CN105273747B - 一种浆态床加氢反应器的控温措施及其设计方法和用途 - Google Patents
一种浆态床加氢反应器的控温措施及其设计方法和用途 Download PDFInfo
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- CN105273747B CN105273747B CN201510796589.5A CN201510796589A CN105273747B CN 105273747 B CN105273747 B CN 105273747B CN 201510796589 A CN201510796589 A CN 201510796589A CN 105273747 B CN105273747 B CN 105273747B
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- 238000005984 hydrogenation reaction Methods 0.000 title claims abstract description 25
- 239000002002 slurry Substances 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 title claims abstract description 16
- 238000013461 design Methods 0.000 title claims abstract description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 14
- 239000001257 hydrogen Substances 0.000 claims abstract description 14
- 230000009467 reduction Effects 0.000 claims description 15
- 230000006837 decompression Effects 0.000 claims description 8
- 239000007858 starting material Substances 0.000 claims description 5
- 230000002159 abnormal effect Effects 0.000 claims description 3
- 238000009530 blood pressure measurement Methods 0.000 claims description 3
- 239000003245 coal Substances 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 230000000694 effects Effects 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- 239000003921 oil Substances 0.000 description 10
- 238000006243 chemical reaction Methods 0.000 description 9
- 238000007599 discharging Methods 0.000 description 6
- 230000008569 process Effects 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 239000000295 fuel oil Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000010426 asphalt Substances 0.000 description 2
- 238000003490 calendering Methods 0.000 description 2
- 230000003197 catalytic effect Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 238000007600 charging Methods 0.000 description 2
- 239000011280 coal tar Substances 0.000 description 2
- 239000010779 crude oil Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000002802 bituminous coal Substances 0.000 description 1
- 238000004517 catalytic hydrocracking Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000002826 coolant Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000003077 lignite Substances 0.000 description 1
- 238000007726 management method Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000008054 signal transmission Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
- C10G47/36—Controlling or regulating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1809—Controlling processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
- B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
- B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
- B01J8/224—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement
- B01J8/226—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement internally, i.e. the particles rotate within the vessel
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
- B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
- B01J8/224—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement
- B01J8/228—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement externally, i.e. the particles leaving the vessel and subsequently re-entering it
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/08—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts
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- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05D—SYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
- G05D23/00—Control of temperature
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- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05D—SYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
- G05D23/00—Control of temperature
- G05D23/01—Control of temperature without auxiliary power
- G05D23/12—Control of temperature without auxiliary power with sensing element responsive to pressure or volume changes in a confined fluid
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- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05D—SYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
- G05D23/00—Control of temperature
- G05D23/19—Control of temperature characterised by the use of electric means
- G05D23/1917—Control of temperature characterised by the use of electric means using digital means
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- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00026—Controlling or regulating the heat exchange system
- B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
- B01J2208/00044—Temperature measurement
- B01J2208/00061—Temperature measurement of the reactants
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00026—Controlling or regulating the heat exchange system
- B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
- B01J2208/0007—Pressure measurement
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00628—Controlling the composition of the reactive mixture
- B01J2208/00637—Means for stopping or slowing down the reaction
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00716—Means for reactor start-up
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00743—Feeding or discharging of solids
- B01J2208/00752—Feeding
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Combustion & Propulsion (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Automation & Control Theory (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
Description
Claims (7)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510796589.5A CN105273747B (zh) | 2015-11-18 | 2015-11-18 | 一种浆态床加氢反应器的控温措施及其设计方法和用途 |
US15/777,338 US11111446B2 (en) | 2015-11-18 | 2015-11-30 | Temperature-controlling measure for the hydrogenation slurry bed reactor and its design method and use |
PCT/CN2015/096023 WO2017084114A1 (zh) | 2015-11-18 | 2015-11-30 | 一种浆态床加氢反应器的控温措施及其设计方法和用途 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201510796589.5A CN105273747B (zh) | 2015-11-18 | 2015-11-18 | 一种浆态床加氢反应器的控温措施及其设计方法和用途 |
Publications (2)
Publication Number | Publication Date |
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CN105273747A CN105273747A (zh) | 2016-01-27 |
CN105273747B true CN105273747B (zh) | 2017-05-03 |
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CN201510796589.5A Active CN105273747B (zh) | 2015-11-18 | 2015-11-18 | 一种浆态床加氢反应器的控温措施及其设计方法和用途 |
Country Status (3)
Country | Link |
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US (1) | US11111446B2 (zh) |
CN (1) | CN105273747B (zh) |
WO (1) | WO2017084114A1 (zh) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107805520B (zh) * | 2016-09-09 | 2020-06-09 | 北京华石联合能源科技发展有限公司 | 一种悬浮床加氢泄放工艺 |
CN106957675B (zh) * | 2017-03-31 | 2018-03-06 | 北京中科诚毅科技发展有限公司 | 一种加氢工艺的温度及压力控制方法及其设计方法和用途 |
CN108970544A (zh) * | 2017-06-02 | 2018-12-11 | 何巨堂 | 一种气液料上流加氢反应器的液相产物回流动力增加方法 |
CN107390752A (zh) * | 2017-08-23 | 2017-11-24 | 南京扬子精细化工有限责任公司 | 一种实时监测控制*** |
CN107694483B (zh) * | 2017-09-22 | 2018-12-21 | 北京中科诚毅科技发展有限公司 | 一种加氢反应器及其设计方法与用途 |
CN107674703B (zh) * | 2017-11-07 | 2019-10-22 | 河北新启元能源技术开发股份有限公司 | 一种煤焦油加氢中反应进料温度控制装置 |
CN110669548A (zh) * | 2019-09-02 | 2020-01-10 | 国家能源集团宁夏煤业有限责任公司 | 加氢裂化反应器连锁保护控制方法和控制*** |
CN116948683B (zh) * | 2023-09-15 | 2023-12-12 | 克拉玛依市先能科创重油开发有限公司 | 以环烷基渣油与乙烯裂解焦油为原料的浆态床反应在线切换方法 |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4249908A (en) * | 1979-09-11 | 1981-02-10 | Phillips Petroleum Company | Temperature control of exothermic reactions |
US4491924A (en) * | 1982-04-22 | 1985-01-01 | The Babcock & Wilcox Company | Olefin oxidation reactor temperature control |
US4617110A (en) * | 1984-06-11 | 1986-10-14 | Phillips Petroleum Company | Control of a hydrofining process for hydrocarbon-containing feed streams which process employs a hydrodemetallization reactor in series with a hydrodesulfurization reactor |
US4551238A (en) * | 1984-11-06 | 1985-11-05 | Mobil Oil Corporation | Method and apparatus for pressure-cascade separation and stabilization of mixed phase hydrocarbonaceous products |
US4681674A (en) * | 1985-11-07 | 1987-07-21 | Mobil Oil Corporation | Fixed bed catalytic reactor system with improved liquid distribution |
US4707245A (en) * | 1985-12-20 | 1987-11-17 | Lummus Crest, Inc. | Temperature control for hydrogenation reactions |
US5000924A (en) * | 1987-06-02 | 1991-03-19 | Elsagainternational B.V. | Autoacceleration control for exothermic reactors |
CN101281696A (zh) * | 2008-03-13 | 2008-10-08 | 华东理工大学 | 一种化工生产实训装置 |
US8008534B2 (en) * | 2008-06-30 | 2011-08-30 | Uop Llc | Liquid phase hydroprocessing with temperature management |
WO2010038396A1 (ja) * | 2008-09-30 | 2010-04-08 | 独立行政法人石油天然ガス・金属鉱物資源機構 | 炭化水素化合物合成反応ユニット及びその運転方法 |
PL2226375T3 (pl) * | 2009-03-04 | 2012-10-31 | Ifp Energies Now | Sposób ciągłego uwodorniania surowców zawierających trigliceryd |
EP2311554A1 (en) | 2009-10-07 | 2011-04-20 | Linde Aktiengesellschaft | Method for reaction control of exothermic reaction and apparatus therefore |
CN202995359U (zh) * | 2012-11-09 | 2013-06-12 | 内蒙古伊泰煤制油有限责任公司 | 一种浆态床反应器停车联锁*** |
CN203552089U (zh) | 2013-10-08 | 2014-04-16 | 内蒙古伊泰煤制油有限责任公司 | 一种浆态床反应器的温控保护装置 |
CN104818050A (zh) * | 2015-05-07 | 2015-08-05 | 北京中科诚毅科技发展有限公司 | 一种多重优化的浆态床加氢反应器及其用途与设计方法 |
CN104888666A (zh) * | 2015-05-07 | 2015-09-09 | 北京中科诚毅科技发展有限公司 | 一种浆态床反应器控温方法及其设计方法和用途 |
-
2015
- 2015-11-18 CN CN201510796589.5A patent/CN105273747B/zh active Active
- 2015-11-30 WO PCT/CN2015/096023 patent/WO2017084114A1/zh active Application Filing
- 2015-11-30 US US15/777,338 patent/US11111446B2/en active Active
Also Published As
Publication number | Publication date |
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WO2017084114A1 (zh) | 2017-05-26 |
US20190249092A1 (en) | 2019-08-15 |
US11111446B2 (en) | 2021-09-07 |
CN105273747A (zh) | 2016-01-27 |
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