CN105331146A - Aminohexylaminomethyltriethoxy silane assistant agent - Google Patents
Aminohexylaminomethyltriethoxy silane assistant agent Download PDFInfo
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- CN105331146A CN105331146A CN201510866297.4A CN201510866297A CN105331146A CN 105331146 A CN105331146 A CN 105331146A CN 201510866297 A CN201510866297 A CN 201510866297A CN 105331146 A CN105331146 A CN 105331146A
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- silane
- resin
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- triethoxyl silane
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Abstract
The invention discloses an aminohexylaminomethyltriethoxy silane assistant agent. The agent is prepared from 15-28 parts of aminohexylaminomethyltriethoxy silane, 5-6 parts of aminoethyl-aminopropylmethylbimethoxy silane, 5-8 parts of dipropylene glycol, 3-8 parts of pentaerythritol rosin europium resin, 25-30 parts of coconut oil fatty acid diethanolamide, 5-8 parts of sodium carbonate, 3-5 parts of sodium acrylate-4-vinyl pyridine copolymer, 10-12 parts of di-n-octyltin oxide, 3-5 parts of polyvinyl acetal resin, 3-5 parts of dodecyl dimethyl benzyl ammonium bromide, 20-30 parts of alcohol and 350-400 parts of water. The agent has the advantages of being suitable for large-scale production, low in production cost and the like.
Description
Technical field
The invention belongs to a kind of functional agent producing non-metallic powder.
Background technology
At present, calcium carbonate is widely used in papermaking, plastics, plastics film, chemical fibre, rubber, tackiness agent, sealing agent, daily-use chemical industry, makeup, building materials, coating, paint, ink, putty, sealing wax, putty, carpet veneer is packed, medicine, food is (as chewing gum, chocolate), in feed, its effect has: increase small product size, reduce costs, improve processing characteristics (as adjusting viscosity, rheological property, curability), improve dimensional stability, reinforcement or half reinforcement, improve printing performance, improve physicals (as thermotolerance, extinction, wear resistance, flame retardant resistance, whiteness, glossiness) etc., for obtaining more superior performance, auxiliary agent is all adopted to carry out activation treatment.
Summary of the invention
The object of the invention is to; A kind of hexanediamine ylmethyl triethoxyl silane auxiliary agent and preparation method thereof is proposed.
Hexanediamine ylmethyl triethoxyl silane auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by hexanediamine ylmethyl triethoxyl silane 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms.
The preparation method of hexanediamine ylmethyl triethoxyl silane auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by hexanediamine ylmethyl triethoxyl silane 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
The present invention compared with prior art its beneficial effect is: have design science reasonable, and technique is simple, safe reliability, is easy to control, easy to operate, is applicable to scale operation, the advantages such as production cost is low.
Embodiment
Below in conjunction with embodiment, the invention will be further described, but embodiments of the present invention are not limited thereto.
All raw materials of the present invention can buy acquisition.
Embodiment 1, the preparation of hexanediamine ylmethyl triethoxyl silane auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by hexanediamine ylmethyl triethoxyl silane 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 2, the preparation of hexanediamine ylmethyl triethoxyl silane auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by hexanediamine ylmethyl triethoxyl silane 15 parts, aminoethyl third aminopropyltriethoxy methoxy silane 5 parts, Dipropylene glycol mono-n-butyl Ether 5 parts, rosin pentaerythritol ester europium resin 3 parts, cocoanut fatty acid diethanolamide 25 parts, 5 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 3 parts, di-n-octyltin oxide 10 parts, polyvinyl acetal resin 3 parts, dodecyl dimethyl benzyl ammonium bromide 3 parts, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 3, the preparation of hexanediamine ylmethyl triethoxyl silane auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by hexanediamine ylmethyl triethoxyl silane 28 parts, aminoethyl third aminopropyltriethoxy methoxy silane 6 parts, Dipropylene glycol mono-n-butyl Ether 8 parts, rosin pentaerythritol ester europium resin 8 parts, cocoanut fatty acid diethanolamide 30 parts, 8 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 5 parts, di-n-octyltin oxide 12 parts, polyvinyl acetal resin 5 parts, dodecyl dimethyl benzyl ammonium bromide 5 parts, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 4, the preparation of hexanediamine ylmethyl triethoxyl silane auxiliary agent of the present invention, it is characterized in that: by weight, its formula is by hexanediamine ylmethyl triethoxyl silane 28 parts, aminoethyl third aminopropyltriethoxy methoxy silane 5 parts, Dipropylene glycol mono-n-butyl Ether 8 parts, rosin pentaerythritol ester europium resin 3 parts, cocoanut fatty acid diethanolamide 30 parts, 5 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 5 parts, di-n-octyltin oxide 10 parts, polyvinyl acetal resin 5 parts, dodecyl dimethyl benzyl ammonium bromide 3 parts, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Product of the present invention, uses through production firm, and produce modified superfine water-ground limestone functional product, reaction effect is fine.
Part material illustrates:
1, described rosin pentaerythritol ester europium resin, the method that can be preferably ZL201410078259.8 by the Chinese patent patent No. obtains.
2, aminoethyl third aminopropyltriethoxy methoxy silane, embodiment Nanjing Xu Yang Chemical Co., Ltd. product, trade(brand)name: precoated sand highly efficient intensifying agent silicon XY-812.
3, hexanediamine ylmethyl triethoxyl silane, molecular formula: NH
2(CH
2)
6nHCH
2si (OC
2h
5)
3.
Claims (2)
1. a hexanediamine ylmethyl triethoxyl silane auxiliary agent, it is characterized in that: by weight, its formula is by hexanediamine ylmethyl triethoxyl silane 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms.
2. the preparation method of a hexanediamine ylmethyl triethoxyl silane auxiliary agent, it is characterized in that: by weight, its formula is by hexanediamine ylmethyl triethoxyl silane 15-28 part, aminoethyl third aminopropyltriethoxy methoxy silane 5-6 part, Dipropylene glycol mono-n-butyl Ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 350-400 part forms, first with ethanol by rosin europium resin dissolves, after adding water 350-400 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510866297.4A CN105331146A (en) | 2015-11-29 | 2015-11-29 | Aminohexylaminomethyltriethoxy silane assistant agent |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510866297.4A CN105331146A (en) | 2015-11-29 | 2015-11-29 | Aminohexylaminomethyltriethoxy silane assistant agent |
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| CN105331146A true CN105331146A (en) | 2016-02-17 |
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|---|---|---|---|
| CN201510866297.4A Pending CN105331146A (en) | 2015-11-29 | 2015-11-29 | Aminohexylaminomethyltriethoxy silane assistant agent |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101134852A (en) * | 2007-10-15 | 2008-03-05 | 江苏河海纳米科技股份有限公司 | Inorganic powder organic surface modifying method |
| CN101921446A (en) * | 2010-08-30 | 2010-12-22 | 佛山安亿纳米材料有限公司 | Master batch and preparation method thereof |
| CN103820032A (en) * | 2014-03-05 | 2014-05-28 | 张雅静 | Preparation method of pentaerythrite colophony europium resin |
| CN104371376A (en) * | 2014-10-31 | 2015-02-25 | 陈显鹏 | Glycidol ether superfine calcium carbonate powder assistant |
| CN104403266A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Amino resin-containing calcium carbonate powder modifier |
| CN104403246A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Ultrafine calcium carbonate powder acetal modifier |
| CN104403367A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Calcium carbonate gamma-aminopropyl triethoxy silane modifier |
| CN104479412A (en) * | 2014-11-26 | 2015-04-01 | 甘振辉 | Preparation method of polydimethyl siloxane ground limestone superfine powder |
-
2015
- 2015-11-29 CN CN201510866297.4A patent/CN105331146A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101134852A (en) * | 2007-10-15 | 2008-03-05 | 江苏河海纳米科技股份有限公司 | Inorganic powder organic surface modifying method |
| CN101921446A (en) * | 2010-08-30 | 2010-12-22 | 佛山安亿纳米材料有限公司 | Master batch and preparation method thereof |
| CN103820032A (en) * | 2014-03-05 | 2014-05-28 | 张雅静 | Preparation method of pentaerythrite colophony europium resin |
| CN104371376A (en) * | 2014-10-31 | 2015-02-25 | 陈显鹏 | Glycidol ether superfine calcium carbonate powder assistant |
| CN104403266A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Amino resin-containing calcium carbonate powder modifier |
| CN104403246A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Ultrafine calcium carbonate powder acetal modifier |
| CN104403367A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Calcium carbonate gamma-aminopropyl triethoxy silane modifier |
| CN104479412A (en) * | 2014-11-26 | 2015-04-01 | 甘振辉 | Preparation method of polydimethyl siloxane ground limestone superfine powder |
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Application publication date: 20160217 |