CN105462446A - Door UV-curable paint and preparation method thereof - Google Patents

Door UV-curable paint and preparation method thereof Download PDF

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Publication number
CN105462446A
CN105462446A CN201510837049.7A CN201510837049A CN105462446A CN 105462446 A CN105462446 A CN 105462446A CN 201510837049 A CN201510837049 A CN 201510837049A CN 105462446 A CN105462446 A CN 105462446A
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CN
China
Prior art keywords
parts
acrylic resin
mill base
prescription
filling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510837049.7A
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Chinese (zh)
Inventor
叶德志
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Jdl Door Industry Co Ltd
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Anhui Jdl Door Industry Co Ltd
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Filing date
Publication date
Application filed by Anhui Jdl Door Industry Co Ltd filed Critical Anhui Jdl Door Industry Co Ltd
Priority to CN201510837049.7A priority Critical patent/CN105462446A/en
Publication of CN105462446A publication Critical patent/CN105462446A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • C09D163/10Epoxy resins modified by unsaturated compounds
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/61Additives non-macromolecular inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/60Additives non-macromolecular
    • C09D7/63Additives non-macromolecular organic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

A door UV-curable paint is composed of the following components by weight: 50-70 parts of epoxy acrylic resin, 5-12 parts of acrylic resin, 8-15 parts of urea formaldehyde resin, 15-20 parts of a non floating type aluminum powder, 1-2 parts of 2,4,6-trimethylbenzoyl-diphenyl phosphine oxide, 3-6 parts of dimethyl silicone oil, 1-2 parts of p-methylbenzene sulfonic acid, 2-4 parts of calcium naphthenate, 3-4 parts of lithopone, 5-8 parts of bentonite, 2-5 parts of dioctyl stearate, 15-20 parts of xylene, 4-5 parts of butyl acetate, 10-15 parts of a 200# solvent oil, and 2-8 parts of butanol. The preparation method has the advantages of simple process, fast curing speed, strong product adhesion power, and aging resistance.

Description

A kind of door ultraviolet-cured paint and preparation method thereof
Technical field
The present invention relates to technical field of coatings, particularly a kind of door ultraviolet-cured paint and preparation method thereof.
Background technology
In current door processing industry, the technique for the paint of door external coating is more complicated, and curing speed is slow, and production difficulty is high, surface effect and sticking power poor.
For the problems referred to above, the invention provides a kind of door ultraviolet-cured paint and preparation method thereof, technique is simple, and curing speed is fast, and product strong adhesion is ageing-resistant.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of door ultraviolet-cured paint and preparation method thereof.Effectively can solving existing door, to paint technical recipe more complicated, and curing speed is slow, and production difficulty is high, surface effect and the poor problem of sticking power.
Epoxy acrylic resin 50-70 part, acrylic resin 5-12 part, urea-formaldehyde resin 8-15 part, non-floating type aluminium powder 15-20 part, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 1-2 part, dimethyl silicone oil 3-6 part, p-methyl benzenesulfonic acid 1-2 part, calcium naphthenate 2-4 part, zinc sulfide white 3-4 part, wilkinite 5-8 part, stearic acid dioctyl ester 2-5 part, dimethylbenzene 15-20 part, butylacetate 4-5 part, 200# solvent oil 10-15 part, butanols 2-8 part.
Further, described door ultraviolet-cured paint also comprises color material 1-3 part.
Present invention also offers the preparation method of described door ultraviolet-cured paint:
1. take wilkinite and dimethylbenzene by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. take by filling a prescription 50% of epoxy acrylic resin liquid measure, 50% of 50% of acrylic resin liquid measure and urea-formaldehyde resin liquid measure, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, control grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with by residual epoxide acrylic resin, acrylic resin and the urea-formaldehyde resin taken of filling a prescription, the mill base in shredder is ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
Beneficial effect of the present invention is, provides a kind of door ultraviolet-cured paint and preparation method thereof, and technique is simple, and curing speed is fast, and product strong adhesion is ageing-resistant.
Embodiment
Be further described the specific embodiment of the present invention below in conjunction with embodiment, following examples only for technical scheme of the present invention is clearly described, and can not limit the scope of the invention with this.
Embodiment 1
The concrete technical scheme of the present invention is as follows:
A kind of door ultraviolet-cured paint, it is characterized in that, by weight, it is made up of following component:
Epoxy acrylic resin 55 parts, acrylic resin 10 parts, urea-formaldehyde resin 13 parts, non-floating type aluminium powder 19 parts, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 1 part, dimethyl silicone oil 5 parts, p-methyl benzenesulfonic acid 1 part, calcium naphthenate 3 parts, 4 parts, zinc sulfide white, wilkinite 6 parts, stearic acid dioctyl ester 4 parts, dimethylbenzene 13 parts, butylacetate 4 parts, 200# solvent oil 13 parts, 6 parts, butanols.
Present invention also offers the preparation method of described door ultraviolet-cured paint:
1. take wilkinite and dimethylbenzene by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. take by filling a prescription 50% of epoxy acrylic resin liquid measure, 50% of 50% of acrylic resin liquid measure and urea-formaldehyde resin liquid measure, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, control grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with by residual epoxide acrylic resin, acrylic resin and the urea-formaldehyde resin taken of filling a prescription, the mill base in shredder is ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
Embodiment 2
The concrete technical scheme of the present invention is as follows:
A kind of door ultraviolet-cured paint, it is characterized in that, by weight, it is made up of following component:
Epoxy acrylic resin 50 parts, acrylic resin 5 parts, urea-formaldehyde resin 15 parts, non-floating type aluminium powder 15 parts, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 2 parts, dimethyl silicone oil 3 parts, p-methyl benzenesulfonic acid 1 part, calcium naphthenate 4 parts, 4 parts, zinc sulfide white, wilkinite 5 parts, stearic acid dioctyl ester 2 parts, dimethylbenzene 20 parts, butylacetate 5 parts, 200# solvent oil 15 parts, 2 parts, butanols, 1 part, color material.
Present invention also offers the preparation method of described door ultraviolet-cured paint:
1. take wilkinite and dimethylbenzene by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. take by filling a prescription 50% of epoxy acrylic resin liquid measure, 50% of 50% of acrylic resin liquid measure and urea-formaldehyde resin liquid measure, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, control grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with by residual epoxide acrylic resin, acrylic resin and the urea-formaldehyde resin taken of filling a prescription, the mill base in shredder is ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
Embodiment 3
The concrete technical scheme of the present invention is as follows:
Epoxy acrylic resin 70 parts, acrylic resin 12 parts, urea-formaldehyde resin 8 parts, non-floating type aluminium powder 20 parts, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 1 part, dimethyl silicone oil 6 parts, p-methyl benzenesulfonic acid 2 parts, calcium naphthenate 2 parts, 3 parts, zinc sulfide white, wilkinite 8 parts, stearic acid dioctyl ester 2 parts, dimethylbenzene 15 parts, butylacetate 4 parts, 200# solvent oil 10 parts, 2 parts, butanols, 3 parts, color material.
Present invention also offers the preparation method of described door ultraviolet-cured paint:
1. take wilkinite and dimethylbenzene by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. take by filling a prescription 50% of epoxy acrylic resin liquid measure, 50% of 50% of acrylic resin liquid measure and urea-formaldehyde resin liquid measure, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, control grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with by residual epoxide acrylic resin, acrylic resin and the urea-formaldehyde resin taken of filling a prescription, the mill base in shredder is ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
The above is only preferred embodiments of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the technology of the present invention principle; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.

Claims (3)

1. a door ultraviolet-cured paint, is characterized in that, by weight, it is made up of following component:
Epoxy acrylic resin 50-70 part, acrylic resin 5-12 part, urea-formaldehyde resin 8-15 part, non-floating type aluminium powder 15-20 part, 2; 4,6-trimethylbenzoy-dipheny phosphine oxide 1-2 part, dimethyl silicone oil 3-6 part, p-methyl benzenesulfonic acid 1-2 part, calcium naphthenate 2-4 part, zinc sulfide white 3-4 part, wilkinite 5-8 part, stearic acid dioctyl ester 2-5 part, dimethylbenzene 15-20 part, butylacetate 4-5 part, 200# solvent oil 10-15 part, butanols 2-8 part.
2. a kind of door ultraviolet-cured paint as claimed in claim 1, is characterized in that, describedly also comprises color material 1-3 part.
3. a kind of door ultraviolet-cured paint as claimed in claim 1 or 2, is characterized in that, the preparation method of described door ultraviolet-cured paint is as follows:
1. take wilkinite and dimethylbenzene by formula, at use stirrer moderate-speed mixer 15min after mixing, form native cream;
2. take by filling a prescription 50% of epoxy acrylic resin liquid measure, 50% of 50% of acrylic resin liquid measure and urea-formaldehyde resin liquid measure, mix with the native cream 1. produced to step, add by the non-floating type aluminium powder, the zinc sulfide white and 2 that take of filling a prescription, 4,6-trimethylbenzoy-dipheny phosphine oxide, then stirrer is started, high-speed stirring 15min;
3. the mill base that 2. step produces is added shredder and start grinding, regulate mill base flow, control grinding temperature not higher than 50 DEG C, after fineness reaches 20 μm, with by residual epoxide acrylic resin, acrylic resin and the urea-formaldehyde resin taken of filling a prescription, the mill base in shredder is ejected;
4. mill base step 3. produced is introduced in paint mixing tank and is stirred, and adds by the dimethyl silicone oil taken of filling a prescription, moderate-speed mixer 30min;
5. mill base step 4. produced is introduced in paint mixing tank and is stirred, and then adds by other components taken of filling a prescription, moderate-speed mixer 30min;
6. mill base specification 180 mesh filter screen step 5. produced filters, packaging.
CN201510837049.7A 2015-11-24 2015-11-24 Door UV-curable paint and preparation method thereof Pending CN105462446A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510837049.7A CN105462446A (en) 2015-11-24 2015-11-24 Door UV-curable paint and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201510837049.7A CN105462446A (en) 2015-11-24 2015-11-24 Door UV-curable paint and preparation method thereof

Publications (1)

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CN105462446A true CN105462446A (en) 2016-04-06

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107699111A (en) * 2017-09-11 2018-02-16 南通盛赫园林古建筑工程有限公司 A kind of light curing and anticorrosive agent of timber

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102070981A (en) * 2010-12-02 2011-05-25 广州慧谷化学有限公司 Ultraviolet curing paint and preparation method and application thereof
CN103554403A (en) * 2013-10-30 2014-02-05 刘芳 Aqueous photo-curable amino resin and preparation method
CN104945980A (en) * 2015-06-18 2015-09-30 成都纳硕科技有限公司 Photocurable coating with improved thermal conductivity
CN104945983A (en) * 2015-06-18 2015-09-30 成都纳硕科技有限公司 UV-curable low-shrinkage environment-friendly coating
CN104945981A (en) * 2015-06-18 2015-09-30 成都纳硕科技有限公司 Photo-curing anticorrosive paint for timber

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102070981A (en) * 2010-12-02 2011-05-25 广州慧谷化学有限公司 Ultraviolet curing paint and preparation method and application thereof
CN103554403A (en) * 2013-10-30 2014-02-05 刘芳 Aqueous photo-curable amino resin and preparation method
CN104945980A (en) * 2015-06-18 2015-09-30 成都纳硕科技有限公司 Photocurable coating with improved thermal conductivity
CN104945983A (en) * 2015-06-18 2015-09-30 成都纳硕科技有限公司 UV-curable low-shrinkage environment-friendly coating
CN104945981A (en) * 2015-06-18 2015-09-30 成都纳硕科技有限公司 Photo-curing anticorrosive paint for timber

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107699111A (en) * 2017-09-11 2018-02-16 南通盛赫园林古建筑工程有限公司 A kind of light curing and anticorrosive agent of timber

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Application publication date: 20160406