CN105544239B - A kind of bamboo fibre colouring method based on mangosteen natural dye - Google Patents
A kind of bamboo fibre colouring method based on mangosteen natural dye Download PDFInfo
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- CN105544239B CN105544239B CN201610037839.1A CN201610037839A CN105544239B CN 105544239 B CN105544239 B CN 105544239B CN 201610037839 A CN201610037839 A CN 201610037839A CN 105544239 B CN105544239 B CN 105544239B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
- Cosmetics (AREA)
Abstract
The present invention provides a kind of bamboo fibre colouring method based on mangosteen natural dye, and concrete operation step is：(1) the fresh mangosteen shell after will be edible, which is cleaned, to be dried, powdered mangosteen shell is obtained after crushing, then powdered mangosteen shell is placed in the ethanol water containing sodium hydroxide, 15 20s of ultrasonication, reflux extraction 2 times, it filtrate will merge twice, and citric acid is added, and be concentrated to give mangosteen natural dye；(2) with bath raio 1:40, natural bamboo fibres are impregnated in 1 5% sodium hydrate aqueous solution, 5 10min of soaking at room temperature, take out, be washed to neutrality, obtain the natural bamboo fibres of oxygenation pretreatment；(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, constant temperature oscillation, take out, washing and drying dyed after natural bamboo fibres.The present invention carries out dyeing processing using the natural dye liquor of mangosteen to natural bamboo fibres, imparts the color characteristics of green natural, remains antibacterial green good characteristic, and do not influence feel.
Description
Technical field：
The invention belongs to textile material technical fields, and in particular to a kind of bamboo fibre dyeing side based on mangosteen natural dye
Method.
Background technology：
With the continuous development of science and technology, science and technology also brings corresponding secondary work while bringing convenient
With then more and more people begin to focus on health, and concern is natural.Natural pigment is safe, green, nontoxic by it and receives
The pro-gaze of people, the natural dye prepared by natural pigment are liked because its color and luster elegance is soft, characteristic is natural by consumer
Love.
Mangosteen, also referred to as garcinia mangostana, mangosteen, wind fruit etc., originate in Indonesia and Malaysia, Yunnan Province of China,
Also there is plantation on the ground such as Guangxi, Guangdong, Fujian.Mangosteen is a kind of typical tropical fruit (tree), is known as the laudatory title of queen in fruit, mangosteen
Seed be arranged radially, be rich in abundant protein, carbohydrate and lipid, mangosteen shell is dark purple, puckery cool in nature, contains fruit
Glue, crude fibre and a variety of pharmacological components, such as double benzene pyrrones, flavonoids, Anthraquinones, carbohydrate, have antibacterial bacteriostatic, resist
Ultraviolet light and antioxidant activity effect.Contain tannic acid and uranidin in mangosteen shell, for tanning or dyeing, and this color
Element is strong with the affinity of fiber, once there is application in conjunction with would become hard to remove, therefore using mangosteen shell as the raw material of natural dye
Value.
A kind of preparation side of mangosteen hull natural dye disclosed in Chinese patent CN 103483855B (publication date 2014.1.1)
Mangosteen shell is cleaned, is dried, after mechanical crushing by method and its application and colouring method, and mangosteen shell crushed material is added to hydroxide
In the ethanol water of sodium, reflux extraction filtering distillation obtains mangosteen hull natural dye, then by mangosteen natural dye after matchmaker
Dyeing dyes protein fibre.Mangosteen shell extract prepared by this method is bright-coloured dark brown, and absorbance is high,
And it can assign silk fiber different colors by different mordants.Chinese patent CN 104727165A (publication date
2015.6.24 a kind of dyeing of real silk fabric disclosed in), by real silk fabric after chitosan pre-processes, then with chitosan
For mordant, mangosteen hull natural dye dyes real silk fabric as dyestuff, by postfinishing process such as fixation of soaping, obtains
The real silk fabric all good to color fastness and feel.
By the above-mentioned prior art it is found that the natural dye extracted from mangosteen shell has been attempted for silk, sheep wool and cotton
In fabric, certain progress is obtained, but research of the mangosteen natural dye in terms of bamboo fibre dyeing has been not yet reported that.Bamboo
Fiber belongs to the green fiber that can be breathed, and can be also equipped with natural lasting anti-microbial property in transient absorption and evaporable water, this
Invention applies to mangosteen natural dye in bamboo fibre dyeing, excludes damage of the dyeing to its green natural performance.
Invention content：
The technical problem to be solved in the present invention is to provide a kind of bamboo fibre colouring methods based on mangosteen natural dye, will use
Physics gimmick extracts mangosteen natural dye, the bamboo fibre mangosteen natural dye that will be crossed through oxygenation pretreatment in the mangosteen after eating
Direct staining, this preparation method is easy, and the recovery rate of mangosteen natural dye is high, and the dye-uptake of bamboo fibre is high.
In order to solve the above technical problems, the technical scheme is that：
A kind of bamboo fibre colouring method based on mangosteen natural dye, it is characterised in that：Include the following steps：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, and powdered mangosteen shell is obtained after crushing, then will be powdered
Mangosteen shell is placed in the ethanol water containing sodium hydroxide, ultrasonication 15-20s, reflux extraction 2 times, filtrate will be closed twice
And and citric acid is added, be concentrated to give mangosteen natural dye；
(2) with bath raio 1:40, natural bamboo fibres are impregnated in the sodium hydrate aqueous solution of 1-5%, soaking at room temperature 5-
10min takes out, is washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment；
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, constant temperature oscillation,
Take out, washing and drying dyed after natural bamboo fibres.
As a preferred embodiment of the above technical solution, in the step (1), it is 50-80 mesh that powdered mangosteen shell, which obtains grain size,.
As a preferred embodiment of the above technical solution, in the step (1), sodium hydroxide in the ethanol water of sodium hydroxide
Content is 1g/L, and the ratio of ethyl alcohol and water is 3-4:1.
As a preferred embodiment of the above technical solution, in the step (1), the ethanol water of powdered mangosteen shell and sodium hydroxide
The mass ratio of solution is 1:50-100.
As a preferred embodiment of the above technical solution, in the step (1), the power of ultrasonic wave is 1000-1500W.
As a preferred embodiment of the above technical solution, in the step (1), the pH value of mangosteen natural dye is 3-7.
As a preferred embodiment of the above technical solution, in the step (1), mangosteen natural dye wavelength be 531nm at most
Big absorbance is 0.67-0.92.
As a preferred embodiment of the above technical solution, in the step (3), the temperature of constant temperature oscillation is 60-80 DEG C, vibrates 30-
50min。
As a preferred embodiment of the above technical solution, in the step (3), the color fastness of the natural bamboo fibres after dyeing is 4-5
Grade.
Compared with prior art, the invention has the advantages that：
(1) present invention is combined using physics with chemical gimmick, and being combined with solvent extraction by ultrasonic technique can be quickly
Pigment in efficient extraction mangosteen shell, extraction time is short, and recovery rate is high, simplifies the process time, improves working efficiency.
(2) natural bamboo fibres are dyed using direct staining technology in the present invention, in order to improve natural bamboo fibres
Dye-uptake, by natural bamboo fibres through oxygenation pretreatment, the stainabilitys of the natural bamboo fibres after oxygenation pretreatment improves, and color fastness and
Color depth is all improved.
(3) present invention carries out dyeing processing using the natural dye liquor of mangosteen to natural bamboo fibres, imparts the face of green natural
Color characteristic, remains the antibacterial green good characteristic of natural bamboo fibres, and does not influence the feel of fiber.
Specific implementation mode：
Below in conjunction with specific embodiment, the present invention will be described in detail, herein illustrative examples and explanation of the invention
For explaining the present invention, but it is not as a limitation of the invention.
Embodiment 1：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, then the mangosteen shell that 50 mesh powder shapes are obtained after crushing is pressed
The powdered mangosteen shell of 1 parts by weight is placed in 50 parts of the ethanol water of 75% containing sodium hydroxide by parts by weight meter,
The content of middle sodium hydroxide is 1g/L, and 15s is handled under the ultrasonic wave of 1000W, and reflux extraction 2 times filtrate will merge twice, and
Citric acid is added, adjusts pH value to 3, is concentrated to give mangosteen natural dye, mangosteen natural dye is in the maximum that wavelength is at 531nm
Absorbance is 0.67.
(2) with bath raio 1:40, natural bamboo fibres are impregnated in 1% sodium hydrate aqueous solution, soaking at room temperature 5min takes
Go out, be washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment.
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, at 60 DEG C
Constant temperature oscillation 30min, take out, washing and drying dyed after natural bamboo fibres.
Embodiment 2：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, then the mangosteen shell that 80 mesh powder shapes are obtained after crushing is pressed
The powdered mangosteen shell of 1 parts by weight is placed in 100 parts of the ethanol water of 80% containing sodium hydroxide by parts by weight meter,
Wherein the content of sodium hydroxide is 1g/L, and 20s is handled under the ultrasonic wave of 1500W, and reflux extraction 2 times filtrate will merge twice,
And citric acid is added, adjust pH value to 7, be concentrated to give mangosteen natural dye, mangosteen natural dye wavelength be at 531nm most
Big absorbance is 0.92.
(2) with bath raio 1:40, natural bamboo fibres are impregnated in 5% sodium hydrate aqueous solution, soaking at room temperature 10min,
It takes out, is washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment.
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, at 80 DEG C
Constant temperature oscillation 50min, take out, washing and drying dyed after natural bamboo fibres.
Embodiment 3：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, then the mangosteen shell that 60 mesh powder shapes are obtained after crushing is pressed
The powdered mangosteen shell of 1 parts by weight is placed in the ethanol water of 80 parts of the 75-80% containing sodium hydroxide by parts by weight meter
In, wherein the content of sodium hydroxide is 1g/L, and 18s is handled under the ultrasonic wave of 1200W, and reflux extraction 2 times filtrate will close twice
And and be added citric acid, adjust pH value to 5, be concentrated to give mangosteen natural dye, mangosteen natural dye is at 531nm in wavelength
Maximum absorbance be 0.82.
(2) with bath raio 1:40, natural bamboo fibres are impregnated in 3% sodium hydrate aqueous solution, soaking at room temperature 7min takes
Go out, be washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment.
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, at 70 DEG C
Constant temperature oscillation 40min, take out, washing and drying dyed after natural bamboo fibres.
Embodiment 4：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, then the mangosteen shell that 70 mesh powder shapes are obtained after crushing is pressed
The powdered mangosteen shell of 1 parts by weight is placed in the ethanol water of 80 parts of the 75-80% containing sodium hydroxide by parts by weight meter
In, wherein the content of sodium hydroxide is 1g/L, and 20s is handled under the ultrasonic wave of 1100W, and reflux extraction 2 times filtrate will close twice
And and be added citric acid, adjust pH value to 6, be concentrated to give mangosteen natural dye, mangosteen natural dye is at 531nm in wavelength
Maximum absorbance be 0.75.
(2) with bath raio 1:40, natural bamboo fibres are impregnated in 4% sodium hydrate aqueous solution, soaking at room temperature 5min takes
Go out, be washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment.
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, at 75 DEG C
Constant temperature oscillation 30min, take out, washing and drying dyed after natural bamboo fibres.
Embodiment 5：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, then the mangosteen shell that 50 mesh powder shapes are obtained after crushing is pressed
The powdered mangosteen shell of 1 parts by weight is placed in 100 parts of the ethanol water of 75% containing sodium hydroxide by parts by weight meter,
Wherein the content of sodium hydroxide is 1g/L, and 20s is handled under the ultrasonic wave of 1000W, and reflux extraction 2 times filtrate will merge twice,
And citric acid is added, adjust pH value to 4, be concentrated to give mangosteen natural dye, mangosteen natural dye wavelength be at 531nm most
Big absorbance is 0.79.
(2) with bath raio 1:40, natural bamboo fibres are impregnated in 2% sodium hydrate aqueous solution, soaking at room temperature 8min takes
Go out, be washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment.
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, at 65 DEG C
Constant temperature oscillation 45min, take out, washing and drying dyed after natural bamboo fibres.
Embodiment 6：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, then the mangosteen shell that 50 mesh powder shapes are obtained after crushing is pressed
The powdered mangosteen shell of 1 parts by weight is placed in 50 parts of the ethanol water of 80% containing sodium hydroxide by parts by weight meter,
The content of middle sodium hydroxide is 1g/L, and 15s is handled under the ultrasonic wave of 1500W, and reflux extraction 2 times filtrate will merge twice, and
Citric acid is added, adjusts pH value to 6, is concentrated to give mangosteen natural dye, mangosteen natural dye is in the maximum that wavelength is at 531nm
Absorbance is 0.87.
(2) with bath raio 1:40, natural bamboo fibres are impregnated in the sodium hydrate aqueous solution of 1-5%, soaking at room temperature 8min,
It takes out, is washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment.
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, at 70 DEG C
Constant temperature oscillation 35min, take out, washing and drying dyed after natural bamboo fibres.
Embodiment 7：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, then the mangosteen shell that 80 mesh powder shapes are obtained after crushing is pressed
The powdered mangosteen shell of 1 parts by weight is placed in 80 parts of the ethanol water of 80% containing sodium hydroxide by parts by weight meter,
The content of middle sodium hydroxide is 1g/L, and 18s is handled under the ultrasonic wave of 1300W, and reflux extraction 2 times filtrate will merge twice, and
Citric acid is added, adjusts pH value to 5, is concentrated to give mangosteen natural dye, mangosteen natural dye is in the maximum that wavelength is at 531nm
Absorbance is 0.86.
(2) with bath raio 1:40, natural bamboo fibres are impregnated in the sodium hydrate aqueous solution of 1-5%, soaking at room temperature 6min,
It takes out, is washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment.
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, at 70 DEG C
Constant temperature oscillation 45min, take out, washing and drying dyed after natural bamboo fibres.
Embodiment 8：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, then the mangosteen shell that 80 mesh powder shapes are obtained after crushing is pressed
The powdered mangosteen shell of 1 parts by weight is placed in 60 parts of the ethanol water of 75% containing sodium hydroxide by parts by weight meter,
The content of middle sodium hydroxide is 1g/L, and 15s is handled under the ultrasonic wave of 1500W, and reflux extraction 2 times filtrate will merge twice, and
Citric acid is added, adjusts pH value to 5, is concentrated to give mangosteen natural dye, mangosteen natural dye is in the maximum that wavelength is at 531nm
Absorbance is 0.78.
(2) with bath raio 1:40, natural bamboo fibres are impregnated in the sodium hydrate aqueous solution of 1-5%, soaking at room temperature
10min takes out, is washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment.
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, at 80 DEG C
Constant temperature oscillation 35min, take out, washing and drying dyed after natural bamboo fibres.
After testing, the color depth of the natural bamboo fibres after the dyeing that prepared by embodiment 1-8, the knot of color fastness and antibiotic property
Fruit is as follows：
As seen from the above table, the color depth of the natural bamboo fibres after the dyeing that prepared by the present invention is good, and color fastness is high, is also equipped with
Certain anti-microbial property.
The above-described embodiments merely illustrate the principles and effects of the present invention, and is not intended to limit the present invention.It is any ripe
The personage for knowing this technology can all carry out modifications and changes to above-described embodiment without violating the spirit and scope of the present invention.Cause
This, institute is complete without departing from the spirit and technical ideas disclosed in the present invention by those of ordinary skill in the art such as
At all equivalent modifications or change, should by the present invention claim be covered.
Claims (1)
1. a kind of bamboo fibre colouring method based on mangosteen natural dye, it is characterised in that：Include the following steps：
(1) the fresh mangosteen shell after eating, which is cleaned, to be dried, and powdered mangosteen shell is obtained after crushing, then by powdered mangosteen
Shell is placed in the ethanol water containing sodium hydroxide, ultrasonication 15-20s, reflux extraction 2 times, filtrate will be merged twice, and
Citric acid is added, is concentrated to give mangosteen natural dye；
(2) with bath raio 1:40, natural bamboo fibres are impregnated in the sodium hydrate aqueous solution of 1-5%, soaking at room temperature 5-10min,
It takes out, is washed to neutrality, obtains the natural bamboo fibres of oxygenation pretreatment；
(3) with bath raio 1:100, the natural bamboo fibres of oxygenation pretreatment are placed in mangosteen natural dye and are impregnated, constant temperature oscillation takes
Go out, washing and drying dyed after natural bamboo fibres；
Wherein, in the step (1), it is 50-80 mesh that powdered mangosteen shell, which obtains grain size, hydrogen in the ethanol water of sodium hydroxide
The content of sodium oxide molybdena is 1g/L, and the ratio of ethyl alcohol and water is 3-4:1, the ethanol water of powdered mangosteen shell and sodium hydroxide
Mass ratio be 1:The power of 50-100, ultrasonic wave are 1000-1500W, and the pH value of mangosteen natural dye is 3-7, and mangosteen is natural
It is 0.67-0.92 that dyestuff, which is maximum absorbance at 531nm in wavelength,；
Wherein, in the step (3), the temperature of constant temperature oscillation is 60-80 DEG C, vibrates 30-50min, the natural bamboo after dyeing is fine
The color fastness of dimension is 4-5 grades.
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| CN108978260B (en) * | 2018-06-18 | 2021-11-12 | 广东欣薇尔服装有限公司 | Dyeing method of natural beet red pigment |
| CN111235915B (en) * | 2020-03-23 | 2021-08-17 | 德州学院 | Bamboo fiber fabric dyeing method based on mahonia broadleaf plant dye |
| CN111893640A (en) * | 2020-07-15 | 2020-11-06 | 何炽斌 | Colored non-woven fabric paper towel and preparation method thereof |
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| KR20030051562A (en) * | 2003-06-09 | 2003-06-25 | 이태훈 | Manufacturing method of natural yellow lacquer dyes and dyeing method of natural fiber using the same |
| CN1263922C (en) * | 2004-09-08 | 2006-07-12 | 江西农业大学 | Bamboo fiber processing process |
| CN102899930A (en) * | 2011-07-26 | 2013-01-30 | 李发勇 | Hematoxylon dyeing method applied on original bamboo fiber bedding |
| CN102864651B (en) * | 2012-10-12 | 2014-06-25 | 浙江绿卿竹业科技有限公司 | Method for coloring bamboo fiber fabric with tea leaves |
| CN103276606A (en) * | 2013-06-08 | 2013-09-04 | 太仓市芸芸化纤有限公司 | Natural dye dyeing method of bamboo fiber fabric |
| CN103483855B (en) * | 2013-10-09 | 2015-06-17 | 浙江理工大学 | Preparation method of mangosteen shell natural dye, application and staining method thereof |
| CN104499360A (en) * | 2014-11-03 | 2015-04-08 | 广西南宁至简至凡科技咨询有限公司 | Manufacture technology for mixed type bamboo-pulp kraft paper |
| CN104727165A (en) * | 2015-04-02 | 2015-06-24 | 太仓市诚乐化纤有限公司 | Process of dyeing silk fabric |
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Effective date of registration: 20201215 Address after: No.18-91, Gongye Road, South Taihu high tech Industrial Park, Wuxing District, Huzhou City, Zhejiang Province Patentee after: Zhejiang julibao Textile Technology Co., Ltd Address before: 215000 2 Taishan Road, high tech Zone, Suzhou, Jiangsu (Room 101 and 201, zone A, test center, Poji science and Technology Pioneer Park) Patentee before: SUZHOU INSILK Co.,Ltd. |