DEG C Celsius, and pressure is normal pressure；
Being sufficiently mixed for the UV oligomer and UV monomer is conducive to using relatively higher temperature；
Step 2: being slowly added to 7% photoinitiator, 15% flatting silica and 1% in completed step 1 process
Levelling agent, and turn on agitator is mixed；
Illustrate as an example, the mixing time of the step 2 is 10 minutes, and the stirring rate of the blender is
500 revs/min；
Illustrate as an example, the stirring condition of the step 2 is room temperature, normal pressure；
Step 3: being slowly added to 2% defoaming agent, and turn on agitator after step 2 end of operation；
Illustrate as an example, the rate of the blender of the step 3 is 60 revs/min, and mixing time is 20 minutes；
Stirring condition is room temperature, normal pressure；
After preferred embodiment processing and fabricating referring to a kind of preparation method of above-mentioned UV coating dumb light ink, the ink
Ink physical property under optimization formula ratio and raw material are as follows:
Viscosity: 4# glasss of tests, 30 seconds；Solidification energy: 20mj/cm2；
Ethanol-tolerant: two-way alcohol wear resistant instrument, 500g power, >=50 times；
It is anti-scratch: linear scratch hardness tester, 249# electrical motor driven, no trace；
Glossiness: 2 ± 1, Grossmeters test；
It is above-described to be merely a preferred embodiment of the present invention, it should be understood that the explanation of above embodiments is only used
In facilitating the understanding of the method and its core concept of the invention, it is not intended to limit the scope of protection of the present invention, it is all of the invention
Any modification for being made within thought and principle, equivalent replacement etc., should all be included in the protection scope of the present invention.
Claims (8)
1. a kind of UV is coated with dumb light ink, which is characterized in that its component includes: UV oligomer, UV monomer, photoinitiator, delustring
Powder, defoaming agent and levelling agent；
A kind of UV coating dumb light ink includes: UV oligomer by mass percentage: 50-80%, UV monomer: 10-35%,
Photoinitiator: 3-9%, flatting silica: 10-45%, defoaming agent: 0.2-2% and levelling agent: 0.2-2%.
2. a kind of UV according to claim 1 is coated with dumb light ink, which is characterized in that a kind of UV coating dumb light ink
By mass percentage include: UV oligomer: 55%, UV monomer: 20%, photoinitiator: 7%, flatting silica: 15%, defoaming agent:
2%, levelling agent: 1%.
3. a kind of UV according to claim 1 is coated with dumb light ink, which is characterized in that the UV monomer is Sartomer
CD420, CD551, SR285, SR339, SR395, SR340, SR238, SR506 or Changxing chemical monomer EM210, EM211,
EM212、EM218、EM2191、EM90、EM75、EM70、EM2202、EM221、EM222、EM223、EM225、EM265、EM235、
One of EM2380, EM231, or German Kening Co., Ltd 4006,4061,4017,4149,4127 or combination.
4. a kind of UV according to claim 1 is coated with dumb light ink, which is characterized in that the UV oligomer is Sartomer
CN1963, CN2101, CN111, CN115, CN119, CN120, CN121, CN2251, CN2253, CN1045M, or German Corning
3016-20R, 4703,5010,5432,6019,6623,6893-20R or Changxing chemistry 621A80,6210G, 6215-100,
One of 623A80,6148J75,6175-2,6196,6197,6353,6314C, 6350,6063,6068,8000A or group
It closes.
5. a kind of UV according to claim 1 is coated with dumb light ink, which is characterized in that the photoinitiator is Ciba
The D-1173 of company, 184,754,369,829,907,2022 or Tianjin Jiu company 1101,1103,1104,1108,
1055,1020,1024 or Tianjin English power IHT-PI 151, IHT-PI 1173, IHT-PI 910, IHT-PI MBF, IHT-
One of PI 1000, IHT-PI 500 or combination.
6. a kind of UV according to claim 1 is coated with dumb light ink, which is characterized in that the flatting silica, which is that Suzhou is comprehensive, to be ground
KMR-3TA, KMR-3EA, KMR-180A or the U.S. step figure Tospearl 240, DSA-6, Tospearl 2000B or the U.S.
The HY-690 of MSE company, CP4-8991, SY7000, C803, C906 of W. R. Grace & Co, day Bender mountain FM14, Degussa
One of ACEMA TT300, TT600, TS100, OK412, OK607, OK500, OK520 or combination.
7. a kind of UV according to claim 1 is coated with dumb light ink, which is characterized in that the defoaming agent is DOW CORNING
BYK-066, BYK-67N, BYK-67, BYK-066N of DC-51, DC-7, DC-8621, Antifoam-A or Bi Ke chemistry, or
Digao 930, Foamax N, 902, or Japan step figure TSA750S or Guangzhou ten thousand at one of defoaming agent BYC-6800 or
Combination.
8. a kind of UV according to claim 1 is coated with dumb light ink, which is characterized in that the levelling agent is DOW CORNING
One of DC-3, DC-57 or Digao 432,410,450, GlideB1484,440 or Guangzhou Zhuo energy trade RM2020 or
Person's combination.
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| CN201510967678.1A CN105585898B (en) | 2015-12-21 | 2015-12-21 | A kind of UV coating dumb light ink and preparation method thereof |
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| CN106318026A (en) * | 2016-08-23 | 2017-01-11 | 苏州裕同印刷有限公司 | Friction-resistant matt varnish |
| CN110684444A (en) * | 2019-11-12 | 2020-01-14 | 苏州美盈森环保科技有限公司 | High-adhesion UV matte gloss oil and preparation method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104194485A (en) * | 2014-08-26 | 2014-12-10 | 南昌欧菲生物识别技术有限公司 | Noctilucent ink, fingerprint identification device using same and terminal equipment |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104194485A (en) * | 2014-08-26 | 2014-12-10 | 南昌欧菲生物识别技术有限公司 | Noctilucent ink, fingerprint identification device using same and terminal equipment |
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Effective date of registration: 20171024 Address after: Ten 239500 Tan Industrial Park, Quanjiao County, Anhui, Chuzhou Applicant after: CHUZHOU JQDK NEW MATERIAL Co.,Ltd. Address before: 214000, Wuxi, Wuxi, Jiangsu photoelectric new materials science and technology park will be No. 88, shore road, Room 606 Applicant before: Wang Jingquan |
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Address after: 239500 Chuzhou City, Chuzhou, Anhui Province, Quanjiao County, ten Tan Industrial Park Patentee after: Jinqiao Deke New Materials Co.,Ltd. Address before: 239500 Chuzhou City, Chuzhou, Anhui Province, Quanjiao County, ten Tan Industrial Park Patentee before: CHUZHOU JQDK NEW MATERIAL Co.,Ltd. |
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