CN105503196A - 一种用于航模展览的陶瓷航模的加工方法 - Google Patents

一种用于航模展览的陶瓷航模的加工方法 Download PDF

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CN105503196A
CN105503196A CN201610005571.3A CN201610005571A CN105503196A CN 105503196 A CN105503196 A CN 105503196A CN 201610005571 A CN201610005571 A CN 201610005571A CN 105503196 A CN105503196 A CN 105503196A
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刘铭泽
唐怀滨
麻闻旭
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Abstract

一种用于航模展览的陶瓷航模的加工方法，它涉及一种用于航模展览的陶瓷航模的加工方法。本发明是要解决陶瓷航模上釉后在烧制的过程中存在机翼经过高温烧制后会变折甚至断裂，同时陶瓷航模在平时易受到氧化的问题。方法：一、模具的制备；二、浆料的制备；三、成型；四、上釉；五、釉烧。本发明用于制备陶瓷航模。

Description

一种用于航模展览的陶瓷航模的加工方法
技术领域
本发明涉及一种用于航模展览的陶瓷航模的加工方法。
背景技术
从1996年开始，中国航模爱好者队伍开始以每年30％的速度迅速增长，也推动了中国航模产业的发展。1994年国内能买到的最便宜的航模是4000元的进口产品，如今同样质量的国产产品只要1000元。价格的大幅回落意味着玩航模的门槛大大降低，消费人群的激增和可预见的市场潜力似乎预示着一项朝阳产业的诞生。因此航模展览会也应运而生，在展览过程中就需要相应的陶瓷制品作为宣传手段，但现有陶瓷航模上釉后在烧制的过程中存在机翼经过高温烧制后会变折甚至断裂的问题，从而影响了产品的最终成型，大大增加了陶瓷飞机模型的烧制难度，成品率极低。
发明内容
本发明要解决陶瓷航模上釉后在烧制的过程中存在机翼经过高温烧制后会变折甚至断裂，同时陶瓷航模在平时易受到氧化的问题，而提供了一种用于航模展览的陶瓷航模的加工方法。
本发明一种用于航模展览的陶瓷航模的加工方法是通过以下步骤进行的：
一、按照所需尺寸设计模具，得到航模模具；
二、将SiC粉体加入到无水乙醇中，然后再加入分散剂PEI，超声处理90min，得到混合液；所述SiC粉体的粒径为50nm～500nm；
三、球磨：将步骤二得到的混合液倒入聚四氟乙烯球磨罐中进行球磨，以WC球为磨球，球磨转速为300r/min，球磨时间为16h，得到浆料；
四、干燥：将步骤三得到的浆料采用旋转干燥仪进行真空旋转干燥，转速为60r/min～150r/min，干燥温度为80℃～100℃，得到干燥的粉体；
五、热压烧结：将步骤四中得到的干燥的粉体研磨过400目筛后，装入步骤一得到的航模模具中，在烧结温度为1400℃～1600℃、烧结压力为20MPa～40MPa的条件下采用真空热压烧结炉热压烧结1h～3h，得到热压烧结后的陶瓷航模；
六、将热压烧结后的陶瓷航模冷却至室温，然后上釉，将釉水全部覆盖于热压烧结后的陶瓷航模的表面，得到上釉后的陶瓷航模；将上釉后的陶瓷航模的机身底部的釉水抹净，将上釉后的陶瓷航模的左右两机翼底部分别设置一个支撑架体，然后送入窑内进行釉烧，釉烧完成后得到陶瓷航模。
本发明的有益效果在于：
本发明加工方法新颖、操作简单、大大降低烧制难度、成品率高的特点。本发明通过粉末烧结，粉体的表面能是烧结过程中的重要驱动力，粉体粒径的减小使其表面能增大，从而导致烧结驱动力的增大，使得烧结致密化过程更加容易进行，可以实现在低温下制备超高温的陶瓷航模，有利于材料性能的提升。使得在航模展览的过程中不易受损。
具体实施方式
具体实施方式一：本实施方式一种用于航模展览的陶瓷航模的加工方法是通过以下步骤进行的：
一、按照所需尺寸设计模具，得到航模模具；
二、将SiC粉体加入到无水乙醇中，然后再加入分散剂PEI，超声处理90min，得到混合液；所述SiC粉体的粒径为50nm～500nm；
三、球磨：将步骤二得到的混合液倒入聚四氟乙烯球磨罐中进行球磨，以WC球为磨球，球磨转速为300r/min，球磨时间为16h，得到浆料；
四、干燥：将步骤三得到的浆料采用旋转干燥仪进行真空旋转干燥，转速为60r/min～150r/min，干燥温度为80℃～100℃，得到干燥的粉体；
五、热压烧结：将步骤四中得到的干燥的粉体研磨过400目筛后，装入步骤一得到的航模模具中，在烧结温度为1400℃～1600℃、烧结压力为20MPa～40MPa的条件下采用真空热压烧结炉热压烧结1h～3h，得到热压烧结后的陶瓷航模；
六、将热压烧结后的陶瓷航模冷却至室温，然后上釉，将釉水全部覆盖于热压烧结后的陶瓷航模的表面，得到上釉后的陶瓷航模；将上釉后的陶瓷航模的机身底部的釉水抹净，将上釉后的陶瓷航模的左右两机翼底部分别设置一个支撑架体，然后送入窑内进行釉烧，釉烧完成后得到陶瓷航模。
本实施方式所述釉烧工序完成后，支撑架体与陶瓷航模的机翼底部并不会粘结在一起，在高温釉烧的过程中，支撑架体在高温釉烧的环境中并不会熔化，因此机翼在支撑架体的全程支撑作用下并不会折断，从而大大提高陶瓷飞机模型的釉烧成功率。
具体实施方式二：本实施方式与具体实施方式一不同的是：步骤一中所述SiC粉体的粒径为300nm。其他与具体实施方式一相同。
具体实施方式三：本实施方式与具体实施方式一或二不同的是：步骤四中所述转速为100r/min。其他与具体实施方式一或二相同。
具体实施方式四：本实施方式与具体实施方式一至三之一不同的是：步骤四中所述干燥温度为95℃。其他与具体实施方式一至三之一相同。
具体实施方式五：本实施方式与具体实施方式一至四之一不同的是：步骤六中所述釉烧的温度为1200℃。其他与具体实施方式一至四之一相同。
具体实施方式六：本实施方式与具体实施方式一至五之一不同的是：步骤六中所述支撑架体为高温耐火材料。其他与具体实施方式一至五之一相同。
具体实施方式七：本实施方式与具体实施方式一至六之一不同的是：步骤六中所述支撑架体设置在两侧机翼靠近尾端的四分之一处。其他与具体实施方式一至六之一相同。
通过以下实施例验证本发明的有益效果：
实施例一：一种用于航模展览的陶瓷航模的加工方法是通过以下步骤进行的：
一、按照所需尺寸设计模具，得到航模模具；
二、将SiC粉体加入到无水乙醇中，然后再加入分散剂PEI，超声处理90min，得到混合液；所述SiC粉体的粒径为200nm；
三、球磨：将步骤二得到的混合液倒入聚四氟乙烯球磨罐中进行球磨，以WC球为磨球，球磨转速为300r/min，球磨时间为16h，得到浆料；
四、干燥：将步骤三得到的浆料采用旋转干燥仪进行真空旋转干燥，转速为100r/min，干燥温度为100℃，得到干燥的粉体；
五、热压烧结：将步骤四中得到的干燥的粉体研磨过400目筛后，装入步骤一得到的航模模具中，在烧结温度为1400℃、烧结压力为20MPa的条件下采用真空热压烧结炉热压烧结2h，得到热压烧结后的陶瓷航模；
六、将热压烧结后的陶瓷航模冷却至室温，然后上釉，将釉水全部覆盖于热压烧结后的陶瓷航模的表面，得到上釉后的陶瓷航模；将上釉后的陶瓷航模的机身底部的釉水抹净，将上釉后的陶瓷航模的左右两机翼底部分别设置一个支撑架体，然后送入窑内进行釉烧，釉烧完成后得到陶瓷航模。
本实施例加工方法新颖、操作简单、大大降低烧制难度、成品率高的特点。本实施例通过粉末烧结，粉体的表面能是烧结过程中的重要驱动力，粉体粒径的减小使其表面能增大，从而导致烧结驱动力的增大，使得烧结致密化过程更加容易进行，可以实现在低温下制备超高温的陶瓷航模，有利于材料性能的提升。使得在航模展览的过程中不易受损。

Claims (7)

1.一种用于航模展览的陶瓷航模的加工方法，其特征在于用于航模展览的陶瓷航模的加工方法是通过以下步骤进行的：
一、按照所需尺寸设计模具，得到航模模具；
二、将SiC粉体加入到无水乙醇中，然后再加入分散剂PEI，超声处理90min，得到混合液；所述SiC粉体的粒径为50nm～500nm；
三、球磨：将步骤二得到的混合液倒入聚四氟乙烯球磨罐中进行球磨，以WC球为磨球，球磨转速为300r/min，球磨时间为16h，得到浆料；
四、干燥：将步骤三得到的浆料采用旋转干燥仪进行真空旋转干燥，转速为60r/min～150r/min，干燥温度为80℃～100℃，得到干燥的粉体；
五、热压烧结：将步骤四中得到的干燥的粉体研磨过400目筛后，装入步骤一得到的航模模具中，在烧结温度为1400℃～1600℃、烧结压力为20MPa～40MPa的条件下采用真空热压烧结炉热压烧结1h～3h，得到热压烧结后的陶瓷航模；
六、将热压烧结后的陶瓷航模冷却至室温，然后上釉，将釉水全部覆盖于热压烧结后的陶瓷航模的表面，得到上釉后的陶瓷航模；将上釉后的陶瓷航模的机身底部的釉水抹净，将上釉后的陶瓷航模的左右两机翼底部分别设置一个支撑架体，然后送入窑内进行釉烧，釉烧完成后得到陶瓷航模。
2.根据权利要求1所述的一种用于航模展览的陶瓷航模的加工方法，其特征在于步骤一中所述SiC粉体的粒径为300nm。
3.根据权利要求1所述的一种用于航模展览的陶瓷航模的加工方法，其特征在于步骤四中所述转速为100r/min。
4.根据权利要求1所述的一种用于航模展览的陶瓷航模的加工方法，其特征在于步骤四中所述干燥温度为95℃。
5.根据权利要求1所述的一种用于航模展览的陶瓷航模的加工方法，其特征在于步骤六中所述釉烧的温度为1200℃。
6.根据权利要求1所述的一种用于航模展览的陶瓷航模的加工方法，其特征在于步骤六中所述支撑架体为高温耐火材料。
7.根据权利要求1所述的一种用于航模展览的陶瓷航模的加工方法，其特征在于步骤六中所述支撑架体设置在两侧机翼靠近尾端的四分之一处。
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