CN105525506A - Preparation method of textile heat insulation coating - Google Patents

Preparation method of textile heat insulation coating Download PDF

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Publication number
CN105525506A
CN105525506A CN201511002064.6A CN201511002064A CN105525506A CN 105525506 A CN105525506 A CN 105525506A CN 201511002064 A CN201511002064 A CN 201511002064A CN 105525506 A CN105525506 A CN 105525506A
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Prior art keywords
parts
calcium carbonate
ammonium sulfate
polyvinyl chloride
zinc oxide
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CN201511002064.6A
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Inventor
左士祥
杨阳
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Suzhou Yuxi New Material Technology Co Ltd
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Suzhou Yuxi New Material Technology Co Ltd
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Priority to CN201511002064.6A priority Critical patent/CN105525506A/en
Publication of CN105525506A publication Critical patent/CN105525506A/en
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic Table; Zincates; Cadmates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
    • D06M11/59—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with ammonia; with complexes of organic amines with inorganic substances
    • D06M11/60—Ammonia as a gas or in solution
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/74—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon or graphite; with carbides; with graphitic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/76—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/325—Amines
    • D06M13/335—Amines having an amino group bound to a carbon atom of a six-membered aromatic ring
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/402—Amides imides, sulfamic acids
    • D06M13/425—Carbamic or thiocarbamic acids or derivatives thereof, e.g. urethanes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/244—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of halogenated hydrocarbons
    • D06M15/248—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of halogenated hydrocarbons containing chlorine
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/30—Flame or heat resistance, fire retardancy properties

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a preparation method of a textile heat insulation coating. The method comprises the following steps: 1, adding ammonia water, zinc oxide, soft soap, ammonia sulfate and deionized water to a reaction kettle provided with a stirrer, a thermometer and a reflux condenser tube, and stirring above materials; 2, adding sodium polyacrylate, a styrene acrylic emulsion, light calcium carbonate and polyvinyl chloride, eliminating air in the reaction kettle, heating while stirring above material to 65-75DEG C, and carrying out heat insulation for 1-3h; and 3, adding talcum powder, N-phenyl-1-naphthylamine, rubber scarlet or carbon black, heavy calcium carbonate and zinc dimethyldithiocarbamate, heating and stirring the obtained material until uniformity, cooling the uniform material, grinding the cooled material in a sand mill, and filtering the ground material to obtain the textile heat insulation coating. The surface drying time of the above product is 10-30min, and the hard drying time of the product is 50-90min; the fire resistance time is 30-60s, and the fire resistance weight loss is 2-4g; the adhesion is 98-100%, the impact strength is 60-70cm, the levelability is extremely good, and a coating film can resist saturated calcium hydrate immersion for 10-20d; the coating film does not shed or mildew after being immersed in water for 20-30d; the gloss is 96-100%, the flexibility is 1-5mm, and the service life of the coating film is long; and the sagging resistance and the storage stability of the product are good.

Description

A kind of preparation method of insulating moulding coating of weaving
Technical field
The application relates to a kind of insulating moulding coating, particularly relates to a kind of preparation method of insulating moulding coating of weaving.
Background technology
Existing insulating moulding coating product great majority are applied in concrete or metal structure surface plays effect of heat insulation, and the pliability of this kind of insulating moulding coating, compactness and tack are generally poor, should not be painted on textiles, carry out heat-insulation and heat-preservation.But along with the extensive use of outdoor textiles and sunshade, the requirement of people to the heat preservation and insulation of textiles is also more and more higher.
Therefore, how to design the weaving insulating moulding coating that a kind of adhesion strength is high, fast drying, tensile strength are high, fracture elongation is high and the resistance to combustion time is long, to meet the need of market, be very important.
Summary of the invention
the technical problem solved:
The present invention is directed to that existing weaving insulating moulding coating fungicidal properties is poor, service life is short, technical problem that acid and alkali-resistance, flame retardant effect difference and resistance to water are all not poor and a kind of preparation method of insulating moulding coating of weaving is provided.
technical scheme:
Weave the preparation method of insulating moulding coating, it is characterized in that: concrete steps are as follows:
The first step: ammoniacal liquor, zinc oxide, soft soap, ammonium sulfate and deionized water are dropped into and is equipped with in the reactor of agitator, thermometer and reflux condensing tube, rotate with 50r/min, stir 10-30min;
Second step: add Sodium Polyacrylate, benzene emulsion, precipitated calcium carbonate and polyvinyl chloride again, gets rid of in reactor after air, and warming while stirring, to 65-75 DEG C, is incubated 1-3h;
3rd step: add surplus stock talcum powder, N-phenyl-1-naphthylamine, rubber bright red or carbon black, calcium bicarbonate and zine dimethyldithiocarbamate, be warming up to 80-90 DEG C stir after cooling, sand mill is ground to fineness 10-20 μm, after filtration, namely obtains product.
Preferably, the raw materials by weight portion proportioning of weaving insulating moulding coating of the present invention is as follows: deionized water 100 parts, benzene emulsion 30-50 part, talcum powder 2-8 part, precipitated calcium carbonate 8-12 part, ammoniacal liquor 4-8 part, polyvinyl chloride 30-50 part, zinc oxide 3-7 part, N-phenyl-1-naphthylamine 1-5 part, soft soap 5-25 part, bright red or the carbon black 0.4-0.8 part of rubber, ammonium sulfate 1.5-3.5 part, calcium bicarbonate 20-40 part, Sodium Polyacrylate 2-8 part, zine dimethyldithiocarbamate 1-5 part.
Preferred, the raw materials by weight portion proportioning of weaving insulating moulding coating of the present invention is as follows: deionized water 100 parts, benzene emulsion 40 parts, talcum powder 5 parts, precipitated calcium carbonate 10 parts, ammoniacal liquor 6 parts, polyvinyl chloride 40 parts, 5 parts, zinc oxide, N-phenyl-1-naphthylamine 3 parts, soft soap 15 parts, carbon black 0.6 part, 2.5 parts, ammonium sulfate, calcium bicarbonate 30 parts, Sodium Polyacrylate 5 parts, zine dimethyldithiocarbamate 3 parts.
beneficial effect:
Compared to the prior art the above technical scheme of the present invention, has following technique effect: 1, select benzene emulsion and talcum powder, precipitated calcium carbonate to arrange in pairs or groups and use, product surface drying time 10-30min, does solid work 50-90min; Combinationally using 2, by soft soap, polyvinyl chloride and ammonium sulfate, brings resistance to combustion time 30-60s, Fire retardance: weightless 2-4g; 3, the synergy of zinc oxide, ammonium sulfate and Sodium Polyacrylate, product adhesive force 98-100%, impact strength 60-70cm, levelability is fabulous, soaks 10-20d in the resistance to saturated calcium hydroxide of film; 4, used by ammoniacal liquor, bright red or carbon black and N-phenyl-1-naphthylamine the collocation of zine dimethyldithiocarbamate, rubber, produce synergy, thus bring product soak in water 20-30d do not come off, mildewproof; Gloss 96-100%, pliability 1-5mm, film long service life; Sag resistance and excellent storage stability, the widespread production not division of history into periods can replace current material.
Detailed description of the invention
embodiment 1
Proportioning takes deionized water 100 parts by weight, benzene emulsion 30 parts, talcum powder 2 parts, precipitated calcium carbonate 8 parts, ammoniacal liquor 4 parts, polyvinyl chloride 30 parts, 3 parts, zinc oxide, N-phenyl-1-naphthylamine 1 part, soft soap 5 parts, bright red 0.4 part of rubber, 1.5 parts, ammonium sulfate, calcium bicarbonate 20 parts, Sodium Polyacrylate 2 parts, zine dimethyldithiocarbamate 1 part.
Ammoniacal liquor, zinc oxide, soft soap, ammonium sulfate and deionized water being dropped into is equipped with in the reactor of agitator, thermometer and reflux condensing tube, rotates with 50r/min, stirs 10min.Add Sodium Polyacrylate, benzene emulsion, precipitated calcium carbonate and polyvinyl chloride again, get rid of in reactor after air, warming while stirring to 65 DEG C, insulation 1h; Add surplus stock, be warming up to 80 DEG C stir after cooling, sand mill is ground to fineness 10 μm, after filtration, namely obtains product.
Benzene emulsion and talcum powder, precipitated calcium carbonate are arranged in pairs or groups and are used, and product surface drying time 30min, does solid work 90min; By combinationally using of soft soap, polyvinyl chloride and ammonium sulfate, bring resistance to combustion time 30s, Fire retardance: weightless 4g; The synergy of zinc oxide, ammonium sulfate and Sodium Polyacrylate, product adhesive force 98%, impact strength 60cm, levelability is fabulous, soaks 10d in the resistance to saturated calcium hydroxide of film; The collocation of the bright red and N-phenyl-1-naphthylamine of ammoniacal liquor, zine dimethyldithiocarbamate, rubber uses, and produces synergy, thus bring product soak in water 20d do not come off, mildewproof; Gloss 96%, pliability 1mm, film long service life; Sag resistance and excellent storage stability.
embodiment 2
Proportioning takes deionized water 100 parts by weight, benzene emulsion 50 parts, talcum powder 8 parts, precipitated calcium carbonate 12 parts, ammoniacal liquor 8 parts, polyvinyl chloride 50 parts, 7 parts, zinc oxide, N-phenyl-1-naphthylamine 5 parts, soft soap 25 parts, bright red 0.8 part of rubber, 3.5 parts, ammonium sulfate, calcium bicarbonate 40 parts, Sodium Polyacrylate 8 parts, zine dimethyldithiocarbamate 5 parts.
Ammoniacal liquor, zinc oxide, soft soap, ammonium sulfate and deionized water being dropped into is equipped with in the reactor of agitator, thermometer and reflux condensing tube, rotates with 50r/min, stirs 30min.Add Sodium Polyacrylate, benzene emulsion, precipitated calcium carbonate and polyvinyl chloride again, get rid of in reactor after air, warming while stirring to 75 DEG C, insulation 3h; Add surplus stock, be warming up to 90 DEG C stir after cooling, sand mill is ground to fineness 20 μm, after filtration, namely obtains product.
Benzene emulsion and talcum powder, precipitated calcium carbonate are arranged in pairs or groups and are used, and product surface drying time 25min, does solid work 80min; By combinationally using of soft soap, polyvinyl chloride and ammonium sulfate, bring resistance to combustion time 40s, Fire retardance: weightless 3.5g; The synergy of zinc oxide, ammonium sulfate and Sodium Polyacrylate, product adhesive force 98.5%, impact strength 62cm, levelability is fabulous, soaks 12d in the resistance to saturated calcium hydroxide of film; The collocation of the bright red and N-phenyl-1-naphthylamine of ammoniacal liquor, zine dimethyldithiocarbamate, rubber uses, and produces synergy, thus bring product soak in water 22d do not come off, mildewproof; Gloss 97%, pliability 2mm, film long service life; Sag resistance and excellent storage stability.
embodiment 3
Proportioning takes deionized water 100 parts by weight, benzene emulsion 35 parts, talcum powder 3 parts, precipitated calcium carbonate 9 parts, ammoniacal liquor 5 parts, polyvinyl chloride 35 parts, 4 parts, zinc oxide, N-phenyl-1-naphthylamine 2 parts, soft soap 10 parts, bright red 0.5 part of rubber, 2 parts, ammonium sulfate, calcium bicarbonate 25 parts, Sodium Polyacrylate 4 parts, zine dimethyldithiocarbamate 2 parts.
Ammoniacal liquor, zinc oxide, soft soap, ammonium sulfate and deionized water being dropped into is equipped with in the reactor of agitator, thermometer and reflux condensing tube, rotates with 50r/min, stirs 10min.Add Sodium Polyacrylate, benzene emulsion, precipitated calcium carbonate and polyvinyl chloride again, get rid of in reactor after air, warming while stirring to 65 DEG C, insulation 1h; Add surplus stock, be warming up to 80 DEG C stir after cooling, sand mill is ground to fineness 10 μm, after filtration, namely obtains product.
Benzene emulsion and talcum powder, precipitated calcium carbonate are arranged in pairs or groups and are used, and product surface drying time 20min, does solid work 70min; By combinationally using of soft soap, polyvinyl chloride and ammonium sulfate, bring resistance to combustion time 45s, Fire retardance: weightless 3g; The synergy of zinc oxide, ammonium sulfate and Sodium Polyacrylate, product adhesive force 99%, impact strength 65cm, levelability is fabulous, soaks 15d in the resistance to saturated calcium hydroxide of film; The collocation of the bright red and N-phenyl-1-naphthylamine of ammoniacal liquor, zine dimethyldithiocarbamate, rubber uses, and produces synergy, thus bring product soak in water 25d do not come off, mildewproof; Gloss 98%, pliability 3mm, film long service life; Sag resistance and excellent storage stability.
embodiment 4
Proportioning takes deionized water 100 parts by weight, benzene emulsion 45 parts, talcum powder 7 parts, precipitated calcium carbonate 11 parts, ammoniacal liquor 7 parts, polyvinyl chloride 45 parts, 6 parts, zinc oxide, N-phenyl-1-naphthylamine 4 parts, soft soap 20 parts, carbon black 0.7 part, 3 parts, ammonium sulfate, calcium bicarbonate 35 parts, Sodium Polyacrylate 6 parts, zine dimethyldithiocarbamate 4 parts.
Ammoniacal liquor, zinc oxide, soft soap, ammonium sulfate and deionized water being dropped into is equipped with in the reactor of agitator, thermometer and reflux condensing tube, rotates with 50r/min, stirs 30min.Add Sodium Polyacrylate, benzene emulsion, precipitated calcium carbonate and polyvinyl chloride again, get rid of in reactor after air, warming while stirring to 75 DEG C, insulation 3h; Add surplus stock, be warming up to 90 DEG C stir after cooling, sand mill is ground to fineness 20 μm, after filtration, namely obtains product.
Benzene emulsion and talcum powder, precipitated calcium carbonate are arranged in pairs or groups and are used, and product surface drying time 15min, does solid work 60min; By combinationally using of soft soap, polyvinyl chloride and ammonium sulfate, bring resistance to combustion time 50s, Fire retardance: weightless 2.5g; The synergy of zinc oxide, ammonium sulfate and Sodium Polyacrylate, product adhesive force 99%, impact strength 66cm, levelability is fabulous, soaks 18d in the resistance to saturated calcium hydroxide of film; The collocation of ammoniacal liquor, zine dimethyldithiocarbamate, carbon black and N-phenyl-1-naphthylamine uses, and produces synergy, thus bring product soak in water 27d do not come off, mildewproof; Gloss 99%, pliability 4mm, film long service life; Sag resistance and excellent storage stability.
embodiment 5
Proportioning takes deionized water 100 parts by weight, benzene emulsion 40 parts, talcum powder 5 parts, precipitated calcium carbonate 10 parts, ammoniacal liquor 6 parts, polyvinyl chloride 40 parts, 5 parts, zinc oxide, N-phenyl-1-naphthylamine 3 parts, soft soap 15 parts, carbon black 0.6 part, 2.5 parts, ammonium sulfate, calcium bicarbonate 30 parts, Sodium Polyacrylate 5 parts, zine dimethyldithiocarbamate 3 parts.
Ammoniacal liquor, zinc oxide, soft soap, ammonium sulfate and deionized water being dropped into is equipped with in the reactor of agitator, thermometer and reflux condensing tube, rotates with 50r/min, stirs 20min.Add Sodium Polyacrylate, benzene emulsion, precipitated calcium carbonate and polyvinyl chloride again, get rid of in reactor after air, warming while stirring to 70 DEG C, insulation 2h; Add surplus stock, be warming up to 85 DEG C stir after cooling, sand mill is ground to fineness 15 μm, after filtration, namely obtains product.
Benzene emulsion and talcum powder, precipitated calcium carbonate are arranged in pairs or groups and are used, and product surface drying time 10min, does solid work 50min; By combinationally using of soft soap, polyvinyl chloride and ammonium sulfate, bring resistance to combustion time 60s, Fire retardance, weightless 2g; The synergy of zinc oxide, ammonium sulfate and Sodium Polyacrylate, product adhesive force 100%, impact strength 70cm, levelability is fabulous, soaks 20d in the resistance to saturated calcium hydroxide of film; The collocation of ammoniacal liquor, zine dimethyldithiocarbamate, carbon black and N-phenyl-1-naphthylamine uses, and produces synergy, thus bring product soak in water 30d do not come off, mildewproof; Gloss 100%, pliability 5mm, film long service life; Sag resistance and excellent storage stability.
All components in above embodiment all can business be bought.
Above-described embodiment is just for setting forth the content of the application, instead of restriction, and any change therefore in the implication suitable with claims of the application and scope, all should think to be included in the scope of claims.

Claims (3)

1. weave the preparation method of insulating moulding coating, it is characterized in that: concrete steps are as follows:
The first step: ammoniacal liquor, zinc oxide, soft soap, ammonium sulfate and deionized water are dropped into and is equipped with in the reactor of agitator, thermometer and reflux condensing tube, rotate with 50r/min, stir 10-30min;
Second step: add Sodium Polyacrylate, benzene emulsion, precipitated calcium carbonate and polyvinyl chloride again, gets rid of in reactor after air, and warming while stirring, to 65-75 DEG C, is incubated 1-3h;
3rd step: add talcum powder, N-phenyl-1-naphthylamine, rubber bright red or carbon black, calcium bicarbonate and zine dimethyldithiocarbamate, be warming up to 80-90 DEG C stir after cooling, sand mill is ground to fineness 10-20 μm, after filtration, namely obtains product.
2. the preparation method of a kind of insulating moulding coating of weaving according to claim 1, it is characterized in that: the raw materials by weight portion proportioning of described weaving insulating moulding coating is as follows: deionized water 100 parts, benzene emulsion 30-50 part, talcum powder 2-8 part, precipitated calcium carbonate 8-12 part, ammoniacal liquor 4-8 part, polyvinyl chloride 30-50 part, zinc oxide 3-7 part, N-phenyl-1-naphthylamine 1-5 part, soft soap 5-25 part, bright red or the carbon black 0.4-0.8 part of rubber, ammonium sulfate 1.5-3.5 part, calcium bicarbonate 20-40 part, Sodium Polyacrylate 2-8 part, zine dimethyldithiocarbamate 1-5 part.
3. the preparation method of a kind of insulating moulding coating of weaving according to claim 1, is characterized in that, the raw materials by weight portion proportioning of described weaving insulating moulding coating is as follows: deionized water 100 parts, benzene emulsion 40 parts, talcum powder 5 parts, precipitated calcium carbonate 10 parts, ammoniacal liquor 6 parts, polyvinyl chloride 40 parts, 5 parts, zinc oxide, N-phenyl-1-naphthylamine 3 parts, soft soap 15 parts, carbon black 0.6 part, 2.5 parts, ammonium sulfate, calcium bicarbonate 30 parts, Sodium Polyacrylate 5 parts, zine dimethyldithiocarbamate 3 parts.
CN201511002064.6A 2015-12-29 2015-12-29 Preparation method of textile heat insulation coating Pending CN105525506A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1095392A (en) * 1994-02-04 1994-11-23 天津津澳乳胶制品有限公司 Foamed coating for fabric liner
CN102899913A (en) * 2011-07-29 2013-01-30 上海大巨龙蓬盖新材料有限公司 Manufacturing method for terylene strengthened filament weaving pattern rubber bottom coiled material
CN104060494A (en) * 2014-05-09 2014-09-24 湖南恒瀚高新技术有限公司 Multi-proof thermosensitive paper free of top coating and manufacture process thereof
CN104146580A (en) * 2014-08-14 2014-11-19 浙江辰鸿纺织品科技有限公司 Shading intumescent coating curtain

Patent Citations (4)

* Cited by examiner, † Cited by third party
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