CN105232424B - A kind of microcapsule-type mascara - Google Patents

A kind of microcapsule-type mascara Download PDF

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Publication number
CN105232424B
CN105232424B CN201510705448.8A CN201510705448A CN105232424B CN 105232424 B CN105232424 B CN 105232424B CN 201510705448 A CN201510705448 A CN 201510705448A CN 105232424 B CN105232424 B CN 105232424B
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China
Prior art keywords
parts
microcapsule
present
eyelashes
mascara
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Application number
CN201510705448.8A
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Chinese (zh)
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CN105232424A (en
Inventor
袁彦洁
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Chongqing Xiaowan Biotechnology Co., Ltd.
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CHONGQING XIAOWAN TRADE Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/11Encapsulated compositions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/925Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/10Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42Colour properties
    • A61K2800/43Pigments; Dyes

Abstract

The invention discloses a kind of microcapsule-type mascaras, for a kind of microcapsules of nucleocapsid, cyst material includes gelatin, chitosan and Arabic gum, and core materials include natural pigment, ginseng alcohol extract, avocado oil, beeswax, glycerin monostearate, sodium cellulose glycolate, tween and neopelex.Microcapsule-type mascara of the present invention plays colour developing effect by natural black pigment, avoids the injury of color lake and synthetic food color to human body, has health efficacy;And the present invention brings to microcapsule-type mascara of the present invention by black sesame melanin and the collaboration compatibility effect of ginseng alcohol extract and promotes eyelashes growth, the effect of preventing deplumation, make eyelashes more pitch-black dense, impart the new purposes of mascara;The present invention is also by avocado oil and the collaboration compatibility effect of black rice pigments, the effect of microcapsule-type mascara of the present invention is more made to have both moist eyelashes, moisturizing eyelashes, multiple consumption experience is brought to consumer.

Description

A kind of microcapsule-type mascara
Technical field
The invention belongs to microcapsules technology fields, and in particular to a kind of microcapsule-type mascara.
Background technology
Mascara is the cosmetics being applied on eyelashes, its role is to which eyelashes is made to seem that dense, fine length, volume are stuck up, is added The color of deep eyelashes, the eyes allowed after smearing mascara, which seem deep, god.With the improvement of living standards, people are increasingly Self-image is paid close attention to, mascara receives the concern of more and more people seeking beauties, becomes current necessary cosmetics.
Existing mascara product majority uses color lake or synthetic food color as main color developing agent, however these are aobvious For toner mostly containing a large amount of heavy metal component, these heavy metal components constitute the potential risk for causing cancer, are added to these The mascara of heavy metal color developing agent naturally also has certain healthy hidden danger, and serious threat the health of consumer.How to provide A kind of mascara product with healthy color developing agent, becomes urgent problem in mascara production process.
With the continuous renewal of mascara product, consumer is also being not that single beautifying functions will to mascara product It asks, how while eyelashes are beautified, multiple consumption experience is brought to consumer, start to become consumer for eyelashes of new generation An urgent demand of cream product.
Invention content
For deficiencies of the prior art, the technical problems to be solved by the invention are:How to provide a kind of micro- Capsule-type mascara makes it have effects that color developing agent is safe and healthy simultaneously, nourish maintenance eyelashes, promote eyelashes growth.
In order to solve the above-mentioned technical problem, the present invention adopts the following technical scheme that:A kind of microcapsule-type mascara, for one kind The mass ratio of the microcapsules of nucleocapsid, cyst material and core materials is 1:2~1:4;The parts by weight of the cyst material are such as Under:4 ~ 10 parts of 5 ~ 15 parts of gelatin, 3 ~ 8 parts of chitosan and Arabic gum;The parts by weight of the core materials are as follows:Semen sesami nigrum color Plain 2 ~ 5 parts, 1 ~ 3 part of black rice pigments, 0.5 ~ 1.5 part of acorn nut shell brown pigment, 2 ~ 5 parts of ginseng alcohol extract, 5 ~ 10 parts of avocado oil, beeswax 12 ~ 26 parts, 6 ~ 14 parts of glycerin monostearate, 4 ~ 6 parts of sodium carboxymethylcellulose, 2 ~ 5 parts of tween and neopelex 1.5 ~ 3 parts.
Compared with prior art, the present invention has the advantages that:
1st, the present invention uses natural pigment as color developing agent, using natural materials as active constituent, because of natural materials Matter is unstable, is easily destroyed by external environment, therefore present invention spy embeds natural materials using microcapsules technology, is protecting Protect natural materials activity not be destroyed while, also avoid the lipid phase in capsule-core easily air-dry, air-dry after cannot make With the problem of occur.
2nd, microcapsule-type mascara particle of the present invention is regular spherical shape, and cyst wall has uniform thickness, and with uniform Intensity, the problem of microcapsules are perfect spherical not to be destroyed, capsule-core will not be caused to reveal can be retained, product storage is effectively ensured It deposits, transport, will not be damaged during shelf life.
2nd, microcapsule-type mascara of the present invention protects natural pigment, the natural active matter of capsule-core by embedding means Shield, embedding effect is good, and embedding rate is up to 97%, and capsule-core can be protected not influenced by extraneous undesirable element, be further ensured that product Stability characteristic (quality) can experience the function that active material is brought when ensureing consumer using microcapsule-type mascara of the present invention.
3rd, the present invention plays colour developing effect by natural pigment, avoids the wound of color lake and synthetic food color to human body Evil has health efficacy;And the present invention is by black sesame melanin and the collaboration compatibility effect of ginseng alcohol extract, it is micro- to the present invention Capsule-type mascara, which is brought, promotes eyelashes growth, the effect of preventing deplumation, make eyelashes more pitch-black dense, imparts eyelashes The new purposes of cream;The present invention more makes microcapsule-type eyelashes of the present invention also by avocado oil and the collaboration compatibility effect of black rice pigments Cream has both the effect of moist eyelashes, moisturizing eyelashes, and multiple consumption experience is brought to consumer.
4th, the present invention carries more convenient to use compared to existing mascara, during use microcapsules receive squeezing action will Rupture, and then the natural pigment of capsule-core and active material is made to play effect, it brings beautification eyelashes, nourish the effect of eyelashes.
5th, on the basis of microcapsule-type mascara core materials of the present invention are considered, present invention selection gelatin, shell gather As cyst material, collaboration plays the embedding effect to capsule-core, has good embedding effect for sugar and Arabic gum;And due to capsule Wall material gelatin has certain water profit effect, and microcapsule-type mascara of the present invention is caused to have certain moistening.
Specific embodiment
The present invention is described in further detail with reference to embodiment.
In the present invention unless otherwise instructed, raw materials used is commercially available.
Microcapsule-type mascara of the present invention is prepared with the following method:
(1)Take gelatin distilled water impregnate swelling 1 ~ 2 h after, be configured at 60 ~ 75 DEG C mass concentration be 5 ~ 7% it is bright Glue solution;
(2)Arabic gum and chitosan are taken, distilled water is added in, is dissolved by heating at 50 ~ 65 DEG C, obtain mixed solution A;Its In, the mass concentration of Arabic gum is 2 ~ 4% in mixed solution A;
(3)Ginseng alcohol extract and avocado oil are weighed, is uniformly mixed, 15 ~ 25 s of microwave treatment at 40 ~ 60 DEG C;Wherein, it is micro- Wave power is 550 ~ 780W;
(4)To step 3)Natural pigment, beeswax, glycerin monostearate, carboxylic first are added in mixture after microwave treatment Base sodium cellulosate, tween and neopelex are ultrasonically treated 2 ~ 3 min at 60 ~ 80 DEG C;Wherein, ultrasonic power is 300~450W;
(5)To step 4)Mixture after ultrasound uses homogenizer using after 3 ~ 8min of ultrahigh speed dispersion machine emulsion dispersion Homogeneous 3 times, obtains homogenizing fluid;Wherein, the rotating speed of the dispersion machine is 1500 ~ 2600 r/min, and the homogenization pressure of homogenizer is 38~46 MPa;
(6)By step 1)Gelatin solution obtained and step 5)Homogenizing fluid obtained is uniformly mixed, and uses high speed dispersor After disperseing 3 ~ 6 min, step 2 is added in)Mixed solution A obtained obtains mixed solution B;
(7)By step 6)Mixed solution B adjusts pH to 4.1 ~ 4.9, and the solution after adjusting is reacted 15 ~ 25 in 45 ~ 55 DEG C min;
(8)To step 7)20 ~ 28 mL propionic aldehyde, 0.5 ~ 1.5 h of ultrasonic reaction are added in mixed solution B after reaction;Its In, ultrasonic power is 350 ~ 500W;
(9)By step 8)Solution after reaction centrifuges 5 ~ 10 min with the centrifugal speed of 6000 ~ 7000 r/min, discards Clear liquid;Water washing and precipitating is simultaneously centrifuged three times with same centrifugal condition, obtains wet microcapsules;
(10)By step 9)Obtained wet microcapsules are after -60 ~ -70 DEG C of 28 ~ 32h of pre-freeze, 8 ~ 16 h of vacuum freeze drying, Obtain the microcapsule-type mascara.
Embodiment 1:
A kind of microcapsule-type mascara, is a kind of microcapsules of nucleocapsid, and cyst material is:50 g gelatin, chitosan 30g, Arabic gum 40g;Core materials are:Black sesame pigment 20g, black rice pigments 10g, acorn nut shell brown pigment 5g, ginseng alcohol extracting Object 20g, avocado oil 50g, beeswax 120g, glycerin monostearate 60g, sodium carboxymethylcellulose 40g, polysorbas20 g and dodecane Base benzene sulfonic acid sodium salt 15g.
Embodiment 2:
A kind of microcapsule-type mascara, is a kind of microcapsules of nucleocapsid, and cyst material is:150 g gelatin, chitosan 80g, Arabic gum 100g;Core materials are:Black sesame pigment 50g, black rice pigments 30g, acorn nut shell brown pigment 15g, panaxynol Extract 50g, avocado oil 100g, beeswax 180g, glycerin monostearate 95g, sodium carboxymethylcellulose 60g, tween 50g and 12 Sodium alkyl benzene sulfonate 30g.
Embodiment 3:
A kind of microcapsule-type mascara, is a kind of microcapsules of nucleocapsid, and cyst material is:60 g gelatin, chitosan 45 g, 55 g of Arabic gum;Core materials are:40 g of black sesame pigment, black rice pigments 20g, 10 g of acorn nut shell brown pigment, ginseng Alcohol extract 30g, avocado oil 60g, beeswax 260g, glycerin monostearate 140g, sodium carboxymethylcellulose 40g, polysorbas20 g and ten Dialkyl benzene sulfonic acids sodium 20g.
It is measured by experiment, 1 microcapsule-type mascara embedding rate of embodiment is 93.98%, 2 microcapsule-type eyelashes of embodiment Cream embedding rate is 95.49%, and 3 microcapsule-type mascara embedding rate of embodiment is 97.06%, illustrates microcapsule-type mascara of the present invention It is good to embed effect, there is splendid protective effect to the substance of embedding, can be effectively prevented capsule-core natural pigment and activity into Divide loss of activity.
The present invention plays colour developing effect by natural pigment, avoids the injury of color lake and synthetic food color to human body, With health efficacy;And the present invention gives the present invention micro- glue by black sesame melanin and the collaboration compatibility effect of ginseng alcohol extract Bladder type mascara, which is brought, promotes eyelashes growth, the effect of preventing deplumation, make eyelashes more pitch-black dense, imparts mascara New purposes;The present invention more makes microcapsule-type mascara of the present invention also by avocado oil and the collaboration compatibility effect of black rice pigments The effect of having both moist eyelashes, moisturizing eyelashes brings multiple consumption experience to consumer.
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although applicant The present invention is described in detail with reference to preferred embodiment, it will be understood by those of ordinary skill in the art that, to the present invention's Technical solution is modified or replaced equivalently, and without departing from the objective and range of technical solution of the present invention, should all be covered In scope of the presently claimed invention.

Claims (2)

1. a kind of microcapsule-type mascara, which is characterized in that be a kind of microcapsules of nucleocapsid, cyst material and core materials Mass ratio be 1:2~1:4;
The parts by weight of the cyst material are as follows:4 ~ 10 parts of 5 ~ 15 parts of gelatin, 3 ~ 8 parts of chitosan and Arabic gum;The capsule The parts by weight of core material are as follows:2 ~ 5 parts of black sesame pigment, 1 ~ 3 part of black rice pigments, 0.5 ~ 1.5 part of acorn nut shell brown pigment, ginseng 2 ~ 5 parts of alcohol extract, 5 ~ 10 parts of avocado oil, 12 ~ 26 parts of beeswax, 6 ~ 14 parts of glycerin monostearate, sodium carboxymethylcellulose 4 ~ 6 1.5 ~ 3 parts of part, 2 ~ 5 parts of tween and neopelex.
2. a kind of microcapsule-type mascara, which is characterized in that be a kind of microcapsules of nucleocapsid, cyst material and core materials Mass ratio be 1:2~1:4;
The parts by weight of the cyst material are as follows:4 parts of 5 parts of gelatin, 3 parts of chitosan and Arabic gum;The core materials Parts by weight are as follows:2 parts of black sesame pigment, 1 part of black rice pigments, 0.5 part of acorn nut shell brown pigment, 2 parts of ginseng alcohol extract, avocado oil 5 parts, 12 parts of beeswax, 6 parts of glycerin monostearate, 4 parts of sodium carboxymethylcellulose, 2 parts of tween and neopelex 1.5 Part.
CN201510705448.8A 2015-10-27 2015-10-27 A kind of microcapsule-type mascara Active CN105232424B (en)

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CN105232424B true CN105232424B (en) 2018-07-06

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Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107349112B (en) * 2017-05-27 2018-09-18 清远初曲智能科技有限公司 It is a kind of to reduce the moist color-changing lipstick and preparation method thereof of the long-acting deep moisturizing of cheilogramma

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6391288B1 (en) * 1999-07-27 2002-05-21 Shiseido Co., Ltd. Microcapsule and method of making the same
CN104398393A (en) * 2014-12-01 2015-03-11 重庆小丸科贸有限公司 Microcapsule lipstick wrapped with natural pigment

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6391288B1 (en) * 1999-07-27 2002-05-21 Shiseido Co., Ltd. Microcapsule and method of making the same
CN104398393A (en) * 2014-12-01 2015-03-11 重庆小丸科贸有限公司 Microcapsule lipstick wrapped with natural pigment

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Address after: 401519 Chongqing Hechuan Industrial Park weir village two

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