CN105482329A - Distearoyl isopropoxy aluminate aid - Google Patents
Distearoyl isopropoxy aluminate aid Download PDFInfo
- Publication number
- CN105482329A CN105482329A CN201510861271.0A CN201510861271A CN105482329A CN 105482329 A CN105482329 A CN 105482329A CN 201510861271 A CN201510861271 A CN 201510861271A CN 105482329 A CN105482329 A CN 105482329A
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- Prior art keywords
- parts
- acid esters
- aluminum isopropoxide
- ethanol
- distearyl acyl
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L29/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers
- C08L29/14—Homopolymers or copolymers of acetals or ketals obtained by polymerisation of unsaturated acetals or ketals or by after-treatment of polymers of unsaturated alcohols
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L33/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- C08L33/02—Homopolymers or copolymers of acids; Metal or ammonium salts thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L93/00—Compositions of natural resins; Compositions of derivatives thereof
- C08L93/04—Rosin
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Paints Or Removers (AREA)
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Abstract
An distearoyl isopropoxy aluminate aid comprises 15-28 parts of distearoyl isopropoxy aluminate, 5-6 parts of aminoethyl-alanyl-propyl-methyl-methoxysilane, 5-8 parts of dipropylene glycol mono-n-butyl ether, 3-8 parts of pentaerythritol rosin europium resin, 25-30 parts of cocoanut fatty acid diethanolamide, 5-8 parts of sodium carbonate, 3-5 parts of a sodium acrylate-4-vinyl pyridine copolymer, 10-12 parts of di-n-octyltin oxide, 3-5 parts of polyvinyl acetal resin, 3-5 parts of lauryl dimethyl benzyl ammonium bromide, 20-30 parts of ethanol and 350-400 parts of water, and has the advantages that raw materials are easily obtained, cost production is low, effects are significant, and the like.
Description
Technical field
The invention belongs to a kind of functional agent producing non-metallic powder.
Background technology
At present, calcium carbonate is widely used in papermaking, plastics, plastics film, chemical fibre, rubber, tackiness agent, sealing agent, daily-use chemical industry, makeup, building materials, coating, paint, ink, putty, sealing wax, putty, carpet veneer is packed, medicine, food is (as chewing gum, chocolate), in feed, its effect has: increase small product size, reduce costs, improve processing characteristics (as adjusting viscosity, rheological property, curability), improve dimensional stability, reinforcement or half reinforcement, improve printing performance, improve physicals (as thermotolerance, extinction, wear resistance, flame retardant resistance, whiteness, glossiness) etc., for obtaining more superior performance, auxiliary agent is all adopted to carry out activation treatment.
Summary of the invention
The object of the invention is to; A kind of distearyl acyl-oxygen aluminum isopropoxide acid esters auxiliary agent and preparation method thereof is proposed.
Distearyl acyl-oxygen aluminum isopropoxide acid esters auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by distearyl acyl-oxygen aluminum isopropoxide acid esters 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms.
The preparation method of distearyl acyl-oxygen aluminum isopropoxide acid esters auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by distearyl acyl-oxygen aluminum isopropoxide acid esters 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
The present invention compared with prior art its beneficial effect is: have design science reasonable, and technique is simple, safe reliability, is easy to control, easy to operate, is applicable to scale operation, the advantages such as production cost is low.
Embodiment
Below in conjunction with embodiment, the invention will be further described, but embodiments of the present invention are not limited thereto.
All raw materials of the present invention can buy acquisition.
Embodiment 1, the preparation of distearyl acyl-oxygen aluminum isopropoxide acid esters auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by distearyl acyl-oxygen aluminum isopropoxide acid esters 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 2, the preparation of distearyl acyl-oxygen aluminum isopropoxide acid esters auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by distearyl acyl-oxygen aluminum isopropoxide acid esters 15 parts, aminoethyl third aminopropyltriethoxy methoxy silane 5 parts, Dipropylene glycol mono-n-butyl Ether 5 parts, rosin pentaerythritol ester europium resin 3 parts, cocoanut fatty acid diethanolamide 25 parts, 5 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 3 parts, di-n-octyltin oxide 10 parts, polyvinyl acetal resin 3 parts, dodecyl dimethyl benzyl ammonium bromide 3 parts, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 3, the preparation of distearyl acyl-oxygen aluminum isopropoxide acid esters auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by distearyl acyl-oxygen aluminum isopropoxide acid esters 28 parts, aminoethyl third aminopropyltriethoxy methoxy silane 6 parts, Dipropylene glycol mono-n-butyl Ether 8 parts, rosin pentaerythritol ester europium resin 8 parts, cocoanut fatty acid diethanolamide 30 parts, 8 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 5 parts, di-n-octyltin oxide 12 parts, polyvinyl acetal resin 5 parts, dodecyl dimethyl benzyl ammonium bromide 5 parts, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 4, the preparation of distearyl acyl-oxygen aluminum isopropoxide acid esters auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by distearyl acyl-oxygen aluminum isopropoxide acid esters 28 parts, aminoethyl third aminopropyltriethoxy methoxy silane 5 parts, Dipropylene glycol mono-n-butyl Ether 8 parts, rosin pentaerythritol ester europium resin 3 parts, cocoanut fatty acid diethanolamide 30 parts, 5 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 5 parts, di-n-octyltin oxide 10 parts, polyvinyl acetal resin 5 parts, dodecyl dimethyl benzyl ammonium bromide 3 parts, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Product of the present invention, uses through production firm, and produce modified superfine water-ground limestone functional product, reaction effect is fine.
Part material illustrates:
1, described rosin pentaerythritol ester europium resin, the method that can be preferably ZL201410078259.8 by the Chinese patent patent No. obtains.
2, aminoethyl third aminopropyltriethoxy methoxy silane, embodiment Nanjing Xu Yang Chemical Co., Ltd. product, trade(brand)name: precoated sand highly efficient intensifying agent silicon XY-812.
3, distearyl acyl-oxygen aluminum isopropoxide acid esters, English name: Distearoylisopropoxyaluminate.
Claims (2)
1. a distearyl acyl-oxygen aluminum isopropoxide acid esters auxiliary agent, it is characterized in that: by weight, its formula is by distearyl acyl-oxygen aluminum isopropoxide acid esters 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms.
2. the preparation method of a distearyl acyl-oxygen aluminum isopropoxide acid esters auxiliary agent, it is characterized in that: by weight, its formula is by distearyl acyl-oxygen aluminum isopropoxide acid esters 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510861271.0A CN105482329A (en) | 2015-11-26 | 2015-11-26 | Distearoyl isopropoxy aluminate aid |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510861271.0A CN105482329A (en) | 2015-11-26 | 2015-11-26 | Distearoyl isopropoxy aluminate aid |
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| CN105482329A true CN105482329A (en) | 2016-04-13 |
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| CN201510861271.0A Pending CN105482329A (en) | 2015-11-26 | 2015-11-26 | Distearoyl isopropoxy aluminate aid |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114524959A (en) * | 2022-04-14 | 2022-05-24 | 安徽大学 | Ceramic nano-cellulose reinforced full-biodegradable material composite membrane and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103820032A (en) * | 2014-03-05 | 2014-05-28 | 张雅静 | Preparation method of pentaerythrite colophony europium resin |
| CN104403246A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Ultrafine calcium carbonate powder acetal modifier |
-
2015
- 2015-11-26 CN CN201510861271.0A patent/CN105482329A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103820032A (en) * | 2014-03-05 | 2014-05-28 | 张雅静 | Preparation method of pentaerythrite colophony europium resin |
| CN104403246A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Ultrafine calcium carbonate powder acetal modifier |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114524959A (en) * | 2022-04-14 | 2022-05-24 | 安徽大学 | Ceramic nano-cellulose reinforced full-biodegradable material composite membrane and preparation method thereof |
| CN114524959B (en) * | 2022-04-14 | 2024-01-30 | 安徽大学 | Ceramic nanocellulose reinforced full-biodegradable material composite membrane and preparation method thereof |
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Application publication date: 20160413 |
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