CN105296275A - Fructus cannabis health care baijiu and brewing method thereof - Google Patents

Fructus cannabis health care baijiu and brewing method thereof Download PDF

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Publication number
CN105296275A
CN105296275A CN201510611949.XA CN201510611949A CN105296275A CN 105296275 A CN105296275 A CN 105296275A CN 201510611949 A CN201510611949 A CN 201510611949A CN 105296275 A CN105296275 A CN 105296275A
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fructus cannabis
fire
numb
acid
raw material
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CN105296275B (en
Inventor
张兴
郭春景
赵立涛
孙宇峰
张冬青
唐焕伟
刘颖
于革
刘新杰
杨雪冰
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Heilongjiang Academy of Sciences
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Abstract

The invention belongs to the field of brewing of a beverage, and in particular relates to fructus cannabis health care baijiu and a brewing method thereof. The brewing method disclosed by the invention comprises the following steps: screening hemp seeds and removing impurities; grinding and hulling the hemp seeds with impurities removed so as to obtain fructus cannabis; drying the obtained fructus cannabis at low temperature; coarsely crushing the dried fructus cannabis and performing extruding-expansion on the coarsely crushed fructus cannabis, and then grinding so as to obtain a fructus cannabis edible raw material mainly containing fructus cannabis grease and fructus cannabis protein; soaking the edible raw material in pure water with weight being 2-4 times the total weight of the edible raw material for 24-36h; adding 0.2-0.5g/L of a dried yeast for fermenting for 3-5 days; and filtering and removing dregs so as to obtain fermented baijiu. The fructus cannabis health care baijiu prepared by the invention can avoid the introduction of high temperature, a chemical reagent and an enzyme, and can better keep the original structures of nutrient substances, grease and protein in fructus cannabis.

Description

A kind of fiery numb health-care spirit and brewing method thereof
Technical field
The invention belongs to beverage brewing field, be specifically related to a kind of fiery numb health-care spirit and brewing method thereof.
Background technology
Hemp Seed is again cannabis,fructus, Chinese fiber crops benevolence or numb benevolence, is the dry mature fruit of moraceae plants hemp---and fiery numb seed is through the product of shelling.Modern study shows, Hemp Seed lipid content 43% ~ 48%, beyond oil removing, also contains the protein of about 30%, the sugar of about 5% and abundant calcium, phosphorus, iron, zinc, manganese.In addition, Hemp Seed is also rich in fatty oil, and containing unsaturated fatty acidss such as a large amount of oleic acid, linolic acid, linolenic acid in fatty oil, its content is up to 89.2%, and particularly wherein linolenic acid content reaches more than 20%, and these nutritive substances are very useful to human body.Wherein, the ratio (ω-6) of linoleic acid plus linolenic acid: (ω-3), close to 3:1, meets internationally recognized nutritive props standard; Fructus cannabis oil can improve the enzyme activities such as SOD/GSH-Px, and the ability removing DPPH free radical has exceeded sweet oil, is suitable as a kind of oxidation resistant dietary sources.The primary amino acid of hemp seeds protein matter is arginine, Histidine, sulfur-containing amino acid, the effect in human body of arginine, Histidine is extremely important, methionine(Met) in sulfur-containing amino acid and halfcystine are that generation biological enzyme is necessary, and Hemp Seed is one of quality plant dietary protein origin.Technology is not also had to disclose Hemp Seed as auxiliary material brewing spirit at present.
Summary of the invention
The object of the present invention is to provide a kind of nutritious fire fiber crops health-care spirit, the present invention also aims to the brewing method that the numb health-care spirit of a kind of fire is provided.
The object of the present invention is achieved like this:
A kind of fiery numb health-care spirit, containing palmitinic acid 50-72mg, stearic acid 10-21mg, oleic acid 5-11mg, linolic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fiery numb protein 157-200mg, choline 150mg in every 500mL white wine.
A brewing method for the numb health-care spirit of fire, comprises the steps:
(1) impurity is removed in numb for fire seed screening;
(2) numb for fire seed is carried out rice huller and grind shelling, obtain Hemp Seed;
(3) oven drying at low temperature: fallen apart by the Hemp Seed through screening and be paved into Hemp Seed material bed, carry out oven drying at low temperature at 30 DEG C-45 DEG C, drying time is 24-72 hour, makes fiery numb seed moisture content≤5%;
(4) carry out extruding puffing by after Hemp Seed coarse reduction, then obtain by fiery sesame oil fat and fire fiber crops albumen through milling be main fire fiber crops edible raw material;
(5) pure water adding weight 2 ~ 4 times soaks 24 ~ 36 hours;
(6) add dry yeast 0.2 ~ 0.5g/L, ferment 3 ~ 5 days;
(7) obtain fermented wine after filter residue, then add in the good white wine of brew to every 500mL white wine containing palmitinic acid 50-72mg, stearic acid 10-21mg, oleic acid 5-11mg, linolic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fiery numb protein 157-200mg, choline 150mg.
Fire fiber crops edible raw material in described step (4) carries out deodorizing process to the Hemp Seed after coarse reduction after extruding puffing, and the weight ratio of described fermented wine and white wine is 1:10 ~ 1:4.
Beneficial effect of the present invention is:
The fire fiber crops health-care spirit be prepared from by the present invention can not introduce high temperature, chemical reagent and enzyme, better can keep the structure of original nutritive substance, grease and the protein in fiery fiber crops.
Accompanying drawing explanation
Fig. 1 is 40 hours drying time differing temps protein storage schematic diagram.
The schematic diagram of Fig. 2 to be temperature be 37 degrees Celsius of different time protein contents.
It is the contrast schematic diagram that every 30 parts of numb edible raw materials of fire add wolfberry fruit number and muscarine content shown in Fig. 3.
It is the contrast schematic diagram that every 30 parts of numb edible raw materials of fire add wolfberry fruit number and muscarine content shown in Fig. 4.
Fig. 5 is proportionlity and the anticancer effect figure of vaccinium oxycoccus pigment extract and garlicin extract.
Embodiment
Below in conjunction with accompanying drawing, the present invention is described further.
Embodiment 1
Containing palmitinic acid 50-72mg, stearic acid 10-21mg, oleic acid 5-11mg, linolic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fiery numb protein 157-200mg, choline 150mg in every 500mL white wine.
Embodiment 2
A brewing method for the numb health-care spirit of fire, comprises the steps:
(1) impurity is removed in numb for fire seed screening;
(2) numb for fire seed is carried out rice huller and grind shelling, obtain Hemp Seed;
(3) oven drying at low temperature: fallen apart by the Hemp Seed through screening and be paved into Hemp Seed material bed, carry out oven drying at low temperature at 30 DEG C-45 DEG C, drying time is 24-72 hour, makes fiery numb seed moisture content≤5%;
(4) carry out extruding puffing by after Hemp Seed coarse reduction, then obtain by fiery sesame oil fat and fire fiber crops albumen through milling be main fire fiber crops edible raw material;
(5) pure water adding weight 2 ~ 4 times soaks 24 ~ 36 hours;
(6) add dry yeast 0.2 ~ 0.5g/L, ferment 3 ~ 5 days;
(7) obtain fermented wine after filter residue, then add in the good white wine of brew to every 500mL white wine containing palmitinic acid 50-72mg, stearic acid 10-21mg, oleic acid 5-11mg, linolic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fiery numb protein 157-200mg, choline 150mg.
Embodiment 3
Be with the difference of embodiment 2: the fire fiber crops edible raw material in described step (4) carries out deodorizing process to the Hemp Seed after coarse reduction after extruding puffing, and the weight ratio of described fermented wine and white wine is 1:10 ~ 1:4.
Embodiment 4
Identical with embodiment 2, difference is that in described step (3), the time of oven drying at low temperature and the pass of bake out temperature are:
T=-0.002t 2-0.372t+55.0840h≥t≥24h;
T=-0.21875t+45.7572h≥t≥40h;
Wherein t represents the time, T represents bake out temperature, and described Hemp Seed material bed thickness is less than or equal to 2cm, the wind speed≤3m/s on Hemp Seed material bed surface, preferred parameter t=26, T=44.056, t=40, T=37, t=50, T=34.81, t=60, T=32.625.
Hemp Seed can be made under the prerequisite at utmost keeping nutritive substance to lose moisture through inspection Hemp Seed under this oven dry relation, namely both ensured that temperature was below the temperature that the Hemp Seed that sets out is rotten, maximum time dries moisture wherein as much as possible simultaneously.The schematic diagram of the different bake out temperature protein content at 40 hours as shown in Figure 1, abscissa unit degree Celsius, ordinate zou percentage composition shared by protein.The schematic diagram of Fig. 2 to be temperature be 37 degrees Celsius of different time protein contents.Abscissa unit is hour, and ordinate zou is percentage composition shared by protein.Through a series of experiment and data analysis, we find that the little drying effect constantly of drying time 40 is best when bake out temperature is at 37 DEG C, and namely the structure of Hemp Seed inside does not change and drying time is the shortest substantially.
Embodiment 5
Identical with embodiment 2, difference be obtain through milling be main fire fiber crops edible raw material by fiery sesame oil fat and fire fiber crops albumen in add Solanaceae fruit and grind the magma that obtains and carry out stirring and obtain the numb edible raw material of final fire.The muscarine content in fiery numb edible raw material and content of choline can be made to decline by adding Solanaceae fruit magma, the food safety of fiery numb edible raw material can be ensured further.
Embodiment 6
Identical with embodiment 5, difference be described Solanaceae fruit grind the magma obtained Solanaceae fruit is carried out physical grinding after volume ratio 1:0.5 be watered stirring after obtain.
Embodiment 7
Identical with embodiment 5, difference is the one at least selected in capsicum, tomato, eggplant, wolfberry fruit, Calyx seu Fructus physalis, black nightshade, potato, root of Manchurian Currant of preferred Solanaceae fruit.The contrast schematic diagram that every 30 parts of numb edible raw materials of fire add wolfberry fruit number and muscarine content as shown in Figure 3.
The mass ratio that the numb edible raw material of preferred fire and capsicum grind the magma obtained is 15:1; The mass ratio that the numb edible raw material of fire and tomato grind the magma obtained is 17:1; The mass ratio that the numb edible raw material of fire and eggplant grind the magma obtained is 17:1; The mass ratio that the numb edible raw material of fire and wolfberry fruit grind the magma obtained is 33:1; The mass ratio that the numb edible raw material of fire and Calyx seu Fructus physalis grind the magma obtained is 37:1; The mass ratio that the numb edible raw material of fire and black nightshade grind the magma obtained is 43:1; The mass ratio that the numb edible raw material of fire and potato grind the magma obtained is 17:1; The mass ratio that the numb edible raw material of fire and root of Manchurian Currant grind the magma obtained is 35:1.Muscarine content≤0.01mg/kg now in fiery numb edible raw material, content of choline 7-8mg/kg.The contrast schematic diagram that every 30 parts of numb edible raw materials of fire add wolfberry fruit number and muscarine content as shown in Figure 4.
By Fig. 3, Fig. 4 and experimental analysis known when wolfberry fruit magma mass ratio is 33:1 in the present invention on the basis of suppression muscarine content as much as possible reservation content of choline as much as possible.
Embodiment 8
Identical with embodiment 2, difference is that the centrifugal rotational speed of centrifugally operated is 7000r/min, centrifugation time is 20min, also precipitation process is comprised in the middle of described cold press and centrifugally operated, in described lipid acid, palmitic acid content is 7.2g/100g, stearic acid content is 2.1g/100g, oleic acid content is 11g/100g, linoleic acid content be 56.3g/100g and alpha-linolenic acid content is 21.2g/100g, and described fire fiber crops protein content is 57%-70%.
Other steps are identical with any one in embodiment 4 ~ 10, and difference is that fiery numb protein powder is prepared from as follows:
(1) use fiery numb edible raw material to carry out mechanical normal temperature cold press and centrifugally operated obtain fiery sesame oil fat and fire fiber crops protein stratified mixture;
(2) use 0.22 μm or the 0.45 μm of semi-permeable membranes stratified mixture to fiery sesame oil fat and fire fiber crops albumen to be separated and obtain fiery sesame oil fat;
(3) low pressure is carried out to fire remaining after separation fiber crops protein and vacuumize gasification process, further filtering grease, obtain the fire fiber crops protein dregs of rice that purity is higher;
(4) numb for the fire protein dregs of rice are carried out fine grainding powder process and obtain fiery numb protein powder.
Embodiment 9
Other steps are identical with any one in embodiment 1 ~ 8, and difference is, also at least add the one in cyanidin extract and garlicin extract in the numb edible raw material of fire.
Described vaccinium oxycoccus pigment extract is made by the following method:
A, blue berry to be smashed, to be incorporated as its concentration of 4 ~ 4.5 times be the aqueous ethanolic solution of 80% ~ 90% to example in mass ratio, by the ultrasonic wave of 180W ~ 260W under temperature is 50 ~ 60 DEG C of situations, extracts 3 times, the time of each extraction 60 ~ 80min, after filtration, obtain extracting solution A;
B, blueberry red autumnal leaves to be smashed, to be incorporated as its concentration of 10 ~ 45 times be the aqueous ethanolic solution of 80% ~ 90% to example in mass ratio, by the ultrasonic wave of 180W ~ 260W under temperature is 50 ~ 60 DEG C of situations, extracts 3 times, the time of each extraction 60 ~ 80min, after filtration, obtain extracting solution B;
C, extracting solution A and extracting solution B are mixed after carry out underpressure distillation, pressure-controlling is at 0.12 ~ 0.15MPa, and temperature controls, at 52 ~ 58 DEG C, to obtain concentrated extracting solution;
D, concentrated extracting solution is carried out fractionation by adsorption through AB-8 macroporous resin, adsorb saturated after, carry out wash-out with the aqueous ethanolic solution that concentration is 60 ~ 70%, obtain vaccinium oxycoccus pigment elutriant;
E, carry out concentrating under reduced pressure to vaccinium oxycoccus pigment elutriant, by vaccinium oxycoccus pigment elutriant pressure-controlling at 0.12 ~ 0.15MPa, temperature controls to concentrate at 52 ~ 58 DEG C, and obtain vaccinium oxycoccus pigment extract, its proportion is between 1.15 ~ 1.2;
Garlicin extract obtains by the following method:
1) garlic is put into acetum to soak 10 ~ 12 days, water cleans, and obtains the garlic slurries after deodorizing after fragmentation;
2) will obtain the garlic slurries after deodorizing, row are incorporated as its concentration of 3 ~ 5 times is in mass ratio the aqueous ethanolic solution of 80% ~ 90%, and adjust pH value to be 6, enzymolysis 50 ~ 60min, temperature is 30 ~ 40 DEG C;
3) the garlic slurries after enzymolysis are added the aqueous ethanolic solution that concentration is 80% ~ 90% again, the mass ratio of current garlic slurries and aqueous ethanolic solution is made to be 1:5 ~ 1:8, utilize the ultrasonic wave of 50 ~ 100W to carry out extraction 10 ~ 30min, obtain garlic extract;
4) garlic extract is carried out centrifugal treating, carry out ultrafiltration after secondary filter, ultra-filtration membrane is mineral membrane, and its molecular weight that dams is 8000 ~ 50000Da;
5) will obtain liquid and carry out concentrating under reduced pressure, and obtain garlicin extract, its proportion is 1.08 ~ 1.094g/l.
Blueberry Hua Qingsu and garlicin, can effectively improve body immunity, build up health, delay senility, vision enhancing and also have extensively antibacterial effect, especially bacillus, fungi, virus, ameba, trichomonas vaginitis, pinworm etc. all have suppression killing action, especially strong to the effect of the intestinal bacteria such as intestinal bacteria, dysentery bacterium.
The present invention, except having above-mentioned advantage, also has the effect of potent antitumor, anticancer, especially intestinal cancer, shows by experiment, and the effect of the antitumor and cancer of the ratio synthetic orall liquid of the 4:1 that the present invention adopts is considerably beyond any one in both.
Vaccinium oxycoccus pigment extract x part, garlicin extract y part and water z part, the relation of vaccinium oxycoccus pigment extract, garlicin extract and water meets following requirement:
x = a × y z = 12.5 a × y
Wherein, a is proportion scale, and its span is a ∈ (1,6), can obtain optimum proportion when a value is 4.When a value is 4, situation when the present invention gets 3 to the inhibition of cancer cells surviving rate apparently higher than a, but along with the increase of proportion scale and a value once large time, the inhibition of the present invention to cancer cells surviving rate reduces again gradually, when a value is 20 as shown in Figure 5, the inhibition of the present invention to cancer cells surviving rate obviously reduces.
Fire that the present invention is made fiber crops health-care spirit obtains product of the present invention due to the mode employing oven drying at low temperature and filter membrane direct filtration, do not have tradition to extract the process of high temperature in meaning, chemical reagent extraction and enzymolysis, ensure that in fiery numb seed, lipid acid, protein structure and character do not change as much as possible.The fruit magma simultaneously introducing Solanaceae not only makes the taste of fiery numb edible raw material there occurs change, and inhibits the content of muscarine and choline in fiery fiber crops greatly, and content of choline is remained in the useful scope of human body.According to monitoring raw material content of choline≤10mg/kg, the standard that the white wine adding this raw material is applicable to meeting human body choline intake has the effect promoting brain development, improve memory.

Claims (3)

1. the numb health-care spirit of fire, is characterized in that: containing palmitinic acid 50-72mg, stearic acid 10-21mg, oleic acid 5-11mg, linolic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fiery numb protein 157-200mg, choline 150mg in every 500mL white wine.
2. a brewing method for the numb health-care spirit of fire, is characterized in that, comprise the steps:
(1) impurity is removed in numb for fire seed screening;
(2) numb for fire seed is carried out rice huller and grind shelling, obtain Hemp Seed;
(3) oven drying at low temperature: fallen apart by the Hemp Seed through screening and be paved into Hemp Seed material bed, carry out oven drying at low temperature at 30 DEG C-45 DEG C, drying time is 24-72 hour, makes fiery numb seed moisture content≤5%;
(4) carry out extruding puffing by after Hemp Seed coarse reduction, then obtain by fiery sesame oil fat and fire fiber crops albumen through milling be main fire fiber crops edible raw material;
(5) pure water adding weight 2 ~ 4 times soaks 24 ~ 36 hours;
(6) add dry yeast 0.2 ~ 0.5g/L, ferment 3 ~ 5 days;
(7) obtain fermented wine after filter residue, then add in the good white wine of brew to every 500mL white wine containing palmitinic acid 50-72mg, stearic acid 10-21mg, oleic acid 5-11mg, linolic acid 30-56.3mg, alpha-linolenic acid 10-21.2mg, fiery numb protein 157-200mg, choline 150mg.
3. the brewing method of the numb health-care spirit of a kind of fire according to claim 2, it is characterized in that: the fire fiber crops edible raw material in described step (4) carries out deodorizing process to the Hemp Seed after coarse reduction after extruding puffing, and the weight ratio of described fermented wine and white wine is 1:10 ~ 1:4.
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105820909A (en) * 2016-04-29 2016-08-03 安徽恋尚你食品有限公司 Preparation method of Moringa oleifera white wine
CN109123686A (en) * 2018-08-22 2019-01-04 黑龙江黑科科技有限责任公司 Numb seed powder high protein element meat of one kind fire with health care function and preparation method thereof
CN109355156A (en) * 2018-12-04 2019-02-19 赵为兴 A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice
CN110577870A (en) * 2019-09-20 2019-12-17 云南云酒酒业有限责任公司 Brewing method of sesame-flavor liquor
CN110692881A (en) * 2019-11-01 2020-01-17 云南中医药大学 Pure fructus cannabis health drink
CN113755293A (en) * 2020-06-04 2021-12-07 云南汉盟制药有限公司 Fructus cannabis fatty acid compound wine and preparation method thereof

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CN101508951A (en) * 2009-04-01 2009-08-19 覃怀忠 Wine
CN103356904A (en) * 2013-07-11 2013-10-23 秦春耀 Gastrodia elata wine and preparation method thereof
CN104450156A (en) * 2014-11-21 2015-03-25 国家粮食局科学研究院 Method for extracting grease in fructus cannabis by using aqueous enzymatic method and fructus cannabis protein drink
CN104745396A (en) * 2015-04-14 2015-07-01 江南大学 Method for brewing yellow wine rich in soluble dietary fiber

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CN86100137A (en) * 1986-01-07 1987-07-15 黑龙江商学院 The new technology of making fermented products from dilated grain
KR20020035367A (en) * 2000-11-06 2002-05-11 최태규 Method For Producing Refined Rice Wine Made From Swelled Barley
CN101508951A (en) * 2009-04-01 2009-08-19 覃怀忠 Wine
CN103356904A (en) * 2013-07-11 2013-10-23 秦春耀 Gastrodia elata wine and preparation method thereof
CN104450156A (en) * 2014-11-21 2015-03-25 国家粮食局科学研究院 Method for extracting grease in fructus cannabis by using aqueous enzymatic method and fructus cannabis protein drink
CN104745396A (en) * 2015-04-14 2015-07-01 江南大学 Method for brewing yellow wine rich in soluble dietary fiber

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105820909A (en) * 2016-04-29 2016-08-03 安徽恋尚你食品有限公司 Preparation method of Moringa oleifera white wine
CN109123686A (en) * 2018-08-22 2019-01-04 黑龙江黑科科技有限责任公司 Numb seed powder high protein element meat of one kind fire with health care function and preparation method thereof
CN109355156A (en) * 2018-12-04 2019-02-19 赵为兴 A kind of formula and preparation method thereof of fructus cannabis alcoholic drink mixed with fruit juice
CN110577870A (en) * 2019-09-20 2019-12-17 云南云酒酒业有限责任公司 Brewing method of sesame-flavor liquor
CN110692881A (en) * 2019-11-01 2020-01-17 云南中医药大学 Pure fructus cannabis health drink
CN113755293A (en) * 2020-06-04 2021-12-07 云南汉盟制药有限公司 Fructus cannabis fatty acid compound wine and preparation method thereof

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