CN105326676B - A kind of preparation method of microcapsule-type mascara - Google Patents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/736—Chitin; Chitosan; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
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Abstract
The invention discloses a kind of preparation methods of microcapsule-type mascara, first prepare mixed aqueous solution A, the aqueous gelatin solution of Arabic gum and chitosan；Again by black sesame pigment, black rice pigments, microwave treatment, ultrasonication, emulsion dispersion, homogeneous obtain homogenizing fluid successively for acorn nut shell brown pigment, ginseng alcohol extract, avocado oil, beeswax, glycerin monostearate, sodium cellulose glycolate, tween and neopelex, then homogenizing fluid is mixed with mixed aqueous solution A and aqueous gelatin solution and after high speed dispersion, adjust pH to 4.1 ~ 4.9, by the solution after adjusting after 45 ~ 55 DEG C are reacted 15 ~ 25 min, add in propionic aldehyde ultrasonic reaction, and will solution centrifugation after reaction, washing and it is dry after to obtain the final product.The method of the present invention embedding effect is good, and microcapsule-type mascara collaboration obtained has played healthy colour developing, nourished eyelashes, promotes the effect of eyelashes growth, has good market prospects.
Description
Technical field
The invention belongs to microcapsules technology fields, and in particular to a kind of preparation method of microcapsule-type mascara.
Background technology
Mascara is the cosmetics being applied on eyelashes, its role is to which eyelashes is made to seem that dense, fine length, volume are stuck up, is added
The color of deep eyelashes, the eyes allowed after smearing mascara, which seem deep, god.With the improvement of living standards, people are increasingly
Self-image is paid close attention to, mascara receives the concern of more and more people seeking beauties, becomes current necessary cosmetics.
Existing mascara product majority uses color lake or synthetic food color as main color developing agent, however these are aobvious
For toner mostly containing a large amount of heavy metal component, these heavy metal components constitute the potential risk for causing cancer, are added to these
The mascara of heavy metal color developing agent naturally also has certain healthy hidden danger, and serious threat the health of consumer.
With the continuous renewal of mascara product, consumer is also being not that single beautifying functions will to mascara product
It asks, how while eyelashes are beautified, multiple consumption experience is brought to consumer, start to become consumer for eyelashes of new generation
An urgent demand of cream product.
In conclusion how to provide a kind of not only mascara without healthy hidden danger but also with multiple efficacies, become industry
Interior major issue in the urgent need to address.
Invention content
For deficiencies of the prior art, the technical problems to be solved by the invention are：How to provide a kind of micro-
The preparation method of capsule-type mascara, microcapsule-type mascara obtained is enable to have simultaneously, and color developing agent is safe and healthy, nourishes and protects
It supports eyelashes, promote the effect of eyelashes growth.
In order to solve the above-mentioned technical problem, the present invention adopts the following technical scheme that：A kind of preparation of microcapsule-type mascara
Method includes the following steps：
1）After gelatin distilled water is taken to impregnate 1 ~ 2h of swelling, the gelatin that mass concentration is 5 ~ 7% is configured at 60 ~ 75 DEG C
Aqueous solution；
2）Arabic gum and chitosan are taken, distilled water is added in, is dissolved by heating at 50 ~ 65 DEG C, obtain mixed solution A；Wherein,
The mass concentration of Arabic gum is 2 ~ 4% in mixed solution A；
3）Ginseng alcohol extract and avocado oil are weighed, is uniformly mixed, 15 ~ 25s of microwave treatment at 40 ~ 60 DEG C；Wherein, microwave
Power is 550 ~ 780W；
4）To step 3）Natural pigment, beeswax, glycerin monostearate, carboxymethyl are added in mixture after microwave treatment
Sodium cellulosate, tween and neopelex are ultrasonically treated 2 ~ 3 min at 60 ~ 80 DEG C；Wherein, ultrasonic power 300
~450W；
5）To step 4）It is equal using homogenizer after mixture after ultrasound uses 3 ~ 8min of ultrahigh speed dispersion machine emulsion dispersion
Matter 3 times, obtains homogenizing fluid；Wherein, the rotating speed of the dispersion machine is 1500 ~ 2600 r/min, the homogenization pressure of homogenizer for 38 ~
46 MPa；
6）By step 1）Aqueous gelatin solution obtained and step 5）Homogenizing fluid obtained is uniformly mixed, and uses high speed dispersor
After disperseing 3 ~ 6 min, step 2 is added in）Mixed solution A obtained obtains mixed solution B；
7）By step 6）Mixed solution B adjusts pH to 4.1 ~ 4.9, and the solution after adjusting is reacted 15 ~ 25 in 45 ~ 55 DEG C
min；
8）To step 7）20 ~ 28mL propionic aldehyde, 0.5 ~ 1.5h of ultrasonic reaction are added in mixed solution B after reaction；Wherein, surpass
Acoustical power is 350 ~ 500W；
9）By step 8）Solution after reaction centrifuges 5 ~ 10min with the centrifugal speed of 6000 ~ 7000r/min, discards supernatant
Liquid；Water washing and precipitating is simultaneously centrifuged three times with same centrifugal condition, obtains wet microcapsules；
10）By step 9）After -60 ~ -70 DEG C of 28 ~ 32h of pre-freeze, 8 ~ 16h of vacuum freeze drying is obtained obtained wet microcapsules
To the microcapsule-type mascara；
The parts by weight of each raw material are as follows：5 ~ 15 parts of gelatin, 3 ~ 8 parts of chitosan, 4 ~ 10 parts of Arabic gum, Semen sesami nigrum
2 ~ 5 parts of pigment, 1 ~ 3 part of black rice pigments, 0.5 ~ 1.5 part of acorn nut shell brown pigment, 2 ~ 5 parts of ginseng alcohol extract, 5 ~ 10 parts of avocado oil, bee
12 ~ 26 parts of wax, 6 ~ 14 parts of glycerin monostearate, 4 ~ 6 parts of sodium carboxymethylcellulose, 2 ~ 5 parts of tween and dodecyl benzene sulfonic acid
1.5 ~ 3 parts of sodium.
Compared with prior art, the present invention has the advantages that：
1st, the present invention uses natural pigment as color developing agent, using natural materials as active constituent, because of natural materials
Matter is unstable, is easily destroyed by external environment, therefore present invention spy embeds natural materials using microcapsules technology, is protecting
Protect natural materials activity not be destroyed while, also avoid the lipid phase in capsule-core easily air-dry, air-dry after cannot make
With the problem of occur.
2nd, microcapsule-type mascara particle made from the method for the present invention is used as regular spherical shape, and cyst wall has uniform thick
Degree, and with uniform intensity, the problem of perfect spherical shape of microcapsules is not destroyed, capsule-core will not be caused to reveal can be retained, had
Effect ensures to be damaged during product storage, transport, shelf life.
2nd, microcapsule-type mascara produced by the present invention is by embedding natural pigment, natural active matter of the means to capsule-core
It is protected, embedding effect is good, and embedding rate is up to 97%, and capsule-core can be protected not influenced by extraneous undesirable element, be further ensured that
The stability characteristic (quality) of product can experience the work(that active material is brought when ensureing consumer using microcapsule-type mascara of the present invention
Energy.
3rd, the present invention plays colour developing effect by natural pigment, avoids the wound of color lake and synthetic food color to human body
Evil has health efficacy；And the present invention is by black sesame melanin and the collaboration compatibility effect of ginseng alcohol extract, it is micro- to the present invention
Capsule-type mascara, which is brought, promotes eyelashes growth, the effect of preventing deplumation, make eyelashes more pitch-black dense, imparts eyelashes
The new purposes of cream；The present invention more makes microcapsule-type eyelashes of the present invention also by avocado oil and the collaboration compatibility effect of black rice pigments
Cream has both the effect of moist eyelashes, moisturizing eyelashes, and multiple consumption experience is brought to consumer.
4th, the present invention carries more convenient to use compared to existing mascara, during use microcapsules receive squeezing action will
Rupture, and then the natural pigment of capsule-core and active material is made to play effect, it brings beautification eyelashes, nourish the effect of eyelashes.
5th, on the basis of microcapsule-type mascara core materials of the present invention are considered, present invention selection gelatin, shell gather
As cyst material, collaboration plays the embedding effect to capsule-core, has good embedding effect for sugar and Arabic gum；And due to capsule
Wall material gelatin has certain water profit effect, and microcapsule-type mascara of the present invention is caused to have certain moistening.
6th, moreover, the present invention is on the basis of the capsule-core and cyst material property for considering selection, by creating
Property experiment, find only just to make by preparation method of the present invention made from microcapsule-type mascara capsule-core substance it is more equal
Even dispersion can more play the colour developing of collaboration compatibility and active effect, obtain excellent effect.
Specific embodiment
The present invention is described in further detail with reference to embodiment.
In the present invention unless otherwise instructed, raw materials used is commercially available.
Embodiment 1：
Each raw material weight that the present embodiment uses is as follows：50 g gelatin, chitosan 30g, Arabic gum 40g, Semen sesami nigrum color
Plain 20g, black rice pigments 10g, acorn nut shell brown pigment 5g, ginseng alcohol extract 20g, avocado oil 50g, beeswax 120g, monostearate are sweet
Grease 60g, sodium carboxymethylcellulose 40g, Tween-80 20g and neopelex 15g.
The present embodiment microcapsule-type mascara is prepared with the following method：
1）After gelatin distilled water is taken to impregnate swelling 1h, the aqueous gelatin solution that mass concentration is 5% is configured at 60 DEG C；
2）Arabic gum and chitosan are taken, distilled water is added in, is dissolved by heating at 50 DEG C, obtain mixed solution A；Wherein, it mixes
The mass concentration for closing Arabic gum in solution A is 2%；
3）Ginseng alcohol extract and avocado oil are weighed, is uniformly mixed, the microwave treatment 15s at 40 DEG C；Wherein, microwave power is
550W；
4）To step 3）Natural pigment, beeswax, glycerin monostearate, carboxymethyl are added in mixture after microwave treatment
Sodium cellulosate, Tween-80 and neopelex are ultrasonically treated 2 min at 60 DEG C；Wherein, ultrasonic power 300W；
5）To step 4）Mixture after ultrasound uses homogenizer homogeneous using after ultrahigh speed dispersion machine emulsion dispersion 3min
3 times, obtain homogenizing fluid；Wherein, the rotating speed of the dispersion machine is 1500 r/min, and the homogenization pressure of homogenizer is 38 MPa；
6）By step 1）Aqueous gelatin solution obtained and step 5）Homogenizing fluid obtained is uniformly mixed, and uses high speed dispersor
After disperseing 3 min, step 2 is added in）Mixed solution A obtained obtains mixed solution B；
7）By step 6）Mixed solution B adjusts pH to 4.1, and the solution after adjusting is reacted 15min in 45 DEG C；
8）To step 7）20mL propionic aldehyde, ultrasonic reaction 0.5h are added in mixed solution B after reaction；Wherein, ultrasonic power
For 350W；
9）By step 8）Solution after reaction centrifuges 5min with the centrifugal speed of 6000r/min, discards supernatant liquid；Washing is heavy
It forms sediment and is centrifuged three times with same centrifugal condition, obtain wet microcapsules；
10）By step 9）Obtained wet microcapsules are after -60 DEG C of pre-freeze 28h, vacuum freeze drying 8h, obtain micro- glue
Bladder type mascara.
Embodiment 2：
Each raw material weight that the present embodiment uses is as follows：150g gelatin, chitosan 80g, Arabic gum 100g, Semen sesami nigrum color
Plain 50g, black rice pigments 30g, acorn nut shell brown pigment 15g, ginseng alcohol extract 50g, avocado oil 100g, beeswax 180g, monostearate
Glyceride 95g, sodium carboxymethylcellulose 60g, Tween-80 50g and neopelex 30g.
The present embodiment microcapsule-type mascara is prepared with the following method：
1）After gelatin distilled water is taken to impregnate swelling 2h, the aqueous gelatin solution that mass concentration is 7% is configured at 75 DEG C；
2）Arabic gum and chitosan are taken, distilled water is added in, is dissolved by heating at 65 DEG C, obtain mixed solution A；Wherein, it mixes
The mass concentration for closing Arabic gum in solution A is 4%；
3）Ginseng alcohol extract and avocado oil are weighed, is uniformly mixed, the microwave treatment 25s at 60 DEG C；Wherein, microwave power is
780W；
4）To step 3）Natural pigment, beeswax, glycerin monostearate, carboxymethyl are added in mixture after microwave treatment
Sodium cellulosate, Tween-80 and neopelex are ultrasonically treated 3 min at 80 DEG C；Wherein, ultrasonic power 450W；
5）To step 4）Mixture after ultrasound uses homogenizer homogeneous using after ultrahigh speed dispersion machine emulsion dispersion 8min
3 times, obtain homogenizing fluid；Wherein, the rotating speed of the dispersion machine is 2600 r/min, and the homogenization pressure of homogenizer is 46 MPa；
6）By step 1）Aqueous gelatin solution obtained and step 5）Homogenizing fluid obtained is uniformly mixed, and uses high speed dispersor
After disperseing 6 min, step 2 is added in）Mixed solution A obtained obtains mixed solution B；
7）By step 6）Mixed solution B adjusts pH to 4.9, and the solution after adjusting is reacted 25min in 55 DEG C；
8）To step 7）28mL propionic aldehyde, ultrasonic reaction 1.5h are added in mixed solution B after reaction；Wherein, ultrasonic power
For 500W；
9）By step 8）Solution after reaction centrifuges 10min with the centrifugal speed of 7000r/min, discards supernatant liquid；Washing
It precipitates and is centrifuged three times with same centrifugal condition, obtain wet microcapsules；
10）By step 9）Obtained wet microcapsules are after -70 DEG C of pre-freeze 32h, vacuum freeze drying 16h, obtain described micro-
Capsule-type mascara.
Embodiment 3：
Each raw material weight that the present embodiment uses is as follows：60g gelatin, chitosan 45g, Arabic gum 55g, black sesame pigment
40 g, black rice pigments 20g, 10 g of acorn nut shell brown pigment, ginseng alcohol extract 30g, avocado oil 60g, beeswax 260g, monostearate are sweet
Grease 140g, sodium carboxymethylcellulose 40g, polysorbas20 g and neopelex 20g.
The present embodiment microcapsule-type mascara is prepared with the following method：
1）After gelatin distilled water is taken to impregnate swelling 1.5h, it is water-soluble that the gelatin that mass concentration is 6% is configured at 68 DEG C
Liquid；
2）Arabic gum and chitosan are taken, distilled water is added in, is dissolved by heating at 58 DEG C, obtain mixed solution A；Wherein, it mixes
The mass concentration for closing Arabic gum in solution A is 3%；
3）Ginseng alcohol extract and avocado oil are weighed, is uniformly mixed, the microwave treatment 20s at 50 DEG C；Wherein, microwave power is
650 W；
4）To step 3）Natural pigment, beeswax, glycerin monostearate, carboxymethyl are added in mixture after microwave treatment
Sodium cellulosate, tween and neopelex are ultrasonically treated 3 min at 70 DEG C；Wherein, ultrasonic power is 380 W；
5）To step 4）Mixture after ultrasound uses homogenizer homogeneous using after ultrahigh speed dispersion machine emulsion dispersion 5min
3 times, obtain homogenizing fluid；Wherein, the rotating speed of the dispersion machine is 2200 r/min, and the homogenization pressure of homogenizer is 42 MPa；
6）By step 1）Aqueous gelatin solution obtained and step 5）Homogenizing fluid obtained is uniformly mixed, and uses high speed dispersor
After disperseing 5 min, step 2 is added in）Mixed solution A obtained obtains mixed solution B；
7）By step 6）Mixed solution B adjusts pH to 4.5, and the solution after adjusting is reacted 18min in 52 DEG C；
8）To step 7）25mL propionic aldehyde, ultrasonic reaction 1h are added in mixed solution B after reaction；Wherein, ultrasonic power is
400W；
9）By step 8）Solution after reaction centrifuges 10min with the centrifugal speed of 6500r/min, discards supernatant liquid；Washing
It precipitates and is centrifuged three times with same centrifugal condition, obtain wet microcapsules；
10）By step 9）Obtained wet microcapsules are after -70 DEG C of pre-freeze 30h, vacuum freeze drying 14h, obtain described micro-
Capsule-type mascara.
It is measured by experiment, 1 microcapsule-type mascara embedding rate of embodiment is 93.98%, 2 microcapsule-type eyelashes of embodiment
Cream embedding rate is 95.49%, and 3 microcapsule-type mascara embedding rate of embodiment is 97.06%, illustrates microcapsule-type mascara of the present invention
It is good to embed effect, there is splendid protective effect to the substance of embedding, can be effectively prevented capsule-core natural pigment and activity into
Divide loss of activity.
Microcapsule-type mascara produced by the present invention plays colour developing effect by natural pigment, avoids color lake and artificial conjunction
Injury into pigment to human body has health efficacy；And the present invention is matched by the collaboration of black sesame melanin and ginseng alcohol extract
5 effects bring to microcapsule-type mascara of the present invention and promote eyelashes growth, prevent deplumation, make eyelashes more pitch-black dense
The effect of, impart the new purposes of mascara；The present invention also by avocado oil and the collaboration compatibility effect of black rice pigments, more makes this
Invention microcapsule-type mascara has both the effect of moist eyelashes, moisturizing eyelashes, and multiple consumption experience is brought to consumer.
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although applicant
The present invention is described in detail with reference to preferred embodiment, it will be understood by those of ordinary skill in the art that, to the present invention's
Technical solution is modified or replaced equivalently, and without departing from the objective and range of technical solution of the present invention, should all be covered
In scope of the presently claimed invention.
Claims (3)
1. a kind of preparation method of microcapsule-type mascara, which is characterized in that the parts by weight of each raw material are as follows：Gelatin 5 ~ 15
Part, 3 ~ 8 parts of chitosan, 4 ~ 10 parts of Arabic gum, 2 ~ 5 parts of black sesame pigment, 1 ~ 3 part of black rice pigments, acorn nut shell brown pigment 0.5 ~
1.5 parts, 2 ~ 5 parts of ginseng alcohol extract, 5 ~ 10 parts of avocado oil, 12 ~ 26 parts of beeswax, 6 ~ 14 parts of glycerin monostearate, carboxymethyl it is fine
1.5 ~ 3 parts of plain 4 ~ 6 parts of the sodium of dimension, 2 ~ 5 parts of tween and neopelex；Its preparation includes the following steps：
1）After gelatin distilled water is taken to impregnate 1 ~ 2 h of swelling, it is water-soluble that the gelatin that mass concentration is 5 ~ 7% is configured at 60 ~ 75 DEG C
Liquid；
2）Arabic gum and chitosan are taken, distilled water is added in, is dissolved by heating at 50 ~ 65 DEG C, obtain mixed solution A；Wherein, it mixes
The mass concentration of Arabic gum is 2 ~ 4% in solution A；
3）Ginseng alcohol extract and avocado oil are weighed, is uniformly mixed, 15 ~ 25 s of microwave treatment at 40 ~ 60 DEG C；Wherein, microwave work(
Rate is 650W；
4）To step 3）Natural pigment, beeswax, glycerin monostearate, carboxymethyl cellulose are added in mixture after microwave treatment
Plain sodium, tween and neopelex are ultrasonically treated 2 ~ 3 min at 60 ~ 80 DEG C；Wherein, ultrasonic power 380W；Institute
It states natural pigment and includes black sesame pigment, black rice pigments and acorn nut shell brown pigment；
5）To step 4）Mixture after ultrasound uses homogenizer homogeneous 3 using after 3 ~ 8min of ultrahigh speed dispersion machine emulsion dispersion
It is secondary, obtain homogenizing fluid；Wherein, the rotating speed of the dispersion machine is 2200r/min, and the homogenization pressure of homogenizer is 42 MPa；
6）By step 1）Aqueous gelatin solution obtained and step 5）Homogenizing fluid obtained is uniformly mixed, and is disperseed using high speed dispersor
After 3 ~ 6 min, step 2 is added in）Mixed solution A obtained obtains mixed solution B；
7）By step 6）Mixed solution B adjusts pH to 4.1 ~ 4.9, and the solution after adjusting is reacted 18 min in 52 DEG C；
8）To step 7）25 mL propionic aldehyde, ultrasonic reaction 1h are added in mixed solution B after reaction；Wherein, ultrasonic power for 350 ~
500W；
9）By step 8）Solution after reaction centrifuges 5 ~ 10 min with the centrifugal speed of 6000 ~ 7000 r/min, discards supernatant liquid；
Water washing and precipitating is simultaneously centrifuged three times with same centrifugal condition, obtains wet microcapsules；
10）By step 9）After -60 ~ -70 DEG C of 28 ~ 32h of pre-freeze, 8 ~ 16 h of vacuum freeze drying is obtained obtained wet microcapsules
The microcapsule-type mascara.
2. the preparation method of microcapsule-type mascara according to claim 1, which is characterized in that the parts by weight of each raw material
Number is as follows：5 parts of gelatin, 3 parts of chitosan, 4 parts of Arabic gum, 2 parts of black sesame pigment, 1 part of black rice pigments, acorn nut shell brown pigment
0.5 part, 2 parts of ginseng alcohol extract, 5 parts of avocado oil, 12 parts of beeswax, 6 parts of glycerin monostearate, 4 parts of sodium carboxymethylcellulose, spit
1.5 parts of 2 parts of temperature and neopelex.
3. the preparation method of microcapsule-type mascara according to claim 1, which is characterized in that the tween is Tween-80.
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|---|---|---|---|---|
| US6391288B1 (en) * | 1999-07-27 | 2002-05-21 | Shiseido Co., Ltd. | Microcapsule and method of making the same |
| CN103070811A (en) * | 2013-02-05 | 2013-05-01 | 广东食品药品职业学院 | Tea tree oil antibacterial microcapsule and preparation method and application thereof |
| CN104398393A (en) * | 2014-12-01 | 2015-03-11 | 重庆小丸科贸有限公司 | Microcapsule lipstick wrapped with natural pigment |
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