CN105419841B - Method for preparing jerusalem artichoke alcohol pyrolyzed enteromorpha renewable energy bio-oil - Google Patents
Method for preparing jerusalem artichoke alcohol pyrolyzed enteromorpha renewable energy bio-oil Download PDFInfo
- Publication number
- CN105419841B CN105419841B CN201510877314.4A CN201510877314A CN105419841B CN 105419841 B CN105419841 B CN 105419841B CN 201510877314 A CN201510877314 A CN 201510877314A CN 105419841 B CN105419841 B CN 105419841B
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- CN
- China
- Prior art keywords
- jerusalem artichoke
- alcohol
- oil
- obtains
- entermorpha
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 240000008892 Helianthus tuberosus Species 0.000 title claims abstract description 74
- 235000003230 Helianthus tuberosus Nutrition 0.000 title claims abstract description 74
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 title claims abstract description 44
- 239000012075 bio-oil Substances 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title abstract description 11
- 241000196252 Ulva Species 0.000 title abstract description 5
- 238000000855 fermentation Methods 0.000 claims abstract description 32
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 230000004151 fermentation Effects 0.000 claims abstract description 26
- 239000007788 liquid Substances 0.000 claims abstract description 25
- 238000000197 pyrolysis Methods 0.000 claims abstract description 21
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 19
- 235000019270 ammonium chloride Nutrition 0.000 claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 11
- 238000001914 filtration Methods 0.000 claims abstract description 8
- 239000000843 powder Substances 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 24
- 230000001954 sterilising effect Effects 0.000 claims description 17
- 230000001172 regenerating effect Effects 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 15
- 238000010438 heat treatment Methods 0.000 claims description 13
- 239000000047 product Substances 0.000 claims description 13
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 12
- 239000012153 distilled water Substances 0.000 claims description 12
- 239000000706 filtrate Substances 0.000 claims description 12
- 239000011521 glass Substances 0.000 claims description 12
- 238000009413 insulation Methods 0.000 claims description 11
- 239000000779 smoke Substances 0.000 claims description 11
- 238000007605 air drying Methods 0.000 claims description 9
- 230000007062 hydrolysis Effects 0.000 claims description 9
- 238000006460 hydrolysis reaction Methods 0.000 claims description 9
- 229920001202 Inulin Polymers 0.000 claims description 7
- 238000004821 distillation Methods 0.000 claims description 7
- 230000002255 enzymatic effect Effects 0.000 claims description 7
- 239000012467 final product Substances 0.000 claims description 7
- JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 claims description 7
- 229940029339 inulin Drugs 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 7
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims description 6
- 230000004913 activation Effects 0.000 claims description 6
- 238000001816 cooling Methods 0.000 claims description 6
- 239000008103 glucose Substances 0.000 claims description 6
- 239000004570 mortar (masonry) Substances 0.000 claims description 6
- 229910052757 nitrogen Inorganic materials 0.000 claims description 6
- 238000004806 packaging method and process Methods 0.000 claims description 6
- 239000003755 preservative agent Substances 0.000 claims description 6
- 230000002335 preservative effect Effects 0.000 claims description 6
- 238000010992 reflux Methods 0.000 claims description 6
- 238000004659 sterilization and disinfection Methods 0.000 claims description 6
- 239000000725 suspension Substances 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- 238000000926 separation method Methods 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 241000894006 Bacteria Species 0.000 claims 1
- 239000002994 raw material Substances 0.000 abstract description 8
- 238000009833 condensation Methods 0.000 abstract description 6
- 230000005494 condensation Effects 0.000 abstract description 6
- 239000003183 carcinogenic agent Substances 0.000 abstract description 3
- 108010090785 inulinase Proteins 0.000 abstract description 3
- 238000002485 combustion reaction Methods 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 abstract description 2
- 230000003301 hydrolyzing effect Effects 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 230000001988 toxicity Effects 0.000 abstract 1
- 231100000419 toxicity Toxicity 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 38
- 239000000446 fuel Substances 0.000 description 15
- 235000013339 cereals Nutrition 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 231100001245 air toxic agent Toxicity 0.000 description 4
- 230000000711 cancerogenic effect Effects 0.000 description 4
- 230000003247 decreasing effect Effects 0.000 description 4
- 239000002803 fossil fuel Substances 0.000 description 4
- 238000010348 incorporation Methods 0.000 description 4
- 244000061456 Solanum tuberosum Species 0.000 description 2
- 235000002595 Solanum tuberosum Nutrition 0.000 description 2
- 231100000357 carcinogen Toxicity 0.000 description 2
- 231100000315 carcinogenic Toxicity 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 235000007516 Chrysanthemum Nutrition 0.000 description 1
- 244000189548 Chrysanthemum x morifolium Species 0.000 description 1
- 244000205754 Colocasia esculenta Species 0.000 description 1
- 235000006481 Colocasia esculenta Nutrition 0.000 description 1
- 241000195493 Cryptophyta Species 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000206607 Porphyra umbilicalis Species 0.000 description 1
- 240000006394 Sorghum bicolor Species 0.000 description 1
- 235000007230 Sorghum bicolor Nutrition 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 241000406704 Ulva clathrata Species 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000010775 animal oil Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 235000013379 molasses Nutrition 0.000 description 1
- 239000010413 mother solution Substances 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 230000001473 noxious effect Effects 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- CVHZOJJKTDOEJC-UHFFFAOYSA-N saccharin Chemical compound C1=CC=C2C(=O)NS(=O)(=O)C2=C1 CVHZOJJKTDOEJC-UHFFFAOYSA-N 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 210000000582 semen Anatomy 0.000 description 1
- 235000011888 snacks Nutrition 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/10—Feedstock materials
- C10G2300/1011—Biomass
- C10G2300/1014—Biomass of vegetal origin
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Liquid Carbonaceous Fuels (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510877314.4A CN105419841B (en) | 2015-12-03 | 2015-12-03 | Method for preparing jerusalem artichoke alcohol pyrolyzed enteromorpha renewable energy bio-oil |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510877314.4A CN105419841B (en) | 2015-12-03 | 2015-12-03 | Method for preparing jerusalem artichoke alcohol pyrolyzed enteromorpha renewable energy bio-oil |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105419841A CN105419841A (en) | 2016-03-23 |
CN105419841B true CN105419841B (en) | 2017-02-01 |
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Family Applications (1)
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CN201510877314.4A Active CN105419841B (en) | 2015-12-03 | 2015-12-03 | Method for preparing jerusalem artichoke alcohol pyrolyzed enteromorpha renewable energy bio-oil |
Country Status (1)
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CN (1) | CN105419841B (en) |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2144084C1 (en) * | 1998-11-06 | 2000-01-10 | Московский Государственный Университет пищевых производств | Method of production of ethyl alcohol from jerusalem artichoke |
CN1952163B (en) * | 2006-11-03 | 2011-05-04 | 天津市工业微生物研究所 | Process for preparing ethanol from stem and leaf of jerusalem artichoke |
CA2699406C (en) * | 2007-09-12 | 2019-09-03 | Martek Biosciences Corporation | Biological oils and production and uses thereof |
CN101659874A (en) * | 2009-08-07 | 2010-03-03 | 烟台海岸带可持续发展研究所 | Method for preparing biological oil by thermally cracking Enteromorpha prolifera |
SE534859C2 (en) * | 2010-06-28 | 2012-01-24 | Skandinavisk Kemiinformation Ab | Process for producing fuel from lignocellulosic material |
CN104004582B (en) * | 2014-06-13 | 2016-07-06 | 沈阳航空航天大学 | Lignocellulose biomass prepares the method for bio oil reactant and bio oil |
CN104277857B (en) * | 2014-09-25 | 2016-04-06 | 中国农业大学 | Bio-crude oil prepared by a kind of algae and raw glycerine co grinding method and method |
-
2015
- 2015-12-03 CN CN201510877314.4A patent/CN105419841B/en active Active
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CN105419841A (en) | 2016-03-23 |
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Legal Events
Date | Code | Title | Description |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C41 | Transfer of patent application or patent right or utility model | ||
CB03 | Change of inventor or designer information |
Inventor after: Liu Zhiwei Inventor before: Gao Dayuan Inventor before: Lin Dawei Inventor before: Zhang Fan |
|
COR | Change of bibliographic data | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20161117 Address after: 350200 Fujian city of Changle province Wu Hangxi Town Road No. 5 Building 6 No. 601 Applicant after: Liu Zhiwei Address before: 213164 Jiangsu province Changzhou New District Xinli Garden Building 5 room 1202, unit B Applicant before: Gao Dayuan |
|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CP02 | Change in the address of a patent holder | ||
CP02 | Change in the address of a patent holder |
Address after: No. 36, Baima Industrial Park, Gaogang District, Taizhou City, Jiangsu Province Patentee after: Liu Zhiwei Address before: 350200 Fujian city of Changle province Wu Hangxi Town Road No. 5 Building 6 No. 601 Patentee before: Liu Zhiwei |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20201222 Address after: Room 403-1, No.1 Yanwu street, Tongling Town, Dongshan County, Zhangzhou City, Fujian Province 363401 Patentee after: Zhangzhou kuledo Information Technology Co.,Ltd. Address before: No.36, Baima Town Industrial Park, Gaogang District, Taizhou City, Jiangsu Province Patentee before: Liu Zhiwei |
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TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20240426 Address after: 528000, Room 604, Opel Building, No. 12 Jiangwan 1st Road, Zhangcha Street, Chancheng District, Foshan City, Guangdong Province (Residence Declaration) Patentee after: Foshan Hantu Environmental Protection Technology Co.,Ltd. Country or region after: China Address before: Room 403-1, No.1 Yanwu street, Tongling Town, Dongshan County, Zhangzhou City, Fujian Province 363401 Patentee before: Zhangzhou kuledo Information Technology Co.,Ltd. Country or region before: China |